Attachment C: 40 CFR Part 180 - Tolerances and Exemptions from Tolerances for Pesticide Chemicals in Food

Attachment C_40 CFR Part 180.pdf

Tolerance Petitions for Pesticides on Food/Feed Crops and New Inert Ingredients

Attachment C: 40 CFR Part 180 - Tolerances and Exemptions from Tolerances for Pesticide Chemicals in Food

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PART 180—TOLERANCES AND EXEMPTIONS FOR PESTICIDE CHEMICAL RESIDUES IN
FOOD

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Subpart A—Definitions and Interpretative Regulations

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§ 180.1
§ 180.3
§ 180.4
§ 180.5
§ 180.6

Definitions and interpretations.
Tolerances for related pesticide chemicals.
Exceptions.
Zero tolerances.
Pesticide tolerances regarding milk, eggs, meat, and/or poultry; statement of policy.

Subpart B—Procedural Regulations
§ 180.7 Petitions proposing tolerances or exemptions for pesticide residues in or on raw
agricultural commodities or processed foods.
§ 180.8 Withdrawal of petitions without prejudice.
§ 180.9 Substantive amendments to petitions.
§ 180.29 Establishment, modification, and revocation of tolerance on initiative of Administrator.
§ 180.30 Judicial review.
§ 180.31 Temporary tolerances.
§ 180.32 Procedure for modifying and revoking tolerances or exemptions from tolerances.
§ 180.33 Fees.
§ 180.34 Tests on the amount of residue remaining.
§ 180.35 Tests for potentiation.
§ 180.40 Tolerances for crop groups.
§ 180.41 Crop group tables.
Subpart C—Specific Tolerances

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§ 180.101 Specific tolerances; general provisions.
§ 180.103 Captan; tolerances for residues.
§ 180.106 Diuron; tolerances for residues.
§ 180.108 Acephate; tolerances for residues.
§ 180.110 Maneb; tolerances for residues.
§ 180.111 Malathion; tolerances for residues.
§ 180.114 Ferbam; tolerances for residues.
§ 180.116 Ziram; tolerances for residues.
§ 180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.
§ 180.121 Methyl parathion; tolerances for residues.
§ 180.122 Parathion; tolerances for residues.
§ 180.123 Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances
for residues.
§ 180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.
§ 180.127 Piperonyl butoxide; tolerances for residues.
§ 180.128 Pyrethrins; tolerances for residues.
§ 180.129 o-Phenylphenol and its sodium salt; tolerances for residues.
§ 180.130 Hydrogen Cyanide; tolerances for residues.
§ 180.132 Thiram; tolerances for residues.
§ 180.133 Lindane; tolerances for residues.
§ 180.136 Basic copper carbonate; tolerance for residues.
§ 180.142 2,4-D; tolerances for residues.
§ 180.144 Cyhexatin; tolerances for residues.
§ 180.145 Fluorine compounds; tolerances for residues.
§ 180.149 Mineral oil; tolerances for residues.
§ 180.151 Ethylene oxide; tolerances for residues.
§ 180.153 Diazinon; tolerances for residues.
§ 180.154 O,O -Dimethyl S -[(4-oxo-1,2,3-benzotriazin-3(4 H )-yl)methyl]phosphorodithioate;
tolerances for residues.
§ 180.155 1-Naphthaleneacetic acid; tolerances for residues.
§ 180.157 Methyl 3-[(dimethoxyphosphinyl) oxy]butenoate, alpha and beta isomers; tolerances
for residues.
§ 180.163 1,1-Bis(4-chlorophenyl)-2,2,2-trichloroethanol; tolerances for residues.
§ 180.169 Carbaryl; tolerances for residues.
§ 180.172 Dodine; tolerances for residues.
§ 180.173 Ethion; tolerances for residues.
§ 180.175 Maleic hydrazide; tolerances for residues.
§ 180.176 Mancozeb; tolerances for residues.
§ 180.178 Ethoxyquin; tolerances for residues.
§ 180.180 Orthoarsenic acid; tolerance for residues.
§ 180.181 Chlorpropham; tolerances for residues.
§ 180.182 Endosulfan; tolerances for residues.
§ 180.183 O,O -Diethyl S -[2-(ethylthio)ethyl] phosphorodithioate; tolerances for residues.
§ 180.184 Linuron; tolerances for residues.
§ 180.185 DCPA; tolerances for residues.
§ 180.189 Coumaphos; tolerances for residues.
§ 180.190 Diphenylamine; tolerances for residues.
§ 180.191 Folpet; tolerances for residues.
§ 180.198 Trichlorfon; tolerances for residues.
§ 180.200 Dicloran; tolerances for residues.
§ 180.202 p -Chlorophenoxyacetic acid; tolerances for residues.
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§ 180.204 Dimethoate; tolerances for residues.
§ 180.205 Paraquat; tolerances for residues.
§ 180.206 Phorate; tolerances for residues.
§ 180.207 Trifluralin; tolerances for residues.
§ 180.208 Benfluralin; tolerances for residues.
§ 180.209 Terbacil; tolerances for residues.
§ 180.210 Bromacil; tolerances for residues.
§ 180.211 Propachlor; tolerances for residues.
§ 180.212 S -Ethyl cyclohexylethylthiocarbamate; tolerances for residues.
§ 180.213 Simazine; tolerances for residues.
§ 180.214 Fenthion; tolerances for residues.
§ 180.215 Naled; tolerances for residues.
§ 180.217 Ammoniates for [ethylenebis-(dithiocarbamato)] zinc and ethylenebis [dithiocarbamic
acid] bimolecular and trimolecular cyclic anhydrosulfides and disulfides; tolerances for residues.
§ 180.220 Atrazine; tolerances for residues.
§ 180.221 O -Ethyl S -phenyl ethylphosphonodithioate; tolerances for residues.
§ 180.222 Prometryn; tolerances for residues.
§ 180.225 Phosphine; tolerances for residues.
§ 180.226 Diquat; tolerances for residues.
§ 180.227 Dicamba; tolerances for residues.
§ 180.228 S -Ethyl hexahydro- 1H -azepine-1-carbothioate; tolerances for residues.
§ 180.229 Fluometuron; tolerances for residues.
§ 180.231 Dichlobenil; tolerances for residues.
§ 180.232 Butylate; tolerances for residues.
§ 180.235 Dichlorvos; tolerances for residues.
§ 180.236 Triphenyltin hydroxide; tolerances for residues.
§ 180.239 Phosphamidon; tolerancesfor residues.
§ 180.241 Bensulide; tolerances for residues.
§ 180.242 Thiabendazole; tolerances for residues.
§ 180.243 Propazine; tolerances for residues.
§ 180.245 Streptomycin; tolerances for residues.
§ 180.249 Alachlor; tolerances for residues.
§ 180.252 Tetrachlorvinphos; tolerances for residues.
§ 180.253 Methomyl; tolerances for residues.
§ 180.254 Carbofuran; tolerances for residues.
§ 180.257 Chloroneb; tolerances for residues.
§ 180.258 Ametryn; tolerances for residues.
§ 180.259 Propargite; tolerances for residues.
§ 180.261 N -(Mercaptomethyl) phthalimide S -( O,O -dimethyl phosphorodithioate) and its
oxygen analog; tolerances for residues.
§ 180.262 Ethoprop; tolerances for residues.
§ 180.263 Phosalone; tolerances for residues.
§ 180.269 Aldicarb; tolerances for residues.
§ 180.272 Tribuphos; tolerances for residues.
§ 180.274 Propanil; tolerances for residues.
§ 180.275 Chlorothalonil; tolerances for residues.
§ 180.276 Formetanate hydrochloride; tolerances for residues.
§ 180.278 Phenmedipham; tolerances for residues.
§ 180.284 Zinc phosphide; tolerances for residues.
§ 180.287 Amitraz; tolerances for residues.
§ 180.288 2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.
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§ 180.289 Methanearsonic acid; tolerances for residues.
§ 180.291 Pentachloronitrobenzene; tolerance for residues.
§ 180.292 Picloram; tolerances for residues.
§ 180.293 Endothall; tolerances for residues.
§ 180.294 Benomyl; tolerances for residues.
§ 180.296 Dimethyl phosphate of 3-hydroxy- N -methyl- cis -crotonamide; tolerances for residues.
§ 180.297 N -1-Naphthyl phthalamicacid; tolerances for residues.
§ 180.298 Methidathion; tolerances for residues.
§ 180.299 Dicrotophos; tolerances for residues.
§ 180.300 Ethephon; tolerances for residues.
§ 180.301 Carboxin; tolerances for residues.
§ 180.303 Oxamyl; tolerances for residues.
§ 180.304 Oryzalin; tolerances for residues.
§ 180.309 &b.alpha;-Naphthaleneacetamide; tolerances for residues.
§ 180.311 Cacodylic acid; tolerances for residues.
§ 180.312 4-Aminopyridine; tolerances for residues.
§ 180.314 Triallate; tolerances for residues.
§ 180.315 Methamidophos; tolerances for residues.
§ 180.316 Pyrazon; tolerances for residues.
§ 180.317 Propyzamide; tolerances for residues.
§ 180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.
§ 180.319 Interim tolerances.
§ 180.324 Bromoxynil; tolerances for residues.
§ 180.325 2-(m-Chlorophenoxy) propionic acid; tolerances for residues.
§ 180.328 Napropamide; tolerances for residues.
§ 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.
§ 180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.
§ 180.332 Metribuzin; tolerances for residues.
§ 180.337 Oxytetracycline; tolerance for residues.
§ 180.339 MCPA; tolerances for residues.
§ 180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances
for residues.
§ 180.342 Chlorpyrifos; tolerances for residues.
§ 180.345 Ethofumesate; tolerances for residues.
§ 180.349 Fenamiphos; tolerances for residues.
§ 180.350 Nitrapyrin; tolerances forresidues.
§ 180.352 Terbufos; tolerances for residues.
§ 180.353 Desmedipham; tolerances for residues.
§ 180.355 Bentazon; tolerances for residues.
§ 180.356 Norflurazon; tolerances for residues.
§ 180.360 Asulam; tolerance for residues.
§ 180.361 Pendimethalin; tolerances for residues.
§ 180.362 Hexakis (2-methyl-2-phenylpropyl)distannoxane; tolerances for residues.
§ 180.364 Glyphosate; tolerances for residues.
§ 180.367 n -Octyl bicycloheptenedicarboximide; tolerances for residues.
§ 180.368 Metolachlor; tolerances for residues.
§ 180.369 Difenzoquat; tolerances for residues.
§ 180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.
§ 180.371 Thiophanate-methyl; tolerances for residues.
§ 180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.
§ 180.373 [Reserved]
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§ 180.377 Diflubenzuron; tolerances for residues.
§ 180.378 Permethrin; tolerances for residues.
§ 180.379 Cyano(3-phenoxyphenyl)methyl-4-chloro-&b.alpha;-(1-methylethyl) benzeneacetate;
tolerances for residues.
§ 180.380 Vinclozolin; tolerances for residues.
§ 180.381 Oxyfluorfen; tolerances for residues.
§ 180.383 Sodium salt of acifluorfen; tolerances for residues.
§ 180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.
§ 180.385 Diclofop-methyl; tolerances for residues.
§§ 180.388-180.389 [Reserved]
§ 180.390 Tebuthiuron; tolerances for residues.
§ 180.395 Hydramethylnon; tolerances for residues.
§ 180.396 Hexazinone; tolerances for residues.
§ 180.399 Iprodione; tolerances for residues.
§ 180.401 Thiobencarb; tolerances for residues.
§ 180.403 Thidiazuron; tolerances for residues.
§ 180.404 Profenofos; tolerances for residues.
§ 180.405 Chlorsulfuron; tolerances for residues.
§ 180.406 Dimethipin; tolerances for residues.
§ 180.407 Thiodicarb; tolerances for residues.
§ 180.408 Metalaxyl; tolerances for residues.
§ 180.409 Pirimiphos-methyl; tolerances for residues.
§ 180.410 Triadimefon; tolerances for residues.
§ 180.411 Fluazifop-P-butyl; tolerances for residues.
§ 180.412 Sethoxydim; tolerances for residues.
§ 180.413 Imazalil; tolerances for residues.
§ 180.414 Cyromazine; tolerances for residues.
§ 180.415 Aluminum tris ( O -ethylphosphonate); tolerances for residues.
§ 180.416 Ethalfluralin; tolerances for residues.
§ 180.417 Triclopyr; tolerances for residues.
§ 180.418 Cypermethrin and an isomer zeta-cypermethrin; tolerances for residues.
§ 180.419 Chlorpyrifos-methyl; tolerances for residues.
§ 180.420 Fluridone; tolerances for residues.
§ 180.421 Fenarimol; tolerances for residues.
§ 180.422 Tralomethrin; tolerances for residues.
§ 180.425 Clomazone; tolerances for residues.
§ 180.426 2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1 H -imidazol-2-yl]-3-quinoline
carboxylic acid; tolerance for residues.
§ 180.427 Tau-Fluvalinate; tolerances for residues.
§ 180.428 Metsulfuron methyl; tolerances for residues.
§ 180.429 Chlorimuron ethyl; tolerances for residues.
§ 180.430 Fenoxaprop-ethyl; tolerances for residues.
§ 180.431 Clopyralid; tolerances for residues.
§ 180.432 Lactofen; tolerances for residues.
§ 180.433 Fomesafen; tolerances for residues.
§ 180.434 Propiconazole; tolerances for residues.
§ 180.435 Deltamethrin; tolerances for residues.
§ 180.436 Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.
§ 180.437 Methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)- p -toluate and methyl 6-(4isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)- m -toluate; tolerances for residues.
§ 180.438 Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for residues.
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§ 180.439
§ 180.440
§ 180.441
§ 180.442
§ 180.443
§ 180.444
§ 180.445
§ 180.446
§ 180.447
§ 180.448
§ 180.449

Thifensulfuron methyl; tolerances for residues.
Tefluthrin; tolerances for residues.
Quizalofop ethyl; tolerances for residues.
Bifenthrin; tolerances for residues.
Myclobutanil; tolerances for residues.
Sulfur dioxide; tolerances for residues.
Bensulfuron methyl; tolerances for residues.
Clofentezine; tolerances for residues.
Imazethapyr; tolerances for residues.
Hexythiazox; tolerance for residues.
Avermectin B1 and its delta-8,9-isomer; tolerances for residues.

§ 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol;
tolerances for residues.
§ 180.451 Tribenuron methyl; tolerances for residues.
§ 180.452 Primisulfuron-methyl; tolerances for residues.
§ 180.454 Nicosulfuron, [3-pyridinecarboxamide, 2-((((4,6-dimethoxypyrimidin-2-yl)aminocarbonyl)
aminosulfonyl))-N,N-dimethyl]; tolerances for residues.
§ 180.455 Procymidone; tolerances for residues.
§ 180.456 Oxadixyl; tolerances for residues.
§ 180.457 Beta-([1,1′-biphenyl]-4-yloxy)-alpha-(1,1-dimethylethyl)-1 H -1,2,4-triazole-1-ethanol;
tolerances for residues.
§ 180.458 Clethodim; tolerances for residues.
§ 180.459 Triasulfuron; tolerances for residues.
§ 180.460 Benoxacor; tolerances for residues.
§ 180.461 Cadusafos; tolerances for residues.
§ 180.462 Pyridate; tolerances for residues.
§ 180.463 Quinclorac; tolerances for residues.
§ 180.464 Dimethenamid; tolerances for residues.
§ 180.465 4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.
§ 180.466 Fenpropathrin; tolerances for residues.
§ 180.467 Carbon disulfide; tolerances for residues.
§ 180.468 Flumetsulam; tolerances for residues.
§ 180.469 Dichlormid; tolerances for residues.
§ 180.470 Acetochlor; tolerances for residues.
§ 180.471 Furilazole; tolerances for residues.
§ 180.472 Imidacloprid; tolerances for residues.
§ 180.473 Glufosinate ammonium; tolerances for residues.
§ 180.474 Tebuconazole; tolerances for residues.
§ 180.475 Difenoconazole; tolerances for residues.
§ 180.476 Triflumizole; tolerances for residues.
§ 180.477 Flumiclorac pentyl; tolerances for residues.
§ 180.478 Rimsulfuron; tolerances for residues
§ 180.479 Halosulfuron-methyl; tolerances for residues.
§ 180.480 Fenbuconazole; tolerances for residues.
§ 180.481 Prosulfuron; tolerances for residues.
§ 180.482 Tebufenozide; tolerances for residues.
§ 180.483 O -[2-(1,1-Dimethylethyl)-5-pyrimidinyl] O -ethyl- O -(1-methylethyl) phosphorothioate;
tolerances for residues.
§ 180.484 Flutolanil ( N -(3-(1-methylethoxy)phenyl)-2-(trifluoromethyl)benzamide); tolerances for
residues.

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§ 180.485 Cyproconazole; tolerances for residues.
§ 180.486 Phosphorothioic acid, 0,0 -diethyl 0 -(1,2,2,2-tetrachloroethyl) ester; tolerances for
residues.
§ 180.487 Pyrithiobac sodium; tolerances for residues.
§ 180.490 Imazapic-ammonium; tolerances for residues.
§ 180.491 Propylene oxide; tolerances for residues.
§ 180.492 Triflusulfuron methyl; tolerances for residues.
§ 180.493 Dimethomorph; tolerances for residues.
§ 180.494 Pyridaben; tolerance for residues.
§ 180.495 Spinosad; tolerances for residues.
§ 180.496 Thiazopyr; tolerances for residues.
§ 180.497 Clofencet; tolerances for residues.
§ 180.498 Sulfentrazone; tolerances for residues.
§ 180.499 Propamocarb hydrochloride, tolerances for residues.
§ 180.500 Imazapyr; tolerances for residues.
§ 180.501 Hydroprene; tolerances for residues.
§ 180.502 Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for residues.
§ 180.503 Cymoxanil, tolerance for residues.
§ 180.504 [Reserved]
§ 180.505 Emamectin; tolerances for residues.
§ 180.506 Cyclanilide; tolerances for residues.
§ 180.507 Azoxystrobin; tolerances for residues.
§ 180.509 Mefenpyr-diethyl; tolerance for residues.
§ 180.510 Pyriproxyfen; tolerances for residues.
§ 180.511 Buprofezin; tolerances for residues.
§ 180.512 [Reserved]
§ 180.513 Chlorfenapyr; tolerances for residues.
§ 180.514 Cloransulam-methyl; tolerances for residues.
§ 180.515 Carfentrazone-ethyl; tolerances for residues.
§ 180.516 Fludioxonil; tolerances for residues.
§ 180.517 Fipronil; tolerances for residues.
§ 180.518 Pyrimethanil; tolerances for residues.
§ 180.519 Bromide ion and residual bromine; tolerances for residues.
§ 180.521 Fumigants for grain-mill machinery; tolerances for residues.
§ 180.522 Fumigants for processed grains used in production of fermented malt beverage;
tolerances for residues.
§ 180.523 Metaldehyde; tolerances for residues.
§ 180.525 Resmethrin; tolerances for residues.
§ 180.526 Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.
§ 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 4-fluoro-N-methylethyl
benzenamine tolerances for residues.
§ 180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol methylcarbamate; tolerances for residues.
§ 180.532 Cyprodinil; tolerances for residues.
§ 180.533 Esfenvalerate; tolerances for residues.
§ 180.535 Fluroxypyr 1-methylheptyl ester; tolerances for residues.
§ 180.536 Triazamate; tolerances for residues.
§ 180.537 Isoxaflutole; tolerances for residues.
§ 180.538 Copper; tolerances for residues.
§ 180.539 d-Limonene; tolerances for residues.
§ 180.540 Fenitrothion; tolerances for residues.
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§ 180.541 Propetamphos; tolerances for residues.
§ 180.543 Diclosulam; tolerances for residues.
§ 180.544 Methoxyfenozide; tolerances for residues.
§ 180.545 Prallethrin ( RS )-2-methyl-4-oxo-3-(2-propynyl)cyclopent-2-enyl (1 RS )- cis, trans chrysanthemate; tolerances for residues.
§ 180.546 Mefenoxam; tolerances for residues.
§ 180.547 Prohexadione calcium; tolerances for residues.
§ 180.548 Tralkoxydim; tolerances for residues.
§ 180.549 Diflufenzopyr; tolerances for residues.
§ 180.550 Arsanilic acid [(4-aminophenyl) arsonic acid]; tolerances for residues.
§ 180.551 Fluthiacet-methyl; tolerances for residues.
§ 180.552 Sulfosulfuron; tolerances for residues.
§ 180.553 Fenhexamid; tolerances for residues.
§ 180.554 Kresoxim-methyl; tolerances for residues.
§ 180.555 Trifloxystrobin; tolerances for residues.
§ 180.556 Pymetrozine; tolerances for residues.
§ 180.557 Tetraconazole; tolerances for residues.
§ 180.558 N,N -diethyl-2-(4-methylbenzyloxy)ethylamine hydrochloride; tolerances for residues.
§ 180.559 Clodinafop-propargyl; tolerances for residues.
§ 180.560 Cloquintocet-mexyl; tolerances for residues.
§ 180.561 Acibenzolar- S -methyl; tolerances for residues.
§ 180.562 Flucarbazone-sodium; tolerances for residues.
§ 180.563 Ethametsulfuron-methyl; tolerances for residues.
§ 180.564 Indoxacarb; tolerances for residues.
§ 180.565 Thiamethoxam; tolerances for residues.
§ 180.566 Fenpyroximate; tolerances for residues.
§ 180.567 Zoxamide; tolerances for residues.
§ 180.568 Flumioxazin; tolerances for residues.
§ 180.569 Forchlorfenuron; tolerances for residues.
§ 180.570 Isoxadifen-ethyl; tolerances for residues.
§ 180.571 Mesotrione; tolerances for residues.
§ 180.572 Bifenazate; tolerance for residues.
§ 180.573 Tepraloxydim; tolerances for residues.
§ 180.574 Fluazinam; tolerances for residues.
§ 180.575 Sulfuryl fluoride; tolerances for residues.
§ 180.576 Cyhalofop-butyl; tolerances for residues.
§ 180.577 Bispyribac-sodium; tolerances for residues.
§ 180.578 Acetamiprid; tolerances for residues.
§ 180.579 Fenamidone; tolerances for residues.
§ 180.580 Iodosulfuron-Methyl-Sodium; tolerances for residues.
§ 180.581 Iprovalicarb; tolerances for residues.
§ 180.582 Pyraclostrobin; tolerances for residues.
§ 180.583 Triticonazole; tolerances for residues.
§ 180.584 Tolylfluanid; tolerances for residues.
§ 180.585 Pyraflufen-ethyl; tolerances for residues.
§ 180.586 Clothianidin; tolerances for residues.
§ 180.587 Famoxadone; tolerance for residues.
§ 180.588 Quinoxyfen; tolerances for residues.
§ 180.589 Boscalid; tolerances for residues.
§ 180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.
§ 180.591 Trifloxysulfuron; tolerances for residues.
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§ 180.592
§ 180.593
§ 180.594
§ 180.595
§ 180.596
§ 180.597
§ 180.598
§ 180.599
§ 180.600
§ 180.601
§ 180.602
§ 180.603
§ 180.604
§ 180.605
§ 180.607
§ 180.608
§ 180.609
§ 180.610
§ 180.611
§ 180.612
§ 180.613
§ 180.614
§ 180.615
§ 180.616
§ 180.617
§ 180.618
§ 180.619
§ 180.620
§ 180.621
§ 180.622
§ 180.623
§ 180.624
§ 180.625
§ 180.626
§ 180.627
§ 180.628
§ 180.629
§ 180.630
§ 180.631
§ 180.632
§ 180.633
§ 180.634
§ 180.635
§ 180.636
§ 180.637
§ 180.638
§ 180.639
§ 180.640
§ 180.641
§ 180.642
§ 180.643

Butafenacil; tolerances for residues.
Etoxazole; tolerances for residues.
Thiacloprid; tolerances for residues.
Flufenpyr-ethyl; tolerances for residues.
Fosthiazate; tolerances for residues.
Mesosulfuron-methyl; tolerances for residues.
Novaluron; tolerances for residues.
Acequinocyl; tolerances for residues.
Propoxycarbazone; tolerances for residues
Cyazofamid; tolerances for residues.
Spiroxamine; tolerances for residues.
Dinotefuran; tolerances for residues.
Mepanipyrim; tolerances for residues.
Penoxsulam; tolerances for residues.
Spiromesifen; tolerances for residues.
Spirodiclofen; tolerances for residues.
Fluoxastrobin; tolerances for residues.
Aminopyralid; tolerances for residues.
Pinoxaden; tolerances for residues.
Topramezone; tolerances for residues.
Flonicamid; tolerances for residues.
Kasugamycin; tolerances for residues.
Amicarbazone; tolerances for residues.
Fenpropimorph; tolerances for residues.
Metconazole; tolerances for residues.
Benthiavalicarb-isopropyl; tolerance for residues.
Epoxiconazole; tolerances for residues.
Etofenprox; tolerances for residues.
Dithianon; tolerances for residues.
Ethaboxam; tolerances for residues.
Flufenoxuron; tolerances for residues.
Metrafenone; tolerances for residues.
Orthosulfamuron; tolerances for residues.
Prothioconazole; tolerances for residues.
Fluopicolide; tolerances for residues.
Chlorantraniliprole; tolerances for residues.
Flutriafol; tolerance for residues.
Flusilazole; tolerances for residues.
Pyrasulfotole; tolerances for residues.
Fenazaquin; import tolerances for residues.
Florasulam; tolerances for residues.
Tembotrione; tolerances for residues.
Spinetoram; tolerances for residues.
1,3-dichloropropene; tolerances for residues.
Mandipropamid; tolerances for residues.
Pyroxsulam; tolerances for residues.
Flubendiamide; tolerances for residues.
Pyridalyl; tolerances for residues.
Spirotetramat; tolerances for residues.
Gentamicin; tolerances for residues.
Uniconazole; tolerances for residues.

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§ 180.644
§ 180.645
§ 180.646
§ 180.647

Cyprosulfamide; tolerances for residues.
Thiencarbazone-methyl; tolerances for residues.
Ipconazole; tolerances for residues.
d-Phenothrin; tolerances for residues.

Subpart D—Exemptions From Tolerances
§ 180.900 Exemptions from the requirement of a tolerance.
§ 180.905 Pesticide chemicals; exemptions from the requirement of a tolerance.
§ 180.910 Inert ingredients used pre- and post-harvest; exemptions from the requirement of a
tolerance.
§ 180.920 Inert ingredients used pre-harvest; exemptions from the requirement of a tolerance.
§ 180.930 Inert ingredients applied to animals; exemptions from the requirement of a tolerance.
§ 180.940 Tolerance exemptions for active and inert ingredients for use in antimicrobial
formulations (Food-contact surface sanitizing solutions).
§ 180.950 Tolerance exemptions for minimal risk active and inert ingredients.
§ 180.960 Polymers; exemptions from the requirement of a tolerance.
§ 180.1011 Viable spores of the microorganism Bacillus thuringiensis Berliner; exemption from
the requirement of a tolerance.
§ 180.1016 Ethylene; exemption from the requirement of a tolerance.
§ 180.1017 Diatomaceous earth; exemption from the requirement of a tolerance.
§ 180.1019 Sulfuric acid; exemption from the requirement of a tolerance.
§ 180.1020 Sodium chlorate; exemption from the requirement of a tolerance.
§ 180.1021 Copper; exemption from the requirement of a tolerance.
§ 180.1022 Iodine-detergent complex; exemption from the requirement of a tolerance.
§ 180.1023 Propanoic acid; exemptions from the requirement of a tolerance.
§ 180.1025 Xylene; exemption from the requirement of a tolerance.
§ 180.1027 Nuclear polyhedrosis virus of Heliothis zea; exemption from the requirement of a
tolerance.
§ 180.1033 Methoprene; exemption from the requirement of a tolerance.
§ 180.1035 Pine oil; exemption from the requirement of a tolerance.
§ 180.1037 Polybutenes; exemption from the requirement of a tolerance.
§ 180.1040 Ethylene glycol; exemption from the requirement of a tolerance.
§ 180.1041 Nosema locustae; exemption from the requirement of a tolerance.
§ 180.1043 Gossyplure; exemption from the requirement of a tolerance.
§ 180.1049 Carbon dioxide; exemption from the requirement of a tolerance.
§ 180.1050 Nitrogen; exemption from the requirements of a tolerance.
§ 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine; exemption from the requirement of a
tolerance.
§ 180.1054 Calcium hypochlorite; exemptions from the requirement of a tolerance.
§ 180.1056 Boiled linseed oil; exemption from requirement of tolerance.
§ 180.1057 Phytophthora palmivora; exemption from requirement of tolerance.
§ 180.1058 Sodium diacetate; exemption from the requirement of a tolerance.
§ 180.1064 Tomato pinworm insect pheromone; exemption from the requirement of a tolerance.
§ 180.1065 2-Amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one;
exemption from the requirement of a tolerance.
§ 180.1067 Methyl eugenol and malathion combination; exemption from the requirement of a
tolerance.
§ 180.1068 C12-C18 fatty acid potassium salts; exemption from the requirement of a tolerance.
§ 180.1069 ( Z )-11-Hexadecenal; exemption from the requirement of a tolerance.
§ 180.1070 Sodium chlorite; exemption from the requirement of a tolerance.
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§ 180.1071 Peanuts, Tree Nuts, Milk, Soybeans, Eggs, Fish, Crustacea, and Wheat; exemption
from the requirement of a tolerance.
§ 180.1072 Poly- D -glucosamine (chitosan); exemption from the requirement of a tolerance.
§ 180.1073 Isomate-M; exemption from the requirement of a tolerance.
§ 180.1074 F.D.&C. Blue No. 1; exemption from the requirement of a tolerance.
§ 180.1075 Colletotrichum gloeosporioides f. sp. aeschynomene; exemption from the
requirement of a tolerance.
§ 180.1076 Viable spores of the microorganism Bacillus popilliae; exemption from the
requirement of a tolerance.
§ 180.1080 Plant volatiles and pheromone; exemptions from the requirement of a tolerance.
§ 180.1083 Dimethyl sulfoxide; exemption from the requirement of a tolerance.
§ 180.1084 Monocarbamide dihydrogen sulfate; exemption from the requirement of a tolerance.
§ 180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11-trimethyl-2,6,10-dodecatriene-3ol; exemption from the requirement of a tolerance.
§ 180.1087 Sesame stalks; exemption from the requirement of a tolerance.
§ 180.1089 Poly- N -acetyl- D -glucosamine; exemption from the requirement of tolerance.
§ 180.1090 Lactic acid; exemption from the requirement of a tolerance.
§ 180.1091 Aluminum isopropoxide and aluminum secondary butoxide; exemption from the
requirement of a tolerance.
§ 180.1092 Menthol; exemption from the requirement of a tolerance.
§ 180.1095 Chlorine gas; exemptions from the requirement of a tolerance.
§ 180.1097 GBM-ROPE; exemption from the requirement of a tolerance.
§ 180.1098 Gibberellins [Gibberellic Acids (GA3 and GA4 + GA7), and Sodium or Potassium
Gibberellate]; exemption from the requirement of a tolerance.
§ 180.1100 Gliocladium virens isolate GL-21; exemption from the requirement of a tolerance.
§ 180.1101 Parasitic (parasitoid) and predatory insects; exemption from the requirement of a
tolerance.
§ 180.1102 Trichoderma harzianum KRL-AG2 (ATCC #20847) strain T–22; exemption from
requirement of a tolerance.
§ 180.1103 Isomate-C; exemption from the requirement of a tolerance.
§ 180.1107 Delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed
Pseudomonas fluorescens; exemption from the requirement of a tolerance.
§ 180.1108 Delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed
Pseudomonas fluorescens; exemption from the requirement of a tolerance.
§ 180.1110 3-Carbamyl-2,4,5-trichlorobenzoic acid; exemption from the requirement of a
tolerance.
§ 180.1111 Bacillus subtilis GB03; exemption from the requirement of a tolerance.
§ 180.1113 Lagenidium giganteum ; exemption from the requirement of a tolerance.
§ 180.1114 Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and
Pseudomonas syringae 742RS; exemptions from the requirement of a tolerance.
§ 180.1118 Spodoptera exigua nuclear polyhedrosis virus; exemption from the requirement of a
tolerance.
§ 180.1119 Azadirachtin; exemption from the requirement of a tolerance.
§ 180.1120 Streptomyces sp. strain K61; exemption from the requirement of a tolerance.
§ 180.1121 Boric acid and its salts, borax (sodium borate decahydrate), disodium octaborate
tetrahydrate, boric oxide (boric anhydride), sodium borate and sodium metaborate; exemptions
from the requirement of a tolerance.
§ 180.1122 Inert ingredients of semiochemical dispensers; exemptions from the requirement of a
tolerance.
§ 180.1124 Arthropod pheromones; exemption from the requirement of a tolerance.
§ 180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; exemption from the requirement of a tolerance.
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§ 180.1127 Biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde,
cinnamyl alcohol, 4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol,
indole, and 1,2,4-trimethoxybenzene; exemptions from the requirement of a tolerance.
§ 180.1128 Bacillus subtilis MBI 600; exemption from the requirement of a tolerance.
§ 180.1130 N -( n -octyl)-2-pyrrolidone and N -( n -dodecyl)-2-pyrrolidone; exemptions from the
requirement of a tolerance.
§ 180.1131 Ampelomyces quisqualis isolate M10; exemption from the requirement of a tolerance.
§ 180.1135 Pasteuria penetrans; exemption from the requirement of a tolerance.
§ 180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of a tolerance.
§ 180.1140 Sodium o -nitrophenolate; exemption from the requirement of a tolerance.
§ 180.1141 Sodium p -nitrophenolate; exemption from the requirement of a tolerance.
§ 180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of a tolerance.
§ 180.1143 Methyl anthranilate; exemption from the requirement of a tolerance.
§ 180.1144 Candida oleophila isolate I-182; exemption from the requirement of a tolerance.
§ 180.1145 Pseudomonas syringae; exemption from the requirement of a tolerance.
§ 180.1146 Beauveria bassiana Strain GHA; exemption from the requirement of a tolerance.
§ 180.1148 Occlusion Bodies of the Granulosis Virus of Cydia pomenella; tolerance exemption.
§ 180.1149 Inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha falcifera;
exemption from the requirement of a tolerance.
§ 180.1150 6-Benzyladenine; exemption from the requirement of a tolerance.
§ 180.1153 Lepidopteran pheromones; exemption from the requirement of a tolerance.
§ 180.1154 CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki
encapsulated in killed Pseudomonas fluorescens, and the expression plasmid and cloning vector
genetic constructs.
§ 180.1156 Cinnamaldehyde; exemption from the requirement of a tolerance.
§ 180.1157 Cytokinins; exemption from the requirement of a tolerance.
§ 180.1158 Auxins; exemption from the requirement of a tolerance.
§ 180.1159 Pelargonic acid; exemption from the requirement of tolerances.
§ 180.1160 Jojoba oil; exemption from the requirement of a tolerance.
§ 180.1161 Clarified hydrophobic extract of neem oil; exemption from the requirement of a
tolerance.
§ 180.1162 Acrylate polymers and copolymers; exemption from the requirement of a tolerance.
§ 180.1163 Killed Myrothecium verrucaria; exemption from the requirement of a tolerance.
§ 180.1165 Capsaicin; exemption from the requirement of a tolerance.
§ 180.1167 Allyl isothiocyanate as a component of food grade oil of mustard; exemption from the
requirement of a tolerance.
§ 180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance.
§ 180.1177 Potassium bicarbonate; exemption from the requirement of a tolerance.
§ 180.1178 Formic acid; exemption from the requirement of a tolerance.
§ 180.1179 Plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and
Rhizophoria mangle; exemption from the requirement of a tolerance.
§ 180.1180 Kaolin; exemption from the requirement of a tolerance.
§ 180.1181 Bacillus cereus strain BPO1; exemption from the requirement of a tolerance.
§ 180.1187 L-glutamic acid; exemption from the requirement of a tolerance.
§ 180.1188 Gamma aminobutyric acid; exemption from the requirement of a tolerance.
§ 180.1189 Methyl salicylate; exemption from the requirement of a tolerance.
§ 180.1191 Ferric phosphate; exemption from the requirement of a tolerance.
§ 180.1193 Potassium dihydrogen phosphate; exemption from the requirement of a tolerance.
§ 180.1195 Titanium dioxide.
§ 180.1196 Peroxyacetic acid; exemption from the requirement of a tolerance.
§ 180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance.
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§ 180.1198 Gliocladium catenulatum strain J1446; exemption from the requirement of a
tolerance.
§ 180.1199 Lysophosphatidylethanolamine (LPE); exemption from the requirement of a tolerance.
§ 180.1200 Pseudomonas fluorescens strain PRA–25; temporary exemption from the
requirement of a tolerance.
§ 180.1201 Trichoderma harzianum strain T-39; exemption from the requirement of a tolerance.
§ 180.1202 Bacillus sphaericus; exemption from the requirement of a tolerance.
§ 180.1204 Harpin protein; exemption from the requirement of a tolerance.
§ 180.1205 Beauveria bassiana ATCC #74040; exemption from the requirements of a tolerance.
§ 180.1206 Aspergillus flavus AF36; exemption from the requirement of a tolerance.
§ 180.1207 N-acyl sarcosines and sodium N-acyl sarcosinates; exemption from the requirement
of a tolerance.
§ 180.1209 Bacillus subtilis strain QST 713; exemption from the requirement of a tolerance.
§ 180.1210 Phosphorous acid; exemption from the requirement of a tolerance.
§ 180.1212 Pseudomonas chlororaphis Strain 63–28; exemption from the requirement of a
tolerance.
§ 180.1213 Coniothyrium minitans strain CON/M/91–08; exemption from the requirement of a
tolerance.
§ 180.1218 Indian Meal Moth Granulosis Virus; exemption from the requirement of a tolerance.
§ 180.1219 Foramsulfuron; exemption from the requirement of a tolerance.
§ 180.1220 1-Methylcyclopropene; exemption from the requirement of a tolerance.
§ 180.1221 Pseudozyma flocculosa strain PF-A22 UL; exemption from the requirement of a
tolerance.
§ 180.1222 Sucrose octanoate esters; exemption from the requirement of a tolerance.
§ 180.1223 Imazamox; exemption from the requirement of a tolerance.
§ 180.1224 Bacillus pumilus GB34; exemption from the requirement of a tolerance.
§ 180.1225 Decanoic acid; exemption from the requirement of a tolerance.
§ 180.1226 Bacillus pumilus strain QST2808; temporary exemption from the requirement of a
tolerance.
§ 180.1228 Diallyl sulfides; exemption from the requirement of a tolerance.
§ 180.1230 Ferrous sulfate; exemption from the requirement of a tolerance.
§ 180.1231 Lime; exemption from the requirement of a tolerance.
§ 180.1232 Lime-sulfur; exemption from the requirement of a tolerance.
§ 180.1233 Potassium sorbate; exemption from the requirement of a tolerance.
§ 180.1234 Sodium carbonate; exemption from the requirement of a tolerance.
§ 180.1235 Sodium hypochlorite; exemption from the requirement of a tolerance.
§ 180.1236 Sulfur; exemption from the requirement of a tolerance.
§ 180.1237 Sodium metasilicate; exemption from the requirement of a tolerance.
§ 180.1240 Thymol; exemption from the requirement of a tolerance.
§ 180.1241 Eucalyptus oil; exemption from the requirement of a tolerance.
§ 180.1243 Bacillus subtilis var. amyloliquefaciens strain FZB24; exemption from the
requirement of a tolerance.
§ 180.1244 Ammonium bicarbonate; exemption from the requirement of a tolerance.
§ 180.1245 Rhamnolipid biosurfactant; exemption from the requirement of a tolerance.
§ 180.1246 Yeast Extract Hydrolysate fromSaccharomyces cerevisiae:exemption from the
requirement of a tolerance.
§ 180.1248 Exemption of citronellol from the requirement of a tolerance.
§ 180.1250 C8, C10, and C12 fatty acid monoesters of glycerol and propylene glycol; exemption
from the requirement of a tolerance.
§ 180.1251 Geraniol; exemption from the requirement of a tolerance.
§ 180.1253 Streptomyces lydicus WYEC 108; exemption from the requirement of a tolerance.
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§ 180.1254 Aspergillus flavus NRRL 21882 on peanut; exemption from requirement of a
tolerance.
§ 180.1255 Bacillus pumilus strain QST 2808; exemption from the requirement of a tolerance.
§ 180.1256 Alternaria destruens strain 059; exemption from the requirement of a tolerance.
§ 180.1257 Paecilomyces lilacinus strain 251; exemption from the requirement of a tolerance.
§ 180.1258 Acetic acid; exemption from the requirement of a tolerance.
§ 180.1259 Reynoutria sachalinensis extract; exemption from the requirement of a tolerance.
§ 180.1260 Muscodor albus QST 20799 and the volatiles produced on rehydration; exemption
from the requirement of a tolerance.
§ 180.1261 Xanthomonas campestris pv. vesicatoria and Pseudomonas syringae pv. tomato
specific Bacteriophages.
§ 180.1262 Sorbitol octanoate; exemption from the requirement of a tolerance.
§ 180.1263 Tetrahydrofurfuryl alcohol; exemption from the requirement of a tolerance.
§ 180.1267 Pantoea agglomerans strain C9–1; exemption from the requirement of a tolerance.
§ 180.1268 Potassium silicate; exemption from the requirement of a tolerance.
§ 180.1269 Bacillus mycoides Isolate J: exemption from the requirement of a tolerance.
§ 180.1270 Isophorone; exemption from the requirement of a tolerance.
§ 180.1271 Eucalyptus oil; exemption from the requirement of a tolerance.
§ 180.1272 Pantoea agglomerans strain E325; exemption from the requirement of a tolerance.
§ 180.1273 Beauveria bassiana HF23; exemption from the requirement of a tolerance.
§ 180.1274 Tris (2-ethylhexyl) phosphate; exemption from the requirement of a tolerance.
§ 180.1275 Pythium; exception from the requirement of a tolerance.
§ 180.1276 Tobacco mild green mosaic tobamovirus (TMGMV); temporary exemption from the
requirement of a tolerance.
§ 180.1277 Dibasic esters; exemption from the requirement of a tolerance.
§ 180.1278 Quillaja saponaria extract (saponins); exemption from the requirement of a tolerance.
§ 180.1279 Zucchini yellow mosaic virus—weak strain; exemption from the requirement of a
tolerance.
§ 180.1280 Poly(hexamethylenebiguanide) hydrochloride (PHMB); exemption from the
requirement of a tolerance.
§ 180.1281 S-Abscisic Acid; temporary exemption from the requirement of a tolerance.
§ 180.1282 Bacillus firmus I-1582; exemption from the requirement of a tolerance.
§ 180.1283 (Z)-7,8-epoxy-2-methyloctadecane (Disparlure); exemption from the requirement of a
tolerance.
§ 180.1284 Ammonium salts of higher fatty acids (C8–C18saturated; C8–C12unsaturated);
exemption from the requirement of a tolerance.
§ 180.1285 Polyoxin D zinc salt; exemption from the requirement of a tolerance.
§ 180.1287 Extract of Chenopodium ambrosioides near ambrosioides ; exemption from the
requirement of a tolerance.
§ 180.1288 Tristyrylphenol ethoxylates; exemption from the requirement of a tolerance.
§ 180.1289 Candida oleophila Strain O; exemption from the requirement of a tolerance.
§ 180.1290 Pasteuria usgae ; temporary exemption from the requirement of a tolerance.
Subpart E—Pesticide Chemicals Not Requiring a Tolerance or an Exemption From a
Tolerance
§ 180.2000
§ 180.2003
§ 180.2010
§ 180.2020

Scope.
Definitions.
Threshold of regulation determinations.
Non-food determinations.

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Authority: 21 U.S.C. 321(q), 346a and 371.
Source: 36 FR 22540, Nov. 25, 1971, unless otherwise noted.
Editorial Note: Nomenclature changes to part 180 appear at 62 FR 66023, Dec. 17, 1997.

GLOSSARY
Note: The items in this glossary were compiled as an aid to the users of the Code of Federal
Regulations. Inclusion or exclusion from this glossary has no legal significance.
APPLI = APPLICATION
C-I MET = CHOLINESTERASE-INHIBITING METABOLITES
CARB = CARBAMATES
EPWRR = EDIBLE PORTION WITH RIND REMOVED
EXC = EXCEPT
I (IN PPM COLUMN) = INTERIM TOLERANCE
INC = INCLUDING
K=CWHR = KERNEL PLUS COB WITH HUSK REMOVED
MBYP = MEAT BYPRODUCTS
MIN = MINIMUM
N (IN PPM COLUMN) = NEGLIGIBLE RESIDUES
NMT = NOT MORE THAN
NON-PER BAG/PKGD RAC = NON-PERISHABLE PACKAGED OR BAGGED RAW
AGRICULTURAL COMMODITY
PPM = PART(S) PER MILLION
POST-H = POSTHARVEST APPLICATION
PRE-H = PREHARVEST APPLICATION
PRE-S = PRESLAUGHTER APPLICATION
PRODS = PRODUCTS rollert
T (IN PPM COLUMN) = TEMPORARY TOLERANCE

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[41 FR 4537, Jan. 30, 1976]
Subpart A—Definitions and Interpretative Regulations
top

§ 180.1 Definitions and interpretations.
top
(a) Administrator, without qualification, means the Administrator of the Environmental Protection Agency.
(b) Agency, without qualification, means the Environmental Protection Agency.
(c) FFDCA means the Federal Food, Drug, and Cosmetic Act, as amended, 21 U.S.C. 301–392.
(d) Raw agricultural commodities include, among other things, fresh fruits, whether or not they have been
washed and colored or otherwise treated in their unpeeled natural form; vegetables in their raw or natural
state, whether or not they have been stripped of their outer leaves, waxed, prepared into fresh green
salads, etc.; grains, nuts, eggs, raw milk, meats, and similar agricultural produce. It does not include foods
that have been processed, fabricated, or manufactured by cooking, freezing, dehydrating, or milling.
(e) Where a raw agricultural commodity bearing a pesticide chemical residue that has been exempted
from the requirement of a tolerance, or which is within a tolerance permitted under FFDCA section 408, is
used in preparing a processed food, the processed food will not be considered unsafe within the meaning
of FFDCA sections 402 and 408(a), despite the lack of a tolerance or exemption for the pesticide chemical
residue in the processed food, if:
(1) The pesticide chemical has been used in or on the raw agricultural commodity in conformity with a
tolerance under this section;
(2) The pesticide chemical residue has been removed to the extent possible in good manufacturing
practice; and
(3) The concentration of the pesticide chemical residue in the processed food is not greater than the
tolerance prescribed for the pesticide chemical residue on the raw agricultural commodity.
(f) For the purpose of computing fees as required by §180.33, each group of related crops listed in §180.34
(e) and each crop group or subgroup listed in §180.41 is counted as a single raw agricultural commodity in
a petition or request for tolerances or exemption from the requirement of a tolerance.
(g) Tolerances and exemptions established for pesticide chemicals in or on the general category of raw
agricultural commodities listed in column A apply to the corresponding specific raw agricultural
commodities listed in column B. However, a tolerance or exemption for a specific commodity in column B
does not apply to the general category in column A.

A

B

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Alfalfa

Medicago sativa L.
Subsp. sativa
Onobrychis
viciifolia Scop
clover, esparcet); and Lotus
corniculatus L
varieties and/or hybrids of these.

, (alfalfa, lucerne);
. (sainfoin, holy
. (trefoil); and

Banana

Banana, plantain.

Bean

Cicer arietinum
(chickpea,
spp. (including sweet lupine,
garbanzo bean); Lupinus
white sweet lupine, white lupine, and grain lupine).
Phaseolus
spp. (including kidney bean, lima
bean, mung bean, navy bean, pinto bean, snap bean, and waxbean;
Vicia faba
(broad bean, fava bean);
Vigna
spp. (including asparagus bean, blackeyed pea and
cowpea).

Bean, dry

All beans above in dry form only.

Bean, succulent All beans above in succulent form only.
Blackberry

Rubus eubatus
(including bingleberry,
black satin berry, boysenberry Cherokee blackberry, Chesterberry,
Cheyenne blackberry, coryberry, darrowberry, dewberry, Dirksen
thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry,
Lucretiaberry, mammoth blackberry, marionberry, nectarberry,
olallieberry, Oregon evergreen berry, phenomenalberry, rangerberry,
ravenberry, rossberry, Shawnee blackberry, and varieties and/or
hybrids of these).

Broccoli

Broccoli, chinese broccoli (gia lon, white flowering broccoli).

Cabbage

Cabbage, Chinese cabbage (tight-heading varieties only).

Caneberry

Rubus
spp. (including blackberry);
Rubus caesius
(youngberry);
Rubus loganbaccus
(loganberry);
Rubus idaeus
(red and black raspberry);
cultivars, varieties, and/or hybrids of these.

Celery

Celery, Florence fennel (sweet anise, sweet fennel, finochio) (fresh
leaves and stalks only).

Cherry

Cherry, sweet, and cherry, tart.

Endive

Endive, escarole.

Fruit, citrus

Grapefruit, lemon, lime, orange, tangelo, tangerine, citrus citron,
kumquat, and hybrids of these.

Garlic

Garlic, great headed; garlic, and serpent garlic.

Lettuce

Lettuce, head; and lettuce, leaf

Lettuce, head

Lettuce, head; crisphead varieties only

Lettuce, leaf

Lettuce, leaf; cos (romaine), butterhead varieties

Marjoram

Origanum
spp. (includes sweet or annual marjoram,
wild marjoram or oregano, and pot marjoram).

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Melon

Muskmelon, including hybrids and/or varieties of
Cucumis melo
(including true cantaloupe,
cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew
melon, honey balls, Persian melon, golden pershaw melon, mango
melon, pineapple melon, snake melon); and watermelon, including
hybrids and/or varieties of ( Citrullus
spp.).

Muskmelon

Cucumis melo
(includes true cantaloupe,
cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew
melon, honey balls, Persian melon, golden pershaw melon, mango
melon, pineapple melon, snake melon, and other varieties and/or
hybrids of these.)

Onion

Bulb onion; green onion; and garlic.

Onion, bulb

Bulb onion; garlic; great headed garlic; serpent garlic; Chinese onion;
pearl onion; potato onion; and shallot, bulb.

Onion, green

Green onion; lady's leek; leek; wild leek; Beltsville bunching onion;
fresh onion; tree onion, tops; Welsh onion; and shallot, fresh leaves.

Peach

Peach, nectarine

Pea

Cajanus cajan
(includes pigeon
spp. (includes chickpea and garbanzo bean);
pea); Cicer
Lens culinaris
(lentil);
Pisum
spp. (includes dwarf pea, garden pea, green pea,
English pea, field pea, and edible pod pea). [Note: A variety of pesticide
tolerances have been previously established for pea and/or bean.
Chickpea/garbanzo bean is now classified in both the bean and the pea
categories. For garbanzo bean/chickpea only, the highest established
pea or bean tolerance will apply to pesticide residues found in this
commodity.]

Pea, dry

All peas in dry form only.

Pea, succulent

All peas in succulent form only.

Pepper

All varieties of pepper including pimento and bell, hot, and sweet
pepper.

Radish,
oriental, roots

Raphanus sativus
var.
longipinnatus
(roots and tops),
including Chinese or Japanese radish (both white and red), winter
radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Radish,
oriental, tops)

Raphanus sativus
var.
longipinnatus
(roots and tops),
including Chinese or Japanese radish (both white and red), winter
radish, daikon, lobok, lo pak, and other cultivars and/or hybrids of these.

Rapeseed

Brassica napus
, B.
, and Crambe
campestris
abyssinica
(oilseed-producing varieties only
which include canola and crambe.)

Raspberry

Rubus
spp. (including bababerry; black raspberry; blackcap;
caneberry; framboise; frambueso; himbeere; keriberry; mayberry; red
raspberry; thimbleberry; tulameen; yellow raspberry; and cultivars,
varieties, and/or hybrids of these).

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Sorghum,
grain, grain

Sorghum
spp. [sorghum, grain, sudangrass (seed crop),
and hybrids of these grown for its seed].

Sorghum,
forage, stover

Sorghum
spp. [sorghum, forage; sorghum, stover;
sudangrass, and hybrids of these grown for forage and/or stover.

Squash

Pumpkin, summer squash, and winter squash.

Sugar apple

Annona squamosa L
.
(sugar apple, sweetsop, anon), and its hybrid A.
squamosa L. x A.
cherimoya M
. (atemoya). Also A.
. (true custard apple).
reticulata L

Squash,
summer

Fruits of the gourd ( Cucurbitaceae
)
family that are consumed when immature, 100% of the fruit is edible
either cooked or raw, once picked it cannot be stored, has a soft rind
which is easily penetrated, and if seeds were harvested they would not
germinate; e.g., Cucurbita pepo
( i.e.
, crookneck squash, straightneck squash, scallop
spp.
squash, and vegetable marrow); Lagenaria
, spaghetti squash, hyotan, cucuzza);
( i.e.
Luffa
spp. ( i.e.
, hechima, Chinese okra);
Momordica
spp. ( i.e.
, bitter melon,
balsam pear, balsam apple, Chinese cucumber);
Sechium edule
(chayote); and other
cultivars and/or hybrids of these.

Sweet potato

Sweet potato, yam.

Tangerine

Tangerine (mandarin or mandarin orange); tangelo, tangor, and other
hybrids of tangerine with other citrus.

Tomato

Tomato, tomatillo.

Turnip tops or
turnip greens

Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip
greens).

Wheat

Wheat, triticale.

(h) Unless otherwise specified, tolerances and exemptions established under the regulations in this part
apply to residues from only preharvest application of the chemical.
(i) Unless otherwise specified in this paragraph or in tolerance regulations prescribed in this part for
specific pesticide chemicals, the raw agricultural commodity or processed food to be examined for
pesticide residues, shall consist of the whole raw agricultural commodity or processed food.
(1) The raw agricultural commodity bananas, when examined for pesticide residues, shall not include any
crown tissue or stalk.
(2) Shell shall be removed and discarded from nuts before examination for pesticide residues.
(3) Caps (hulls) shall be removed and discarded from strawberries before examination for pesticide
residues.
(4) Stems shall be removed and discarded from melons before examination for pesticide residues.
(5) Roots, stems, and outer sheaths (or husks) shall be removed and discarded from garlic bulbs and dry
bulb onions, and only the garlic cloves and onion bulbs shall be examined for pesticide residues.

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(6) Where a tolerance is established on a root vegetable including tops and/or with tops, and the tops and
the roots are marketed together, they shall be analyzed separately and neither the pesticide residue on
the roots nor the pesticide residue on the tops shall exceed the tolerance level, except that in the case of
carrots, parsnips, and rutabagas, the tops shall be removed and discarded before analyzing roots for
pesticide residues.
(7) The crowns (leaves at the top of the fruit) shall be removed and discarded from pineapples before
examination for pesticide residues.
(8) The term lima beans means the beans and the pod.
(9) The term peanuts means the peanut meat after removal of the hulls.
(10) For processed foods consisting primarily of one ingredient and sold in a form requiring further
preparation prior to consumption (e.g., fruit juice concentrates, dehydrated vegetables, and powdered
potatoes), the processed food to be examined for residues shall be the whole processed commodity after
compensating for or reconstituting to the commodity's normal moisture content, unless a tolerance for the
concentrated or dehydrated food form is included in this part. If there exists a tolerance for a specific
pesticide on the processed food in its concentrated or dehydrated food form, for the purpose of
determining whether the food is in compliance with that tolerance, the processed food to be examined for
residues shall be the whole processed commodity on an “as is” basis.
(j) The term pesticide chemical shall have the meaning specified in FFDCA section 201(q)(1), as
amended, except as provided in §180.4.
(k) The term negligible residue means any amount of a pesticide chemical remaining in or on a raw
agricultural commodity or group of raw agricultural commodities that would result in a daily intake regarded
as toxicologically insignificant on the basis of scientific judgment of adequate safety data. Ordinarily this
will add to the diet an amount which will be less than 1/2,000th of the amount that has been demonstrated
to have no effect from feeding studies on the most sensitive animal species tested. Such toxicity studies
shall usually include at least 90-day feeding studies in two species of mammals.
(l) The term nonperishable raw agricultural commodity means any raw agricultural commodity not subject
to rapid decay or deterioration that would render it unfit for consumption. Examples are cocoa beans,
coffee beans, field-dried beans, field-dried peas, grains, and nuts. Not included are eggs, milk, meat,
poultry, fresh fruits, and vegetables such as onions, parsnips, potatoes, and carrots.
(m) The term tolerance with regional registration means any tolerance which is established for pesticide
residues resulting from the use of the pesticide pursuant to a regional registration. Such a tolerance is
supported by residue data from specific growing regions for a raw agricultural commodity. Individual
tolerances with regional registration are designated in separate subsections in 40 CFR 180.101 through
180.999, as appropriate. Additional residue data which are representative of the proposed use area are
required to expand the geographical area of usage of a pesticide on a raw agricultural commodity having
an established “tolerance with regional registration.” Persons seeking geographically broader registration
of a crop having a “tolerance with regional registration” should contact the appropriate EPA product
manager concerning additional residue data required to expand the use area.
(n) The term pesticide chemical residue shall have the meaning specified in FFDCA section 201(q)(2), as
amended, except as provided in §180.4.
(o) The term food commodity means:
(1) Any raw agricultural commodity (food or feed) as defined in section 201(r) of the Federal Food, Drug,
and Cosmetic Act (FFDCA); and
(2) Any processed food or feed as defined in section 201(gg) of the FFDCA.

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[36 FR 22540, Nov. 25, 1971]
Editorial Note: ForFederal Registercitations affecting §180.1, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.3 Tolerances for related pesticide chemicals.
top
(a) Pesticide chemicals that cause related pharmacological effects will be regarded, in the absence of
evidence to the contrary, as having an additive deleterious action. (For example, many pesticide
chemicals within each of the following groups have related pharmacological effects: Chlorinated organic
pesticides, arsenic-containing chemicals, metallic dithiocarbamates, cholinesterase-inhibiting pesticides.)
(b) Tolerances established for such related pesticide chemicals may limit the amount of a common
component (such as As2O3) that may be present, or may limit the amount of biological activity (such as
cholinesterase inhibition) that may be present, or may limit the total amount of related pesticide chemicals
(such as chlorinated organic pesticides) that may be present.
(c)(1) Where tolerances for inorganic bromide in or on the same raw agricultural commodity are set in two
or more sections in this part (example: §§180.123 and 180.199), the overall quantity of inorganic bromide
to be tolerated from use of the same pesticide in different modes of application or from two or more
pesticide chemicals for which tolerances are established is the highest of the separate applicable
tolerances. For example, where the bromide tolerance on asparagus from methyl bromide commodity
fumigation is 100 parts per million (40 CFR 180.123) and on asparagus from methyl bromide soil
treatment is 300 parts per million (40 CFR 180.199), the overall inorganic bromide tolerance for asparagus
grown on methyl bromide-treated soil and also fumigated with methyl bromide after harvest is 300 parts
per million.
(2) Where tolerances are established in terms of inorganic bromide residues only from use of organic
bromide fumigants on raw agricutural commodities, such tolerances are sufficient to protect the public
health, and no additional concurrent tolerances for the organic pesticide chemicals from such use are
necessary. This conclusion is based on evidence of the dissipation of the organic pesticide or its
conversion to inorganic bromide residues in the food when ready to eat.
(d)(1) Where tolerances are established for both calcium cyanide and hydrogen cyanide on the same raw
agricultural commodity, the total amount of such pesticides shall not yield more residue than that permitted
by the larger of the two tolerances, calculated as hydrogen cyanide.
(2) Where tolerances are established for residues of both O,O -diethyl S -[2-(ethylthio)ethyl]
phosphorodithioate and demeton (a mixture of O,O -diethyl O -(and S -) [2-(ethylthio)ethyl]
phosphorothioates) on the same raw agricultural commodity, the total amount of such pesticides shall not
yield more residue than that permitted by the larger of the two tolerances, calculated as demeton.
(3) Where tolerances are established for both terpene polychlorinates (chlorinated mixture of camphene,
pinene, and related terpenes, containing 65–66 percent chlorine) and toxaphene (chlorinated camphene
containing 67–69 percent chlorine) on the same raw agricultural commodities, the total amount of such
pesticides shall not yield more residue than that permitted by the larger of the two tolerances, calculated
as a chlorinated terpene of molecular weight 396.6 containing 67 percent chlorine.
(4) Where a tolerance is established for more than one pesticide containing arsenic found in, or on a raw
agricultural commodity, the total amount of such pesticide shall not exceed the highest established
tolerance calculated as As2O3.
(5) Where tolerances are established for more than one member of the class of dithiocarbamates listed in
paragraph (e)(3) of this section on the same raw agricultural commodity, the total residue of such

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pesticides shall not exceed that permitted by the highest tolerance established for any one member of the
class, calculated as zinc ethylenebisdithiocarbamate.
(6) Where tolerances are established for residues of both S,S,S -tributyl phosphorotrithioate and tributyl
phosphorotrithioite in or on the same raw agricultural commodity, the total amount of such pesticides shall
not yield more residue than that permitted by the higher of the two tolerances, calculated as S,S,S -tributyl
phosphorotrithioate.
(7) Where tolerances are established for residues of α-naphthaleneacetamide and/or α-naphthaleneacetic
acid in or on the same raw agricultural commodity, the total amount of such pesticides shall not yield more
residue than that permitted by the higher of the two tolerances, calculated as α-naphthaleneacetic acid.
(8) Where tolerances are established for residues of O,S -dimethyl phosphoramidothioate, resulting from
the use of acephate ( O,S -dimethyl acetylphos-phoramidothioate) and/or O,S dimethylphosphoramidothioate on the same agricultural commodity, the total amount of O,S -dimethylphosphoramidothioate shall not yield more residue than that permitted by the higher of the two tolerances.
(9) Where a tolerance is established for more than one pesticide having the metabolites 1-(3,4dichlorophenyl)-3-methylurea (DCPMU) and 3,4-dichlorophenylurea (DCPU) found in or on a raw
agricultural commodity, the total amount of such residues shall not exceed the highest established
tolerance for a pesticide having these metabolites.
(10) Where a tolerance is established for more than one pesticide having as metabolites compounds
containing the benzimidazole moiety found in or on a raw agricultural commodity, the total amount of such
residues shall not exceed the highest established tolerance for a pesticide having these metabolites.
(11) Where a tolerance is established for triclopyr, chloropyrifos, and chlorpyrifos-methyl having the
common metabolite 3,5,6-trichloro-2-pyridinol on the same raw agricultural commodity, the total amount of
such residues shall not exceed the highest established tolerance for any of the pesticides having the
metabolites.
(12) Where tolerances are established for more than one pesticide having the metabolite 3,5,6-trichloro-2pyridinol found in or on the raw agricultural commodity, the total amount of such residues shall not exceed
the highest established tolerance for a pesticide having this metabolite.
(13) Where tolerances are established for residues of methomyl, resulting from the use of thiodicarb and/
or methomyl on the same raw agricultural commodity, the total amount of methomyl shall not yield more
residue than that permitted by the higher of the two tolerances.
(e) Except as noted in paragraphs (e)(1) and (2) of this section, where residues from two or more
chemicals in the same class are present in or on a raw agricultural commodity the tolerance for the total of
such residues shall be the same as that for the chemical having the lowest numerical tolerance in this
class, unless a higher tolerance level is specifically provided for the combined residues by a regulation in
this part.
(1) Where residues from two or more chemicals in the same class are present in or on a raw agricultural
commodity and there are available methods that permit quantitative determination of each residue, the
quantity of combined residues that are within the tolerance may be determined as follows:
(i) Determine the quantity of each residue present.
(ii) Divide the quantity of each residue by the tolerance that would apply if it occurred alone, and multiply
by 100 to determine the percentage of the permitted amount of residue present.
(iii) Add the percentages so obtained for all residues present.
(iv) The sum of the percentages shall not exceed 100 percent.

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(2) Where residues from two or more chemicals in the same class are present in or on a raw agricultural
commodity and there are available methods that permit quantitative determinations of one or more, but not
all, of the residues, the amounts of such residues as may be determinable shall be deducted from the total
amount of residues present and the remainder shall have the same tolerance as that for the chemical
having the lowest numerical tolerance in that class. The quantity of combined residues that are within the
tolerance may be determined as follows:
(i) Determine the quantity of each determinable residue present.
(ii) Deduct the amounts of such residues from the total amount of residues present and consider the
remainder to have the same tolerance as that for the chemical having the lowest numerical tolerance in
that class.
(iii) Divide the quantity of each determinable residue by the tolerance that would apply if it occurred alone
and the quantity of the remaining residue by the tolerance for the chemical having the lowest numerical
tolerance in that class and multiply by 100 to determine the percentage of the permitted amount of residue
present.
(iv) Add the percentages so obtained for all residues present.
(v) The sum of the percentages shall not exceed 100 percent.
(3) The following pesticides are members of the class of dithiocarbamates:

A mixture of 5.2 parts by weight of ammoniates of [ethylenebis (dithiocarbamato)] zinc with 1 part
by weight ethylenebis [dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and
disulfides.
2-Chloroallyl diethyldithiocarbamate.
Coordination product of zinc ion and maneb containing 20 percent manganese, 2.5 percent zinc,
and 77.5 percent ethylenebisdithiocarbamate.
Ferbam.
Maneb.
Manganous dimethyldithiocarbamate.
Sodium dimethyldithiocarbamate.
Thiram.
Zineb.
Ziram.
(4) The following are members of the class of chlorinated organic pesticides:

Aldrin.
BHC (benzene hexachloride).

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1,1-Bis( p -chlorophenyl)-2,2,2-trichloroethanol.
Chlorbenside ( p -chlorobenzyl p -chlorophenyl sulfide).
Chlordane.
Chlorobenzilate (ethyl 4,4′-dichlorobenzilate).
p -Chlorophenoxyacetic acid.
p -Chlorophenyl-2,4,5-trichlorophenyl sulfide.
2,4-D (2,4-dichlorophenoxyacetic acid).
DDD (TDE).
DDT.
1,1-Dichloro-2,2-bis( p -ethylphenyl) ethane.
2,6-Dichloro-4-nitroaniline.
2,4-Dichlorophenyl p -nitrophenyl ether.
Dieldrin.
Dodecachlorooctahydro-1,3,4-metheno-2 H -cyclobuta[ cd ]pentalene.
Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, 6,9,9a-hexahydro-6,9-methano-2,4,3benzodioxathiepin-3-oxide).
Endosulfan sulfate (6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3benzodioxathiepin-3,3-dioxide).
Heptachlor (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a-tetrahydro-4,7-methanoindene).
Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro-2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7methanoindene).
Hexachlorophene (2,2′-methylenebis(3,4,6-trichlorophenol) and its monosodium salt.
Isopropyl 4,4′-dichlorobenzilate.
Lindane.
Methoxychlor.
Ovex ( p -chlorophenyl p -chlorobenzenesulfonate).
Sesone (sodium 2,4-dichlorophenoxyethyl sulfate, SES).
Sodium 2,4-dichlorophenoxyacetate.
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Sodium trichloroacetate.
Sulphenone ( p -chlorophenyl phenyl sulfone).
Terpene polychlorinates (chlorinated mixture of camphene, pinene, and related terpenes 65-66
percent chlorine).
2,3,5,6-Tetrachloronitrobenzene.
Tetradifon (2,4,5,4′-tetrachlorodiphenyl sulfone).
Toxaphene (chlorinated camphene).
Trichlorobenzoic acid.
Trichlorobenzyl chloride.
(5) The following are members of the class of cholinesterase-inhibiting pesticides:

Acephate ( O,S -dimethyl acetyl-phosphoramidothioate) and its cholinesterase-inhibiting
metabolite O,S -dimethyl phosphoramidothioate.
Aldicarb (2-methyl-2-(methylthio) propionaldehyde O -(methylcarbamoyl)oxime) and its
chlorinesterase-inhibiting metabolites 2-methyl-2-(methylsulfinyl)propionaldehyde O (methycarbamoyl) oxime and 2-methyl-2-(methylsulfonyl)propionaldehyde O -(methylcarbamoyl)
oxime.
4- tert -Butyl-2-chlorophenyl methyl methyl phosphoramidate.
S-[( tert -Butylthio)methyl] O,O -diethyl phosphorodithioate and its cholinesterase-inhibiting
metabolites.
Carbaryl (1-naphthyl N -methylcarbamate).
Carbofuran (2,3,-dihydro-2,2-dimethyl-7-benzofuranyl- N -methylcarbamate).
Carbofuran metabolite (2,3-dihydro-2,2-dimethyl-3-hydroxy-7-benofuranyl N -methylcarbamate).
Carbophenothion ( S -[( p -chlorophenyl) thiolmethyl] O,O -diethyl phosphorodithioate) and its
cholinesterase-inhibiting metabolites.
Chlorpyrifos ( O,O -diethyl O -(3,5,6-trichloro-2-pyridyl)phosphorothioate).
Chlorpyrifos-methyl ( O,O -dimethyl- O -(3,5,6-trichloro-2-pyridyl) phosphorothioate.
2-Chloro-1-(2,4,5-trichlorophenyl)vinyl dimethyl phosphate.
2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl phosphate.
Coumaphos ( O,O -diethyl O -3-chloro-4-methyl-2-oxo-2 H -1-benzopyran-7-yl phosran-7-yl
phosphate).

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Coumaphos oxygen analog ( O,O -diethyl O -3-chloro-4-methyl-2-oxo-2 H -1-benzopyphorothioate).
Dialifor ( S -(2-chloro-1-phthalimidoethyl) O,O -diethyl phosphorodithioate).
Dialifor oxygen analog ( S -(2-chloro-1-phthalimidoethyl) O,O -diethyl phosphorothioate).
Demeton (a mixture of O,O -diethyl O -(and S ) [2-ethylthio)ethyl] phosphorothioates).
Ethiolate ( S -ethyl diethylthiocarbamate).
2,2-Dichlorovinyl dimethyl phosphate.
O,O -Diethyl S -[2-(ethylthio)ethyl] phosphorodithioate and its cholinesterase-inhibiting metabolites.
O,O -Diethyl O -(2-diethylamino-6-methyl-4-pyrimidinyl) phosphorothioate and its oxygen analog
diethyl 2-diethylamino-6-methyl-4-pyrimidinyl phosphate.
O,O -Diethyl O -(2-isoprophyl-4-methyl-6-pyrimidinyl) phosphorothioate.
O,O -Diethyl O -[ p -(methylsulfinyl)phenyl] phosphorothioate and its cholinesterase-inhibiting
metabolites.
Diethyl 2-pyrazinyl phosphate.
O,O -Diethyl O -2-pyrazinyl phosphorothioate.
S -( O,O -Diisopropyl phosphorodithioate) of N -(2-mercaptoethyl) benzenesulfonamide
S -( O,O -Diisopropyl phosphorodithioate) of N -(2-mercaptoethyl) benzenesulfonamide
2-(Dimethylamino)-5.6-dimethyl-4-pyrimidinyl dimethylcarbamate and its metabolites 5,6-dimethyl2-(formylmethylamino)-4-pyrimidinyl dimethylcarbamate and 5,6-dimethyl-2-(methylamino)-4pyrimidinyl dimethylcarbamate (both calculated as parent).
Dimethoate ( O,O -dimethyl S -( N -methyl-carbamoylmethyl) phosphorodithioate).
Dimethoate oxygen analog ( O,O -dimethyl S -( N -methylcarbamoylmethyl) phosphorothioate).
O,O -Dimethyl O-p -(dimethylsulfamoyl) phenyl phosphate.
O,O -Dimethyl O-p- (dimethylsulfamoyl) phenyl phosphorothioate.
3,5-Dimethyl-4-(methylthio) phenyl methylcarbamate.
O,O -Dimethyl S -[4-oxo-1,2,3-benzotriazin-3-(4 H )-ylmethyl] phosphorodithioate.
Dimethyl phosphate of 3-hydroxy- N,N -dimethyl- cis -crotonamide.
Dimethyl phosphate of 3-hydroxy- N -methyl- cis -crotonamide.
Dimethyl phosphate of α-methylbenzyl 3-hydroxy- cis -crotonate.

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O,O -Dimethyl 2,2,2-trichloro-1-hydroxyethyl phosphonate.
O,O -Dimethyl phosphorodithioate, S -ester with 4-(mercaptomethyl)-2-methozy-Δ2-1,3,4thiadiazolin-5-one.
Dioxathion (2,3- p -dioxanedithiol S,S -bis ( O,O -diethylphosphorodithioate)) containing
approximately 70 percent cis and trans isomers and approximately 30 percent related compounds.
EPN.
Ethephon ((2- - chloroethyl) phosphonic acid).
Ethion.
Ethion oxygen analog ( S -[[(diethoxyphosphinothioyl)thio] methyl] O,O -diethyl phosphorothioate).
O- Ethyl O -[4-(methylthio) phenyl] S -propyl phosphorodithioate and its cholinesterase-inhibiting
metabolites.
O -Ethyl S,S -dipropylphosphorodithioate.
Ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl) phosphoramidate and its cholinesteraseinhibiting metabolites.
O -Ethyl S -phenyl ethylphosphonodithioate.
O -Ethyl S -phenyl ethylphosphonothiolate.
m -(1-Ethylpropyl)phenyl methylcarbamate.
S -[2-Ethylsulfinyl)ethyl] O,O -dimethyl phosphorothioate and its cholinesterase-inhibiting
metabolites, (primarily S -[2-(ethyl-sulfonyl)ethyl] O,O -dimethyl phosphorothioate).
Fenthion ( O,O -dimethyl O -[3-methyl-4-(methylthio)phenyl]phosphorothioate and its
cholinesterase-inhibiting metabolites.
Malathion.
N -(Mercaptomethyl)phthalimide S -( O,O -dimethyl phosphorodithioate).
N -(Mercaptomethyl)phthalimide S -( O,O -dimethyl phosphorothioate).
Methomyl ( S -methyl N -[(methylcarbamoyl)oxy]thioacetimidate).
1-Methoxycarbonyl-1-propen-2-yl dimethyl phosphate and its beta isomer.
m -(1-Methylbutyl)phenyl methylcarbamate.
Methyl parathion.
Naled (1,2-dibromo-2,2-dichloroethyl dimethyl phosphate).

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Oxamyl (methyl N′,N′-dimethyl-N-[(methylcarbamoyl)oxy]-1-thiooxamimidate)
Parathion.
Phorate ( O,O -diethyl S -(ethylthio)methyl phosphorodithioate) and its cholinesterase-inhibiting
metabolites.
Phosalone ( S -(6-chloro-3-mercaptomethyl)-2-benzoxazolinone) O,O -diethyl phosphorodithioate).
Phosphamidon (2-chloro-2-diethylcarbamoyl-1-methylvinyl dimethyl phosphate) including all of its
related cholinesterase-inhibiting compounds.
Pirimiphos-methyl O -[2-diethylamino-6-methyl-pyrimidinyl) O , O -dimethyl phosphorothioate
Ronnel.
Schradan (octamethylpyrophosphoramide).
Tetraethyl pyrophosphate.
O,O,O′,O′ -Tetramethyl O,O′ -sulfinyldi- p -phenylene phosphorothioate.
O,O,O′,O′ -Tetramethyl O,O′ -thiodi- p -phenylene phosphorothioate.
Tributyl phosphorotritlioite.
S,S,S -Tributyl phosphorothrithioate.
3,4,5-Trimethylphenyl methylcarbamate and its isomer 2,3,5-trimethylphenyl methylcarbamate.
(6) The following pesticides are members of the class of dinitrophenols:

2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate, mixture of.
4,6-Dinitro- o -cresol and its sodium salt.
Dinoseb (2- sec -butyl-4,6-dinitrophenol) and its alkanolamine, ammonium, and sodium salts.
[41 FR 8969, Mar. 2, 1976]
Editorial Note: ForFederal Registercitations affecting §180.3, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.4 Exceptions.
top
The substances listed in this section are excepted from the definitions of “pesticide chemical” and
“pesticide chemical residue” under FFDCA section 201(q)(3) and are therefore exempt from regulation
under FFDCA section 402(a)(2)(B) and 408. These substances are subject to regulation by the Food and
Drug Administration as food additives under FFDCA section 409.

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(a) Inert ingredients in food packaging treated with a pesticide, when such inert ingredients are the
components of the food packaging material (e.g. paper and paperboard, coatings, adhesives, and
polymers).
(b) [Reserved]
[63 FR 10720, Mar. 4, 1998, as amended at 73 FR 54976, Sept. 24, 2008]

§ 180.5 Zero tolerances.
top
A zero tolerance means that no amount of the pesticide chemical may remain on the raw agricultural
commodity when it is offered for shipment. A zero tolerance for a pesticide chemical in or on a raw
agricultural commodity may be established because, among other reasons:
(a) A safe level of the pesticide chemical in the diet of two different species of warm-blooded animals has
not been reliably determined.
(b) The chemical is carcinogenic to or has other alarming physiological effects upon one or more of the
species of the test animals used, when fed in the diet of such animals.
(c) The pesticide chemical is toxic, but is normally used at times when, or in such manner that, fruit,
vegetables, or other raw agricultural commodities will not bear or contain it.
(d) All residue of the pesticide chemical is normally removed through good agricultural practice such as
washing or brushing or through weathering or other changes in the chemical itself, prior to introduction of
the raw agricultural commodity into interstate commerce.

§ 180.6 Pesticide tolerances regarding milk, eggs, meat, and/or poultry; statement of
policy.
top
(a) When establishing tolerances for pesticide residues in or on raw agricultural commodities,
consideration is always given to possible residues of those pesticide chemicals or their conversion
products entering the diet of man through the ingestion of milk, eggs, meat, and/or poultry produced by
animals fed agricultural products bearing such pesticide residues. In each instance an evaluation of all
available data will result in a conclusion either:
(1) That finite residues will actually be incurred in these foods from feed use of the raw agricultural
commodity including its byproducts; or
(2) That it is not possible to establish with certainty whether finite residues will be incurred, but there is a
reasonable expectation of finite residues; or
(3) That it is not possible to establish with certainty whether finite residues will be incurred, but there is no
reasonable expectation of finite residues.
(b) When the data show that finite residues will actually be incurred in milk, eggs, meat, and/or poultry, a
tolerance will be established on the raw agricultural commodity used as feed provided that tolerances can
be established at the same time, on the basis of the toxicological and other data available, for the finite
residues incurred in milk, eggs, meat, and/or poultry. When it is not possible to determine with certainty
whether finite residues will be incurred in milk, eggs, meat, and/or poultry but there is a reasonable
expectation of finite residues in light of data reflecting exaggerated pesticides levels in feeding studies, a

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tolerance will be established on the raw agricultural commodity provided that appropriate tolerances can
be established at the same time, on the basis of the toxicological and other data available, for the finite
residues likely to be incurred in these foods through the feed use of the raw agricultural commodity or its
byproducts. When it is not possible to determine with certainty whether finite residues will be incurred in
milk, eggs, meat, and/or poultry but there is no reasonable expectation of finite residues in light of data
such as those reflecting exaggerated pesticide levels in feeding studies and those elucidating the
biochemistry of the pesticide chemical in the animal, a tolerance may be established on the raw
agricultural commodity without the necessity of a tolerance on food products derived from the animal.
(c) The principles outlined in paragraphs (a) and (b) of this section will also be followed with respect to
tolerances for residues which will actually be incurred or are reasonably to be expected in milk, eggs,
meat, and/or poultry by the use of pesticides directly on the animal or administered purposely in the feed
or drinking water.
(d) Tolerances contemplated by paragraphs (a) and (b) of this section will in addition to toxicological
considerations be conditioned on the availability of a practicable analytical method to determine the
pesticide residue; that is, the method must be sensitive and reliable at the tolerance level or in special
cases at a higher level where such level is deemed satisfactory and safe in light of the toxicity of the
pesticide residue and of the unlikelihood of such residue exceeding the tolerance. The analytical methods
to be used for enforcement purposes will be those set forth in the “Pesticide Analytical Manual” (see
§180.101(c)). The sensitivities of these methods are expressed in that manual.

Subpart B—Procedural Regulations
top

§ 180.7 Petitions proposing tolerances or exemptions for pesticide residues in or on
raw agricultural commodities or processed foods.
top
(a) Petitions to be filed with the Agency under the provisions of FFDCA section 408(d) shall be submitted
in duplicate. If any part of the material submitted is in a foreign language, it shall be accompanied by an
accurate and complete English translation. The petition shall be accompanied by an advance deposit for
fees described in §180.33. The petition shall state the petitioner's mail address to which notice of objection
under FFDCA section 408(g)(2) may be sent. The petition must be signed by the petitioner or by his
attorney or agent, or (if a corporation) by an authorized official.
(b) Petitions shall include the following information:
(1) An informative summary of the petition and of the data, information, and arguments submitted or cited
in support of the petition. Both a paper and electronic copy of the summary should be submitted. The
electronic copy should be formatted according to the Office of Pesticide Programs' current standard for
electronic data submission as specified at http://www.epa.gov/pesticides/regulating/registering/
submissions/index.htm .
(2) A statement that the petitioner agrees that such summary or any information it contains may be
published as a part of the notice of filing of the petition to be published under FFDCA section 408(d)(3)
and as a part of a proposed or final regulation issued under FFDCA section 408.
(3) The name, chemical identity, and composition of the pesticide chemical residue and of the pesticide
chemical that produces the residue.
(4) Data showing the recommended amount, frequency, method, and time of application of the pesticide
chemical.

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(5) Full reports of tests and investigations made with respect to the safety of the pesticide chemical,
including full information as to the methods and controls used in conducting those tests and investigations.
(6) Full reports of tests and investigations made with respect to the nature and amount of the pesticide
chemical residue that is likely to remain in or on the food, including a description of the analytical methods
used. (See §180.34 for further information about residue tests.)
(7) Proposed tolerances for the pesticide chemical residue if tolerances are proposed.
(8) Practicable methods for removing any amount of the residue that would exceed any proposed
tolerance.
(9) A practical method for detecting and measuring the levels of the pesticide chemical residue in or on the
food, or for exemptions, a statement why such a method is not needed.
(10) If the petition relates to a tolerance for a processed food, reports of investigations conducted using
the processing method(s) used to produce that food.
(11) Such information as the Administrator may require to make the determination under FFDCA section
408(b)(2)(C).
(12) Such information as the Administrator may require on whether the pesticide chemical may have an
effect in humans that is similar to an effect produced by a naturally occurring estrogen or other endocrine
effects.
(13) Information regarding exposure to the pesticide chemical residue due to any tolerance or exemption
already granted for such residue.
(14) Information concerning any maximum residue level established by the Codex Alimentarius
Commission for the pesticide chemical residue addressed in the petition. If a Codex maximum residue
level has been established for the pesticide chemical residue and the petitioner does not propose that this
level be adopted, a statement explaining the reasons for this departure from the Codex level.
(15) Such other data and information as the Administrator requires by regulation to support the petition.
(16) Reasonable grounds in support of the petition.
(c) The data specified under paragraphs (b)(1) through (b)(16) of this section should be on separate
sheets or sets of sheets, suitably identified. If such data have already been submitted with an earlier
application, the present petition may incorporate it by reference to the earlier one.
(d) Except as noted in paragraph (e) of this section, a petition shall not be accepted for filing if any of the
data prescribed by FFDCA section 408(d) are lacking or are not set forth so as to be readily understood.
The availability to the public of information provided to, or otherwise obtained by, the Agency under this
part shall be governed by part 2 of this chapter. The Administrator shall make the full text of the summary
referenced in paragraph (b)(1) of this section available to the public in the public docket at http://www.
regulations.gov no later than publication in theFederal Registerof the notice of the petition filing.
(e) The Administrator shall notify the petitioner within 15 days after its receipt of acceptance or
nonacceptance of a petition, and if not accepted the reasons therefor. If petitioner desires, the petitioner
may supplement a deficient petition after notification as to deficiencies. If the petitioner does not wish to
supplement or explain the petition and requests in writing that it be filed as submitted, the petition shall be
filed and the petitioner so notified.
(f) A notice of the filing of a petition for a pesticide chemical residue tolerance that the Administrator
determines has met the requirements of paragraph (b) of this section shall be published in theFederal
Registerby the Administrator within 30 days after such determination. The notice shall state the name of
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the pesticide chemical residue and the commodities for which a tolerance is sought and announce the
availability of a description of the analytical methods available to the Administrator for the detection and
measurement of the pesticide chemical residue with respect to which the petition is filed or shall set forth
the petitioner's statement of why such a method is not needed. The notice shall explicitly reference the
specific docket identification number in the public docket at http://www.regulations.gov where the full text
of the summary required in paragraph (b) of this section is located, and refer interested parties to this
document for further information on the petition. The full text of the summary may be omitted from the
notice.
(g) The Administrator may request a sample of the pesticide chemical at any time while a petition is under
consideration. The Administrator shall specify in its request for a sample of the pesticide chemical, a
quantity which it deems adequate to permit tests of analytical methods used to determine residues of the
pesticide chemical and of methods proposed by the petitioner for removing any residues of the chemical
that exceed the tolerance proposed.
(h) The Administrator shall determine, in accordance with the Act, whether to issue an order that
establishes, modifies, or revokes a tolerance regulation (whether or not in accord with the action proposed
by the petitioner), whether to publish a proposed tolerance regulation and request public comment thereon
under §180.29, or whether to deny the petition. The Administrator shall publish in theFederal Registersuch
order or proposed regulation. After receiving comments on any proposed regulation, the Administrator
may issue an order that establishes, modifies, or revokes a tolerance regulation. An order published under
this section shall describe briefly how to submit objections and requests for a hearing under part 178 of
this chapter. A regulation issued under this section shall be effective on the date of publication in
theFederal Registerunless otherwise provided in the regulation.
[70 FR 33360, June 8, 2005, as amended at 73 FR 75600, Dec. 12, 2008]

§ 180.8 Withdrawal of petitions without prejudice.
top
In some cases the Administrator will notify the petitioner that the petition, while technically complete, is
inadequate to justify the establishment of a tolerance or the tolerance requested by petitioner. This may be
due to the fact that the data are not sufficiently clear or complete. In such cases, the petitioner may
withdraw the petition pending its clarification or the obtaining of additional data. This withdrawal may be
without prejudice to a future filing. A deposit for fees as specified in §180.33 shall accompany the
resubmission of the petition.
[70 FR 33361, June 8, 2005]

§ 180.9 Substantive amendments to petitions.
top
After a petition has been filed, the petitioner may submit additional information or data in support thereof,
but in such cases the petition will be given a new filing date.
[70 FR 33361, June 8, 2005]

§ 180.29 Establishment, modification, and revocation of tolerance on initiative of
Administrator.
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(a) Upon the Administrator's own initiative, the Administrator may propose, under FFDCA section 408(e),

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the issuance of a regulation establishing a tolerance for a pesticide chemical or exempting it from the
necessity of a tolerance, or a regulation modifying or revoking an existing tolerance or exemption.
(b) The Administrator shall provide a period of not less than 60 days for persons to comment on the
proposed regulation, except that a shorter period for comment may be provided if the Administrator for
good cause finds that it would be in the public interest to do so and states the reasons for the finding in the
notice of proposed rulemaking.
(c) After reviewing any timely comments received, the Administrator may by order establish, modify, or
revoke a tolerance regulation, which order and regulation shall be published in theFederal Register.An
order published under this section shall state that persons may submit objections and requests for a
hearing in the manner described in part 178 of this chapter.
(d) Any final regulation issued under this section shall be effective on the date of publication in theFederal
Registerunless otherwise provided in the regulation.
[70 FR 33361, June 8, 2005]

§ 180.30 Judicial review.
top
(a) Under FFDCA section 408(h), judicial review is available in the United States Courts of Appeal as to
the following actions:
(1) Regulations establishing general procedures and requirements under FFDCA section 408(e)(1)(C).
(2) Orders issued under FFDCA section 408(f)(1)(C) requiring the submission of data.
(3) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to establishment, modification,
or revocation of a tolerance or exemption under FFDCA section 408(d)(4), or any regulation that is the
subject of such an order. The underlying action here is Agency disposition of a petition seeking the
establishment, modification, or revocation of a tolerance or exemption.
(4) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the denial of a petition under
FFDCA section 408(d)(4).
(5) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the establishment,
modification, suspension, or revocation of a tolerance or exemption under FFDCA section 408(e)(1)(A) or
(e)(1)(B). The underlying action here is the establishment, modification, suspension, or revocation of a
tolerance or exemption upon the initiative of EPA including EPA actions pursuant to FFDCA sections 408
(b)(2)(B)(v), 408(b)(2)(E)(ii), 408(d)(4)(C)(ii), 408(l)(4), and 408(q)(1).
(6) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the revocation or modification
of a tolerance or exemption under FFDCA section 408(f)(2) for noncompliance with requirements for the
submission of data.
(7) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to rules issued under FFDCA
sections 408(n)(3) and 408(d) or (e) regarding determinations pertaining to State authority to establish
regulatory limits on pesticide chemical residues.
(8) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to orders issued under FFDCA
section 408(n)(5)(C) authorizing States to establish regulatory limits not identical to certain tolerances or
exemptions.
(b) Any issue as to which review is or was obtainable under paragraph (a) of this section shall not be the
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subject of judicial review under any other provision of law. In part, this means that, for the Agency actions
subject to the objection procedure in FFDCA section 408(g)(2), judicial review is not available unless an
adversely affected party exhausts these objection procedures, and any petition procedures preliminary
thereto.
[70 FR 33362, June 8, 2005]

§ 180.31 Temporary tolerances.
top
(a) A temporary tolerance (or exemption from a tolerance) established under the authority of FFDCA
section 408(r) shall be deemed to be a tolerance (or exemption from the requirement of a tolerance) for
the purposes of FFDCA section 408(a)(1) or (a)(2) and for the purposes of §180.30.
(b) A request for a temporary tolerance or a temporary exemption from a tolerance by a person who has
obtained or is seeking an experimental permit for a pesticide chemical under the Federal Insecticide,
Fungicide, and Rodenticide Act shall be accompanied by such data as are available on subjects outlined
in §180.7(b) and an advance deposit to cover fees as provided in §180.33.
(c) To obtain a temporary tolerance, a requestor must comply with the petition procedures specified in
FFDCA section 408(d) and §180.7 except as provided in this section.
(d) A temporary tolerance or exemption from a tolerance may be issued for a period designed to allow the
orderly marketing of the raw agricultural commodities produced while testing a pesticide chemical under
an experimental permit issued under authority of the Federal Insecticide, Fungicide, and Rodenticide Act if
the Administrator concludes that the safety standard in FFDCA section 408(b)(2) or (c), as applicable, is
met. Subject to the requirements of FFDCA section 408(e), a temporary tolerance or exemption from a
tolerance may be revoked if the experimental permit is revoked, or may be revoked at any time if it
develops that the application for a temporary tolerance contains a misstatement of a material fact or that
new scientific data or experience with the pesticide chemical indicates that it does not meet the safety
standard in FFDCA section 408(b)(2) or (c), as applicable.
(e) Conditions under which a temporary tolerance is established shall include:
(1) A limitation on the amount of the chemical to be used on the designated crops permitted under the
experimental permit.
(2) A limitation for the use of the chemical on the designated crops to bona fide experimental use by
qualified persons as indicated in the experimental permit.
(3) A requirement that the person or firm which obtains the experimental permit for which the temporary
tolerance is established will immediately inform the Environmental Protection Agency of any reports on
findings from the experimental use that have a bearing on safety.
(4) A requirement that the person or firm which obtained the experimental permit for which the temporary
tolerance is established will keep records of production, distribution, and performance for a period of 2
years and, on request, at any reasonable time, make these records available to any authorized officer or
employee of the Environmental Protection Agency.
[70 FR 33362, June 8, 2005]

§ 180.32 Procedure for modifying and revoking tolerances or exemptions from
tolerances.
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(a) The Administrator on his/her own initiative may propose the issuance of a regulation modifying or
revoking a tolerance for a pesticide chemical residue on raw agricultural commodities or processed foods
or modifying or revoking an exemption from tolerance for such residue.
(b) Any person may file with the Administrator a petition proposing the issuance of a regulation modifying
or revoking a tolerance or exemption from a tolerance for a pesticide chemical residue. The petition shall
furnish reasonable grounds for the action sought. Reasonable grounds shall include an explanation
showing wherein the person has a substantial interest in such tolerance or exemption from tolerance and
an assertion of facts (supported by data if available) showing that new uses for the pesticide chemical
have been developed or old uses abandoned, that new data are available as to toxicity of the chemical, or
that experience with the application of the tolerance or exemption from tolerance may justify its
modification or revocation. Evidence that a person has registered or has submitted an application for the
registration of a pesticide under the Federal Insecticide, Fungicide, and Rodenticide Act will be regarded
as evidence that the person has a substantial interest in a tolerance or exemption from the requirement of
a tolerance for a pesticide chemical that consists in whole or in part of the pesticide. New data should be
furnished in the form specified in §180.7(b) for submitting petitions, as applicable.
(c) The procedures for completing action on an Administrator initiated proposal or a petition shall be those
specified in §§180.29 and 180.7, as applicable.
[70 FR 33362, June 8, 2005]

§ 180.33 Fees.
top
(a) Each petition for the establishment of a new tolerance or a tolerance higher than already established,
shall be accompanied by a fee of $80,950, plus $2,025 for each raw agricultural commodity more than
nine on which the establishment of a tolerance is requested, except as provided in paragraphs (b), (d),
and (h) of this section.
(b) Each petition for the establishment of a tolerance at a lower numerical level or levels than a tolerance
already established for the same pesticide chemical, or for the establishment of a tolerance on additional
raw agricultural commodities at the same numerical level as a tolerance already established for the same
pesticide chemical, shall be accompanied by a fee of $18,500 plus $1,225 for each raw agricultural
commodity on which a tolerance is requested.
(c) Each petition for an exemption from the requirement of a tolerance or repeal of an exemption shall be
accompanied by a fee of $14,925.
(d) Each petition or request for a temporary tolerance or a temporary exemption from the requirement of a
tolerance shall be accompanied by a fee of $32,325 except as provided in paragraph (e) of this section. A
petition or request to renew or extend such temporary tolerance or temporary exemption shall be
accompanied by a fee of $4,600.
(e) A petition or request for a temporary tolerance for a pesticide chemical which has a tolerance for other
uses at the same numerical level or a higher numerical level shall be accompanied by a fee of $16,075,
plus $1,225 for each raw agricultural commodity on which the temporary tolerance is sought.
(f) Each petition for revocation of a tolerance shall be accompanied by a fee of $10,125. Such fee is not
required when, in connection with the change sought under this paragraph, a petition is filed for the
establishment of new tolerances to take the place of those sought to be revoked and a fee is paid as
required by paragraph (a) of this section.
(g) If a petition or a request is not accepted for processing because it is technically incomplete, the fee,
less $2,025 for handling and initial review, shall be returned. If a petition is withdrawn by the petitioner
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after initial processing, but before significant Agency scientific review has begun, the fee, less $2,025 for
handling and initial review, shall be returned. If an unacceptable or withdrawn petition is resubmitted, it
shall be accompanied by the fee that would be required if it were being submitted for the first time.
(h) Each petition for a crop group tolerance, regardless of the number of raw agricultural commodities
involved, shall be accompanied by a fee equal to the fee required by the analogous category for a single
tolerance that is not a crop group tolerance, i.e. , paragraphs (a) through (f) of this section, without a
charge for each commodity where that would otherwise apply.
(i) Objections under section 408(d)(5) of the Act shall be accompanied by a filing fee of $4,050.
(j) The person who files a petition for judicial review of an order under section 408(h) of the Act shall pay
the costs of preparing the record on which the order is based unless the person has no financial interest in
the petition for judicial review.
(k) No fee under this section will be imposed on the Interregional Research Project Number 4 (IR-4
Program).
(l) The Administrator may waive or refund part or all of any fee imposed by this section if the Administrator
determines in his or her sole discretion that such a waiver or refund will promote the public interest or that
payment of the fee would work an unreasonable hardship on the person on whom the fee is imposed. A
request for waiver or refund of a fee shall be submitted to the Office of Pesticide Programs' Document
Processing Desk at the appropriate address as set forth in 40 CFR 150.17(a) or (b). A fee of $2,025 shall
accompany every request for a waiver or refund, as specified in paragraph (m) of this section, except that
the fee under this paragraph shall not be imposed on any person who has no financial interest in any
action requested by such person under paragraphs (a) through (j) of this section. The fee for requesting a
waiver or refund shall be refunded if the request is granted.
(m) All deposits and fees required by the regulations in this part shall be paid by money order, bank draft,
or certified check drawn to the order of the Environmental Protection Agency. All deposits and fees shall
be forwarded to the Environmental Protection Agency, Headquarters Accounting Operations Branch,
Office of Pesticide Programs (Tolerance Fees), P.O. Box 360277M, Pittsburgh, PA 15251. The payments
should be specifically labeled “Tolerance Petition Fees” and should be accompanied only by a copy of the
letter or petition requesting the tolerance. The actual letter or petition, along with supporting data, shall be
forwarded within 30 days of payment to the Office of Pesticide Programs' Document Processing Desk at
the appropriate address as set forth in 40 CFR 150.17(a) or (b). A petition will not be accepted for
processing until the required fees have been submitted. A petition for which a waiver of fees has been
requested will not be accepted for processing until the fee has been waived or, if the waiver has been
denied, the proper fee is submitted after notice of denial. A request for waiver or refund will not be
accepted after scientific review has begun on a petition.
(n) This fee schedule will be changed annually by the same percentage as the percent change in the
Federal General Schedule (GS) pay scale. In addition, processing costs and fees will periodically be
reviewed and changes will be made to the schedule as necessary. When automatic adjustments are made
based on the GS pay scale, the new fee schedule will be published in theFederal Registeras a final rule to
become effective 30 days or more after publication, as specified in the rule. When changes are made
based on periodic reviews, the changes will be subject to public comment.
(o) No fee required by this section shall be levied during the period beginning on October 1, 2003, and
ending September 30, 2008.
[68 FR 24371, May 7, 2003, as amended at 69 FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, 2005; 71
FR 35547, June 21, 2006]

§ 180.34 Tests on the amount of residue remaining.
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(a) Data in a petition on the amount of residue remaining in or on a raw agricultural commodity should
establish the residue that may remain when the pesticide chemical is applied according to directions
registered under the Federal Insecticide, Fungicide, and Rodenticide Act, or according to directions
contained in an application for registration. These data should establish the residues that may remain
under conditions most likely to result in high residues on the commodity.
(b) The petition should establish the reliability of the residue data reported in it. Sufficient information
should be submitted about the analytical method to permit competent analysts to apply it successfully.
(c) If the pesticide chemical is absorbed into a living plant or animal when applied (is systemic), residue
data may be needed on each plant or animal on which a tolerance or exemption is requested.
(d) If the pesticide chemical is not absorbed into the living plant or animal when applied (is not systemic), it
may be possible to make a reliable estimate of the residues to be expected on each commodity in a group
of related commodities on the basis of less data than would be required for each commodity in the group,
considered separately.
(e) Each of the following groups of crops lists raw agricultural commodities that are considered to be
related for the purpose of paragraph (d) of this section. Commodities not listed in this paragraph are not
considered to be related for the purpose of paragraph (d) of this section.
(1) Apples, crabapples, pears, quinces.
(2) Avocados, papayas.
(3) Blackberries, boysenberries, dewberries, loganberries, raspberries.
(4) Blueberries, currants, gooseberries, huckleberries.
(5) Cherries, plums, prunes.
(6) Oranges, citrus citron, grapefruit, kumquats, lemons, limes, tangelos, tangerines.
(7) Mangoes, persimmons.
(8) Peaches, apricots, nectarines.
(9) Beans, peas, soybeans (each in dry form).
(10) Beans, peas, soybeans (each in succulent form).
(11) Broccoli, brussels sprouts, cauliflower, kohlrabi.
(12) Cantaloups, honeydew melons, muskmelons, pumpkins, watermelons, winter squash.
(13) Carrots, garden beets, sugar beets, horseradish, parsnips, radishes, rutabagas, salsify roots, turnips.
(14) Celery, fennel.
(15) Cucumbers, summer squash.
(16) Lettuce, endive (escarole), Chinese cabbage, salsify tops.
(17) Onions, garlic, leeks, shallots (green, or in dry bulb form).

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(18) Potatoes, Jerusalem-artichokes, sweetpotatoes, yams.
(19) Spinach, beet tops, collards, dandelion, kale, mustard greens, parsley, Swiss chard, turnip tops,
watercress.
(20) Tomatoes, eggplants, peppers, pimentos.
(21) Pecans, almonds, brazil nuts, bush nuts, butternuts, chestnuts, filberts, hazelnuts, hickory nuts,
walnuts.
(22) Field corn, popcorn, sweet corn (each in grain form).
(23) Milo, sorghum (each in grain form).
(24) Wheat, barley, oats, rice, rye (each in grain form).
(25) Alfalfa, Bermuda grass, bluegrass, brome grass, clovers, cowpea hay, fescue, lespedeza, lupines,
orchard grass, peanut hay, peavine hay, rye grass, soybean hay, sudan grass, timothy, and vetch.
(26) Corn forage, sorghum forage.
(27) Sugarcane, cane sorghum.
[36 FR 22540, Nov. 25, 1971, as amended at 39 FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, 1974; 40
FR 6972, Feb. 18, 1975; 45 FR 82928, Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR 26635, May
17, 1995; 73 FR 75600, Dec. 12, 2008]

§ 180.35 Tests for potentiation.
top
Experiments have shown that certain cholinesterase-inhibiting pesticides when fed together to test
animals are more toxic than the sum of their individual toxicities when fed separately. One substance
potentiates the toxicity of the other. Important toxicological interactions also have been observed between
pesticides and other substances. Wherever there is reason to believe that a pesticide chemical for which a
tolerance is proposed may interact with other pesticide chemicals or other substances to which man is
exposed, it may be necessary to require special experimental data regarding potentiation capacities to
evaluate the safety of the proposed tolerance. This necessarily will be determined on a case-by-case
basis.

§ 180.40 Tolerances for crop groups.
top
(a) Group or subgroup tolerances may be established as a result of:
(1) A petition from a person who has submitted an application for the registration of a pesticide under the
Federal Insecticide, Fungicide, and Rodenticide Act.
(2) On the initiative of the Administrator.
(3) A petition by an interested person.
(b) The tables in §180.41 are to be used in conjunction with this section for the establishment of crop
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group tolerances. Each table in §180.41 lists a group of raw agricultural commodities that are considered
to be related for the purposes of this section. Refer also to §180.1(h) for a listing of commodities for which
established tolerances may be applied to certain other related and similar commodities.
(c) When there is an established or proposed tolerance for all of the representative commodities for a
specific group or subgroup of related commodities, a tolerance may be established for all commodities in
the associated group or subgroup. Tolerances may be established for a crop group or, alternatively,
tolerances may be established for one or more of the subgroups of a crop group.
(d) The representative crops are given as an indication of the minimum residue chemistry data base
acceptable to the Agency for the purposes of establishing a group tolerance. The Agency may, at its
discretion, allow group tolerances when data on suitable substitutes for the representative crops are
available (e.g., limes instead of lemons).
(e) Since a group tolerance reflects maximum residues likely to occur on all individual crops within a
group, the proposed or registered patterns of use for all crops in the group or subgroup must be similar
before a group tolerance is established. The pattern of use consists of the amount of pesticide applied, the
number of times applied, the timing of the first application, the interval between applications, and the
interval between the last application and harvest. The pattern of use will also include the type of
application; for example, soil or foliar application, or application by ground or aerial equipment.
(f) When the crop grouping contains commodities or byproducts that are utilized for animal feed, any
needed tolerance or exemption from a tolerance for the pesticide in meat, milk, poultry and/or eggs must
be established before a tolerance will be granted for the group as a whole. The representative crops
include all crops in the group that could be processed such that residues may concentrate in processed
food and/or feed. Processing data will be required prior to establishment of a group tolerance. Tolerances
will not be granted on a group basis as to processed foods prepared from crops covered by the group
tolerance.
(g) If maximum residues (tolerances) for the representative crops vary by more than a factor of 5 from the
maximum value observed for any crop in the group, a group or subgroup tolerance will ordinarily not be
established. In this case individual crop tolerances, rather than group tolerances, will normally be
established.
(h) Alternatively, a commodity with a residue level significantly higher or lower than the other commodities
in a group may be excluded from the group tolerance (e.g., cereal grains, except corn). In this case an
individual tolerance at the appropriate level for the unique commodity would be established, if necessary.
The alternative approach of excluding a commodity with a significantly higher or lower residue level will not
be used to establish a tolerance for a commodity subgroup. Most subgroups have only two representative
commodities; to exclude one such commodity and its related residue data would likely provide insufficient
residue information to support the remainder of the subgroup. Residue data from crops additional to those
representative crops in a grouping may be required for systemic pesticides.
(i) The commodities included in the groups will be updated periodically either at the initiative of the Agency
or at the request of an interested party. Persons interested in updating this section should contact the
Registration Division of the Office of Pesticide Programs.
(j) When EPA amends a crop group in a manner that expands or contracts the commodities that are
covered by the group, EPA will initially retain the pre-existing as well as the revised crop group in the CFR.
The revised crop group will have the same number as the pre-existing crop group; however, the revised
crop group number will be followed by a hyphen and the final two digits of the year in which it was
established (e.g., if Crop Group 1 is amended in 2007, the revised group will be designated as Crop Group
1-07). If the pre-existing crop group had crop subgroups, these subgroups will be numbered in a similar
fashion in the revised crop group. The name of the revised crop group will not be changed from the preexisting crop group unless the revision so changes the composition of the crop group that the pre-existing
name is no longer accurate. Once a revised crop group is established, EPA will no longer establish
tolerances under the pre-existing crop group. At appropriate times, EPA will amend tolerances for crop
groups that have been superseded by revised crop groups to conform the pre-existing crop group to the
revised crop group. Once all of the tolerances for the pre-existing crop group have been updated, the prehttp://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c=...f&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (39 of 651) [9/8/2009 3:02:16 PM]

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existing crop group will be removed from the CFR.
(k) Establishment of a tolerance does not substitute for the additional need to register the pesticide under
a companion law, the Federal Insecticide, Fungicide, and Rodenticide Act. The Registration Division of the
Office of Pesticide Programs should be contacted concerning procedures for registration of new uses of a
pesticide.
[60 FR 26635, May 17, 1995, as amended at 70 FR 33363, June 8, 2005; 72 FR 69155, Dec. 7, 2007]

§ 180.41 Crop group tables.
top
(a) The tables in this section are to be used in conjunction with §180.40 to establish crop group tolerances.
(b) Commodities not listed are not considered as included in the groups for the purposes of this
paragraph, and individual tolerances must be established. Miscellaneous commodities intentionally not
included in any group include asparagus, avocado, banana, fig, globe artichoke, hops, mango, okra,
papaya, pawpaw, peanut, persimmon, pineapple, water chestnut, and watercress.
(c) Each group is identified by a group name and consists of a list of representative commodities followed
by a list of all commodity members for the group. If the group includes subgroups, each subgroup lists the
subgroup name, the representative commodity or commodities, and the member commodities for the
subgroup. Subgroups, which are a subset of their associated crop group, are established for some but not
all crops groups.
(1) Crop Group 1: Root and Tuber Vegetables Group.
(i) Representative commodities. Carrot, potato, radish, and sugar beet.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 1 and identifies the related
crop subgroups.
Table 1—Crop Group 1: Root and Tuber Vegetables

Related crop
subgroups

Commodities
Arracacha ( Arracacia
xanthorrhiza
Arrowroot ( Maranta
arundinacea

1C, 1D

)

1C, 1D

)

Artichoke, Chinese ( Stachys
affinis
)

1C, 1D

Artichoke, Jerusalem ( Helianthus
)
tuberosus

1C, 1D

Beet, garden ( Beta vulgaris
Beet, sugar ( Beta vulgaris

)

1A, 1B

)

Burdock, edible ( Arctium lappa
Canna, edible (Queensland arrowroot) ( Canna
)
indica

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1A
)

1A, 1B
1C, 1D

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Carrot ( Daucus carota

)

1A, 1B

Cassava, bitter and sweet ( Manihot
esculenta
)

1C, 1D

Celeriac (celery root) ( Apium
graveolens
rapaceum
)

1A, 1B

var.

Chayote (root) ( Sechium edule
Chervil, turnip-rooted
( Chaerophyllum
bulbosum
Chicory ( Cichorium
intybus

)

1A, 1B
).
1A, 1B

)

Chufa ( Cyperus
esculentus

1C, 1D

)

Dasheen (taro) ( Colocasia
esculenta

1C, 1D

)

Ginger ( Zingiber
officinale

1C, 1D

)

Ginseng ( Panax
quinquefolius

1A, 1B

)

Horseradish ( Armoracia
rusticana

1A, 1B

)

Leren ( Calathea allouia
Parsley, turnip-rooted
( Petroselinum
crispum

1C, 1D

)

1A, 1B
var. tuberosum

)

Parsnip ( Pastinaca sativa

)

Potato ( Solanum
tuberosum

)

Radish, oriental (daikon) ( Raphanus
sativus
subvar.
longipinnatus
Rutabaga ( Brassica
campestris
napobrassica
Salsify (oyster plant) ( Tragopogon
porrifolius

)
1A, 1B
)
1A, 1B

).

1A, 1B

)

Salsify, Spanish ( Scolymus
hispanicus

1A, 1B

)

Skirret ( Sium sisarum

1A, 1B
1A, 1B

var.

Salsify, black ( Scorzonera
hispanica

1A, 1B
1C

)

Radish ( Raphanus sativus

Sweet potato ( Ipomoea
batatas

1C, 1D

)
)

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1A, 1B
1C, 1D

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Tanier (cocoyam) ( Xanthosoma
sagittifolium

1C, 1D

)

Turmeric ( Curcuma longa
Turnip ( Brassica rapa
rapa
)
Yam bean (jicama, manoic pea)
( Pachyrhizus

)

1C, 1D

var.

1A, 1B
1C, 1D

spp.)

Yam, true ( Dioscorea

spp.)

1C, 1D

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 1, specifies the
representative commodity(ies) for each subgroup, and lists all the commodities included in each subgroup.
Table 2—Crop Group 1 Subgroup Listing

Representative commodities

Commodities

Crop Subgroup 1A.Root vegetables
subgroup.
Carrot, radish, and sugar beet.

Beet, garden; beet, sugar; burdock,
edible; carrot; celeriac; chervil, turniprooted; chicory; ginseng; horseradish;
parsley, turnip-rooted; parsnip; radish;
radish, oriental; rutabaga; salsify;
salsify, black; salsify, Spanish; skirret;
turnip.

Crop Subgroup 1B.Root vegetables (except
sugar beet) subgroup.
Carrot and radish.

Beet, garden; burdock, edible; carrot;
celeriac; chervil, turnip-rooted; chicory;
ginseng; horseradish; parsley, turniprooted; parsnip; radish; radish, oriental;
rutabaga; salsify; salsify, black; salsify,
Spanish; skirret; turnip.

Crop Subgroup 1C.Tuberous and corm
vegetables subgroup.
Potato.

Arracacha; arrowroot; artichoke,
Chinese; artichoke, Jerusalem; canna,
edible; cassava, bitter and sweet;
chayote (root); chufa; dasheen; ginger;
leren; potato; sweet potato; tanier;
turmeric; yam bean; yam, true.

Crop Subgroup 1D.Tuberous and corm
vegetables (except potato) subgroup.
Sweet potato.

Arracacha; arrowroot; artichoke,
Chinese; artichoke, Jerusalem; canna,
edible; cassava, bitter and sweet;
chayote (root); chufa; dasheen; ginger;
leren; sweet potato; tanier; turmeric;
yam bean; yam, true.

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(2) Crop Group 2. Leaves of Root and Tuber Vegetables (Human Food or Animal Feed) Group (Human
Food or Animal Feed) Group.
(i) Representative commodities. Turnip and garden beet or sugar beet.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 2:

Crop Group 2: Leaves of Root and Tuber Vegetables (Human Food or Animal Feed) Group—
Commodities
Beet, garden ( Beta vulgaris )
Beet, sugar ( Beta vulgaris )
Burdock, edible ( Arctium lappa )
Carrot ( Daucus carota )
Cassava, bitter and sweet ( Manihot esculenta )
Celeriac (celery root) ( Apium graveolens var. rapaceum )
Chervil, turnip-rooted ( Chaerophyllum bulbosum )
Chicory ( Cichorium intybus )
Dasheen (taro) ( Colocasia esculenta )
Parsnip ( Pastinaca sativa )
Radish ( Raphanus sativus )
Radish, oriental (daikon) ( Raphanus sativus subvar. longipinnatus )
Rutabaga ( Brassica campestris var. napobrassica )
Salsify, black ( Scorzonera hispanica )
Sweet potato ( Ipomoea batatas )
Tanier (cocoyam) ( Xanthosoma sagittifolium )
Turnip ( Brassica rapa var. rapa )
Yam, true ( Dioscorea spp.)
(3) Crop Group 3 . Bulb Vegetables ( Allium spp.) Group.
(i) Representative commodities . Onion, green; and onion, dry bulb.
(ii) Commodities . The following is a list of all the commodities in Crop Group 3.
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Crop Group 3: Bulb Vegetable ( Allium spp.) Group—Commodities

Garlic, bulb ( Allium sativum

)

Garlic, great headed, (elephant) ( Allium
ampeloprasum
ampeloprasum

var.
)

Leek ( Allium ampeloprasum
A. porrum, A. tricoccum

,

Onion, dry bulb and green ( Allium cepa,
A. fistulosum

)

)

Onion, Welsh, ( Allium fistulosum

)

Shallot ( Allium cepa

var. cepa

)

(4) Crop Group 3-07 . Bulb Vegetable Group. (i) Representative Commodities . Onion, bulb and onion,
green.
(ii) Table . The following Table 1 lists all the commodities listed in Crop Group 3-07 and identifies the
related crop subgroups.
Table 1—Crop Group 3-07: Bulb Vegetable Group

Related crop
subgroups

Commodities
Chive, fresh leaves ( Allium
schoenoprasum L

3-07B

.)

Chive, Chinese, fresh leaves ( Allium
Rottler ex Spreng)
tuberosum

3-07B

Daylily, bulb ( Hemerocallis
fulva
(L.) L. var. fulva

3-07A

Elegans hosta ( Hosta
Sieboldiana
(Hook.) Engl

)

3-07B
)

Fritillaria, bulb ( Fritillaria
L. fritillary

)

Fritillaria, leaves ( Fritillaria
L. fritillary

)

Garlic, bulb ( Allium sativum
) ( A.
var. sativum
sativum
Common Garlic Group)
Garlic, great headed, bulb ( Allium
ampeloprasum
ampeloprasum
ampeloprasum
Group)

3-07A
3-07B
L.

L. var.
) ( A.
Great Headed Garlic

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3-07A

3-07A

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Garlic, Serpent, bulb ( Allium
sativum
var.
ophioscorodon
or A.
Ophioscorodon Group)
sativum

3-07A

Kurrat ( Allium kurrat
Schweinf. Ex. K.
Krause
or A.
ampeloprasum

3-07B
Kurrat Group)

Lady's leek ( Allium cernuum
Roth)
Leek Allium porrum
A. ampeloprasum L
porrum
ampeloprasum

3-07B
L. (syn:

(L.) J. Gay) ( A.

Leek, wild ( Allium
tricoccum
Lily, bulb ( Lilium
Leichtlinii
maximowiczii,
Lilium lancifolium

. var.

Leek Group)
3-07B

Aiton)
spp. ( Lilium
var.

Onion, Beltsville bunching ( Allium
proliferum
Allium fistulosum
A. cepa
L.)
Onion, bulb ( Allium cepa
cepa
) ( A. cepa

3-07B

3-07A
))

x
(Moench) Schrad.) (syn:

3-07B
L. x

L. var.
Common Onion Group)

3-07A

Onion, Chinese, bulb ( Allium
G. Don.) (syn: A.
chinense
Regel)
bakeri

3-07A

Onion, fresh ( Allium
fistulosum
caespitosum

3-07B

Onion, green ( Allium cepa
cepa
) ( A. cepa
Onion, macrostem ( Allium
macrostemom
Onion, pearl ( Allium porrum
sectivum
or A.
ampeloprasum

L. var.
Makino)
L. var.
Common Onion Group)

3-07B
3-07B

Bunge)
var.

3-07A

Pearl Onion Group)

Onion, potato, bulb ( Allium cepa
aggregatum
G. Don.) ( A.
Aggregatum Group)
cepa

L. var.

Onion, tree, tops ( Allium x
(Moench) Schrad. ex Willd.) (syn:
proliferum
A. cepa
var. proliferum
L. var.
(Moench) Regel; A. cepa
bulbiferum
L.H. Bailey; A.
cepa
L. var. viviparum
(Metz.) Alef.)

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3-07A

3-07B

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Onion, Welsh, tops ( Allium
fistulosum

L.)

Shallot, bulb ( Allium cepa
aggregatum

G. Don.)

Shallot, fresh leaves ( Allium cepa
aggregatum

G. Don.)

3-07B
3-07A

var.
var.

3-07B

Cultivars, varieties, and/or hybrids of these.
(iii) Table . The following Table 2 identifies the crop subgroups for Crop Group 3-07, specifies the
representative commodities for each subgroup and lists all the commodities included in each subgroup.
Table 2—Crop Group 3-07: Subgroup Listing

Representative commodities

Commodities

Crop subgroup 3-07A. Onion, bulb,
subgroup.
Onion, bulb.

Daylily, bulb; fritillaria, bulb; garlic, bulb;
garlic, great-headed, bulb; garlic,
serpent, bulb; lily, bulb; onion, bulb;
onion, Chinese, bulb; onion, pearl;
onion, potato, bulb; shallot, bulb;
cultivars, varieties, and/or hybrids of
these.

Crop subgroup 3-07B. Onion, green,
subgroup.
Onion, green.

Chive, fresh leaves; chive, Chinese,
fresh leaves; elegans hosta; fritillaria,
leaves; kurrat; lady's leek; leek; leek,
wild; Onion, Beltsville bunching; onion,
fresh; onion, green; onion, macrostem;
onion, tree, tops; onion, Welsh, tops;
shallot, fresh leaves; cultivars, varieties,
and/or hybrids of these.

(5) Crop Group 4. Leafy Vegetables (Except Brassica Vegetables) Group.
(i) Representative commodities. Celery, head lettuce, leaf lettuce, and spinach ( Spinacia oleracea ).
(ii) Table. The following table 1 lists all the commodities included in Crop Group 4 and identifies the related
crop subgroups.
Table 1—Crop Group 4: Leafy Vegetables (Except BRASSICA Vegetables) Group

Related crop
subgroups

Commodities
Amaranth (leafy amaranth, Chinese spinach, tampala)
( Amaranthus
spp.)
Arugula (Roquette) ( Eruca sativa
Cardoon ( Cynara
cardunculus

4A
)

4A
4B

)

Celery ( Apium graveolens
dulce
)
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var.

4B

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Celery, Chinese ( Apium
graveolens
secalinum

)

Celtuce ( Lactuca sativa
angustana

4B

var.
var.

)

Chervil ( Anthriscus
cerefolium

4A

)

Chrysanthemum, edible-leaved
( Chrysanthemum
coronarium
coronarium
Chrysanthemum, garland
( Chrysanthemum
coronarium
spatiosum

4B

4A
var.
)
4A
var.

)

Corn salad ( Valerianella
locusta

4A

)

Cress, garden ( Lepidium
)
sativum

4A

Cress, upland (yellow rocket, winter cress)
( Barbarea vulgaris
Dandelion ( Taraxacum
officinale

)

Dock (sorrel) ( Rumex

spp.)

)

4A
4A
4A

Endive (escarole) ( Cichorium
)
endivia

4A

Fennel, Florence (finochio) ( Foeniculum
Azoricum Group)
vulgare

4B

Lettuce, head and leaf ( Lactuca
)
sativa

4A

Orach ( Atriplex
hortensis
Parsley ( Petroselinum
crispum

4A

)

4A

)

Purslane, garden ( Portulaca
oleracea
)
Purslane, winter ( Montia
perfoliata

4A
4A

)

Radicchio (red chicory) ( Cichorium
)
intybus
Rhubarb ( Rheum
rhabarbarum
Spinach ( Spinacia
oleracea

4A

)
)

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4B
4A

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Spinach, New Zealand ( Tetragonia
tetragonioides,
T. expansa

4A
)

Spinach, vine (Malabar spinach, Indian spinach)
( Basella alba
)
Swiss chard ( Beta vulgaris
cicla
)

4A
4B

var.

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 4, specifies the
representative commodities for each subgroup, and lists all the commodities included in each subgroup.
Table 2—Crop Group 4 Subgroup Listing

Representative commodities

Commodities

Crop Subgroup 4A.Leafy greens subgroup.
Head lettuce and leaf lettuce, and spinach
( Spinacia
oleracea
)

Amaranth; arugula; chervil;
chrysanthemum, edibleleaved; chrysanthemum,
garland; corn salad; cress,
garden; cress, upland;
dandelion; dock; endive;
lettuce; orach; parsley;
purslane, garden; purslane,
winter; radicchio (red
chicory); spinach; spinach,
New Zealand; spinach, vine.

Crop Subgroup 4B.Leaf petioles subgroup.
Celery.

Cardoon; celery; celery,
Chinese; celtuce; fennel,
Florence; rhubarb; Swiss
chard.

(6) Crop Group 5. Brassica (Cole) Leafy Vegetables Group.
(i) Representative commodities. Broccoli or cauliflower; cabbage; and mustard greens.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 5 and identifies the related
crop subgroups.
Table 1—Crop Group 5: Brassica (Cole) Leafy Vegetables

Related crop
subgroups

Commodities
Broccoli ( Brassica
oleracea

var. botrytis

)

Broccoli, Chinese (gai lon) ( Brassica
)
alboglabra

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5A
5A

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Broccoli raab (rapini) ( Brassica
campestris
Brussels sprouts ( Brassica
oleracea
gemmifera
Cabbage ( Brassica
oleracea

5B

)

5A

var.
)

5A

)

Cabbage, Chinese (bok choy) ( Brassica
)
chinensis

5B

Cabbage, Chinese (napa) ( Brassica
)
pekinensis

5A

Cabbage, Chinese mustard (gai choy)
( Brassica
)
campestris

5A

Cauliflower ( Brassica
oleracea

var. botrytis

)

Cavalo broccolo ( Brassica
oleracea

var. botrytis

)

Collards ( Brassica
oleracea

var. acephala

)

Kale ( Brassica
oleracea
Kohlrabi ( Brassica
oleracea
gongylodes

var. acephala
var.

5A
5A
5B
5B

)

5A
)

Mizuna ( Brassica rapa
Japonica Group)

5B

Mustard greens ( Brassica
)
juncea

5B

Mustard spinach ( Brassica
rapa
Perviridis Group)

5B

Rape greens ( Brassica
)
napus

5B

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 5, specifies the
representative commodity(ies) for each subgroup, and lists all the commodities included in each subgroup.
Table 2—Crop Group 5 Subgroup Listing

Representative commodities
Crop Subgroup 5A.Head and stem
Brassica
subgroup

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Commodities

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Broccoli or cauliflower; and cabbage

Broccoli; broccoli, Chinese;
brussels sprouts; cabbage;
cabbage, Chinese (napa);
cabbage, Chinese mustard;
cauliflower; cavalo broccolo;
kohlrabi

Crop Subgroup 5B.Leafy Brassica
greens subgroup.
Mustard greens

Broccoli raab; cabbage,
Chinese (bok choy); collards;
kale; mizuna; mustard
greens; mustard spinach;
rape greens

(7) Crop Group 6. Legume Vegetables (Succulent or Dried) Group.
(i) Representative commodities. Bean ( Phaseolus spp.; one succulent cultivar and one dried cultivar); pea
( Pisum spp.; one succulent cultivar and one dried cultivar); and soybean.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 6 and identifies the related
crop subgroups.
Table 1—Crop Group 6: Legume Vegetables (Succulent or Dried)

Related crop
subgroups

Commodities
Bean ( Lupinus
spp.) (includes grain lupin, sweet
lupin, white lupin, and white sweet lupin)

6C

Bean ( Phaseolus
spp.) (includes field bean,
kidney bean, lima bean, navy bean, pinto bean, runner bean, snap
bean, tepary bean, wax bean)

6A, 6B, 6C

Bean ( Vigna
spp.) (includes adzuki bean, asparagus bean,
blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea,
moth bean, mung bean, rice bean, southern pea, urd bean, yardlong
bean)

6A, 6B, 6C

Broad bean (fava bean) ( Vicia faba

)

Chickpea (garbanzo bean) ( Cicer
)
arietinum

6C

Guar ( Cyamopsis
tetragonoloba
Jackbean ( Canavalia
ensiformis

6C

)

6A

)

Lablab bean (hyacinth bean) ( Lablab
)
purpureus
Lentil ( Lens esculenta

6B, 6C

6C
)

Pea ( Pisum
spp.) (includes dwarf pea, edible-pod pea,
English pea, field pea, garden pea, green pea, snow pea, sugar snap
pea)
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6C
6A, 6B, 6C

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Pigeon pea ( Cajanus cajan

)

Soybean ( Glycine max

)

N/A

Soybean (immature seed) ( Glycine max
Sword bean ( Canavalia
gladiata

6A, 6B, 6C
)

6A
6A

)

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 6, specifies the
representative commodities for each subgroup, and lists all the commodities included in each subgroup.
Table 2—Crop Group 6 Subgroup Listing

Representative commodities

Commodities

Crop Subgroup 6A.Edible-podded legume
vegetables subgroup.
Any one succulent cultivar of edible-podded
bean ( Phaseolus
spp.) and any one succulent cultivar of
edible-podded pea ( Pisum
spp.).

Bean ( Phaseolus
spp.) (includes runner bean, snap bean,
wax bean); bean ( Vigna
spp.)
(includes asparagus bean, Chinese
longbean, moth bean, yardlong bean);
jackbean; pea ( Pisum
spp.)
(includes dwarf pea, edible-pod pea, snow
pea, sugar snap pea); pigeon pea; soybean
(immature seed); sword bean.

Crop Subgroup 6B.Succulent shelled pea
and bean subgroup.
Any succulent shelled cultivar of bean
( Phaseolus
spp.)
and garden pea ( Pisum
spp.).

Bean ( Phaseolus
spp.) (includes lima bean (green)); broad
bean (succulent); bean ( Vigna
spp.) (includes blackeyed pea, cowpea,
southern pea); pea ( Pisum
spp.) (includes English pea, garden pea,
green pea); pigeon pea.

Crop Subgroup 6C.Dried shelled pea and
bean (except soybean) subgroup
Any one dried cultivar of bean
( Phaseolus
spp.);
and any one dried cultivar of pea
( Pisum
spp.)

Dried cultivars of bean
spp.) (includes
( Lupinus
grain lupin, sweet lupin, white lupin, and
white sweet lupin);
( Phaseolus
spp.)
(includes field bean, kidney bean, lima bean
(dry), navy bean, pinto bean; tepary bean;
bean ( Vigna
spp.) (includes
adzuki bean, blackeyed pea, catjang,
cowpea, Crowder pea, moth bean, mung
bean, rice bean, southern pea, urd bean);
broad bean (dry); chickpea; guar; lablab
bean; lentil; pea ( Pisum
spp.)
(includes field pea); pigeon pea.

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(8) Crop Group 7. Foliage of Legume Vegetables Group.
(i) Representative commodities. Any cultivar of bean ( Phaseolus spp.), field pea ( Pisum spp.), and
soybean.
(ii) Table. The following table 1 lists the commodities included in Crop Group 7.
Table 1—Crop Group 7: Foliage of Legume Vegetables Group

Representative commodities
Any cultivar of bean ( Phaseolus
spp.), and soybean
and field pea ( Pisum
( Glycine max
)

Commodities
spp.) Plant parts of any legume
vegetable included in the
legume vegetables that
will be used as animal
feed.

(iii) Table. The following table 2 identifies the crop subgroup for Crop Group 7 and specifies the
representative commodities for the subgroup, and lists all the commodities included in the subgroup.
Table 2—Crop Group 7 Subgroup Listing

Representative commodities

Commodities

Crop Subgroup 7A.Foliage of legume vegetables (except
soybeans) subgroup
Any cultivar of bean ( Phaseolus
spp.), and field pea ( Pisum

spp.)

Plant parts of any legume
vegetable (except
soybeans) included in the
legume vegetables group
that will be used as
animal feed.

(9) Crop Group 8. Fruiting Vegetables (Except Cucurbits) Group.
(i) Representative commodities. Tomato, bell pepper, and one cultivar of non-bell pepper.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 8:

Crop Group 8: Fruiting Vegetables (Except Cucurbits)—Commodities
Eggplant ( Solanum melongena )
Groundcherry ( Physalis spp.)
Pepino ( Solanum muricatum )
Pepper ( Capsicum spp.) (includes bell pepper, chili pepper, cooking pepper, pimento, sweet
pepper)
Tomatillo ( Physalis ixocarpa )

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Tomato ( Lycopersicon esculentum )
(10) Crop Group 9. Cucurbit Vegetables Group.
(i) Representative commodities. Cucumber, muskmelon, and summer squash.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 9 and identifies the related
subgroups.
Table 1—Crop Group 9: Cucurbit Vegetables

Related crop
subgroups

Commodities
Chayote (fruit) ( Sechium edule

)

Chinese waxgourd (Chinese preserving melon)
( Benincasa hispida

)

Citron melon ( Citrullus
lanatus
Cucumber ( Cucumis
sativus

var. citroides

)

9B
9A
9B

)

Gherkin ( Cucumis anguria
Gourd, edible ( Lagenaria
hyotan, cucuzza); ( Luffa
acutangula, L.
cylindrica
okra)

9B

)
spp.) (includes

9B
9B

) (includes hechima, Chinese

Momordica
spp. (includes balsam apple,
balsam pear, bitter melon, Chinese cucumber)

9B

Muskmelon (hybrids and/or cultivars of Cucumis
) (includes true cantaloupe, cantaloupe, casaba,
melo
crenshaw melon, golden pershaw melon, honeydew melon, honey
balls, mango melon, Persian melon, pineapple melon, Santa Claus
melon, and snake melon)

9A

Pumpkin ( Cucurbita

9B

spp.)

Squash, summer ( Cucurbita
var. melopepo
) (includes
pepo
crookneck squash, scallop squash, straightneck squash, vegetable
marrow, zucchini)

9B

Squash, winter ( Cucurbita
maxima;
C.
) (includes butternut squash,
moschata
calabaza, hubbard squash); ( C. mixta;
C. pepo
) (includes acorn squash, spaghetti
squash)

9B

Watermelon (includes hybrids and/or varieties of
Citrullus lanatus

9A

)

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 9, specifies the
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representative commodities for each subgroup, and lists all the commodities included in each subgroup.
Table 2—Crop Group 9 Subgroup Listing

Representative
commodities

Commodities

Crop Subgroup 9A.Melon
subgroup
Cantaloupes

Citron melon; muskmelon; watermelon

Crop Subgroup 9B.Squash/
cucumber subgroup
One cultivar of summer
squash and cucumber.

Chayote (fruit); Chinese waxgourd; cucumber; gherkin;
gourd, edible; Momordica
spp.;
pumpkin; squash, summer; squash, winter.

(11) Crop Group 10. Citrus Fruits ( Citrus spp., Fortunella spp.) Group.
(i) Representative commodities. Sweet orange; lemon and grapefruit.
(ii) Commodities. The following is a list of all the commodities in Crop Group 10:

Crop Group 10: Citrus Fruits (Citrus spp., Fortunella spp.) Group—Commodities
Calamondin ( Citrus mitis × Citrofortunella mitis )
Citrus citron ( Citrus medica )
Citrus hybrids ( Citrus spp.) (includes chironja, tangelo, tangor)
Grapefruit ( Citrus paradisi )
Kumquat ( Fortunella spp.)
Lemon ( Citrus jambhiri, Citrus limon )
Lime ( Citrus aurantiifolia )
Mandarin (tangerine) ( Citrus reticulata )
Orange, sour ( Citrus aurantium )
Orange, sweet ( Citrus sinensis )
Pummelo ( Citrus grandis, Citrus maxima )
Satsuma mandarin ( Citrus unshiu )
(12) Crop Group 11: Pome Fruits Group.
(i) Representative commodities. Apple and pear.
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(ii) Commodities. The following is a list of all the commodities included in Crop Group 11:

Crop Group 11: Pome Fruits Group—Commodities
Apple ( Malus domestica )
Crabapple ( Malus spp.)
Loquat ( Eriobotrya japonica )
Mayhaw ( Crataegus aestivalis, C. opaca, and C. rufula )
Pear ( Pyrus communis )
Pear, oriental ( Pyrus pyrifolia )
Quince ( Cydonia oblonga )
(13) Crop Group 12. Stone Fruits Group.
(i) Representative commodities. Sweet cherry or tart cherry; peach; and plum or fresh prune ( Prunus
domestica, Prunus spp.)
(ii) Commodities. The following is a list of all the commodities included in Crop Group 12:

Crop Group 12: Stone Fruits Group—Commodities
Apricot ( Prunus armeniaca )
Cherry, sweet ( Prunus avium ),
Cherry, tart ( Prunus cerasus )
Nectarine ( Prunus persica )
Peach ( Prunus persica )
Plum ( Prunus domestica, Prunus spp.)
Plum, Chickasaw ( Prunus angustifolia )
Plum, Damson ( Prunus domestica spp. insititia )
Plum, Japanese ( Prunus salicina )
Plumcot ( Prunus. armeniaca × P. domestica )
Prune (fresh) ( Prunus domestica, Prunus spp.)
(14) Crop Group 13. Berries Group.

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(i) Representative commodities. Any one blackberry or any one raspberry; and blueberry.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 13 and identifies the
related subgroups.
Table 1—Crop Group 13: Berries Group

Related crop
subgroups

Commodities
Blackberry ( Rubus eubatus
)
(including bingleberry, black satin berry, boysenberry, Cherokee
blackberry, Chesterberry, Cheyenne blackberry, coryberry,
darrowberry, dewberry, Dirksen thornless berry, Himalayaberry,
hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry,
marionberry, nectarberry, olallieberry, Oregon evergreen berry,
phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee
blackberry, youngberry, and varieties and/or hybrids of these)

13A

Blueberry ( Vaccinium

13B

Currant ( Ribes

spp.)
spp.)

Elderberry ( Sambucus
Gooseberry ( Ribes

13B
spp.)

13B

spp.)

13B

Huckleberry ( Gaylussacia
Loganberry ( Rubus
loganobaccus
Raspberry, black and red ( Rubus
occidentalis,
Rubus strigosus,
Rubus idaeus

spp.)

13B
13A

)

13A
)

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 13, specifies the
representative commodities for each subgroup, and lists all the commodities included in each subgroup.
Table 2—Crop Group 13 Subgroups Listing

Representative commodities

Commodities

Crop Subgroup 13A.Caneberry (blackberry
and raspberry) subgroup.
Any one blackberry or any one raspberry.

Blackberry; loganberry; red and black
raspberry; cultivars and/or hybrids of
these.

Crop Subgroup 13B.Bushberry subgroup.
Blueberry, highbush.

Blueberry, highbush and lowbush;
currant; elderberry; gooseberry;
huckleberry.

(15) Crop Group 13-07 . Berry and Small Fruit Crop Group

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(i) Representative commodities . Any one blackberry or any one raspberry; highbush blueberry; elderberry
or mulberry; grape; fuzzy kiwifruit, and strawberry.
(ii) Table . The following Table 1 lists all the commodities listed in Crop Group 13-07 and identifies the
related crop subgroups.
Table 1—Crop Group 13-07: Berry and Small Fruit Crop Group

Related crop
subgroups

Commodities
Amur river grape ( Vitis
amurensis Rupr
Aronia berry ( Aronia

spp.)

Bayberry ( Myrica
Bearberry ( Arctostaphylos
uva-ursi

13-07D, 1307E, 13-07F

)

13-07B

spp.)

13-07C
13-07G, 13-07H

)

Bilberry ( Vaccinium
myrtillus L.)

13-07G, 13-07H

Blackberry ( Rubus
spp.) (including Andean blackberry,
arctic blackberry, bingleberry, black satin berry, boysenberry,
brombeere, California blackberry, Chesterberry, Cherokee blackberry,
Cheyenne blackberry, common blackberry, coryberry, darrowberry,
dewberry, Dirksen thornless berry, evergreen blackberry,
Himalayaberry, hullberry, lavacaberry, loganberry, lowberry,
Lucretiaberry, mammoth blackberry, marionberry, mora, mures
deronce, nectarberry, Northern dewberry, olallieberry, Oregon
evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry,
Shawnee blackberry, Southern dewberry, tayberry, youngberry,
zarzamora, and cultivars, varieties and/or hybrids of these.)

13-07A

Blueberry, highbush ( Vaccinium

13-07B

spp.)

Blueberry, lowbush ( Vaccinium
angustifolium

13-07B

Aiton)

Buffalo currant ( Ribes aureum
Buffaloberry ( Shepherdia
argentea

Pursh)

13-07C

(Pursh) Nutt.)

Che ( Cudrania
tricuspidata

Bur. Ex Lavallee)

Chilean guava ( Myrtus ugni
Chokecherry ( Prunus
virginiana

Mol.)

13-07C
13-07B
13-07C

L.)

Cloudberry ( Rubus
chamaemorus

L.)

Cranberry ( Vaccinium
macrocarpon

Aiton)

Currant, black ( Ribes nigrum

13-07G, 13-07H
13-07G, 13-07H
L.)

Currant, red ( Ribes rubrum
Elderberry ( Sambucus

13-07B

L.)
spp.)

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13-07B
13-07B
13-07B, 13-07C

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European barberry ( Berberis
L.)
vulgaris
Gooseberry ( Ribes

13-07B
spp.)

13-07B, 1307D, 13-07E,
13-07F

Grape (Vitis spp.)

13-07D, 13-07F

Highbush cranberry ( Viburnum
opulus
L. var. Americanum
Honeysuckle, edible ( Lonicera
caerula L
emphyllocalyx
Lonicera caerula L
var . edulis Turcz.
ex herder

Aiton)

13-07B
13-07B

. var.

Nakai,

)

Huckleberry ( Gaylussacia

spp.)

Jostaberry ( Ribes x
nidigrolaria

13-07B

Rud. Bauer and A. Bauer)

13-07B

Juneberry (Saskatoon berry) ( Amelanchier
spp.)

13-07B, 13-07C

Kiwifruit, fuzzy ( Actinidia
deliciosa
Fergusons, Actinida
chinensis

13-07D, 13-07E

A. Chev.) (C.F. Liang and A.R.
Planch.)

Kiwifruit, hardy ( Actinidia
arguta
(Siebold and Zucc.) Planch. ex Miq)
Lingonberry ( Vaccinium
vitis-idaea

13-07D, 1307E, 13-07F
13-07B, 13-07G
13-07H

L.)

Maypop ( Passiflora
incarnata

13-07E, 13-07F

L.)

Mountain pepper berries ( Tasmannia
)(Poir.) A.C.Sm.
lanceolata

13-07C

Mulberry ( Morus

13-07C

spp.)

Muntries ( Kunzea pomifera
Muell.)
Native currant ( Acrotriche
depressa

F.

13-07B

R. BR.)

Partridgeberry ( Mitchella
L.)
repens

13-07G, 13-07H

Phalsa ( Grewia
subinaequalis

DC.)

Pincherry ( Prunus
pensylvanica

L.f.)

Raspberry, black and red ( Rubus
Riberry ( Syzygium
luehmannii

13-07G, 13-07H

spp.)
)

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13-07C
13-07C
13-07A
13-07C

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Salal ( Gaultheria
shallon

13-07B, 13-07C

Pursh.)

Schisandra berry (Schisandra chinensis (Turcz.) Baill.)
Sea buckthorn ( Hippophae
rhamnoides

L.)

Serviceberry ( Sorbus

spp.)

Strawberry ( Fragaria x
ananassa

13-07D, 1307E, 13-07F
13-07B
13-07C
13-07G

Duchesne)

Wild raspberry ( Rubus muelleri
Lefevre ex P.J. Mull)

13-07A

Cultivars, varieties, and/or hybrids of these.
(iii) Table . The following Table 2 identifies the crop subgroups for Crop Group 13-07, specifies the
representative commodities for each subgroup and lists all the commodities included in each subgroup.
Table 2—Crop Group 13-07: Subgroup Listing

Representative commodities

Commodities

Crop Subgroup 13-07A.Caneberry subgroup
Any one blackberry or any one raspberry.

Blackberry; loganberry; raspberry,
red and black; wild raspberry;
cultivars, varieties, and/or hybrids
of these.

Crop Subgroup 13-07B.Bushberry subgroup.
Blueberry, highbush.

Aronia berry; blueberry, highbush;
blueberry, lowbush; buffalo
currant; Chilean guava; currant,
black; currant, red; elderberry;
European, barberry; gooseberry;
cranberry, highbush; honeysuckle,
edible; huckleberry; jostaberry;
Juneberry; lingonberry; native
currant; salal; sea buckthorn;
cultivars, varieties, and/or hybrids
of these.

Crop Subgroup 13-07C.Large shrub/tree berry
subgroup.
Elderberry or mulberry.

Bayberry; buffaloberry; che;
chokecherry; elderberry;
Juneberry; mountain pepper
berries; mulberry; phalsa;
pincherry; riberry; salal;
serviceberry; cultivars, varieties,
and/or hybrids of these.

Crop Subgroup 13-07D.Small fruit vine climbing
subgroup.

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Grape and fuzzy kiwifruit.

Amur river grape; gooseberry;
grape; kiwifruit, fuzzy; kiwifruit,
hardy; Maypop; schisandra berry;
cultivars, varieties, and /or hybrids
of these.

Crop Subgroup 13-07E.Small fruit vine climbing
subgroup, except grape.
Fuzzy kiwifruit.

Amur river grape; gooseberry;
kiwifruit, fuzzy; kiwifruit, hardy;
Maypop; schisandra berry;
cultivars, varieties, and/or hybrids
of these.

Crop Subgroup 13-07F.Small fruit vine climbing
subgroup except fuzzy kiwifruit.
Grape.

Amur river grape; gooseberry;
grape; kiwifruit, hardy; Maypop;
schisandra berry; cultivars
varieties, and/or hybrids of these.

Crop Subgroup 13-07G.Low growing berry
subgroup.
Strawberry.

Bearberry; bilberry; blueberry,
lowbush; cloudberry; cranberry;
lingonberry; muntries;
partridgeberry; strawberry;
cultivars, varieties, and/or hybrids
of these.

Crop Subgroup 13-07H.Low growing berry
subgroup, except strawberry.
Cranberry

Bearberry; bilberry; blueberry,
lowbush; cloudberry; cranberry;
lingonberry; muntries;
partridgeberry; cultivars, varieties,
and/or cultivars of these.

(16) Crop Group 14. Tree Nuts Group.
(i) Representative commodities. Almond and pecan.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 14:

Crop Group 14: Tree Nuts—Commodities
Almond ( Prunus dulcis )
Beech nut ( Fagus spp.)
Brazil nut ( Bertholletia excelsa )
Butternut ( Juglans cinerea )

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Cashew ( Anacardium occidentale )
Chestnut ( Castanea spp.)
Chinquapin ( Castanea pumila )
Filbert (hazelnut) ( Corylus spp.)
Hickory nut ( Carya spp.)
Macadamia nut (bush nut) ( Macadamia spp.)
Pecan ( Carya illinoensis )
Walnut, black and English (Persian) ( Juglans spp.)
(17) Crop Group 15. Cereal Grains Group.
(i) Representative commodities. Corn (fresh sweet corn and dried field corn), rice, sorghum, and wheat.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 15:

Crop Group 15: Cereal Grains—Commodities
Barley ( Hordeum spp.)
Buckwheat ( Fagopyrum esculentum )
Corn ( Zea mays )
Millet, pearl ( Pennisetum glaucum )
Millet, proso ( Panicum milliaceum )
Oats ( Avena spp.)
Popcorn ( Zea mays var. everta )
Rice ( Oryza sativa )
Rye ( Secale cereale )
Sorghum (milo) ( Sorghum spp.)
Teosinte ( Euchlaena mexicana )
Triticale ( Triticum-Secale hybrids)
Wheat ( Triticum spp.)
Wild rice ( Zizania aquatica )

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(18) Crop Group 16. Forage, Fodder and Straw of Cereal Grains Group.
(i) Representative commodities. Corn, wheat, and any other cereal grain crop.
(ii) Commodities. The commodities included in Crop Group 16 are: Forage, fodder, and straw of all
commodities included in the group cereal grains group.
(19) Crop Group 17. Grass Forage, Fodder, and Hay Group.
(i) Representative commodities. Bermuda grass; bluegrass; and bromegrass or fescue.
(ii) Commodities. The commodities included in Crop Group 17 are: Any grass, Gramineae family (either
green or cured) except sugarcane and those included in the cereal grains group, that will be fed to or
grazed by livestock, all pasture and range grasses and grasses grown for hay or silage.
(20) Crop Group 18. Nongrass Animal Feeds (Forage, Fodder, Straw, and Hay) Group.
(i) Representative commodities. Alfalfa and clover ( Trifolium spp.)
(ii) Commodities. The following is a list of all the commodities included in Crop Group 18:

Crop Group 18: Nongrass Animal Feeds (Forage, Fodder, Straw, and Hay) Group—Commodities
Alfalfa ( Medicago sativa subsp. sativa )
Bean, velvet ( Mucuna pruriens var. utilis )
Clover ( Trifolium spp., Melilotus spp.)
Kudzu ( Pueraria lobata )
Lespedeza ( Lespedeza spp.)
Lupin ( Lupinus spp.)
Sainfoin ( Onobrychis viciifolia );
Trefoil ( Lotus spp.)
Vetch ( Vicia spp.)
Vetch, crown ( Coronilla varia )
Vetch, milk ( Astragalus spp).
(21) Crop Group 19. Herbs and Spices Group.
(i) Representative commodities. Basil (fresh and dried); black pepper; chive; and celery seed or dill seed.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 19 and identifies the
related subgroups.
Table 1—Crop Group 19: Herbs and Spices Group
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Related crop
subgroups

Commodities
Allspice ( Pimenta dioica

)

Angelica ( Angelica
archangelica

19B
19A

)

Anise (anise seed) ( Pimpinella
)
anisum

19B

Anise, star ( Illicium verum

)

19B

Annatto (seed)

19B

Balm (lemon balm) ( Melissa
officinalis

19A

)

Basil ( Ocimum basilicum

)

Borage ( Borago
officinalis

19A
19A

)

Burnet ( Sanguisorba
minor
)

19A

Camomile ( Anthemis
nobilis

19A

)

Caper buds ( Capparis
spinosa

19B

)

Caraway ( Carum carvi

)

19B

Caraway, black ( Nigella sativa

)

Cardamom ( Elettaria
cardamomum

)

Cassia bark ( Cinnamomum
aromaticum

)

Cassia buds ( Cinnamomum
aromaticum

)

19B
19B
19B

Catnip ( Nepeta cataria

)

Celery seed ( Apicum
graveolens

Chive, Chinese ( Allium
tuberosum

19A

)

Chive ( Allium
schoenoprasum

19A

)

19A

)

Cinnamon ( Cinnamomum
)
verum

19B

Clary ( Salvia sclarea
Clove buds ( Eugenia
caryophyllata

19A
19B

)

Chervil (dried) ( Anthriscus
cerefolium

19B

)
)

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19B

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Coriander (cilantro or Chinese parsley) (leaf)
( Coriandrum sativum

)

19A

Coriander (cilantro) (seed) ( Coriandrum
)
sativum

19B

Costmary ( Chrysanthemum
balsamita

19A

)

Culantro (leaf) ( Eryngium
foetidum

)

Culantro (seed) ( Eryngium
foetidum

)

19A
19B

Cumin ( Cuminum cyminum
Curry (leaf) ( Murraya
koenigii

)

19B
19A

)

Dill (dillweed) ( Anethum
graveolens

19A

)

Dill (seed) ( Anethum
graveolens

19B

)

Fennel (common) ( Foeniculum
vulgare
)

19B

Fennel, Florence (seed) ( Foeniculum
Azoricum Group)
vulgare

19B

Fenugreek ( Trigonella
foenumgraecum

)

19B

Grains of paradise ( Aframomum
)
melegueta

19B

Horehound ( Marrubium
)
vulgare

19A

Hyssop ( Hyssopus
officinalis
Juniper berry ( Juniperus
communis

)

19B

)

Lavender ( Lavandula
officinalis

)

Lemongrass ( Cymbopogon
citratus

)

Lovage (seed) ( Levisticum
officinale

)

Marigold ( Calendula
officinalis

19A
19A

)

Lovage (leaf) ( Levisticum
officinale

Mace ( Myristica
fragrans

19A

19A
19B
19B

)
)

Marjoram ( Origanum spp.
)
(includes sweet or annual marjoram, wild marjoram or oregano, and
pot marjoram)
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19A
19A

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Mustard (seed) ( Brassica
B.
nigra)

juncea, B.

hirta,

Nasturtium ( Tropaeolum
majus
)

19B
19A

Nutmeg ( Myristica
fragrans

19B

)

Parsley (dried) ( Petroselinum
)
crispum

19A

Pennyroyal ( Mentha pulegium

)

Pepper, black ( Piper nigrum

)

19A
19B

Pepper, white

19B

Poppy (seed) ( Papaver
somniferum

19B

)

Rosemary ( Rosemarinus
officinalis

19A

)

Rue ( Ruta graveolens

)

Saffron ( Crocus sativus

19A

)

Sage ( Salvia
officinalis

19B
19A

)

Savory, summer and winter ( Satureja
)
spp.

19A

Sweet bay (bay leaf) ( Laurus
)
nobilis

19A

Tansy ( Tanacetum
vulgare

19A

)

Tarragon ( Artemisia
dracunculus
Thyme ( Thymus spp.
Vanilla ( Vanilla
planifolia
Wintergreen ( Gaultheria
procumbens

)

19A
19B

)

19A

)

Woodruff ( Galium odorata
Wormwood ( Artemisia
absinthium

19A

)

)

19A
19A

)

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 19, specifies the
representative commodities for each subgroup, and lists all the commodities included in each subgroup.
Table 2—Crop Group 19 Subgroups

Representative commodities

Commodities

Crop Subgroup 19A.Herb
subgroup.

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Basil (fresh and dried) and
chive.

Angelica; balm; basil; borage; burnet; camomile;
catnip; chervil (dried); chive; chive, Chinese, clary;
coriander (leaf); costmary; culantro (leaf); curry (leaf);
dillweed; horehound; hyssop; lavender; lemongrass;
lovage (leaf); marigold; marjoram
( Origanum
spp.); nasturtium;
parsley (dried); pennyroyal; rosemary; rue; sage;
savory, summer and winter; sweet bay; tansy;
tarragon; thyme; wintergreen; woodruff; and
wormwood.

Crop Subgroup 19B.Spice
subgroup.
Black pepper; and celery seed
or dill seed.

Allspice; anise (seed); anise, star; annatto (seed);
caper (buds); caraway; caraway, black; cardamom;
cassia (buds); celery (seed); cinnamon; clove (buds);
coriander (seed); culantro (seed); cumin; dill (seed);
fennel, common; fennel, Florence (seed); fenugreek;
grains of paradise; juniper (berry); lovage (seed);
mace; mustard (seed); nutmeg; pepper, black; pepper,
white; poppy (seed); saffron; and vanilla.

(22) Crop Group 21 . Edible fungi Group.
(i) Representative commodities . White button mushroom and any one oyster mushroom or any Shiitake
mushroom.
(ii) Table . The following is a list of all the commodities in Crop Group 21. There are no related subgroups.
Crop Group 21—Edible Fungi Group—Commodities

Blewitt ( Lepista nuda
Bunashimeji ( Hypsizygus
marrmoreus

)
)

Chinese mushroom ( Volvariella
) (Bull.) Singer
volvacea
Enoki ( Flammulina velutipes
(Curt.) Singer

)

Hime-Matsutake ( Agaricus blazei

) Murill

Hirmeola ( Auricularia auricular

)

Maitake ( Grifola frondosa

)

Morel ( Morchella spp.

)

Nameko ( Pholiota nameko
Net Bearing ( Dictyophora

)
)

Oyster mushroom ( Pleurotus spp.
Pom Pom ( Hericium erinaceus
Reishi mushroom ( Ganoderma lucidum
(Leyss. Fr.) Karst.)
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)
)

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Rodman's agaricus ( Agaricus bitorquis
(Quel.) Saccardo

)

Shiitake mushroom ( Lentinula edodes
Pegl.)
Shimeji ( Tricholoma
conglobatum

(Berk.)

)

Stropharia ( Stropharia spp.
Truffle ( Tuber spp.

)
)

White button mushroom ( Agaricus
bisporous
(Lange) Imbach)
White Jelly Fungi ( Tremella fuciformis

)

[60 FR 26635, May 17, 1995, as amended at 72 FR 69156, 69157, Dec. 7, 2007; 73 FR 52, Jan. 2, 2008]

Subpart C—Specific Tolerances
top
Editorial Note: Nomenclature changes to subpart C appear at 67 FR 41803–41808, June 19, 2002; 67
FR 42393–42397, June 21, 2002; 68 FR 39430–39435, July 1, 2003; 71 FR 74804–74812, Dec. 13, 2006;
72 FR 53137–53151, Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; and 73 FR 60155–60157, Oct. 10,
2008.

§ 180.101 Specific tolerances; general provisions.
top
(a) The tolerances established for pesticide chemicals in this subpart C apply to residues resulting from
their application prior to harvest or slaughter, unless otherwise stated. Tolerances are expressed in terms
of parts by weight of the pesticide chemical per one million parts by weight of the raw agricultural
commodity.
(b) The poisonous and deleterious substances for which tolerances are established by the regulations in
this subpart C are named by their common names wherever practicable, otherwise by their chemical
names.
(c) The analytical methods to be used for determining whether pesticide residues, including negligible
residues, in or on raw agricultural commodities are in compliance with the tolerances established in this
part 180 are identified among the methods contained or referenced in the Food and Drug Administration's
“Pesticide Analytical Manual” which is available from the Food and Drug Administration, Department of
Health, Education, and Welfare, 200 C Street SW., Washington, DC 20204.

§ 180.103 Captan; tolerances for residues.
top
(a)(1) General . Tolerances are established for residues of the fungicide, captan (N-trichloromethylthio-4cyclohexene-1,2-dicarboximide) in or on the following commodities:

Commodity

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Parts per million

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Almond

0.25

Almond, hulls

75.0

Animal feed, nongrass, group 18

0.05

Apple

25.0

Apricot

10.0

Blueberry

20.0

Caneberry, subgroup 13A

25.0

Cherry, sweet

50.0

Cherry, tart

50.0

Cotton, undelinted seed

0.05

Dill, seed

0.05

Flax, seed

0.05

Grape

25.0

Grain, cereal, forage, fodder and straw, group 16

0.05

Grain, cereal, group 15

0.05

Grass, forage

0.05

Grass, hay

0.05

Nectarine

25.0

Okra

0.05

Peach

15.0

Peanut

0.05

Peanut, hay

0.05

Pear

25.0

Plum, prune, fresh

10.0

Rapeseed, forage

0.05

Rapeseed, seed

0.05

Safflower, seed

0.05

Sesame, seed

0.05

Strawberry

20.0

Sunflower, seed

0.05

Vegetable, brassica leafy, group 5

0.05

Vegetable, bulb, group 3

0.05

Vegetable, cucurbit, group 9

0.05

Vegetable, foliage of legume, group 7

0.05

Vegetable, fruiting, group 8

0.05

Vegetable, leafy, except brassica, group 4

0.05

Vegetable, leaves of root and tuber, group 2

0.05

Vegetable, legume, group 6

0.05

Vegetable, root and tuber, group 1

0.05

(2) Tolerances are established for the combined residues of the fungicide, captan (N-trichloromethylthio-4http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c=...f&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (68 of 651) [9/8/2009 3:02:16 PM]

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cyclohexene-1,2-dicarboximide) and its metabolite 1,2,3,6-tetrahydrophthalimide (THPI), measured at
THPI, in or on the following commodities:

Commodity

Parts per million

Cattle, fat

0.15

Cattle, meat

0.20

Cattle, meat byproducts

0.30

Goat, fat

0.15

Goat, meat

0.20

Goat, meat byproducts

0.30

Hog, fat

0.15

Hog, meat

0.20

Hog, meat byproducts

0.30

Horse, fat

0.15

Horse, meat

0.20

Horse, meat byproducts

0.30

Milk

0.10

Sheep, fat

0.15

Sheep, meat

0.20

Sheep, meat byproducts

0.30

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 52016, Sept. 12, 2007]

§ 180.106 Diuron; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the herbicide diuron, 3-(3,4dichlorophenyl)-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline in or on food
commodities, as follows:

Commodity

Parts per million

Alfalfa, forage

3.0

Alfalfa, hay

2.0

Apple

0.1

Artichoke, globe

1

Asparagus

7

Banana

0.1

Berry group 13

0.1

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Cattle, fat

1

Cattle, meat

1

Cattle, meat byproducts

1

Citrus, oil

3.0

Corn, field, grain

0.1

Corn, pop, grain

0.1

Cotton, undelinted seed

0.2

Fish – freshwater finfish, farm raised

2.0

Fruit, citrus, group 10, except lemon

0.05

Goat, fat

1

Goat, meat

1

Goat, meat byproducts

1

Grain, aspirated fractions
Grape

5.0
0.05

Grass, forage, except bermudagrass

2

Grass, hay, except bermudagrass

2

Hazelnut

0.1

Hog, fat

1

Hog, meat

1

Hog, meat byproducts

1

Horse, fat

1

Horse, meat

1

Horse, meat byproducts

1

Lemon
Nut, macadamia
Olive

0.5
0.05
1

Papaya

0.5

Peach

0.1

Pear

1

Pea, field, seed

0.1

Pea, field, vines

2

Pea, field, hay

2

Pecan

0.05

Peppermint, tops

1.5

Pineapple

0.1

Pineapple, process residue

0.4

Sheep, fat

1

Sheep, meat

1

Sheep, meat byproducts

1

Sorghum, grain, forage

2

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Sorghum, grain, grain

0.5

Sorghum, grain, stover

2

Spearmint, tops

1.5

Sugarcane, cane

0.2

Sugarcane, molasses

0.7

Walnut

0.05

Wheat, bran

0.7

Wheat, forage

2

Wheat, grain

0.5

Wheat, hay

2

Wheat, straw

1.5

(b) Section 18 emergency exemptions. Time-limited tolerances are established for combined residues of
the herbicide diuron and its metabolites convertible to 3,4-dichloroaniline in connection with use of the
pesticide under section 18 emergency exemptions granted by EPA. These tolerances will expire and are
revoked on the dates specified in the following table.

Commodity

Parts per million

Catfish

Expiration/Revocation date
2.0

06/30/08

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in § 180.1(n)
are established for the combined residues of the herbicide diuron (3-(3,4-dichlorophenyl)-1,1-dimethylurea
and its metabolites convertible to 3,4-dichloroaniline) in or on the raw agricultural commodities:

Commodity

Parts per million

Barley, bran

0.7

Barley, grain

0.2

Barley, hay
Barley, straw
Cactus

2
1.5
0.05

Clover, forage

0.1

Clover, hay

1.0

Oat, forage

2

Oat, grain
Oat, hay

0.1
2

Oat, straw

1.5

Trefoil, forage

0.1

Trefoil, hay

1.5

Vetch, forage

0.1

Vetch, hay

1.5

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 2164, Jan. 14, 1998, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, 1999; 66
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FR 28671, May 24, 2001; 67 FR 46883, July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR 32540, June
13, 2007; 72 FR 35666, June 29, 2007; 73 FR 54958, Sept. 24, 2008]

§ 180.108 Acephate; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of acephate per se ( O , S -dimethyl
acetylphosphoramidothioate) in or on the following food commodities1 :

Commodity1

Parts per million

Bean, dry, seed

3.0

Bean, succulent

3.0

Brussels sprouts

3.0

Cattle, fat

0.1

Cattle, meat

0.1

Cattle, meat byproducts

0.1

Cauliflower

2.0

Celery

10

Cotton, hulls

1.0

Cotton, meal

1.0

Cotton, undelinted seed

0.5

Cranberry

0.5

Egg

0.1

Goat, fat

0.1

Goat, meat

0.1

Goat, meat byproducts

0.1

Hog, fat

0.1

Hog, meat

0.1

Hog, meat byproducts

0.1

Horse, fat

0.1

Horse, meat

0.1

Horse, meat byproducts

0.1

Lettuce, head

10

Milk

0.1

Peanut

0.2

Pepper

4.0

Peppermint, tops

27

Poultry, fat

0.1

Poultry, meat

0.1

Poultry, meat byproducts

0.1

Sheep, fat

0.1

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Sheep, meat

0.1

Sheep, meat byproducts

0.1

Spearmint, tops

27

Soybean, seed

1.0

1Residues

of the acephate metabolite, methamidophos, are regulated under 40 CFR 180.315

(2) A food tolerance of 0.02 ppm is established for residues of acephate per se ( O , S -dimethyl
acetylphosphoramidothioate) as follows:
(i) In or on all food items (other than those already covered by a higher tolerance as a result of use on
growing crops) in food handling establishments.
(ii) The acephate may be present as a residue from applications of acephate in food handling
establishments, including food service, manufacturing and processing establishments, such as
restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants,
and canneries in accordance with the following prescribed conditions:
(A) Application shall be limited solely to spot and/or crack and crevice treatment in food handling
establishments where food and food products are held, processed, prepared and served. Spray
concentration shall be limited to a maximum of 1.0 percent active ingredient. For crack and crevice
treatments, equipment capable of delivering a pin-stream of insecticide shall be used. For spot treatments,
a coarse, low-pressure spray shall be used to avoid atomization or splashing of the spray. Contamination
of food or food-contact surfaces shall be avoided.
(B) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration . Tolerances with regional registration, as defined in §180.1(m),
are established for residues of acephate per se ( O , S -dimethyl acetylphosphoramidothioate) in or on the
following food commodities:

Commodity

Parts per million

Nut, macadamia

0.05

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 13542, Mar. 20, 1998, as amended at 67 FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008]

§ 180.110 Maneb; tolerances for residues.
top
(a) General. Tolerances for residues of the fungicide maneb (manganous ethylenebisdithiocarbamate),
calculated as zinc ethylenebisdithiocarbamate, are established in or on raw agricultural commodities in the
following table:

Commodity
Almond

Parts per million Expiration/Revocation Date
0.1

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Apple

2

None

10

None

Banana (not more than 0.5 part per
million) shall be in the pulp after
peel is removed and discarded
(preharvest application only)

4

None

Bean, dry, seed

7

None

Bean, succulent

10

None

Beet, sugar, tops

45

None

Broccoli

10

None

Brussels sprouts

10

None

Cabbage

10

None

Cabbage, chinese

10

None

7

None

10

None

5

None

10

None

Corn, sweet, kernel plus cob with
husks removed

5

None

Cranberry

7

None

Cucumber

4

None

Eggplant

7

None

10

None

Fig

7

None

Grape

7

None

Kale

10

None

Kohlrabi

10

None

Lettuce

10

None

4

None

Mustard greens

10

None

Nectarine

10

None

Onion

7

None

Papaya

10

None

Peach

10

None

Pepper

7

None

Potato

0.1

None

Pumpkin

7

None

Squash, summer

4

None

Squash, winter

4

None

Tomato

4

None

10

None

Apricot

Carrot, roots
Cauliflower
Celery
Collards

Endive

Melon

Turnip, greens

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Turnip, roots

7

None

(b) Section 18 emergency exemptions. A time-limited tolerance is established for residues of the fungicide
maneb (manganous ethylenebisdithiocarbamate), calculated as zinc ethylenebisdithiocarbamate, and its
metabolite ethylenethiourea in connection with use of the pesticide under a section 18 emergency
exemption granted by EPA. The tolerance will expire and is revoked on the date specified in the following
table:

Commodity

Parts per million

Walnut

Expiration/revocation date

0.05

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 49924, Sept. 24, 1997, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 13103, Mar. 17, 1999;
64 FR 72284, Dec. 27, 1999; 66 FR 64773, Dec. 14, 2001; 68 FR 37764, June 25, 2003; 70 FR 37696,
June 30, 2005; 70 FR 75739, Dec. 21, 2005; 74 FR 636, Jan. 7, 2009]

§ 180.111 Malathion; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide malathion ( O,O -dimethyl
dithiophosphate of diethyl mercaptosuccinate) in or on the following food commodities:

Commodity
Alfalfa
Almond, hulls

Parts per million
135
50

Almond, postharvest

8

Apple

8

Apricot

8

Asparagus

8

Avocado

8

Barley, grain, postharvest

8

Bean

8

Beet (including tops)

8

Beet, sugar, roots

1

Beet, sugar, tops

8

Blackberry

8

Blueberry

8

Boysenberry

8

Carrot, roots

8

Cattle, fat (PRE-S)

4

Cattle, meat byproducts1(PRE-S)

4

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Cattle, meat1(PRE-S)

4

Chayote, fruit

8

Chayote, roots

8

Cherry

8

Chestnut

1

Clover

135

Corn, forage

8

Corn, grain, postharvest

8

Corn, sweet, kernel plus cob with husks removed

2

Cotton, undelinted seed

2

Cowpea, forage

135

Cowpea, hay

135

Cranberry

8

Cucumber

8

Currant

8

Date, dried fruit

8

Dewberry

8

Eggplant

8

Egg (from application to poultry)
Fig
Flax, seed

0.1
8
0.1

Garlic

8

Goat, fat (PRE-S)

4

Goat, meat byproducts1(PRE-S)

4

Goat, meat1(PRE-S)

4

Gooseberry

8

Grapefruit

8

Grape

8

Grass, forage

135

Grass, hay

135

Guava

8

Hazelnut

1

Hog, fat (PRE-S)

4

Hog, meat byproducts1(PRE-S)

4

Hog, meat1(PRE-S)

4

Hop, dried cones

1

Horseradish

8

Horse, fat (PRE-S)

4

Horse, meat byproducts1(PRE-S)

4

Horse, meat1(PRE-S)

4

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Kumquat

8

Leek

8

Lemon

8

Lentil, seed

8

Lespedeza, hay

135

Lime

8

Loganberry

8

Lupin, seed

8

Mango

8

Melon

8

Milk, fat (from application to dairy cows)

0.5

Mushroom

8

Nectarine

8

Nut, macadamia

1

Oat, grain, postharvest

8

Okra

8

Onion (including green onion)

8

Orange, sweet

8

Papaya

1

Parsnip

8

Passionfruit

8

Pea

8

Pea, field, hay

8

Pea, field, vines

8

Peach

8

Peanut, hay

135

Peanut, postharvest

8

Pear

8

Pecan

8

Pepper

8

Peppermint, tops

8

Pineapple

8

Plum

8

Potato

8

Poultry, fat (PRE-S)

4

Poultry, meat byproducts1(PRE-S)

4

Poultry, meat1(PRE-S)

4

Plum, prune

8

Pumpkin

8

Quince

8

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Radish

8

Raspberry

8

Rice, grain, postharvest

8

Rice, wild

8

Rutabagas

8

Rye, grain, postharvest

8

Safflower, seed

0.2

Salsify (including tops)

8

Shallot, bulb

8

Sheep, fat (PRE-S)

4

Sheep, meat byproducts1(PRE-S)

4

Sheep, meat1(PRE-S)

4

Sorghum, forage

8

Sorghum, grain, grain, postharvest

8

Soybean (dry and succulent)

8

Soybean, forage

135

Soybean, hay

135

Spearmint, tops

8

Squash, summer and winter

8

Strawberry

8

Sunflower, seed (Post-H)

8

Sweet potato, roots

1

Tangerine

8

Tomato

8

Trefoil, forage

135

Trefoil, hay

135

Turnip (including tops)

8

Vegetable, brassica, leafy, group 5

8

Vegetables, leafy, except brassica, group 4

8

Vetch, hay

135

Walnut

8

Wheat, grain, postharvest

8

1The

tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat,
hog, horse, poultry, or sheep.
(2) Malathion may be safely used in accordance with the following conditions:
(i) It is incorporated into paper trays in amounts not exceeding 100 milligrams per square foot.
(ii) Treated paper trays are intended for use only in the drying of grape (raisins).
(iii) Total residues of malathion resulting from drying of grape on treated trays and from application to
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grape before harvest shall not exceed 12 parts per million on processed ready-to-eat raisins.
(3) Residues of malathion in safflower, refined oil from application to the growing safflower plant shall not
exceed 0.6 parts per million.
(4) Malathion may be safely used for the control of insects during the drying of grape (raisins) in
compliance with paragraph (a)(2) of this section by incorporation into paper trays in amounts not
exceeding 100 milligrams per square foot.
(5) Malathion ( O,O- dimethyl dithiophosphate of diethyl mercaptosuccinate) may be safely used in feed in
accordance with the following conditions.
(i) A tolerance of 50 parts per million is established for residues of malathion in citrus, dried pulp for cattle
feed, when present as the result of the application of the pesticide to bagged citrus pulp during storage.
Whether or not tolerances for residues of malathion on the fresh fruit have been established under section
408 of the Act, the total residue of malathion in the citrus, dried pulp shall not exceed 50 parts per million.
(ii) A tolerance of 10 parts per million is established for malathion in nonmedicated cattle feed concentrate
blocks resulting from its application as a pesticide to paper used in packaging the nonmedicated cattle
feed concentrate blocks.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[43 FR 22974, May 30, 1978, as amended at 43 FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, 1979; 45
FR 76145, Nov. 18, 1980; 47 FR 42738, Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR 45183, Nov.
25, 1987; 62 FR 66023, 66025, Dec. 17, 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, June 29, 2007;
73 FR 54959, Sept. 24, 2008]

§ 180.114 Ferbam; tolerances for residues.
top
(a) General . Tolerances are established for residues of the fungicide ferbam (ferric
dimethyldithiocarbamate), calculated as carbon disulfide, in or on the following food commodities:

Commodity

Parts per million

Expiration/Revocation Date

Apple

4.01

None

Bean

7.01

10/27/07

Cabbage

7.01

10/27/07

Cherry

4.01

None

Cranberry

4.01

None

Fruit, citrus, group 10

4.01

None

Grape

4.01

None

Lettuce

7.01

10/27/07

Nectarine

4.01

None

Peach

4.01

None

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Pear

4.01

None

Raspberry

7.01

10/27/07

1Some of these tolerances were established on the basis of data acquired at the public hearings held in
1950 (formerly §180.101) and the remainder were established on the basis of pesticide petitions
presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act
by Pub. L. 518, 83d Congress (68 Stat. 511)

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(m),
are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon
disulfide, in or on the following food commodities:

Commodity

Parts per million

Mango

4.01

1This

tolerance was established on the basis of data acquired at the public hearings held in 1950 (formerly
§180.101) and the remainder was established on the basis of pesticide petitions presented under the
procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d
Congress (68 Stat. 511)
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 57072, Oct. 26, 1998, as amended at 72 FR 53453, Sept. 19, 2007]

§ 180.116 Ziram; tolerances for residues.
top
(a) General. Tolerances are established for residues of the fungicide ziram (zinc dimethyldithiocarbamate),
calculated as zinc ethylenebisdithiocarbamate, in or on the following food commodities:

Commodity

Parts per million

Almond

0.11

Apple

7.01

Apricot

7.01

Blackberry

7.01

Blueberry

7.01

Cherry, sweet

7.01

Cherry, tart

7.01

Grape

7.0

Huckleberry

7.0

Peach

7.0

Pear
Pecan

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7.01
0.1

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Quince

7.01

Strawberry

7.0

Tomato

7.01

1Some of these tolerances were established on the basis of data acquired at the public hearings held in
1950 (formerly §180.101) and the remainder were established on the basis of pesticide petitions
presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act
by Public Law 518, 83d Congress (68 Stat. 511).

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39437, July 1, 2003, as amended at 71 FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, 2008]

§ 180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.
top
Tolerances are established for negligible residues (N) of the herbicide S-ethyl dipropylthiocarbamate in or
on the following raw agricultural commodities:

Commodity

Parts per million

Almond, hulls

0.1(N)

Asparagus

0.1(N)

Castorbean, seed

0.1(N)

Cotton, forage

0.1(N)

Cotton, undelinted seed

0.1(N)

Flax, seed

0.1(N)

Fruit, citrus

0.1(N)

Fruit, small

0.1(N)

Grain, crop

0.1(N)

Grass, forage

0.1(N)

Legume, forage

0.1(N)

Nut

0.1(N)

Pineapple

0.1(N)

Safflower, seed

0.1(N)

Strawberry

0.1(N)

Sunflower, seed

0.1(N)

Vegetable, fruiting

0.1(N)

Vegetable, leafy

0.1(N)

Vegetable, root

0.1(N)

Vegetable, seed and pod

0.1(N)

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[42 FR 9178, Feb. 15, 1977]

§ 180.121 Methyl parathion; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide parathion O, O -Dimethyl- O -pnitrophenyl thiophosphate (the methyl homolog of parathion) in or on the following raw agricultural
commodities:

Commodity
Alfalfa, forage

Parts per million

Expiration/Revocation Date

1.25

None

Alfalfa, hay

5.0

None

Almond

0.1

None

Almond, hulls

3.0

None

Barley

1.0

None

Bean, dry, seed

1.0

1/24/09

Beet, sugar, roots

0.1

1/24/09

Beet, sugar, tops

0.1

1/24/09

Cabbage

1.0

1/24/09

Corn

1.0

None

Corn, field, forage

1.0

None

Corn, sweet, forage

1.0

None

0.75

None

Grass, forage

1.0

None

Hop, dried cones

1.0

1/24/09

Oat

1.0

None

Onion

1.0

None

Peanut

1.0

None

Pea, dry, seed

1.0

1/24/09

Pea, field, vines

1.0

None

Pecan

0.1

1/24/09

Potato

0.1

None

Rapeseed, seed

0.2

None

Rice, grain

1.0

None

Soybean, hay

1.0

None

Soybean, seed

0.1

None

Sunflower, seed

0.2

None

Sweet potato, roots

0.1

None

Walnut

0.1

None

Wheat

1.0

None

Cotton, undelinted seed

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
(e) Revoked tolerances subject to the channel of trade provisions. The following table lists commodities for
which methyl parathion use was unlawful after December 31, 1999, and the revoked tolerances.
Commodities with residues of methyl parathion resulting from lawful use are subject to the channels of
trade provisions of section 408(1)(5) of the FFDCA.

Commodity

Parts per million

Apple

1

Artichoke, globe

1

Beet, garden, roots

1

Beet, garden, tops

1

Broccoli

1

Brussels sprouts

1

Carrot, roots

1

Cauliflower

1

Celery

1

Cherry

1

Collards

1

Grape

1

Kale

1

Kohlrabi

1

Lettuce

1

Mustard greens

1

Nectarine

1

Peach

1

Pear

1

Plum, prune, fresh

1

Rutabaga, roots

1

Rutabaga tops

1

Spinach

1

Tomato

1

Trefoil, forage

1.25

Trefoil, hay

5

Turnip, greens

1

Turnip, roots

1

Vegetable, brassica, leafy, group 5

1

Vetch

1

[66 FR 1245, Jan. 5, 2001, as amended at 66 FR 38955, July 26, 2001; 67 FR 38603, June 5, 2002; 72
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FR 35666, June 29, 2007; 73 FR 54959, Sept. 24, 2008]

§ 180.122 Parathion; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide parathion ( O, O -Diethyl- O -pnitrophenyl thiophosphate) in or on the following raw agricultural commodities:

Commodity

Parts per million

Alfalfa, forage

Expiration/Revocation Date

1.25

12/31/05

Alfalfa, hay

5.0

12/31/05

Barley

1.0

12/31/05

Corn

1.0

12/31/05

Corn, forage

1.0

12/31/05

0.75

12/31/05

Rapeseed, seed

0.2

12/31/05

Sorghum, forage

3.0

12/31/05

Sorghum, grain, grain

0.1

12/31/05

Sorghum, grain, stover

3.0

12/31/05

Soybean

0.1

12/31/05

Soybean, hay

1.0

12/31/05

Sunflower, seed

0.2

12/31/05

Wheat

1.0

12/31/05

Cotton, undelinted seed

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 38603, June 5, 2002]

§ 180.123 Inorganic bromide residues resulting from fumigation with methyl
bromide; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of inorganic bromides (calculated as Br) in or on
the following food commodities which have been fumigated with the antimicrobial agent and insecticide
methyl bromide after harvest (with the exception of strawberry):

Commodity
Alfalfa, hay, postharvest
Almond, postharvest
Apple, postharvest
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Parts per million
50.0
200.0
5.0

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Apricot, postharvest

20.0

Artichoke, jerusalem, postharvest

30.0

Asparagus, postharvest

100.0

Avocado, postharvest

75.0

Barley, grain, postharvest

50.0

Bean, lima, postharvest

50.0

Bean, postharvest

50.0

Bean, snap, succulent, postharvest

50.0

Bean, succulent, postharvest

50.0

Beet, garden, roots, postharvest

30.0

Beet, sugar, roots, postharvest

30.0

Blueberry, postharvest

20.0

Butternut, postharvest

200.0

Cabbage, postharvest

50.0

Cantaloupe, postharvest

20.0

Carrot, roots, postharvest

30.0

Cashew, postharvest
Cherry, sweet, postharvest
Cherry, tart, postharvest
Chestnut, postharvest

200.0
20.0
20
200.0

Cippolini, bulb, postharvest

50.0

Citron, citrus, postharvest

30.0

Cacao bean, roasted bean, postharvest

50.0

Coconut, copra, postharvest

100.0

Coffee, bean, green, postharvest

75.0

Corn, field, grain, postharvest

50.0

Corn, pop, postharvest
Corn, sweet, kernel plus cob with husks removed, postharvest
Cotton, undelinted seed, postharvest
Cucumber, postharvest
Cumin, seed, postharvest

240.0
50.0
200.0
30.0
100.0

Eggplant, postharvest

20.0

Garlic, postharvest

50.0

Ginger, postharvest

100.0

Grapefruit, postharvest

30.0

Grape, postharvest

20.0

Hazelnut, postharvest

200.0

Horseradish, postharvest

30.0

Kumquat, postharvest

30.0

Lemon, postharvest

30.0

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Lime, postharvest

30.0

Mango, postharvest

20.0

Melon, honeydew, postharvest

20.0

Muskmelon, postharvest

20.0

Nectarine, postharvest

20.0

Nut, brazil, postharvest

200.0

Nut, hickory, postharvest

200.0

Nut, macadamia, postharvest

200.0

Oat, postharvest

50.0

Okra, postharvest

30.0

Onion, bulb, postharvest

20.0

Onion, green, postharvest

20.0

Orange, postharvest

30.0

Papaya, postharvest

20.0

Parsnip, roots, postharvest

30.0

Peach, postharvest

20.0

Peanut, postharvest

200.0

Pear, postharvest

5.0

Pea, blackeyed, postharvest

50.0

Pea, postharvest

50.0

Pecan, postharvest

200.0

Pepper, postharvest

30.0

Pimento, postharvest

30.0

Pineapple, postharvest

20.0

Pistachio, postharvest

200.0

Plum, postharvest
Pomegranate, postharvest

20.0
100.0

Potato, postharvest

75.0

Pumpkin, postharvest

20.0

Quince, postharvest

5.0

Radish, postharvest

30.0

Rice, grain, postharvest

50.0

Rutabaga, roots, postharvest

30.0

Rutabaga, tops, postharvest

30.0

Rye, grain, postharvest

50.0

Salsify, roots, postharvest

30.0

Sorghum, grain, grain, postharvest

50.0

Soybean, postharvest

200.0

Squash, summer, postharvest

30.0

Squash, winter, postharvest

20.0

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Squash, zucchini, postharvest

20.0

Strawberry, postharvest

60.0

Sweet potato, postharvest

75.0

Tangerine, postharvest

30.0

Timothy, hay, postharvest

50.0

Tomato, postharvest

20.0

Turnip, roots, postharvest

30.0

Walnut, postharvest

200.0

Watermelon, postharvest

20.0

Wheat

50.0

(2) Inorganic bromide may be present as a residue in certain processed food in accordance with the
following conditions:
(i) When inorganic bromide residues are present as a result of fumigation of the processed food with
methyl bromide or from such fumigation in addition to the authorized use of methyl bromide on the source
raw agricultural commodity, as provided for in this part, the total residues of inorganic bromides (calculated
as Br) shall not exceed the following levels:
(A) 400 parts per million in or on egg, dried and herb, processed and spice.
(B) 325 parts per million in or on cheese, parmesan and cheese, roquefort cheese.
(C) 250 parts per million in or on tomato, concentrated products and fig, dried fruit.
(D) 125 parts per million in or on processed food other than those listed above.
(ii) When inorganic bromide residues are present in malt beverage, fermented in accordance with 21 CFR
172.730(a)(2), the amount shall not exceed 25 parts per million (calculated as Br).
(iii) Where tolerances are established on both the raw agricultural commodities and processed food made
therefrom, the total residues of inorganic bromides in or on the processed food shall not be greater than
those designated in paragraph (a)(2) of this section, unless a higher level is established elsewhere in this
part.
(3) Tolerances are established for residues of inorganic bromides (calculated as Br) as follows:
(i) 400 parts per million for residues in or on dog food, resulting from fumigation with methyl bromide.
(ii) 125 parts per million for residues in or on processed commodities for animal feedstuffs from barley,
corn, grain sorghum, oat, rice, rye and wheat, resulting directly from fumigation with methyl bromide or
from carryover and concentration of residues of inorganic bromides from fumigation of the grains with
methyl bromide.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(n), is
established for residues of inorganic bromides (calculated as Br) in or on the following food commodity
grown in soil fumigated with methyl bromide.

Commodity

Parts per million

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Ginger, postharvest

100

(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74812, Dec. 13, 2006]

§ 180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of
policy.
top
(a) Investigations by the Food and Drug Administration show that peanut hay and peanut shells have been
used as feed for meat and dairy animals. While many growers now harvest peanuts with combines and
leave the hay on the ground to be incorporated into the soil, some growers follow the practice of curing
peanuts on the vines in a stack and save the hay for animal feed. Peanut shells or hulls have been used to
a minor extent as roughage for cattle feed. It has been established that the feeding to cattle of peanut hay
and peanut hulls containing residues of inorganic bromides will contribute considerable residues of
inorganic bromides to the meat and milk.
(b) There are no tolerances for inorganic bromides in meat and milk to cover residues from use of such
peanut hulls as animal feed. Peanut hulls containing residues of inorganic bromides from the use of
methyl bromide are unsuitable as an ingredient in the feed of meat and dairy animals and should not be
represented, sold, or used for that purpose.
[58 FR 65555, Dec. 15, 1993]

§ 180.127 Piperonyl butoxide; tolerances for residues.
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(a) General. (1) Tolerances for residues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl
piperonyl)ether] are established in or on the following food commodities:

Commodity

Parts per million

Almond, postharvest

8

Apple, postharvest

8

Barley, postharvest

20

Bean, postharvest

8

Birdseed, mixtures, postharvest

20

Blackberry, postharvest

8

Blueberry, postharvest

8

Boysenberry, postharvest

8

Buckwheat, grain, postharvest

20

Cattle, fat

0.1

Cattle, meat byproducts

0.1

Cattle, meat

0.1

Cherry, sweet, postharvest

8

Cherry, tart, postharvest

8

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Cacoa bean, roasted bean, postharvest

8

Coconut, copra, postharvest

8

Corn, field, grain, postharvest

20

Corn, pop, postharvest

20

Cotton, undelinted seed, postharvest

8

Crabapple, postharvest

8

Currant, postharvest

8

Dewberry, postharvest

8

Egg

1

Fig, postharvest

8

Flax, seed, postharvest

8

Goat, fat

0.1

Goat, meat byproducts

0.1

Goat, meat

0.1

Gooseberry, postharvest

8

Grape, postharvest

8

Guava, postharvest

8

Hog, fat

0.1

Hog, meat byproducts

0.1

Hog, meat

0.1

Horse, fat

0.1

Horse, meat byproducts

0.1

Horse, meat

0.1

Loganberry, postharvest

8

Mango, postharvest

8

Milk, fat

0.25

Muskmelon, postharvest

8

Oat, postharvest

8

Orange, postharvest

8

Peach, postharvest

8

Peanut, postharvest

8

Pea, postharvest

8

Pear, postharvest

8

Pineapple, postharvest

8

Plum, prune, fresh, postharvest

8

Potato, postharvest

0.25

Poultry, fat

3

Poultry, meat byproducts

3

Poultry, meat

3

Raspberry, postharvest

8

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Rice, postharvest

20

Rye, postharvest

20

Sheep, fat

0.1

Sheep, meat byproducts

0.1

Sheep, meat

0.1

Sorghum, grain, postharvest
Sweet potato, postharvest

8
0.25

Tomato, postharvest

8

Walnut, postharvest

8

Wheat, postharvest

20

(2) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:
(i) It is used or intended for use in combination with pyrethrins for control of insects:
(A) In cereal grain mills and in storage areas for milled cereal grain products, whereby the amount of
piperonyl butoxide is at least equal to but not more than 10 times the amount of pyrethrins in the
formulation.
(B) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60
milligrams per square foot, whereby the amount of piperonyl butoxide is equal to 10 times the amount of
pyrethrins in the formulation. Such treated bags are to be used only for food, dried.
(C) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot
of cloth, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the
formulation. Such treated bags are constructed with waxed paper liners and are to be used only for food,
dried that contain 4 percent fat or less.
(D) In two-ply bags consisting of cellophane/polyolefin sheets bound together by an adhesive layer when it
is incorporated in the adhesive. The treated sheets shall contain not more than 50 milligrams of piperonyl
butoxide per square foot (538 milligrams per square meter). Such treated bags are to be used only for
packaging plum, prune, dried; grape, raisin; and other fruit, dried and are to have a maximum ratio of 3.12
milligrams of piperonyl butoxide per ounce of fruit (0.10 milligram of piperonyl butoxide per gram of
product).
(E) In food processing and food storage areas: Provided, That the food is removed or covered prior to
such use.
(ii) It is used or intended for use in combination with pyrethrins and N-octylbicycloheptene dicarboximide
for insect control in accordance with 21 CFR 178.3730.
(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide in or on:
(A) Grain, cereal, milled fractions when present therein as a result of its use in cereal grain mills and in
storage areas for milled cereal grain products.
(B) Food, dried when present as a result of migration from its use on the outer ply of multiwall paper bags
of 50 pounds or more capacity.
(C) Food treated in accordance with 21 CFR 178.3730.
(D) Food, dried that contain 4 percent fat, or less, when present as a result of migration from its use on the
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cloth of cotton bags of 50 pounds or more capacity constructed with waxed paper liners.
(E) Food treated in accordance with paragraph (a)(2)(i)(D) and (E) of this section.
(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(v) Where tolerances are established on both raw agricultural commodities and processed food made
therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than
that permitted by the larger of the two tolerances.
(3) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:
(i) It is used or intended for use in combination with pyrethrins for control of insects:
(A) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60
milligrams per square foot.
(B) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot
of cloth. Such treated bags are constructed with waxed paper liners and are to be used only for feed, dried
that contain 4 percent fat or less.
(ii) It is used in combination with pyrethrins, whereby the amount of piperonyl butoxide is equal to 10 times
the amount of pyrethrins in the formulation. Such treated bags are to be used only for feed, dried.
(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide when present as
the result of migration:
(A) In or on feed, dried from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.
(B) In or on feed, dried that contain 4 percent fat, or less, from its use on cotton bags of 50 pounds or
more capacity constructed with waxed paper liners.
(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency.
(v) Where tolerances are established on both the raw agricultural commodities and food, processed made
therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than
that permitted by the larger of the two tolerances.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74813, Dec. 13, 2006]

§ 180.128 Pyrethrins; tolerances for residues.
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(a) General . (1) Tolerances for residues of the insecticide pyrethrins ((1S)-2-methyl-4-oxo-3-(2Z)-2,4pentadienylcyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate
(pyrethrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4-pentadienyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c=...f&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (91 of 651) [9/8/2009 3:02:17 PM]

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methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropane-carboxylate (pyrethrin 2), (1S)-3-(2Z)-2-butenyl-2methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate
(cinerin 1), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2-pentenyl2-cyclopenten-1-yl (1R, 3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (jasmolin 1),
and (1S)-2-methyl-4-oxo-3-(2Z)-pentenyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1propenyl]-2,2-dimethylcyclopropanecarboxylate (jasmolin 2)), the insecticidally active principles of
Chrysanthemum cinerariaefolium, which are measured as cumulative residues of pyrethrin 1, cinerin 1,
and jasmolin 1 are not to exceed the following:

Commodity

Parts per million

Almond, postharvest

1.0

Apple, postharvest

1.0

Barley, grain, postharvest

3.0

Bean, succulent, postharvest

1.0

Birdseed, mixtures, postharvest

3.0

Blackberry, postharvest

1.0

Blueberry, postharvest

1.0

Boysenberry, postharvest

1.0

Buckwheat, grain, postharvest

3.0

Cacao bean, roasted bean, postharvest

1.0

Cattle, fat

1.0

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Cherry, sweet, postharvest

1.0

Cherry, tart, postharvest

1.0

Coconut, copra, postharvest

1.0

Corn, field, grain, postharvest

3.0

Corn, pop, grain, postharvest

3.0

Cotton, undelinted seed, postharvest

1.0

Crabapple, postharvest

1.0

Currant, postharvest

1.0

Dewberry, postharvest

1.0

Fig, postharvest

1.0

Flax, seed, postharvest

1.0

Goat, fat

1.0

Goat, meat

0.05

Goat, meat byproducts

0.05

Gooseberry, postharvest

1.0

Grape, postharvest

1.0

Guava, postharvest

1.0

Hog, fat

1.0

Hog, meat

0.05

Hog, meat byproducts

0.05

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Horse, fat

1.0

Horse, meat

0.05

Horse, meat byproducts

0.05

Loganberry, postharvest

1.0

Mango, postharvest

1.0

Milk, fat (reflecting negligible residues in milk)

0.05

Muskmelon, postharvest

1.0

Oat, grain, postharvest

1.0

Orange, postharvest

1.0

Pea, dry, seed, postharvest

1.0

Peach, postharvest

1.0

Peanut, postharvest

1.0

Pear, postharvest

1.0

Pineapple, postharvest

1.0

Plum, prune, fresh, postharvest

1.0

Potato, postharvest

0.05

Raspberry, postharvest

1.0

Rice, grain, postharvest

3.0

Rye, grain, postharvest

3.0

Sheep, fat

1.0

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Sorghum, grain, grain, postharvest
Sweet potato, postharvest

1.0
0.05

Tomato, postharvest

1.0

Walnut, postharvest

1.0

Wheat, grain, postharvest

3.0

(2) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on milled fractions
derived from grain, cereal when present as a result of its use in cereal grain mills and in storage areas for
milled cereal grain products.
(3) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on all food items in
food handling establishments where food and food products are held, processed, prepared and/or served.
Food must be removed or covered prior to use.
(4) Where tolerances are established on both the raw agricultural commodities and processed foods made
there-from, the total residues of pyrethrins in or on the processed food shall not be greater than that
permitted by the larger of the two tolerances.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[71 FR 74814, Dec. 13, 2006, as amended at 73 FR 5108, Jan. 29, 2008]

§ 180.129 o-Phenylphenol and its sodium salt; tolerances for residues.
top
(a) General . Tolerances are established for combined residues of the fungicide o-phenylphenol and
sodium o-phenylphenate, each expressed as o-phenylphenol, from postharvest application of either in or
on the following food commodities:

Commodity
Apple
Cantaloupe (NMT 10 ppm in edible portion)
Carrot, roots
Cherry

Parts per million
25
125
20
5

Citrus fruits

10

Cucumber

10

Lemon

10

Nectarine

5

Orange

10

Pepper, bell

10

Peach

20

Pear

25.0

Pineapple

10

Plum, prune, fresh

20

Sweet potato, roots

15

Tomato

10

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54960, Sept. 24, 2008]

§ 180.130 Hydrogen Cyanide; tolerances for residues.
top
(a) General. A tolerance for residues of the insecticide hydrogen cyanide from postharvest fumigation as a
result of application of sodium cyanide is established as follows: 50 parts per million in or on Fruit, citrus.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[64 FR 39077, July 21, 1999]

§ 180.132 Thiram; tolerances for residues.
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(a) General. Tolerances for residues of the fungicide thiram (tetramethyl thiuram disulfide) in or on raw
agricultural commodities are established as follows:

Commodity

Parts per million

Apple

7.0

Peach

7.0

Strawberry

7.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 49615, July 31, 2002]

§ 180.133 Lindane; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide lindane (gamma isomer of
1,2,3,4,5,6-hexachlorocyclohexane) in or on raw agricultural commodities as follows:

Commodity

Parts per million

Expiration/Revocation Date

Cattle, fat

7.0

10/02/09

Goat, fat

7.0

10/02/09

Hog, fat

4.0

10/02/09

Horse, fat

7.0

10/02/09

Sheep, fat

7.0

10/02/09

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39438, July 1, 2003, as amended at 70 FR 55286, Sept. 21, 2005; 72 FR 53454, Sept. 19, 2007]

§ 180.136 Basic copper carbonate; tolerance for residues.

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The tolerance for residues of the fungicide basic copper carbonate in or on pear from postharvest use of
the chemical is 3 parts per million of combined copper.

§ 180.142 2,4-D; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide, plant regulator, and fungicide 2,4-D
(2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following
food commodities:

Commodity

Parts per million

Almond hulls

0.1

Asparagus

5.0

Barley, bran

4.0

Barley, grain

2.0

Barley, straw

50

Berry, group 13

0.2

Cattle, fat

0.3

Cattle, kidney

4.0

Cattle, meat

0.3

Cattle, meat byproducts, except kidney

0.3

Corn, field, forage

6.0

Corn, field, grain

0.05

Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

50
0.05
50
6.0
0.05
50

Fish

0.1

Fruit, citrus, group 10

3.0

Fruit, pome, group 11

0.05

Fruit, stone, group 12

0.05

Goat, fat

0.3

Goat, kidney

4.0

Goat, meat

0.3

Goat, meat byproducts, except kidney

0.3

Grain, aspirated fractions
Grape
Grass, forage

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40
0.05
360

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Grass, hay

300

Hop, dried cones

0.2

Horse, fat

0.3

Horse, kidney

4.0

Horse, meat

0.3

Horse, meat byproducts, except kidney

0.3

Millet, forage

25

Millet, grain

2.0

Millet, straw

50

Milk
Nut, tree, group 14

0.05
0.2

Oat, forage

25

Oat, grain

2.0

Oat, straw

50

Pistachio

0.05

Potato

0.4

Rice, grain

0.5

Rice, hulls

2.0

Rice, straw

10

Rye, bran

4.0

Rye, forage

25

Rye, grain

2.0

Rye, straw

50

Sheep, fat

0.3

Sheep, kidney

4.0

Sheep, meat

0.3

Sheep, meat byproducts, except kidney

0.3

Shellfish

1.0

Sorghum, grain, forage

0.2

Sorghum, grain, grain

0.2

Sorghum, grain, stover

0.2

Soybean, forage

0.02

Soybean, hay

2.0

Soybean, seed

0.02

Strawberry

0.05

Sugarcane, cane

0.05

Sugarcane, molasses

0.2

Vegetable, leaves of root and tuber, group 2

0.1

Vegetable, root and tuber, except potato, group 1

0.1

Wheat, bran

4.0

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Wheat, forage

25

Wheat, grain

2.0

Wheat, straw

50

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(m),
are established for residues of the herbicide, plant regulator, and fungicide 2,4-D (2,4dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following food
commodities:

Commodity

Parts per million

Rice, wild, grain

0.05

(d) Indirect or inadvertent residues . Tolerances are established for indirect or inadvertent residues of the
herbicide, plant regulator, and fungicide 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated,
determined as the acid, in or on the following food commodities:

Commodity

Parts per million

Animal feed, nongrass, group 18

0.2

Avocado

0.05

Cotton, undelinted seed

0.05

Dill, seed

0.05

Okra

0.05

Vegetable, brassica leafy, group 5

0.4

Vegetable, bulb, group 3

0.05

Vegetable, cucurbit, group 9

0.05

Vegetable, foliage of legume, group 7

0.2

Vegetable, fruiting, group 8

0.05

Vegetable, leafy, except brassica, group 4

0.4

Vegetable, legume, group 6

0.05

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008]

§ 180.144 Cyhexatin; tolerances for residues.
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(a) General. Tolerances are established for combined residues of the pesticide cyhexatin
(tricyclohexylhydroxystannane; CAS Reg. No. 13121–70–5) and its organotin metabolites (calculated as
cyhexatin) in or on the following food commodities:

Commodity

Parts per million

Orange, juice

Expiration/Revocation Date
0.1

(b) Section 18 emergency exemptions. [Reserved]
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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33708, May 24, 2000, as amended at 70 FR 55272, Sept. 21, 2005]

§ 180.145 Fluorine compounds; tolerances for residues.
top
(a) General. (1) Tolerances are established for combined residues of the insecticidal fluorine compounds
cryolite and synthetic cryolite (sodium aluminum fluoride) in or on the following agricultural commodities:

Commodity

Parts per million

Apricot

7

Blackberry

7

Blueberry

7

Boysenberry

7

Broccoli

7

Brussels sprouts

7

Cabbage

7

Cauliflower

7

Collards

7

Cranberry

7

Cucumber

7

Dewberry

7

Eggplant

7

Fruit, citrus

7

Grape

7

Kale

7

Kohlrabi

7

Lettuce, head

7

Lettuce, leaf

7

Loganberry

7

Melon

7

Nectarine

7

Peach

7

Pepper

7

Plum, prune, fresh

7

Pumpkin

7

Raspberry

7

Squash, summer

7

Squash, winter

7

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Strawberry

7

Tomato

7

Youngberry

7

(2) Time-limited tolerances are established for residues of the insecticidal fluorine compounds cryolite and
synthetic cryolite (sodium aluminum fluoride) in or on the commodities as follows:

Commodity

Parts per million

Potato
Potato, processed potato waste

Expiration/revocation date

2.0

11/21/01

22.0

11/21/01

(3) Tolerances are established for residues of fluoride in or on the following commodities from the
postharvest fumigation with sulfuryl fluoride for the control of insects:

Commodity
All processed food commodities not otherwise listed

Parts per million
70

Barley, bran, postharvest

45.0

Barley, flour, postharvest

45.0

Barley, grain, postharvest

15.0

Barley, pearled barley, postharvest

45.0

Cattle, meat, dried
Cheese

40
5.0

Cacao bean, roasted bean, postharvest

20

Coconut, postharvest

40

Coffee, bean, green, postharvest

15

Corn, field, flour, postharvest

35.0

Corn, field, grain, postharvest

10.0

Corn, field, grits, postharvest

10.0

Corn, field, meal, postharvest

30.0

Corn, pop, grain, postharvest

10.0

Cotton, undelinted seed, postharvest

70

Egg, dried

900

Fruit, dried, except grape, raisin, postharvest

3.0

Ginger, postharvest
Grain, aspirated fractions, postharvest
Grape, raisin, postharvest

70
55.0
7.0

Hog, meat

20

Herbs and spices group 19, postharvest

70

Milk, powdered
Millet, grain, postharvest
Nut, pine, postharvest
Nut, tree, Group 14, postharvest
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Oat, flour, postharvest

75.0

Oat, grain, postharvest

25.0

Oat, groats/rolled oats

75.0

Peanut, postharvest

15

Pistachio, postharvest

10.0

Rice, bran, postharvest

31.0

Rice, flour, postharvest

45

Rice, grain, postharvest

12.0

Rice, hulls, postharvest

35.0

Rice, polished rice, postharvest

25.0

Rice, wild, grain, postharvest

25.0

Sorghum, grain, postharvest

40.0

Triticale, grain, postharvest

40.0

Vegetable, legume, group 6, postharvest

70

Wheat, bran, postharvest

40.0

Wheat, flour, postharvest

125.0

Wheat, germ, postharvest

130.0

Wheat, grain, postharvest

40.0

Wheat, milled byproducts, postharvest

130.0

Wheat, shorts, postharvest

40.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined by §180.1(n),
are established for the combined residues of the insecticidal fluorine compounds, cryolite and synthetic
cryolite (sodium aluminum fluoride), in or on the following raw agricultural commodities:

Commodity

Parts per million

Kiwifruit
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74815, Dec. 13, 2006]

§ 180.149 Mineral oil; tolerances for residues.
top
(a) General. (1) For the purposes of this section, the insecticide mineral oil is defined as the refined
petroleum fraction having the following characteristics:
(i) Minimum flashpoint of 300 °F.
(ii) Gravity of 27 to 34 by the American Petroleum Institute standard method.
(iii) Pour point of 30 °F maximum.
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(iv) Color 2 maximum by standards of the American Society for Testing Materials.
(v) Boiling point between 480 °F and 960 °F.
(vi) Viscosity at 100 °F of 100 to 200 seconds Saybolt.
(vii) Unsulfonated residue of 90 percent minimum.
(viii) No sulfur compounds according to the United States Pharmacopeia test under Liquid Petrolatum.
(2) Tolerances for residues of mineral oil as specified in paragraph (a)(1) of this section are established in
or on the following food commodities:

Commodity

Parts per million

Corn, grain, postharvest

200

Sorghum, grain, grain, postharvest

200

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39438, July 1, 2003]

§ 180.151 Ethylene oxide; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the antimicrobial agent and insecticide ethylene
oxide, when used as a postharvest fumigant in or on the following food commodities:

Commodity

Parts per million

Coconut, copra

50

Spices, whole

50

Walnut, black

50

(2) Ethylene oxide may be safely used as a fumigant for the control of microorganisms and insect
infestation in ground spices and other processed natural seasoning materials, except mixtures to which
salt has been added, in accordance with the following prescribed conditions:
(i) Ethylene oxide, either alone or admixed with carbon dioxide or dichlorodifluoromethane, shall be used
in amounts not to exceed that required to accomplish the intended technical effects. If used with
dichlorodifluoromethane, the dichlorodifluoromethane shall conform with the requirements prescribed by
21 CFR 173.355 of this chapter.
(ii) To assure safe use of the fumigant, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency and it shall be used in accordance with such label or labeling.
(iii) Residues of ethylene oxide in ground spices from both postharvest application to whole spices and
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application to the ground spices shall not exceed the established tolerance of 50 parts per million for
residues in whole spices in paragraph (a)(1) of this section.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33695, May 24, 2000]

§ 180.153 Diazinon; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide diazinon, O , O -diethyl O -[6methyl-2-(1-methylethyl)-4-pyrimidinyl]phosphorothioate (CAS No. 333–41–5), in or on the following food
commodities:

Commodity

Parts per million

Almond, hulls

3.0

Apple

0.50

Apricot

0.20

Bean, lima

0.50

Bean, snap, succulent

0.50

Beet, garden, roots

0.75

Beet, garden, tops

0.70

Blueberry

0.50

Caneberry subgroup 13-07A

0.75

Carrot, roots

0.75

Cattle, fat

0.50

Cherry, sweet

0.20

Cherry, tart

0.20

Cranberry

0.50

Endive

0.70

Fig

0.50

Ginseng

0.75

Grape

0.752

Hazelnut

0.50

Kiwifruit1

0.75

Lettuce

0.70

Melon

0.75

Mushroom

0.752

Nectarine

0.20

Onion, bulb

0.75

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Onion, green

0.75

Pea, succulent

0.50

Peach

0.20

Pear

0.50

Pineapple

0.50

Plum, prune, fresh

0.20

Radish

0.50

Rutabaga

0.75

Spinach

0.70

Strawberry

0.50

Tomato

0.75

Vegetable, brassica, leafy, group 5

0.70

Watercress

0.05

1There
2The

are no domestic registrations for kiwifruit as of March 6, 2002.

expiration/revocation date for this tolerance is 9/10/2010.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(m),
are established for residues of the insecticide diazinon, O , O -diethyl O -[6-methyl-2-(1-methylethyl)-4pyrimidinyl]-phosphorothioate (CAS No. 333–41–5), in or on the following food commodities:

Commodity

Parts per million

Almond

0.50

Banana

0.20

Celery

0.70

Cucumber

0.75

Parsley, leaves

0.75

Parsnip

0.50

Pepper

0.5

Potato

0.10

Squash, summer

0.50

Squash, winter

0.75

Sweet potato, roots

0.10

Swiss chard

0.70

Turnip, roots

0.50

Turnip, tops

0.75

(d) Indirect or inadvertent residues. [Reserved]
[47 FR 42738, Sept. 29, 1982]

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Editorial Note: ForFederal Registercitations affecting §180.153, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.154 O,O
-Dimethyl S
-[(4-oxo-1,2,3-benzotriazin-3(4 H
yl)methyl]phosphorodithioate; tolerances for residues.

)-

top
(a) General. Tolerances for residues of the insecticide O,O -dimethyl S -[(4-oxo-1,2,3-benzotriazin-3(4 H )yl)methyl]phosphorodithioate in or on the following raw agricultural commodities:

Commodity

Parts per million

Expiration/Revocation Date

Alfalfa, forage

2.0

None

Alfalfa, hay

5.0

None

Almond

0.2

None

Almond, hulls

5.0

None

Apple

1.5

None

Bean, snap, succulent

2.0

None

Blackberry

2.0

None

Blueberry

5.0

None

Boysenberry

2.0

None

Broccoli

2.0

None

Brussels sprouts

2.0

None

Cabbage

2.0

None

Cauliflower

2.0

None

Celery

2.0

None

Cherry

2.0

None

Clover, forage

2.0

None

Clover, hay

5.0

None

Cotton, undelinted seed

0.5

None

Crabapple

1.5

None

Cranberry

0.5

None

Cucumber

2.0

None

Eggplant

0.3

None

Fruit, citrus, group 10

2.0

None

Grape

4.0

None

Hazelnut

0.3

None

Loganberry

2.0

None

Melon

2.0

None

Onion

2.0

None

Parsley, leaves

5.0

None

Parsley, turnip rooted, roots

2.0

None

Peach

2.0

None

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Pear

1.5

None

Pecan

0.3

None

Pepper

0.3

None

Pistachio

0.3

None

Plum, prune

2.0

None

Potato

0.2

None

Quince

1.5

None

Raspberry

2.0

None

Spinach

2.0

None

Strawberry

2.0

None

Sugarcane, cane

0.3

6/30/00

Tomato, postharvest

2.0

None

Trefoil, forage

2.0

None

Trefoil, hay

5.0

None

Walnut

0.3

None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 38752, June 22, 2000]

§ 180.155 1-Naphthaleneacetic acid; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the plant growth regulator 1-naphthaleneacetic
acid in or on the following raw agricultural commodities:

Commodity

Parts per million

Apple

1

Cherry, sweet
Olive

0.1
0.1(N)

Orange, sweet
Pear
Pineapple (from the application of the sodium salt to the growing
crop)
Quince
Tangerine
(2) Tolerances are established for residues of the ethyl ester of 1-naphthaleneacetic acid in or on the
following raw agricultural commodities:

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0.1
1
0.05
1
0.1

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Commodity

Parts per million

Apple

1

Pear

1

Olive

0.1

(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for residues of the ethyl ester of 1-naphthaleneacetic acid in or on the following raw
agricultural commodities resulting from use of the pesticide pursuant to FIFRA section 18 emergency
exemptions. The tolerances expire and are revoked on the date specified in the following table.

Commodity

Parts per million

Avocado

Expiration/revocation date

0.05

12/31/12

(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[46 FR 23238, Apr. 24, 1981, as amended at 47 FR 33692, Aug. 4, 1982; 48 FR 20054, May 4, 1983; 74
FR 40517, Aug. 12, 2009]

§ 180.157 Methyl 3-[(dimethoxyphosphinyl) oxy]butenoate, alpha and beta isomers;
tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide methyl 3-[(dimethoxyphosphinyl)oxy]
butenoate, alpha and beta isomers, in or on the following raw agricultural commodities:

Commodity

Parts per million

Broccoli

1.0

Cabbage

1.0

Cauliflower

1.0

Celery

1.0

Cucumber

0.2

Grape

0.5

Lettuce

0.5

Melon (determined on the edible portion with rind removed)

0.5

Pea

0.25

Pepper

0.25

Spinach

1.0

Squash, summer

0.25

Strawberry

1.0

Tomato

0.2

Watermelon

0.5

(b) Section 18 emergency exemptions. [Reserved]
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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 41822, Aug. 2, 1999]

§ 180.163 1,1-Bis(4-chlorophenyl)-2,2,2-trichloroethanol; tolerances for residues.
top
(a) General . (1) Tolerances for the combined residues of the insecticide dicofol, 1,1-bis(4-chlorophenyl)2,2,2-trichloroethanol and 1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2,2-trichloroethanol in or on raw
agricultural commodities are established as follows:

Commodity

Parts per million

Apple, wet pomace

38.0

Bean, dry, seed

0.5

Bean, succulent

3.0

Butternut

0.1

Caneberry subgroup 13A

5.0

Chestnut

0.1

Citrus, dried pulp
Citrus oil

12.0
200.0

Cotton, refined oil

0.5

Cotton, undelinted seed

0.1

Fruit, citrus, group 10

6.0

Fruit, pome, group 11

10.0

Fruit, stone, group 12

5.0

Grape

5.0

Grape, raisin
Hazelnut
Hop, dried cones

20.0
0.1
65.0

Nut, hickory

0.1

Nut, macadamia

0.1

Pecan

0.1

Peppermint, oil

30.0

Peppermint, tops

25.0

Spearmint, oil

30.0

Spearmint, tops

25.0

Strawberry

10.0

Tea, dried

50.0

Tea, plucked leaves

30.0

Vegetable, cucurbit, group 9
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Vegetable, fruiting, group 8

2.0

Walnut

0.1

(2) Tolerances for the combined residues of the insecticide dicofol, 1,1-bis(4-chlorophenyl)-2,2,2trichloroethanol, 1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2,2-trichloroethanol, 1,1-bis(4-chlorophenyl)-2,2dichloroethanol, and 1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2-dichloroethanol in or on raw agricultural
commodities are established as follows:

Commodity
Cattle, fat

Parts per million
50.0

Cattle, liver

5.0

Cattle, meat

3.0

Cattle, meat byproducts, except liver

3.0

Egg

0.05

Goat, fat

50.0

Goat, liver

5.0

Goat, meat

3.0

Goat, meat byproducts, except liver

3.0

Hog, fat

50.0

Hog, liver

5.0

Hog, meat

3.0

Hog, meat byproducts, except liver

3.0

Horse, fat

50.0

Horse, liver

5.0

Horse, meat

3.0

Horse, meat byproducts, except liver

3.0

Milk, fat (reflecting 0.75 ppm in whole milk)

22.0

Poultry, fat

0.1

Poultry, meat

0.1

Poultry, meat byproducts

0.1

Sheep, fat

50.0

Sheep, liver

5.0

Sheep, meat

3.0

Sheep, meat byproducts, except liver

3.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34826, June 26, 1998, as amended at 72 FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, 2007]

§ 180.169 Carbaryl; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N methylcarbamate per se , in or on the following food commodities:

Commodity

Parts per million Expiration/revocation date

Alfalfa, forage

50

None

Alfalfa, hay

75

None

Almond, hulls

50

None

Apple, wet pomace

15

None

Asparagus

15

None

Banana

5.0

None

Beet, sugar, roots

0.5

None

Beet, sugar, tops

25

None

3.0

None

21

None

Cactus, fruit

5.0

None

Cactus, pads

12

None

12.0

None

Citrus, oil

20

None

Clover, forage

50

None

Clover, hay

70

None

Corn, field, forage

30

None

0.02

None

20

None

0.02

None

20

None

Corn, sweet, forage

185

None

Corn, sweet, kernel plus cob with
husks removed

0.1

None

Corn, sweet, stover

215

None

Cotton, undelinted seed

5.0

10/31/09

Cranberry

3.0

None

Dandelion, leaves

22

None

Endive

10

None

0.5

None

Fruit, citrus, group 10

10

None

Fruit, pome, group 11

12

None

Fruit, stone, group 12

10

None

Grain, aspirated fractions

70

None

Grape

10

None

Bushberry subgroup 13-07B
Cabbage

Caneberry subgroup 13-07A

Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover

Flax, seed

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Grape, raisin

12

None

Grass, forage

100

None

15

None

3.0

None

10

None

Millet, proso, grain

1.0

None

Millet, proso, straw

20

None

Nut, tree group 14, except walnut

0.1

None

Okra

4.0

None

Olive

10

None

0.25

None

22

None

1.0

None

0.05

None

20

None

Pineapple

2.0

None

Pistachio

0.1

None

Rice, grain

15

None

Rice, hulls

30

None

Rice, straw

60

None

Sorghum grain, forage

30

None

Sorghum grain, grain

10

None

Sorghum grain, stover

30

None

Soybean, forage

15

None

Soybean, hay

15

None

Soybean, seed

0.5

None

22

None

Strawberry

4.0

None

Sunflower, seed

0.5

None

Sweet potato, roots

0.2

None

Trefoil, forage

15

None

Trefoil, hay

25

None

Vegetable, brassica, leafy, group 5,
except cabbage

10

None

Vegetable, cucurbit, group 9

3.0

None

Vegetable, foliage of legume,
subgroup 7A, except soybean

60

None

5.0

None

75

None

Grass, hay
Leaf petiole subgroup 4B
Lettuce

Oyster
Parsley, leaves
Pea and bean, dried shelled, except
soybean, subgroup 6C
Peanut
Peanut, hay

Spinach

Vegetable, fruiting, group 8
Vegetable, leaves of root and tuber,
group 2, except sugar beet tops

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Vegetable, legume, edible podded,
subgroup 6A

10

None

Vegetable, root and tuber, group 1,
except sugar beet and sweet potato

2.0

None

Walnut

1.0

None

Wheat, forage

30

None

Wheat, grain

1.0

None

Wheat, hay

30

None

Wheat, straw

20

None

(2) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N -methylcarbamate,
including its metabolites: 1-naphthol (naphthyl-sulfate); 5,6-dihydrodihydroxycarbaryl; and 5,6dihydrodihydroxy naphthol, calculated as 1-naphthyl N -methylcarbamate and the free and conjugated
residues of carbaryl: 5,6-dihydro-5,6-dihydroxy carbaryl and 5-methoxy-6-hydroxy carbaryl, in or on the
following food commodities:

Commodity

Parts per million

Expiration/revocation date

Cattle, fat

0.5

None

Cattle, meat

1.0

None

Cattle, meat byproducts

3.0

None

Egg

0.5

10/31/09

Goat, fat

0.5

None

Goat, meat

1.0

None

Goat, meat byproducts

3.0

None

Hog, fat

0.5

None

Hog, meat

1.0

None

Hog, meat byproducts

3.0

None

Horse, fat

0.5

None

Horse, meat

1.0

None

Horse, meat byproducts

3.0

None

Milk

1.0

None

Poultry, fat

5.0

10/31/09

Poultry, meat

5.0

10/31/09

Sheep, fat

0.5

None

Sheep, meat

1.0

None

Sheep, meat byproducts

3.0

None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registrations, as defined in §180.1(m),
are established for residues of the insecticide carbaryl, 1-naphthyl N -methylcarbamate per se , in or on
the following food commodities:

Commodity

Parts per million

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Dillweed, fresh leaves

0.2

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33695, May 24, 2000, as amended at 66 FR 38955, July 26, 2001; 67 FR 49615, July 31, 2002; 70
FR 44492, Aug. 3, 2005; 73 FR 52611, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009]

§ 180.172 Dodine; tolerances for residues.
top
(a) General . Tolerances are established for the fungicide dodine (n-dodecylguanidine acetate) in or on the
following food commodities:

Commodity

Parts per million

Apple

5.0

Apple, wet pomace

15.0

Banana

0.50

Cherry, sweet

3.0

Cherry, tart

3.0

Peach

5.0

Peanut

0.013

Pear

5.0

Pecan

0.3

Strawberry

5.0

Walnut

0.3

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 45634, Aug. 6, 2008]

§ 180.173 Ethion; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide ethion ( O,O,O′,O′ -tetraethyl S,S′ methylene bisphosphorodithioate) including its oxygen analog ( S -[[(diethoxyphosphinothioyl)thio] methyl]
O,O- diethyl phosphorothioate) in or on the following raw agricultural commodities:

Commodity

Parts per million Expiration/Revocation Date

Cattle, fat

0.2

10/1/08

Cattle, meat

0.2

10/1/08

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Cattle, meat byproducts

0.2

10/1/08

25.0

10/1/08

Fruit, citrus, group 10

5.0

10/1/08

Goat, fat

0.2

10/1/08

Goat, meat

0.2

10/1/08

Goat, meat byproducts

0.2

10/1/08

Hog, fat

0.2

10/1/08

Hog, meat

0.2

10/1/08

Hog, meat byproducts

0.2

10/1/08

Horse, fat

0.2

10/1/08

Horse, meat

0.2

10/1/08

Horse, meat byproducts

0.2

10/1/08

Milk, fat, reflecting negligible
residues in milk

0.5

10/1/08

Sheep, fat

0.2

10/1/08

Sheep, meat

0.2

10/1/08

Sheep, meat byproducts

0.2

10/1/08

Citrus, dried pulp

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 42739, Sept. 29, 1982, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57073, Oct. 26, 1998; 67
FR 49615, July 31, 2002; 69 FR 43924, July 23, 2004]

§ 180.175 Maleic hydrazide; tolerances for residues.
top
(a) General. (1) Tolerances for residues of the herbicide and plant regulator maleic hydrazide (1,2-dihydro3,6-pyridazinedione) are established in or on the following raw agricultural commodities:

Commodity

Parts per million

Onion, bulb

15.0

Potato

50.0

(2) A food additive known as maleic hydrazide (1,2-dihydro-3,6-pyridazinedione) may be present in potato,
chips when used in accordance with the following conditions:
(i) The food additive is present as a result of the application of a pesticide formulation containing maleic
hydrazide to the growing potato plant in accordance with directions registered by the U.S. Environmental
Protection Agency.
(ii) The label of the pesticide formulation containing the food additive conforms to labeling registered by
the U.S. Environmental Protection Agency.
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(iii) The food additive is present in an amount not to exceed 160 parts per million by weight of the finished
food.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 64293, Dec. 5, 1997, as amended at 64 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, 2002]

§ 180.176 Mancozeb; tolerances for residues.
top
(a) General. Tolerances for residues of a fungicide which is a coordination product of zinc ion and maneb
(manganous ethylene-bisdithiocarbamate) containing 20 percent manganese, 2.5 percent zinc, and 77.5
percent ethylene-bisdithiocarbamate (the whole product calculated as zinc ethylenebisdithiocarbamate),
are established as follows:

Commodity
Apple

Parts per million
7

Asparagus (negligible residue)

0.1

Banana

4.0

Banana, pulp

0.5

Barley, grain

5

Barley, milled feed fractions

20

Barley, straw

25

Beet, sugar, roots

2

Beet, sugar, tops

65

Carrot, roots

2

Celery

5

Corn, field, grain
Corn, forage
Corn, pop, grain
Corn, stover

0.1
5
0.5
5

Corn, sweet, kernel plus cob with husks removed

0.5

Cotton, undelinted seed

0.5

Crabapple

10

Cranberry

7

Cucumber

4

Fennel

10

Grape

7

Kidney

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Liver

0.5

Melon

4

Oat, bran

20

Oat, grain

5

Oat, milled feed fractions

20

Oat, straw

25

Onion, bulb

0.5

Papaya (whole fruit with no residue present in the edible pulp after
the peel is removed and discarded)

10

Peanut

0.5

Peanut, hay

65

Pear

10

Quince

10

Rye, bran

20

Rye, grain

5

Rye, straw

25

Squash, summer

4

Tomato

4

Wheat, grain

5

Wheat, milled byproducts

20

Wheat, straw

25

(b) Section 18 emergency exemptions. A time-limited tolerance is established for combined residues of the
fungicide mancozeb, calculated as zinc ethylenebisdithiocarbamate and it's metabolite ETU in connection
with use of the pesticide under a section 18 emergency exemption granted by EPA. The tolerance will
expire and is revoked on the dates specified in the following table.

Commodity

Parts per million

Ginseng

Expiration/Revocation Date
2.0

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33708, May 24, 2000, as amended at 65 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, 2001;
68 FR 2247, Jan. 16, 2003; 69 FR 29458, May 24, 2004; 71 FR 76199, Dec. 20, 2006]

§ 180.178 Ethoxyquin; tolerances for residues.
top
(a) General. A tolerance is established for residues of the plant regulator ethoxyquin (1,2-dihydro-6-ethoxy2,2,4-trimethylquinoline) from preharvest or postharvest use in or on the following commodity:

Commodity

Parts per million

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Pear

3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 57073, Oct. 26, 1998]

§ 180.180 Orthoarsenic acid; tolerance for residues.
top
(a) General. A tolerance that expires on July 1, 1995, for combined As2O3is established for residues of the
defoliant orthoarsenic acid in or on the following food commodity:

Commodity

Parts per million

Cotton, undelinted seed

4

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003]

§ 180.181 Chlorpropham; tolerances for residues.
top
(a) General . (1) Tolerances are established for residues of the plant regulator and herbicide chlorpropham
(isopropyl m-chlorocarbanilate (CIPC) in or on the following food commodities:

Commodity

Parts per million

Potato

30

Potato, wet peel

40

(2) Tolerances are established for the combined residues of the plant regulator and herbicide
chlorpropham (isopropyl m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham-O-sulfonic
acid (4-HSA) in or on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.20

Cattle, kidney

0.30

Cattle, meat

0.06

Cattle, meat byproducts except kidney

0.06

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Goat, fat

0.20

Goat, kidney

0.30

Goat, meat

0.06

Goat, meat byproducts except kidney

0.06

Hog, fat

0.20

Hog, kidney

0.30

Hog, meat

0.06

Hog, meat byproducts except kidney

0.06

Horse, fat

0.20

Horse, kidney

0.30

Horse, meat

0.06

Horse, meat byproducts except kidney

0.06

Milk

0.30

Sheep, fat

0.20

Sheep, kidney

0.30

Sheep, meat

0.06

Sheep, meat byproducts except kidney

0.06

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[43 FR 52487, Nov. 13, 1978, as amended at 63 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007]

§ 180.182 Endosulfan; tolerances for residues.
top
(a) General . (1) Tolerances are established for the combined residues of the insecticide endosulfan,
6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3-oxide (alpha
and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9ahexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, in or on the following food commodities:

Commodity

Parts per million

Alfalfa, forage

0.3

Alfalfa, hay

1.0

Almond

0.3

Almond, hulls

1.0

Apple

1.0

Apple, wet pomace

5.0

Apricot

2.0

Barley, grain

0.3

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Barley, straw

0.4

Bean

2.0

Blueberry

0.3

Broccoli

3.0

Brussels sprouts

2.0

Cabbage

4.0

Carrot, roots

0.2

Cattle, fat

13.0

Cattle, liver

5.0

Cattle, meat

2.0

Cattle, meat byproducts, except liver

1.0

Cauliflower

2.0

Celery

8.0

Cherry, sweet

2.0

Cherry, tart

2.0

Collards

2.0

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed

12.0
0.2

Corn, sweet, stover

14.0

Cotton, gin byproducts

30.0

Cotton, undelinted seed

1.0

Eggplant

1.0

Goat, fat

13.0

Goat, liver

5.0

Goat, meat

2.0

Goat, meat byproducts, except liver

1.0

Grape

2.0

Hazelnut

0.2

Hog, fat

13.0

Hog, liver

5.0

Hog, meat

2.0

Hog, meat byproducts, except liver

1.0

Horse, fat

13.0

Horse, liver

5.0

Horse, meat

2.0

Horse, meat byproducts, except liver

1.0

Kale

2.0

Lettuce, head

11.0

Lettuce, leaf

6.0

Milk, fat

2.0

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Mustard greens

2.0

Mustard, seed

0.2

Nectarine

2.0

Nut, macadamia

0.2

Oat, grain

0.3

Oat, straw

0.4

Pea, succulent

2.0

Peach

2.0

Pear

2.0

Pecan

0.2

Pepper

2.0

Pineapple

1.0

Pineapple, process residue

20.0

Plum

2.0

Plum, prune

2.0

Potato

0.2

Rapeseed, seed

0.2

Rye, grain

0.3

Rye, straw

0.3

Sheep, fat

13.0

Sheep, liver

5.0

Sheep, meat

2.0

Sheep, meat byproducts, except liver

1.0

Spinach

2.0

Strawberry

2.0

Sugarcane, cane

0.5

Sweet potato, roots

0.15

Tomato

1.0

Turnip, roots

0.2

Turnip, tops

2.0

Vegetable, cucurbit, group 9

1.0

Walnut

0.2

Watercress

2.0

Wheat, grain

0.3

Wheat, straw

0.4

(2) A tolerances of 24 parts per million (ppm) is established for the combined residues of the insecticide
endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, in or on dried tea (reflecting
less than 0.1 ppm residues in beverage tea) resulting from application of the insecticide to growing tea.
(b) Section 18 emergency exemptions. [Reserved]
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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33696, May 24, 2000, as amended at 71 FR 54433, Sept. 15, 2006]

§ 180.183 O,O
tolerances for residues.

-Diethyl S

-[2-(ethylthio)ethyl] phosphorodithioate;

top
(a) General. Tolerances are established for the combined residues of the insecticide O,O -diethyl S -[2(ethylthio)ethyl] phosphorodithioate and its cholinesterase-inhibiting metabolites, calculated as demeton, in
or on the following raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.75

Barley, straw

5.0

Bean, lima

0.75

Bean, snap, succulent

0.75

Broccoli

0.75

Brussels sprouts

0.75

Cabbage

0.75

Cauliflower

0.75

Coffee, bean

0.3

Cotton, undelinted seed

0.75

Lettuce

0.75

Peanut

0.75

Pea, dry, seed

0.75

Pea, field, vines

5.0

Pea, succulent

0.75

Pepper

0.1

Potato

0.75

Spinach

0.75

Tomato

0.75

Wheat, hay

5.0

Wheat, grain

0.3

Wheat, straw

5.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for the combined residues of O,O- diethyl S -[2-(ethylthio)ethyl] phosphorodithioate and its
cholinesterase-inhibiting metabolites, calculated as demeton, in or on the following raw agricultural
commodities:
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Commodity

Parts per million

Asparagus

0.1

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, 2001; 67
FR 41806, June 19, 2002; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 54960, Sept.
24, 2008]

§ 180.184 Linuron; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the herbicide linuron (3-(3,4dichlorophenyl)-1-methoxy-1-methylurea) and its metabolites convertible to 3,4-dichloroaniline, calculated
as linuron, in or on the following food commodities:

Commodity

Parts per million

Asparagus

7.0

Carrot, roots

1.0

Cattle, fat

0.2

Cattle, kidney

2.0

Cattle, liver

2.0

Cattle, meat

0.1

Cattle, meat byproducts except kidney and liver

0.1

Celeriac

1.0

Corn, field, forage

1.0

Corn, field, grain

0.1

Corn, field, stover

6.0

Corn, sweet, forage

1.0

Corn, sweet, kernel plus cob with husks removed

0.25

Corn, sweet, stover

6.0

Cotton, gin byproducts

5.0

Cotton, undelinted seed

0.25

Goat, fat

0.2

Goat, kidney

2.0

Goat, liver

2.0

Goat, meat

0.1

Goat, meat byproducts except kidney and liver

0.1

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.1

Horse, fat

0.2

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Horse, kidney

2.0

Horse, liver

2.0

Horse, meat

0.1

Horse, meat byproducts except kidney and liver

0.1

Milk

0.05

Parsnip, roots

0.05

Parsnip, tops

0.05

Rhubarb

0.5

Sheep, fat

0.2

Sheep, kidney

2.0

Sheep, liver

2.0

Sheep, meat

0.1

Sheep, meat byproducts except kidney and liver

0.1

Sorghum, grain, forage

1.0

Sorghum, grain, grain

0.25

Sorghum, grain, stover

1.0

Soybean, seed

1.0

Soybean, vegetable

1.0

(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for combined residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1methylurea) and its metabolites convertible to 3,4-dichloroaniline, calculated as linuron, in or on the
specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18
emergency exemptions. The tolerance expires and is revoked on the date specified in the table.

Commodity

Parts per
million

Lentil

Expiration/revocation date
0.1

12/31/2011

(c) Tolerances with regional registrations . Tolerances with regional registrations, as defined in §180.1(m),
are established for the combined residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1methylurea) and its metabolites convertible to 3,4-dichloroaniline, calculated as linuron, in or on the
following food commodities:

Commodity

Parts per million

Celery
Parsley, leaves

0.5
0.25

Potato

0.2

Wheat, forage

0.5

Wheat, grain

0.05

Wheat, hay

0.5

Wheat, straw

2.0

(d) Indirect or inadvertent residues. [Reserved]

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[64 FR 41822, Aug. 2, 1999, as amended at 72 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, 2008]

§ 180.185 DCPA; tolerances for residues.
top
(a) General . Tolerances for the combined residues of the herbicide dimethyl tetrachloroterephthalate
(DCPA) and its metabolites monomethyltetrachloroterephthalate (MTP) and tetrachloroterephthalic acid
(TCP) (calculated as dimethyl tetrachloroterephthalate) are established in or on the following food
commodities:

Commodity

Parts per million

Cantaloupe

1.0

Garlic

1.0

Ginseng

2.0

Horseradish

2.0

Muskmelon

1.0

Onion, bulb

1.0

Onion, green

1.0

Strawberry

2.0

Tomato

1.0

Vegetable, brassica, leafy, group 5

5.0

Watermelon

1.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(m),
are established for the combined inadvertent residues of the herbicide dimethyl tetrachloroterephthalate
(DCPA) and its metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid
(TCP) (calculated as DCPA) in or on the following food commodities:

Commodity

Parts per million

Radish, roots

2.0

Radish, tops

15.0

(d) Indirect or inadvertent residues . Tolerances are established for the combined indirect or inadvertent
residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl
tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the
following food commodities:

Commodity

Parts per million

Basil, dried leaves

20.0

Basil, fresh leaves

5.0

Bean, dry

2.0

Bean, mung, seed

2.0

Bean, snap, succulent

2.0

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Celeriac

2.0

Chicory, roots

2.0

Chicory, tops

5.0

Chive

5.0

Coriander, leaves

5.0

Corn, field, forage

0.4

Corn, field, grain

0.05

Corn, field, stover

0.4

Corn, pop, forage

0.4

Corn, pop, grain

0.05

Corn, pop, stover

0.4

Corn, sweet, forage

0.4

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, stover

0.4

Cotton, undelinted seed

0.2

Cucumber

1.0

Dill

5.0

Eggplant

1.0

Lettuce

2.0

Marjoram

5.0

Parsley, dried leaves

20.0

Parsley, leaves

5.0

Pea, blackeyed, seed

2.0

Pepper

2.0

Pimento

2.0

Potato

2.0

Radicchio

5.0

Radish, oriental, roots

2.0

Radish, oriental, tops

2.0

Rutabaga

2.0

Soybean

2.0

Squash, summer

1.0

Squash, winter

1.0

Sweet potato

2.0

Turnip, roots

2.0

Turnip, tops

5.0

Yam, true, tuber

2.0

[72 FR 52018, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, 2008;
74 FR 14744, Apr. 1, 2009]

§ 180.189 Coumaphos; tolerances for residues.
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top
(a) General. Tolerances for residues of the insecticide coumaphos ( O,O -diethyl O -3-chloro-4-methyl-2oxo-2H-1-benzopyran-7-yl phosphorothioate and its oxygen analog ( O,O -diethyl O -3-chloro-4-methyl-2oxo-2H-1-benzopyran-7-yl phosphate) in or on food commodities as follows:

Commodity

Parts per million

Cattle, fat

1.0

Cattle, meat

1.0

Cattle, meat byproducts

1.0

Goat, fat

1.0

Goat, meat

1.0

Goat, meat byproducts

1.0

Hog, fat

1.0

Hog, meat

1.0

Hog, meat byproducts

1.0

Honey

0.15

Honeycomb

45.0

Horse, fat

1.0

Horse, meat

1.0

Horse, meat byproducts

1.0

Milk, fat (=n in whole milk)

0.5

Sheep, fat

1.0

Sheep, meat

1.0

Sheep, meat byproducts

1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 39077, July 21, 1999, as amended at 65 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, 2002; 69
FR 29458, May 24, 2004; 72 FR 28876, May 23, 2007]

§ 180.190 Diphenylamine; tolerances for residues.
top
(a) General. Tolerances for residues of the plant regulator diphenylamine are established in or on the
following commodities:

Commodity
Apple, wet pomace

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Parts per million
30.0

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Apple from preharvest or postharvest use, including use of
impregnated wraps

10.0

Cattle, fat

0.01

Cattle, liver

0.1

Cattle, meat byproducts, except liver

0.01

Cattle, meat

0.01

Goat, fat

0.01

Goat, liver

0.1

Goat, meat byproducts, except liver

0.01

Goat, meat

0.01

Horse, fat

0.01

Horse, liver

0.1

Horse, meat byproducts, except liver

0.01

Horse, meat

0.01

Milk

0.01

Pear (post harvest)

5.0

Sheep, fat

0.01

Sheep, liver

0.1

Sheep, meat byproducts, except liver

0.01

Sheep, meat

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. A time-limited tolerance is established for the indirect or inadvertent
residues of diphenylamine in or on the following commodity:

Commodity

Parts per million

Pear

Expiration/Revocation Date
10

12/1/01

[64 FR 25848, May 13, 1999, as amended at 66 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, 2007]

§ 180.191 Folpet; tolerances for residues.
top
(a) General . Tolerances are established for the fungicide folpet ( N -(trichloromethylthio)phthalimide) in or
on raw agricultural commodities as follows:

Commodity

Parts per million

Apple1

5.0

Cranberry 1

15.0

Cucumber 1

2.0

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Grape 1

50.0

Grape, raisin 1

80.0

Hop, dried cones

120.0
50.0

Lettuce 1
Melon 1

3.0

Onion, bulb 1

2.0

Strawberry 1

5.0
25.0

Tomato 1
1No

U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations as defined in §180.1(m)
are established for the fungicide folpet ( N -(trichloromethylthio)phthalimide) in or on the following raw
agricultural commodity:

Commodity

Parts per million

Avocado

25.0

(d) Indirect or inadvertent residues. [Reserved]
[61 FR 37222, July 17, 1996, as amended at 68 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, 2004; 72
FR 41928, Aug. 1, 2007]

§ 180.198 Trichlorfon; tolerances for residues.
top
(a) General . Tolerances are established for residues of the insecticide trichlorfon (dimethyl (2,2,2-trichloro1-hydroxyethyl) phosphonate) in or on the following food commodities:

Commodity

Parts per million

Cattle, fat1

0.5

Cattle, meat1

0.2

Cattle, meat byproducts1

0.1

1There

are no U.S. registrations for cattle commodities as of June 24, 1999.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 54578, Sept. 26, 2007]

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§ 180.200 Dicloran; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the fungicide 2,6- dichloro-4-nitroaniline in or
on the following raw agricultural commodities. Unless otherwise specified, these tolerances prescribed in
this paragraph provide for residues from preharvest application only.

Commodity

Parts per million

Apricot, postharvest

20

Bean, snap, succulent

20

Carrot, roots, postharvest

10

Celery

15

Cherry, sweet, postharvest

20

Cucumber

5

Endive

10

Garlic

5

Grape

10

Lettuce

10

Nectarine, postharvest

20

Onion

10

Peach, postharvest

20

Plum, prune, fresh, postharvest

15

Potato

0.25

Rhubarb

10

Sweet potato, postharvest

10

Tomato

5

(2) Unless otherwise specified, these tolerances prescribed in this section provide for residues from
preharvest application only.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[46 FR 27938, May 22, 1981, as amended at 63 FR 162, Jan. 5, 1998; 63 FR 57073, Oct. 26, 1998; 64 FR
13096, Mar. 17, 1999; 67 FR 35048, May 17, 2002]

§ 180.202

p

-Chlorophenoxyacetic acid; tolerances for residues.

top
(a) General . A tolerance is established for the combined residues of the plant regulator p chlorophenoxyacetic acid and its metabolite p -chlorophenol to inhibit embryonic root development in or on
the following food commodity:
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Commodity

Parts per million

Bean, mung, sprouts

0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003, as amended at 71 FR 56398, Sept. 27, 2006]

§ 180.204 Dimethoate; tolerances for residues.
top
(a) General. Tolerances are established for total residues of the insecticide dimethoate ( O , O -dimethyl S
-( N - methylcarbamoylmethyl) phosphorodithioate) including its oxygen analog ( O , O -dimethyl S -( Nmethylcarbamoylmethyl) phosphorothioate) in or on the following food commodities:

Commodity

Parts per million

Alfalfa, forage

2.0

Alfalfa, hay

2.0

Bean, dry, seed

2.0

Bean, lima

2.0

Bean, snap, succulent

2.0

Blueberry1

1.0

Broccoli

2.0

Cattle, meat byproducts

0.02

Cauliflower

2.0

Celery

2.0

Citrus, dried pulp

5.0

Corn, field, forage

1.0

Corn, field, grain

0.1

Corn, field, stover

1.0

Corn, pop, grain

0.1

Corn, pop, stover

1.0

Corn, sweet, forage

1.0

Cotton, undelinted seed

0.1

Egg
Endive
Goat, meat byproducts
Grapefruit
Hog, meat byproducts

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0.02
2.0
0.02
2.0
0.02

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Horse, meat byproducts

0.02

Kale

2.0

Lemon

2.0

Lettuce, leaf

2.0

Melon

1.0

Milk

0.002

Mustard greens

2.0

Orange

2.0

Pea

2.0

Pear

2.0

Pecan

0.1

Pepper

2.0

Potato

0.2

Poultry, meat byproducts

0.02

Safflower, seed

0.1

Sheep, meat byproducts

0.02

Sorghum, grain, forage

0.1

Sorghum, grain, grain

0.1

Sorghum, grain, stover

0.1

Soybean, forage

2.0

Soybean, hay

2.0

Soybean, seed

0.05

Swiss chard

2.0

Tangerine

2.0

Tomato

2.0

Turnip, roots

0.2

Turnip, tops

2.0

Wheat, forage

2.0

Wheat, grain

0.04

Wheat, hay

2.0

Wheat, straw

2.0

1There

are U.S. registrations as of August 16, 1996.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(m),
are established for total residues of dimethoate including its oxygen analog in or on the following food
commodities:

Commodity

Parts per million

Asparagus

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0.15

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Brussels sprouts

5.0

Cherry, sweet

2.0

Cherry, tart

2.0

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33697, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, 2008]

§ 180.205 Paraquat; tolerances for residues.
top
(a) General. Tolerances are established for residues of the desiccant, defoliant, and herbicide paraquat
(1,1′-dimethyl-4,4′-bipyridinium-ion) derived from application of either the bis(methyl sulfate) or the
dichloride salt (both calculated as the cation) in or on the following food commodities:

Commodity
Acerola
Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Artichoke, globe
Asparagus

Parts per million
0.05
0.5
75.0
210.0
0.05
0.5

Avocado

0.05

Banana

0.05

Barley, grain

0.05

Barley, hay

3.5

Barley, straw

1.0

Beet, sugar, roots

0.5

Beet, sugar, tops

0.05

Berry group 13

0.05

Cacao bean, bean

0.05

Carrot, roots

0.05

Cattle, fat

0.05

Cattle, kidney

0.5

Cattle, meat

0.05

Cattle, meat byproducts, except kidney

0.05

Coffee, bean, green

0.05

Corn, field, forage

3.0

Corn, field, grain

0.1

Corn, field, stover

10.0

Corn, pop, grain

0.1

Corn, pop, stover

10.0

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Corn, sweet, kernel plus cob with husks removed
Cotton, gin byproducts

0.05
110.0

Cotton, undelinted seed

3.5

Cowpea, forage

0.1

Cowpea, hay

0.4

Cranberry

0.05

Egg

0.01

Endive

0.05

Fig

0.05

Fruit, citrus, group 10

0.05

Fruit, pome, group 11

0.05

Fruit, stone, group 12

0.05

Ginger
Goat, fat
Goat, kidney

0.1
0.05
0.5

Goat, meat

0.05

Goat, meat byproducts, except kidney

0.05

Grain, aspirated fractions

65.0

Grape

0.05

Grass, forage

90.0

Grass, hay

40.0

Guar, seed

0.5

Guava

0.05

Hog, fat

0.05

Hog, kidney

0.5

Hog, meat

0.05

Hog, meat byproducts, except kidney

0.05

Hop, dried cones
Horse, fat
Horse, kidney

0.5
0.05
0.5

Horse, meat

0.05

Horse, meat byproducts, except kidney

0.05

Kiwifruit

0.05

Lentil, seed

0.3

Lettuce

0.05

Milk

0.01

Mint, hay

0.5

Nut, tree, group 14

0.05

Okra

0.05

Olive

0.05

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Onion, bulb

0.1

Onion, green

0.05

Papaya

0.05

Passionfruit

0.2

Pea and bean, dried shelled, except soybean, subgroup 6C, except
guar bean

0.3

Pea and bean, succulent shelled, subgroup 6B

0.05

Pea, field, hay

0.8

Pea, field, vines

0.2

Peanut

0.05

Peanut, hay

0.5

Persimmon

0.05

Pineapple

0.05

Pineapple, process residue

0.25

Pistachio

0.05

Potato

0.5

Rhubarb

0.05

Rice, grain

0.05

Rice, straw

0.06

Safflower, seed

0.05

Sheep, fat

0.05

Sheep, kidney

0.5

Sheep, meat

0.05

Sheep, meat byproducts, except kidney

0.05

Sorghum, forage, forage

0.1

Sorghum, grain, forage

0.1

Sorghum, grain, grain

0.05

Soybean, forage

0.4

Soybean, hay

10.0

Soybean, hulls

4.5

Soybean, seed

0.7

Strawberry

0.25

Sugarcane, cane

0.5

Sugarcane, molasses

3.0

Sunflower, seed

2.0

Turnip, greens

0.05

Turnip, roots

0.05

Vegetable, brassica, leafy, group 5

0.05

Vegetable, cucurbit, group 9

0.05

Vegetable, fruiting, group 8

0.05

Vegetable, legume, edible podded, subgroup 6A

0.05

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Wheat, forage

0.5

Wheat, grain

1.1

Wheat, hay

3.5

Wheat, straw

50.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(n),
are established for residues of the pesticide paraquat (1,1′-dimethyl-4,4′ bipyridinium ion) derived from
application of either the bis(methyl sulfate) or the dichloride salt (both calculated as the cation) in or on the
following food commodities:

Commodity

Parts per million

Cassava

0.05

Pea, pigeon, seed

0.05

Tanier

0.05

Taro, corm

0.1

Tyfon

0.05

Yam, true, tuber

0.05

(d) Indirect or inadvertent residues. [Reserved]
[46 FR 51614, Oct. 21, 1981]
Editorial Note: ForFederal Registercitations affecting §180.205, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.206 Phorate; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the insecticide phorate ( O,O diethyl S (ethylthio) methyl]phosphorodithioate), phorate sulfoxide, phorate sulfone, phorate oxygen
analog, phorate oxygen analog sulfoxide, and phorate oxygen analog sulfone in or on the following food
commodities:

Commodity

Parts per million

Bean, dry, seed

0.05

Bean, succulent

0.05

Beet, sugar, roots

0.3

Beet, sugar, tops

3.0

Coffee, green bean1

0.02

Corn, field, forage

0.5

Corn, field, grain

0.05

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
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0.5
0.05

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Cotton, undelinted seed

0.05

Hop, dried cones

2.0

Peanut

0.1

Potato

0.2

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.1

Soybean, seed

0.05

Sugarcane, cane

0.05

Wheat, forage

1.5

Wheat, grain

0.05

Wheat, hay

1.5

Wheat, straw

0.05

1There are no U.S. registrations as of September 1, 1993 for the use of phorate on the growing crop,
coffee.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, 1998; 66
FR 50833, Oct. 5, 2001; 67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR 53738, Sept.
17, 2008]

§ 180.207 Trifluralin; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide and plant growth regulator trifluralin,
alpha, alpha, alpha-trifluoro-2,6-dinitro- N , N -dipropyl- p -toluidine, in or on the following raw agricultural
commodities:

Commodity

Parts per million

Alfalfa, forage

3.0

Alfalfa, hay

2.0

Almond, hulls

0.05

Asparagus

0.05

Barley, grain

0.05

Barley, hay

0.05

Barley, straw

0.05

Bean, mung, sprouts

2.0

Carrot, roots

1.0

Celery

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0.05

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Corn, field, forage

0.05

Corn, field, grain

0.05

Corn, field, stover

0.05

Cotton, gin byproducts

0.05

Cotton, undelinted seed

0.05

Endive

0.05

Flax, seed

0.05

Fruit, citrus, group 10

0.05

Fruit, stone, group 12

0.05

Grape

0.05

Hop, dried cones

0.05

Mustard, seed

0.05

Nut, tree, group 14

0.05

Okra

0.05

Peanut

0.05

Peanut, hay

0.05

Peppermint, oil

2.0

Peppermint, tops

0.05

Rapeseed, seed

0.05

Safflower, seed

0.05

Sorghum, grain, forage

0.05

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.05

Spearmint, oil

2.0

Spearmint, tops

0.05

Sugarcane, cane

0.05

Sunflower, seed

0.05

Vegetable, brassica, leafy group 5

0.05

Vegetable, bulb, group 3

0.05

Vegetable, cucurbit, group 9

0.05

Vegetable, foliage of legume, group 7

0.05

Vegetable, fruiting, group 8

0.05

Vegetable, leaves of root and tuber, group 2

0.05

Vegetable, legume, group 6

0.05

Vegetable, root and tuber, group 1, except carrot

0.05

Wheat, grain

0.05

Wheat, straw

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[45 FR 42619, June 25, 1980, as amended at 45 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, 1980;
46 FR 37250, July 20, 1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR 57074, Oct.
26, 1998; 64 FR 39082, July 21, 1999; 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. 15, 2006]

§ 180.208 Benfluralin; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide benfluralin, N -butyl- N -ethyl-αααtrifluoro-2,6-dinitro- p -toluidine, in or on the following food commodities:

Commodity

Parts per million

Alfalfa, forage

0.05

Alfalfa, hay

0.05

Clover, forage

0.05

Clover, hay

0.05

Lettuce

0.05

Trefoil, forage

0.05

Trefoil, hay

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003, as amended at 73 FR 52613, Sept. 10, 2008]

§ 180.209 Terbacil; tolerances for residues.
top
(a) General . Tolerances are established for combined residues of the herbicide terbacil, (3-tert-butyl-5chloro-6-methyluracil) and its metabolites [3-tert-butyl-5-chloro-6-hydroxymethyluracil], [6-chloro-2,3dihydro-7-hydroxymethyl 3,3-dimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], and [6-chloro-2,3-dihydro-3,3,7trimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], calculated as terbacil, in or on the following raw agricultural
commodities:

Commodity

Parts per million

Alfalfa, forage

1.0

Alfalfa, hay

2.0

Apple

0.3

Asparagus

0.4

Blueberry

0.2

Caneberry subgroup 13A

0.2

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Peach

0.2

Peppermint, tops

2.0

Spearmint, tops

2.0

Strawberry

0.1

Sugarcane, cane

0.4

Watermelon

1.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 30818, May 31, 2006]

§ 180.210 Bromacil; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide bromacil (5-bromo-3- sec -butyl-6methyluracil) in or on the following food commodities:

Commodity

Parts per million

Fruit, citrus

0.1

Pineapple

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003]

§ 180.211 Propachlor; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the herbicide propachlor (2-chloroN-isopropylacetanilide) and its metabolites containing the N-isopropylaniline moiety, calculated as 2-chloroN-isopropylacetanilide, in or on the following raw agricultural commodities:

Commodity
Cattle, fat
Cattle, kidney

Parts per million
0.05
0.2

Cattle, meat

0.02

Cattle, meat byproducts, except kidney

0.05

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Corn, field, forage

3.0

Corn, field, grain

0.2

Corn, field, stover

1.0

Corn, sweet, forage

3.0

Goat, fat

0.05

Goat, kidney

0.2

Goat, meat

0.02

Goat, meat byproducts, except kidney

0.05

Hog, fat

0.02

Hog, meat

0.02

Hog, meat byproducts

0.02

Horse, fat

0.05

Horse, kidney

0.2

Horse, meat

0.02

Horse, meat byproducts, except kidney

0.05

Milk

0.02

Sheep, fat

0.05

Sheep, kidney

0.2

Sheep, meat

0.02

Sheep, meat byproducts, except kidney

0.05

Sorghum, forage, forage

8.0

Sorghum, grain, forage

8.0

Sorghum, grain, grain

0.25

Sorghum, grain, stover

12.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 25959, June 16, 1982, as amended at 47 FR 28381, June 30, 1982; 47 FR 28626, July 1, 1982; 47
FR 46701, Oct. 20, 1982; 63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007]

§ 180.212

-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.

S

top
(a) General. Tolerances are established for residues of the herbicide S -ethyl
cyclohexylethylthiocarbamate in or on the following food commodities:

Commodity

Parts per million

Beet, garden, roots

0.05(N)

Beet, garden, tops

0.05(N)

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Beet, sugar, roots

0.05(N)

Beet, sugar, tops

0.05(N)

Spinach

0.05(N)

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003]

§ 180.213 Simazine; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the herbicide simazine (2-chloro-4,6bis(ethylamino)-s-triazine) and its two chlorinated degradates (2-amino-4-chloro-6-ethylamino-s-triazine
and 2,4-diamino-6-chloro-s-triazine), the total residue to be measured in or on the following food
commodities:

Commodity

Parts per million

Almond

0.25

Almond, hulls

0.25

Apple

0.20

Avocado

0.20

Blackberry

0.20

Blueberry

0.20

Cattle, meat

0.03

Cattle, meat byproducts

0.03

Cherry

0.25

Corn, field, forage

0.20

Corn, field, grain

0.20

Corn, field, stover

0.25

Corn, pop, grain

0.20

Corn, pop, stover

0.25

Corn, sweet, forage

0.20

Corn, sweet, kernel plus cob with husks removed

0.25

Corn, sweet, stover

0.25

Cranberry

0.25

Currant

0.25

Egg

0.03

Goat, meat

0.03

Goat, meat byproducts

0.03

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Grape

0.20

Grapefruit

0.25

Hazelnut

0.20

Horse, meat

0.03

Horse, meat byproducts

0.03

Lemon

0.25

Loganberry

0.20

Milk

0.03

Nut, macadamia

0.25

Olive

0.20

Orange

0.25

Peach

0.20

Pear

0.25

Pecan

0.20

Plum

0.20

Raspberry

0.20

Sheep, meat

0.03

Sheep, meat byproducts

0.03

Strawberry

0.25

Walnut

0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, 2007; 72
FR 53454, Sept. 19, 2007]

§ 180.214 Fenthion; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide fenthion ( O,O- dimethyl O- [4(methylthio)- m- tolyl] phosphorothioate) and its cholinesterase-inhibiting metabolites in or on the following
raw agricultural commodities:

Commodity

Parts per million

Expiration/Revocation Date

Cattle, fat

0.1

4/1/06

Cattle, meat

0.1

4/1/06

Cattle, meat byproducts

0.1

4/1/06

Hog, fat

0.1

4/1/03

Hog, meat

0.1

4/1/03

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Hog, meat byproducts
Milk

0.1

4/1/03

0.01

4/1/03

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 86492, Dec. 31, 1980, as amended at 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 67
FR 49616, July 31, 2002]

§ 180.215 Naled; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide naled (1,2-dibromo-2,2-dichloroethyl dimethyl phosphate) and its conversion product 2,2-dichlorovinyl dimethyl phosphate, expressed as
naled, resulting from the application of the pesticide to growing crops or from direct application to livestock
and poultry, in or on the following raw agricultural commodities:

Commodity

Parts per million

Almond, hulls

0.5

Almond

0.5

Bean, dry, seed

0.5

Bean, succulent

0.5

Beet, sugar, roots

0.5

Beet, sugar, tops

0.5

Broccoli

1

Brussels sprouts

1

Cabbage

1

Cauliflower

1

Celery

3

Collards

3

Cotton, undelinted seed

0.5

Cucumber

0.5

Eggplant

0.5

Grapefruit
Grape
Grass, forage
Hop, dried cones
Kale
Legume, forage

3
0.5
10
0.5
3
10

Lemon

3

Lettuce

1

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Melon

0.5

Orange, sweet

3

Peach

0.5

Pea, succulent

0.5

Pepper

0.5

Pumpkin

0.5

Safflower, seed

0.5

Spinach

3

Squash, summer

0.5

Squash, winter

0.5

Strawberry

1

Swiss chard

3

Tangerine

3

Tomato

0.5

Turnip, greens

3

Walnut

0.5

(2) A tolerance of 0.5 part per million is established for the pesticide naled in or on all raw agricultural
commodities, except those otherwise listed in this section, from use of the pesticide for area pest
(mosquito and fly) control.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[42 FR 46304, Sept. 15, 1977, as amended at 54 FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998;
66 FR 50833, Oct. 5, 2001]

§ 180.217 Ammoniates for [ethylenebis-(dithiocarbamato)] zinc and ethylenebis
[dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and
disulfides; tolerances for residues.
top
(a) General. Tolerances are established for residues of a fungicide that is a mixture of 5.2 parts by weight
of ammoniates of [ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis [dithiocarbamic
acid] bimolecular and trimolecular cyclic anhydrosulfides and disulfides, calculated as zinc
ethylenebisdithiocarbamate, in or on the following raw agricultural commodities as follows:

Commodity

Parts per million

Apple

2.0

Potato

0.5

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 57074, Oct. 26, 1998]

§ 180.220 Atrazine; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the herbicide atrazine (2-chloro-4ethylamino-6-isopropylamino-s-triazine) and its chlorinated metabolites 2-amino-4-chloro-6-isopropylaminos-triazine, 2-amino-4-chloro-6-ethylamino-s-triazine, and 2,4-diamino-6-chloro-s-triazine, in or on the
following food commodities:

Commodity

Parts per million

Cattle, fat

0.02

Cattle, meat

0.02

Cattle, meat byproducts

0.02

Corn, field, forage

15

Corn, field, grain

0.20

Corn, field, stover

0.5

Corn, pop, forage

1.5

Corn, pop, grain

0.20

Corn, pop, stover

0.5

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

15
0.20
2.0

Goat, fat

0.02

Goat, meat

0.02

Goat, meat byproducts

0.02

Grass, forage

4.0

Grass, hay

4.0

Guava

0.05

Horse, fat

0.02

Horse, meat

0.02

Horse, meat byproducts

0.02

Milk

0.02

Nut, macadamia

0.20

Sheep, fat

0.02

Sheep, meat

0.02

Sheep, meat byproducts

0.02

Sorghum, forage, forage

15

Sorghum, grain forage

15

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Sorghum, grain, grain

0.20

Sorghum, grain, stover

0.50

Sugarcane, cane

0.20

Wheat, forage

1.5

Wheat, grain

0.10

Wheat, hay

5.0

Wheat, straw

0.50

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertant residues of
atrazine, 2-chloro-4-ethylamino-6-isopropylamino-s-triazine, in or on the following raw agricultural
commodity when present therein as a result of application of atrazine to the growing crops in paragraph
(a) of this section:

Commodity

Parts per million

Vegetable, leafy, except brassica, group 4

0.25

[43 FR 29121, July 6, 1978, as amended at 44 FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 1982; 47
FR 8012, Feb. 24, 1982; 63 FR 57075, Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR 6567, Feb. 11,
2004; 72 FR 35666, June 29, 2007; 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July 2, 2008]

§ 180.221
residues.

O

-Ethyl S

-phenyl ethylphosphonodithioate; tolerances for

top
(a) General. Time limited tolerances are established for residues of the insecticide O -Ethyl S phenylethylphosphonodithioate, including its oxygen analog ( O -ethyl S -phenyl ethylphosphonothioate, in
or on the following food commodities:

Commodities

Parts per million Expiration/Revocation date

Asparagus

0.5

12/31/02

Banana

0.1

Do.

Beet, sugar, tops

0.1

Do.

Corn, field, forage

0.1

Do.

Corn, field, grain

0.1

Do.

Corn, field, stover

0.1

Do.

Corn, pop, grain

0.1

Do.

Corn, pop, stover

0.1

Do.

Corn, sweet, forage

0.1

Do.

Corn, sweet, kernel plus cob with
husks removed

0.1

Do.

Corn, sweet, stover

0.1

Do.

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Peanut

0.1

Do.

Peanut, hay

0.1

Do.

Pea, field, hay

0.1

Do.

Pea, field, vines

0.1

Do.

Peppermint, tops

0.1

Do.

Plantain

0.1

Do.

Sorghum, grain, forage

0.1

Do.

Sorghum, grain, grain

0.1

Do.

Sorghum, grain, stover

0.1

Do.

Soybean, forage

0.1

Do.

Soybean, hay

0.1

Do.

Spearmint, tops

0.1

Do.

Strawberry

0.1

Do.

Sugarcane, cane

0.1

Do.

Vegetable, fruiting, group 8

0.1

Do.

Vegetable, leafy

0.1

Do.

Vegetable, root crop

0.1

Do.

Vegetable, seed and pod

0.1

Do.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 39077, July 21, 1999]

§ 180.222 Prometryn; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide prometryn (2,4-bis(isopropylamino)-6methylthio- s -triazine) in or on the following raw agricultural commodities:

Commodity

Parts per million

Carrot, roots1

0.1

Celery

0.5

Corn, grain

0.25

Cotton, undelinted seed

0.25

Pea, pigeon, seed

0.25

1There

are no U.S. registrations as of April 10, 1998 for use on carrots.

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional exemptions. Tolerances with regional registration, as defined in §180.1(n), are
established for residues of the herbicide prometryn (2,4-bis(isopropylamino-6-methylthio- s- triazine) in or
on the following raw agricultural commodity:

Commodity

Parts per million

Dill

0.3

Parsley, leaves

0.1

(d) Indirect or inadvertent residues. [Reserved]
[43 FR 29121, July 6, 1978, as amended at 45 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, 1989; 60
FR 20434, Apr. 26, 1995; 63 FR 17692, Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR 39082, July 21,
1999]

§ 180.225 Phosphine; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of phosphine in or on the following raw
agricultural commodities (RACs) resulting from post-harvest fumigation for the control of insects with
phosphine gas or phosphide compounds that produce phosphine gas.

Commodity

Parts per million

Almond

0.1

Avocado

0.01

Banana

0.01

Barley, grain
Cabbage, Chinese

0.1
0.01

Cacao bean, dried bean

0.1

Cashew

0.1

Citron, citrus

0.01

Coffee, bean, green

0.1

Corn, field, grain

0.1

Corn, pop, grain

0.1

Cotton, undelinted seed

0.1

Date, dried fruit

0.1

Dill, seed

0.01

Eggplant

0.01

Endive

0.01

Grapefruit

0.01

Hazelnut

0.1

Kumquat

0.01

Lemon

0.01

Lettuce

0.01

Lime

0.01

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Mango

0.01

Millet, grain

0.1

Mushroom

0.01

Nut, brazil

0.1

Oat, grain

0.1

Okra

0.01

Orange, sweet

0.01

Papaya

0.01

Peanut

0.1

Pecan

0.1

Pepper

0.01

Persimmon

0.01

Pistachio

0.1

Rice, grain

0.1

Rye, grain

0.1

Safflower, seed

0.1

Salsify, tops

0.01

Sesame, seed

0.1

Sorghum, grain

0.1

Soybean, seed

0.1

Sunflower, seed

0.1

Sweet potato, roots

0.01

Tangelo

0.01

Tangerine

0.01

Tomato

0.01

Vegetable, legume, group 6, except soybean

0.01

Walnut

0.1

Wheat, grain

0.1

(2) Tolerances are established for residues of the fumigant in or on all RACs resulting from preharvest
treatment of pest burrows in agricultural and non-crop land areas.

Commodity

Parts per million

All raw agricultural commodities resulting from preharvest treatment
of pest burrows

0.01

(3) Residues resulting from fumigation of processed food:

Commodity

Parts per million

Processed food
(4) Residues resulting from fumigation of animal feed :

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Commodity

Parts per million

Animal feed

0.1

(5) To assure safe use of this pesticide, it must be used in compliance with the labeling conforming to that
registered by the U.S. Environmental Protection Agency (EPA) under FIFRA. Labeling shall bear a
restriction to aerate the finished food/feed for 48 hours before it is offered to the consumer, unless EPA
specifically determines that a different time period is appropriate. Where appropriate, a warning shall state
that under no condition should any formulation containing aluminum or magnesium phosphide be used so
that it will come in contact with any processed food, except processed brewer's rice, malt, and corn grits
stored in breweries for use in the manufacture of beer.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[64 FR 72950, Dec. 29, 1999, as amended at 71 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, 2007]

§ 180.226 Diquat; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the plant growth regulator and herbicide diquat,
(6,7-dihydrodipyrido (1,2-a:2'1'-c)pyrazinediium) derived from application of the dibromide salt and
calculated as the cation in or on the following food commodities:

Commodity

Parts per million

Alfalfa, seed

3.0

Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Egg

0.05

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.05

Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Milk

0.02

Potato

0.1

Poultry, fat

0.05

Poultry, meat

0.05

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Poultry, meat byproducts

0.05

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Sorghum, grain, grain

2.0

Soybean, seed

0.2

(2)(i) Tolerances are established for residues of the herbicide diquat (6,7-dihydrodipyrido (1,2-a:2,1-c)
pyrazinediium) (calculated as the cation) derived from the application of the dibromide salt to ponds, lakes,
reservoirs, marshes, drainage ditches, canals, streams, and rivers which are slow-moving or quiescent in
programs of the Corps of Engineers or other Federal or State public agencies and to ponds, lakes and
drainage ditches only where there is little or no outflow of water and which are totally under the control of
the user, in or on the following food commodities:

Commodity
Avocado
Berry group 13
Cotton, undelinted seed
Cranberry
Fish

Parts per million
0.2
0.05
0.2
0.05
2.0

Fruit, citrus, group 10

0.05

Fruit, pome, group 11

0.02

Fruit, stone, group 12

0.02

Grain, cereal, forage, fodder and straw, group 16

0.02

Grain, cereal, group 15

0.02

Grape

0.05

Grass, forage, fodder and hay, group 17

0.2

Hop, dried cones

0.2

Nut, tree, group 14

0.02

Shellfish

20.0

Strawberry

0.05

Sugarcane, cane

0.2

Vegetable, brassica, leafy, group 5

0.05

Vegetable, cucurbit, group 9

0.02

Vegetable, foliage of legume, group 7

0.2

Vegetable, fruiting, group 8

0.05

Vegetable, leafy, except brassica, group 4

0.05

Vegetable, root and tuber, group 1

0.02

Vegetable, seed and pod

0.05

(ii) Where tolerances are established at higher levels from other uses of diquat on the subject crops, the
higher tolerances applies also to residues of the aquatic uses cited in this paragraph.
(3) Tolerances are established for the plant growth regulator diquat [6,7-dihydrodipyrido (1,2-a:21/4,11/4http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c...&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (151 of 651) [9/8/2009 3:02:19 PM]

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c) pyrazinediium] derived from application of the dibromide salt and calculated as the cation in or on the
following food commodities:

Commodity

Parts per million

Banana

0.05

Coffee, bean, green

0.05

Soybean, hulls

0.6

(4) There are no U.S. registrations as of December 6, 1995.
(5) A tolerance of 0.5 part per million is established for residues of diquat in potato, granules/flakes and
potato, chips.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33709, May 24, 2000, as amended at 72 FR 41929, Aug. 1, 2007]

§ 180.227 Dicamba; tolerances for residues.
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(a) General. (1) Tolerances are established for the combined residues of the herbicide dicamba (3,6dichloro- o -anisic acid) and its metabolite 3,6-dichloro-5-hydroxy- o- anisic acid in or on the food
commodities as follows:

Commodity

Parts per million

Barley, grain

6.0

Barley, hay

2.0

Barley, straw

15.0

Corn, field, forage

3.0

Corn, field, grain

0.1

Corn, field, stover

3.0

Corn, pop, grain

0.1

Corn, pop, stover

3.0

Corn, sweet, forage

0.50

Corn, sweet, kernel plus cob with husks removed

0.04

Corn, sweet, stover

0.50

Cotton, undelinted seed

0.2

Grass, forage, fodder and hay, group 17, forage

125.0

Grass, forage, fodder and hay, group 17, hay

200.0

Millet, proso, forage

90.0

Millet, proso, grain

2.0

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Millet, proso, hay

40.0

Millet, proso, straw

30.0

Oat, forage

90.0

Oat, grain

2.0

Oat, hay

40.0

Oat, straw

30.0

Rye, forage

90.0

Rye, grain

2.0

Rye, straw

30.0

Sorghum, grain, forage

3.0

Sorghum, grain, grain

4.0

Sorghum, grain, stover

10.0

Sugarcane, cane

0.1

Sugarcane, molasses

2.0

Wheat, forage

90.0

Wheat, grain

2.0

Wheat, hay

40.0

Wheat, straw

30.0

(2) Tolerances are established for the combined residues of the herbicide dicamba (3,6-dichloro- o -anisic
acid) and its metabolite 3,6-dichloro-2-hydroxybenzoic acid in or on the food commodities as follows:

Commodity

Parts per million

Asparagus

4.0

Cattle, fat

0.3

Cattle, kidney

25.0

Cattle, meat

0.25

Cattle, meat byproducts, except kidney

3.0

Goat, fat

0.3

Goat, kidney

25.0

Goat, meat

0.25

Goat, meat byproducts, except kidney

3.0

Hog, fat

0.3

Hog, kidney

25.0

Hog, meat

0.25

Hog, meat byproducts, except kidney

3.0

Horse, fat

0.3

Horse, kidney

25.0

Horse, meat

0.25

Horse, meat byproducts, except kidney

3.0

Milk

0.2

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Sheep, fat

0.3

Sheep, kidney

25.0

Sheep, meat

0.25

Sheep, meat byproducts, except kidney

3.0

(3) Tolerances are established for the combined residues of dicamba (3,6-dichloro- o -anisic and its
metablites 3,6-dichloro-5-hydroxy- o -anisic acid and 3,6-dichloro-2-hydroxybenzoic acid in or on the food
commodities as follows:

Commodity

Parts per million

Grain, aspirated fractions

1000

Soybean, hulls

30.0

Soybean, seed

10.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33709, May 24, 2000, as amended at 72 FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, 2008; 73
FR 54960, Sept. 24, 2008]

§ 180.228 S
for residues.

-Ethyl hexahydro- 1H

-azepine-1-carbothioate; tolerances

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(a) General. Tolerances are established for the herbicide S -ethyl hexahydro-1 1H -azepine-1-carbothioate
in or on the following food commodities:

Commodity

Parts per million

Expiration/Revocation Date

Rice, grain

0.1

9/1/09

Rice, straw

0.1

9/1/09

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003, as amended at 69 FR 58083, Sept. 29, 2004]

§ 180.229 Fluometuron; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of the herbicide fluometuron, N , N -

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dimethyl- N '-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined
as TFMA, in or on the following food commodities:

Commodity

Parts per million

Cotton, gin byproducts

3.5

Cotton, undelinted seed

1.0

(2) Tolerances are established for the combined residues of the herbicide fluometuron, N , N -dimethyl- N '[3-(trifluoromethyl)phenyl]urea, and its metabolites determined as TFMA and the hydroxylated metabolites:
CGA-236431, 1-(4-hydroxy-3-trifluoromethylphenyl)urea; CGA-236432, 1-methyl-3-(4-hydroxy-3trifluoromethylphenyl)urea; and CGA-13211, 1,1-dimethyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea, in or
on the following food commodities:

Commodity

Parts per million

Cattle, meat byproducts

0.1

Egg

0.1

Goat, meat byproducts

0.1

Hog, meat byproducts

0.1

Horse, meat byproducts

0.1

Milk

0.02

Poultry, fat

0.1

Poultry, meat

0.1

Poultry, meat byproducts

0.1

Sheep, meat byproducts

0.1

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for the combined residues of the herbicide
fluometuron, N , N -dimethyl- N '-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline
(TFMA) determined as TFMA, in or on the following food commodities.

Commodity

Parts per million

Grain, cereal, forage, fodder, and straw group 16, forage

3.0

Grain, cereal, forage, fodder, and straw, group 16, stover

6.0

Grain, cereal, group 15

0.5

Peanut

0.1

Peanut, hay

4.0

Peanut, meal

0.2

Soybean, forage

3.0

Soybean, hay

3.0

Soybean, seed

2.0

Rice, hulls

1.0

Wheat, milled byproducts

1.0

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[73 FR 52613, Sept. 10, 2008]

§ 180.231 Dichlobenil; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of the herbicide dichlobenil (2,6dichlorobenzonitrile) and its metabolite 2,6-dichlorobenzamide in or on the following raw agricultural
commodities:

Commodity

Parts per million

Apple

0.5

Bushberry subgroup 13–07B

0.15

Caneberry subgroup 13–07A

0.10

Cranberry

0.1

Fruit, stone, group 12

0.15

Grape

0.15

Hazelnut

0.1

Pear

0.5

Rhubarb

0.06

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[36 FR 22540, Nov. 25, 1971, as amended at 63 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, 2001; 73
FR 50570, Aug. 27, 2008]

§ 180.232 Butylate; tolerances for residues.
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(a) General. Tolerances are established for the herbicide butylate in or on the following food commodities:

Commodity

Parts per million

Corn, field, forage

0.1

Corn, field, grain

0.1

Corn, field, stover

0.1

Corn, pop, forage

0.1

Corn, pop, grain

0.1

Corn, sweet, forage

0.1

Corn, sweet, kernel plus cob with husks removed

0.1

(b) Section 18 emergency exemptions. [Reserved]
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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003]

§ 180.235 Dichlorvos; tolerances for residues.
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(a) General. (1) Tolerances for residues of the insecticide 2,2-dichlorovinyl dimethyl phosphate are
established as follows:

Commodity

Parts per million

Cattle, fat

0.02(N)

Cattle, meat

0.02(N)

Cattle, meat byproducts

0.02(N)

Egg

0.05(N)

Goat, fat

0.02(N)

Goat, meat

0.02(N)

Goat, meat byproducts

0.02(N)

Horse, fat

0.02(N)

Horse, meat

0.02(N)

Horse, meat byproducts

0.02(N)

Milk

0.02(N)

Mushroom (residues expressed as naled)

0.5

Poultry, fat

0.05(N)

Poultry, meat

0.05(N)

Poultry, meat byproducts

0.05(N)

Raw agricultural commodities, nonperishable, bulk stored regardless
of fat content, postharvest

0.5

Raw agricultural commodities nonperishable, packaged or bagged,
containing 6 percent fat or less, postharvest

0.5

Raw agricultural commodities, nonperishable, packaged or bagged,
containing more than 6 percent fat, postharvest

2

Sheep, fat

0.02(N)

Sheep, meat

0.02(N)

Sheep, meat byproducts

0.02(N)

Tomato, postharvest (residues expressed as naled)

0.05

(2) The tolerance of 0.1 part per million prescribed by 21 CFR 556.180 for negligible residues of 2,2dichlorovinyl dimethyl phosphate in the edible tissue of swine covers both its use as an anthelmintic in
swine feed and as an insecticide applied directly to swine.

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(3) Dichlorvos may be present as a residue from application as an insecticide on packaged or bagged
nonperishable processed food (see: 21 CFR 170.3(j)) in an amount in such food not in excess of 0.5 part
per million (ppm). To assure safe use of the insecticide, its label and labeling shall conform to the label
and labeling registered by the U.S. Environmental Protection Agency, and the usage employed shall
conform with such label or labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, 1991;
63 FR 57075, Oct. 26, 1998; 65 FR 33697, May 24, 2000]

§ 180.236 Triphenyltin hydroxide; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the fungicide triphenyltin hydroxide
(TPTH) and its monophenyltin (MPTH) and diphenyltin (DPTH) hydroxide and oxide metabolites,
expressed in terms of parent TPTH, in or on the following raw agricultural commodities:

Commodity

Parts per million

Beet, sugar, roots

0.05

Beet, sugar, tops

10.0

Cattle, fat

0.2

Cattle, kidney

2.0

Cattle, liver

4.0

Cattle, meat

0.5

Goat, fat

0.2

Goat, kidney

2.0

Goat, liver

4.0

Goat, meat

0.5

Hog, fat

0.3

Hog, meat

0.06

Hog, meat byproducts

0.3

Horse, fat

0.2

Horse, kidney

2.0

Horse, liver

4.0

Horse, meat

0.5

Milk

0.06

Pecan

0.05

Potato

0.05

Sheep, fat

0.2

Sheep, kidney

2.0

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Sheep, liver

4.0

Sheep, meat

0.5

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 41929, Aug. 1, 2007]

§ 180.239 Phosphamidon; tolerancesfor residues.
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(a) General. Tolerances (expressed as phosphamidon) for residues of the insecticide phosphamidon (2chloro-2-diethylcarbamoyl-1-methylvinyl dimethyl phosphate) including all of its related cholinesteraseinhibiting compounds in or on raw agricultural commodities are established as follows:

Commodity

Parts per million

Apple

Expiration/Revocation Date
1.0

12/31/02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 46893, July 17, 2002]

§ 180.241 Bensulide; tolerances for residues.
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(a) General . Tolerances are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N (2-mercaptoethyl) benzenesulfonamide including its oxygen analog S -( O,O -diisopropyl
phosphorothioate) of N -(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

Commodity

Parts per million

Onion, bulb

0.10

Vegetable, brassica, leafy group 5

0.15

Vegetable, cucurbits group 9

0.15

Vegetable, fruiting group 8

0.10

Vegetable, leafy except brassica group 4

0.15

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(m),
are established for the residues of S -( O,O -diisopropyl phosphorodithioate) of N -(2-mercaptoethyl)
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benzenesulfonamide including its oxygen analog S -( O,O -diisopropyl phosphorothioate) of N -(2mercaptoethyl) benzenesulfonamide in or on the following food commodities:

Commodity

Parts per million

Carrot, roots

0.10

(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003, as amended at 73 FR 53738, Sept. 17, 2008]

§ 180.242 Thiabendazole; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of the fungicide thiabendazole (2(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and conjugated) in or on the following
food commodities:

Commodity

Parts per million

Apple, wet pomace

12.0

Avocado1

10.0

Banana, postharvest

3.0

Bean, dry, seed

0.1

Beet, sugar, dried pulp

3.5

Beet, sugar, roots

0.25

Beet, sugar, tops

10.0

Cantaloupe1

15.0

Carrot, roots, postharvest

10.0

Citrus, oil

15.0

Fruit, citrus, group 10, postharvest

10.0

Fruit, pome, group 11, postharvest

5.0

Mango

10.0

Mushroom

40.0

Papaya, postharvest

5.0

Potato, postharvest

10.0

Soybean

0.1

Strawberry1

5.0

Sweet potato (postharvest to sweet potato intended only for use as
seed)

0.05

Wheat, grain

1.0

Wheat, straw

1.0

1There

are no U.S. registrations on the indicated commodity.

(2) Tolerances are established for the combined residues of thiabendazole (2-(4-thiazolyl)benzimidazole)
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and its metabolites 5-hydroxythiabendazole (free and conjugated) and benzimidazole in or on the following
food commodities:

Commodity

Parts per million

Cattle, meat

0.1

Cattle, meat byproducts

0.4

Goat, meat byproducts

0.4

Hog, meat byproducts

0.3

Horse, meat byproducts

0.4

Milk

0.1

Sheep, meat byproducts

0.4

(b) Section 18 emergency exemptions . Time-limited tolerances are established for the combined residues
of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and conjugated), in
connection with use of the pesticide under section 18 emergency exemptions granted by EPA. The
tolerances are specified in the following table. The tolerances will expire on the dates specified in the table.

Commodity

Parts per million

Expiration/Revocation Date

Brussels sprout

0.05

12/31/09

Cabbage

0.05

12/31/09

Cauliflower

0.05

12/31/09

Lentil, seed

0.1

12/31/08

(c) Tolerances with regional exemptions. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[42 FR 32783, June 28, 1977]
Editorial Note: ForFederal Registercitations affecting §180.242, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.243 Propazine; tolerances for residues.
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Tolerances are established for negligible residues (N) of the herbicide propazine (2-chloro-4,6-bis
(isopropylamino)- s -triazine in or on the following raw agricultural commodities:

Commodity

Parts per million

Sorghum, forage

0.25(N)

Sorghum, grain, grain

0.25(N)

Sorghum, grain, stover

0.25(N)

Sorghum, sweet

0.25(N)

[43 FR 29121, July 6, 1978]

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§ 180.245 Streptomycin; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the fungicide streptomycin in or on food
commodities as follows:

Commodity

Parts per million

Bean, dry, seed

0.5

Bean, succulent

0.5

Fruit, pome, group 11

0.25

(2) Tolerances are established for residues of the fungicide streptomycin from treatment of seedling plants
before transplanting in or on the following food commodities:

Commodity

Parts per million

Celery

0.25

Pepper

0.25

Tomato

0.25

(3) Tolerances are established for residues of the fungicide streptomycin from treatment of seed pieces in
or on the following food commodity:

Commodity

Parts per million

Potato

0.25

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003, as amended at 73 FR 54960, Sept. 24, 2008]

§ 180.249 Alachlor; tolerances for residues.
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(a) General . Tolerances are established for combined residues of alachlor (2-chloro-2',6'-diethyl- N (methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor in or on the
following raw agricultural commodities.

Commodity

Parts per million

Beans, dry

0.1

Beans, succulent lima

0.1

Cattle, fat
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Cattle, meat byproducts

0.02

Cattle, meat

0.02

Corn, field, forage

2.0

Corn, field, grain

0.2

Corn, field, pop

0.2

Corn, field, stover

2.0

Corn, pop, stover

2.0

Corn, sweet (K+CWHR)

0.05

Corn, sweet, stover

2.0

Cotton, gin byproducts

0.7

Cotton, undelinted seed

0.03

Cowpea, forage

5.0

Cowpea, hay

5.0

Egg

0.02

Goat, fat

0.02

Goat, meat byproducts

0.02

Goat, meat

0.02

Hog, fat

0.02

Hog meat byproducts

0.02

Hog, meat

0.02

Horse, fat

0.02

Horse, meat byproducts

0.02

Horse, meat

0.02

Milk

0.02

Peanut

0.5

Poultry, fat

0.02

Poultry, meat byproducts

0.02

Poultry, meat

0.02

Sheep, fat

0.02

Sheep, meat byproducts

0.02

Sheep, meat

0.02

Sorghum grain, forage

2.0

Sorghum, grain, grain

0.1

Sorghum, grain, stover

1.0

Soybeans, seed

1.0

Sunflower, meal

3.4

Sunflower, seed

2.5

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]

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(d) Indirect or inadvertent residues . Tolerances are established for indirect or inadvertent residues of
alachlor (2-chloro-2',6'-diethyl- N -(methoxymethyl)acetanilide) and its metabolites which can be converted
to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated
as alachlor, in or on the following raw agricultural commodities when present therein as a result of the
application of alachlor to the growing crops in paragraph (a) of this section:

Commodity

Parts per million

Animal feed, nongrass, group 18, forage

1.4

Animal feed, nongrass, group 18, hay

1.2

Grain, cereal, forage, and straw, group 16 except corn, sorghum,
rice, straw

0.8

Grain, cereal, forage, fodder and straw, group 16 except corn,
sorghum, rice, forage

0.6

Grain, cereal, forage, fodder, and straw, group 16 except for corn,
sorghum, rice, hay

0.8

Grain, cereal, group 15 except corn, sorghum, rice

0.05

[72 FR 54584, Sept. 26, 2007]

§ 180.252 Tetrachlorvinphos; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the insecticide tetrachlorvinphos,
( Z )-2-chloro-1-(2,4,5- trichlorophenyl) vinyl dimethyl phosphate, and its metabolites, 1-(2,4,5trichlorophenyl)-ethanol (free and conjugated forms), 2,4,5- trichloroacetophenone, and 1-(2,4,5trichlorophenyl)-ethanediol in/on the following food commodities:

Commodity

Parts per
million

Expiration/Revocation
Date

Cattle, fat (of which no more than 0.1
ppm is tetrachlorvinphos
per se
)

0.2

3/17/10

Cattle, kidney (of which no more than
0.05 ppm is tetrachlorvinphos
per se
)

1.0

3/17/10

Cattle, liver (of which no more than
0.05 ppm is tetrachlorvinphos
per se
)

0.5

3/17/10

Cattle, meat (of which no more than
2.0 ppm is tetrachlorvinphos
per se
)

2.0

3/17/10

Cattle, meat by products, except
kidney and liver

1.0

3/17/10

Egg (of which no more than 0.05 ppm
is tetrachlorvinphos per
se
)

0.2

3/17/10

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Hog, fat (of which no more than 0.1
ppm is tetrachlorvinphos
per se
)

0.2

3/17/10

Hog, kidney (of which no more than
0.05 ppm is tetrachlorvinphos
per se
)

1.0

3/17/10

Hog, liver (of which no more than 0.05
ppm is tetrachlorvinphos
per se
)

0.5

3/17/10

Hog, meat (of which no more than 2.0
ppm is tetrachlorvinphos
per se
)

2.0

3/17/10

Hog, meat byproducts, except kidney
and liver

1.0

3/17/10

Milk, fat (reflecting negligible residues
in whole milk and of which no more
than 0.05 ppm is tetrachlorvinphos
per se
)

0.05

3/17/10

Poultry, fat (of which no more than
7.0 ppm is tetrachlorvinphos
per se
)

7.0

3/17/10

Poultry, liver (of which no more than
0.05 ppm is tetrachlorvinphos
per se
)

2.0

3/17/10

Poultry, meat (of which no more than
3.0 ppm is tetrachlorvinphos
per se
)

3.0

3/17/10

Poultry, meat byproducts, except liver

2.0

3/17/10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 39053, July 21, 1999, as amended at 65 FR 33697, May 24, 2000; 67 FR 49616, July 31, 2002; 73
FR 53738, Sept. 17, 2008]

§ 180.253 Methomyl; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide methomyl ( S -methyl N [(methylcarbamoyl)oxy] thioacetimidate) in or on the food commodities as follows:

Commodity

Parts per million

Alfalfa

10

Apple

1

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Asparagus

2

Avocado

2

Barley, grain

1

Barley, hay

10

Barley, straw

10

Bean, dry, seed
Bean, forage

0.1(N)
10

Bean, succulent

2

Beet, garden, tops

6

Bermudagrass, forage

10

Bermudagrass, hay

40

Blueberry

6

Broccoli

3

Brussels sprouts

2

Cabbage

5

Cabbage, chinese

5

Cauliflower

2

Celery

3

Collards

6

Corn, forage
Corn, grain (inc pop)
Corn, stover

10
0.1(N)
10

Corn, sweet, kernel plus cob with husks removed

0.1(N)

Cotton, undelinted seed

0.1(N)

Cucurbits

0.2(N)

Dandelion, leaves

6

Endive

5

Grapefruit

2

Grape

5

Hop, dried cones1

12

Kale

6

Leek

3.0

Lemon
Lentil, seed

2
0.1

Lettuce

5

Mint, hay

2

Mustard greens

6

Nectarine

5

Oat, forage

10

Oat, grain

1

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Oat, hay

10

Oat, straw

10

Onion, green

3

Orange, sweet

2

Parsley, leaves

6

Pea

5

Pea, field, vines
Peach
Peanut
Pecan
Pepper
Pomegranate

10
5
0.1(N)
0.1
2
0.2(N)

Rye, forage

10

Rye, grain

1

Rye, straw

10

Sorghum, forage

1

Sorghum, grain

0.2(N)

Soybean

0.2(N)

Soybean, forage

10

Spinach

6

Strawberry

2

Swiss chard

6

Tangerine

2

Tomato

1

Turnip, greens

6

Vegetable, brassica, leafy, group 5

6.0

Vegetable, fruiting

0.2(N)

Vegetables, leafy [exc. beet (tops), broccoli, Brussels sprouts,
cabbage, cabbage, Chinese, cauliflower, celery, collards, dandelions,
endive (escarole), kale, lettuce, mustard greens, parsley, spinach,
Swiss chard, turnip, greens (tops), and watercress]

0.2(N)

Vegetable, root

0.2(N)

Watercress

6

Wheat, forage

10

Wheat, grain

1

Wheat, hay

10

Wheat, straw

10

1There

are no U.S. registrations for use of methomyl on hop, dried cone, as of February 14, 1990.

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for residues of methomyl in or on the following food commodities:

Commodity

Parts per million

Pear

4

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33697, May 24, 2000, as amended at 72 FR 35666, June 29, 2007]

§ 180.254 Carbofuran; tolerances for residues.
top
(a) General. Tolerances are established for the combined residues of the insecticide carbofuran (2,3dihydro-2,2-dimethyl-7-benzofuranyl- N -methylcarbamate), its carbamate metabolite-2,3-dihydro-2,2dimethyl-3-hydroxy-7-benzofuranyl- N -methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2dimethyl-7-benzofuranol, 2,3-dihydro-2,2-dimethyl-3,-oxo-7-benzofuranol and 2,3-dihydro-2,2-dimethyl-3,7benzofurandiol in or on the following raw agricultural commodities:

Commodity

Parts per million
(ppm)

Expiration/Revocation date

Alfalfa, forage (of which no more
than 5 ppm are carbamates)

10

12/31/09

Alfalfa, hay (of which no more
than 20 ppm are carbamates)

40

12/31/09

Banana

0.1

12/31/09

Barley, grain (of which not more
than 0.1 ppm is carbamates)

0.2

12/31/09

Barley, straw (of which no more
than 1.0 ppm is carbamates)

5.0

12/31/09

Beet, sugar, roots

0.1

12/31/09

2

12/31/09

0.1

12/31/09

Corn, forage (of which no more
than 5 ppm are carbamates)

25

12/31/09

Corn, grain (including popcorn)
(of which no more than 0.1 ppm
is carbamates)

0.2

12/31/09

Corn, stover (of which no more
than 5 ppm are carbamates)

25

12/31/09

Corn, sweet, kernel plus cob with
husks removed (of which no more
than 0.2 ppm is carbamates)

1.0

12/31/09

Cotton, undelinted seed (of which
no more than 0.2 ppm is
carbamates)

1.0

12/31/09

Beet, sugar, tops (of which no
more than 1 ppm is carbamates)
Coffee, bean, green

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Cranberry (of which no more than
0.3 ppm is carbamates)

0.5

12/31/09

Cucumber (of which not more
than 0.2 ppm is carbamates)

0.4

12/31/09

Grape (of which no more than 0.2
ppm is carbamates)

0.4

12/31/09

Grape, raisin (of which no more
than 1.0 ppm is carbamate

2.0

12/31/09

Grape, raisin, waste (of which no
more than 3.0 ppm is carbamates

6.0

12/31/09

Melon (of which not more than
0.2 ppm is carbamates)

0.4

12/31/09

Milk (of which no more than 0.02
ppm is carbamates)

0.1

12/31/09

Oat, grain (of which not more
than 0.1 ppm is carbamates)

0.2

12/31/09

Oat, straw (of which not more
than 1.0 ppm is carbamates)

5.0

12/31/09

Pepper (of which no more than
0.2 ppm is carbamates)

1

12/31/09

Potato (of which no more than 1
ppm is carbamates)

2

12/31/09

Pumpkin (of which not more than
0.6 ppm is carbamates)

0.8

12/31/09

Rice, grain

0.2

12/31/09

Rice, straw (of which no more
than 0.2 ppm is carbamates)

1

12/31/09

Sorghum, forage (of which no
more than 0.5 ppm is carbamates)

3

12/31/09

0.1

12/31/09

3

12/31/09

Strawberry (of which no more
than 0.2 ppm is carbamates)

0.5

12/31/09

Soybean (of which not more than
0.2 ppm is carbamates)

1.0

12/31/09

Soybean, forage (of which not
more than 20.0 ppm are
carbamates)

35.0

12/31/09

Soybean, hay (of which not more
than 20.0 ppm are carbamates)

35.0

12/31/09

Squash (of which not more than
0.6 ppm is carbamates)

0.8

12/31/09

Sugarcane, cane

0.1

12/31/09

Sorghum, grain, grain
Sorghum, grain, stover (of which
no more than 0.5 ppm is
carbamates)

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Sunflower, seed (of which not
more than 0.5 ppm is carbamates)

1.0

12/31/09

Wheat, grain (of which not more
than 0.1 ppm is carbamates)

0.2

12/31/09

Wheat, straw (of which not more
than 1.0 ppm is carbamates)

5.0

12/31/09

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. Tolerances with regional registration, as defined in §180.1(n), are
established for the combined residues of the insecticide carbofuran (2,3-dihydro-2,2-dimethyl-7benzofuranyl- N -methylcarbamate), its carbamate metabolite 2,3-dihydro-2,2-dimethyl-3-hydroxy-7benzofuranyl- N -methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7-benzofuranol,
2,3-dihydro-2,2-dimethyl-3-oxo-7-benzofuranol, and 2,3-dihydro-2,2-dimethyl-3,7-benzofurandiol in or on
the following raw agricultural commodity:

Commodity

Parts per million
(ppm)

Artichoke, globe (of which not
more than 0.2 ppm is carbamates)

Expiration/Revocation date

0.4

12/31/09

(d) Indirect or inadvertent residues. [Reserved]
[39 FR 20597, June 12, 1974]
Editorial Note: ForFederal Registercitations affecting §180.254, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.257 Chloroneb; tolerances for residues.
top
(a) General . Tolerances are established for residues of the fungicide chloroneb (1,4-dichloro-2,5dimethoxybenzene) and its metabolite 2,5-dichloro-4-methoxyphenol (free and conjugated), calculated as
chloroneb, in or on the following raw agricultural commodities:

Commodity

Parts per million

Bean, dry, seed

0.2

Bean, succulent

0.2

Beet, sugar, roots

0.2

Beet, sugar, tops

0.2

Cowpea, forage

2.0

Cowpea, hay

2.0

Cattle, fat

0.2

Cattle, meat

0.2

Cattle, meat byproducts

0.2

Cotton, gin byproducts

1.0

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Cotton, undelinted seed

0.2

Goat, fat

0.2

Goat, meat

0.2

Goat, meat byproducts

0.2

Hog, fat

0.2

Hog, meat

0.2

Hog, meat byproducts

0.2

Horse, fat

0.2

Horse, meat

0.2

Horse, meat byproducts

0.2

Milk

0.05

Sheep, fat

0.2

Sheep, meat

0.2

Sheep, meat byproducts

0.2

Soybean, forage

2.0

Soybean, hay

2.0

Soybean, seed

0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003, as amended at 72 FR 53460, Sept. 19, 2007]

§ 180.258 Ametryn; tolerances for residues.
top
(a) General. Tolerances are established for residues of the desiccant and herbicide (2-ethylamino)-4(isopropylamino)-6-(methylthio)- s -triazine in or on the following raw agricultural commodities:

Commodity
Banana

Parts per million
0.25

Corn, field, forage

0.1

Corn, field, grain

0.05

Corn, field, stover

0.05

Corn, pop, grain

0.05

Corn, pop, stover

0.05

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Pineapple
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0.5
0.25
0.5
0.05

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Sugarcane, cane

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[43 FR 29121, July 6, 1978, as amended at 48 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, 1983; 52
FR 33237, Sept. 2, 1987; 63 FR 57075, Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008]

§ 180.259 Propargite; tolerances for residues.
top
(a) General. Tolerances are established for residues of the pesticide propargite (2-( p-tert -butylphenoxy)
cyclohexyl 2-propynyl sulfite) in or on the following food commodities.

Commodity

Parts per million

Almond
Almond, hulls

0.1
55.0

Bean, dry, seed

0.2

Cattle, fat

0.1

Cattle, meat

0.1

Cattle, meat byproducts

0.1

Citrus, oil

30.0

Corn, field, forage

10.0

Corn, field, grain

0.1

Corn, field, stover

10.0

Corn, pop, grain

0.1

Corn, pop, stover

10.0

Corn, sweet, forage

10.0

Corn, sweet, stover

10.0

Cotton, undelinted seed

0.1

Egg

0.1

Goat, fat

0.1

Goat, meat

0.1

Goat, meat byproducts

0.1

Grain, aspirated fractions

0.4

Grape

10.0

Grapefruit

5.0

Hog, fat

0.1

Hog, meat

0.1

Hog, meat byproducts

0.1

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Hop, dried cones

100.0

Horse, fat

0.1

Horse, meat

0.1

Horse, meat byproducts

0.1

Lemon

5.0

Milk, fat (0.08 ppm in milk)

2.0

Nectarine

4.0

Orange

10.0

Peanut

0.1

Peppermint, tops

50.0

Poultry, fat

0.1

Potato

0.1

Sheep, fat

0.1

Sheep, meat

0.1

Sheep, meat byproducts

0.1

Sorghum, grain, forage

10.0

Sorghum, grain, grain

5.0

Sorghum, grain, stover

10.0

Spearmint, tops

50.0

Tea, dried

10.0

Walnut

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for residues of propargite in or on the following raw agricultural commodities:

Commodity

Parts per million

Corn, sweet, kernel plus cob with husks removed

0.1

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33710, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008]

§ 180.261 N
-(Mercaptomethyl) phthalimide S
-( O,O
phosphorodithioate) and its oxygen analog; tolerances for residues.

-dimethyl

top
(a) General. Tolerances are established for the sum of the residues for the insecticide N (mercaptomethyl) phthalimide S- ( O,O -dimethyl phosphorodithioate) and its oxygen analog N (mercaptomethyl) phthalimide S -( O,O -dimethyl phosphorothioate) in or on the following raw agricultural
commodities:

Commodity

Parts per million

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Alfalfa

40

Almond, hulls

10

Apple

10

Apricot

5

Blueberry

10

Cattle, fat

0.2

Cattle, meat

0.2

Cattle, meat byproducts

0.2

Cherry
Cotton, undelinted seed
Cranberry

10
0.1
10

Fruit, citrus

5

Goat, fat

0.2

Goat, meat byproducts

0.2

Goat, meat

0.2

Grape

10

Hog, fat

0.2

Hog, meat byproducts

0.2

Hog, meat

0.2

Horse, fat

0.2

Horse, meat byproducts

0.2

Horse, meat

0.2

Kiwifruit

25

Nectarine

5

Nut

0.1(N)

Peach

10

Pear

10

Pea

0.5

Pea, field, hay

10

Pea, field, vines

10

Plum, prune, fresh

5

Potato

0.1

Sheep, fat

0.2

Sheep, meat byproducts

0.2

Sheep, meat

0.2

Sweet potato, roots

10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for the sum of the residue for the insecticide N -(mercaptomethyl) phthalimide S- ( O,O dimethyl phosphorodithioate) and its oxygen analog N -(mercaptomethyl) phthalimide S- ( O,O -dimethyl

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phosphorothioate) in or on the following raw agricultural commodity:

Commodity

Parts per million

Crabapple

20

Pistachio

0.1

(d) Indirect or inadvertent residues. [Reserved]
[43 FR 46538, Oct. 10, 1978, as amended at 45 FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, 1983; 52
FR 48539, Dec. 23, 1987; 53 FR 657, Jan. 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Oct. 26,
1998; 67 FR 49616, July 31, 2002]

§ 180.262 Ethoprop; tolerances for residues.
top
(a) General. Tolerances are established for residues of the nematocide and insecticide ethoprop ( O -ethyl
S,S -dipropyl phosphorodithioate) in or on the following raw agricultural commodities:

Commodity

Parts per million

Banana

0.02

Bean, lima

0.02

Bean, snap, succulent

0.02

Cabbage

0.02

Corn, forage

0.02

Corn, grain

0.02

Corn, stover

0.02

Corn, sweet, kernel plus cob with husks removed

0.02

Cucumber

0.02

Hop, dried cones

0.02

Peppermint, tops

0.02

Pineapple

0.02

Potato

0.02

Spearmint, tops

0.02

Sugarcane, cane

0.02

Sweet potato, roots

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 53004, Nov. 24, 1982, as amended at 48 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 1987; 53
FR 30053, Aug. 10, 1988; 63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR 38955, July
26, 2001; 67 FR 49616, July 31, 2002; 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. 24, 2008]

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§ 180.263 Phosalone; tolerances for residues.
top
Tolerances are established for residues of the insecticide phosalone ( S -(6-chloro-3-(mercaptomethyl)-2benzoxazolinone) O,O, -diethyl phosphorodithioate) in or on the following raw agricultural commodities:

Commodity

Parts per million

Almond

0.1

Apple

10.0

Apricot

15.0

Cherry

15.0

Grape

10.0

Peach

15.0

Pear

10.0

Plum, prune, fresh

15.0

[47 FR 42740, Sept. 29, 1982, as amended at 63 FR 57066, Oct. 26, 1998; 64 FR 3428, Jan. 22, 1999; 67
FR 49616, July 31, 2002]

§ 180.269 Aldicarb; tolerances for residues.
top
(a) General. Tolerances are established for combined residues of the insecticide and nematocide aldicarb
(2-methyl-2-(methylthio)propionaldehyde O -(methylcarbamoyl) oxime and its cholinesterase-inhibiting
metabolites 2-methyl 2-(methylsulfinyl) propionaldehyde O -(methylcarbamoyl) oxime and 2-methyl-2(methylsulfonyl) propionaldehyde O -(methylcarbamoyl) oxime in or on the following food commodities:

Commodity

Parts per million

Bean, dry, seed
Beet, sugar, roots

0.1
0.05

Beet, sugar, tops

1

Citrus, dried pulp

0.6

Coffee, bean, green

0.1

Cotton, undelinted seed

0.1

Cotton, hulls

0.3

Grapefruit

0.3

Lemon

0.3

Lime

0.3

Orange, sweet

0.3

Peanut

0.05

Pecan

0.5

Potato

1

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Sorghum, grain, bran

0.5

Sorghum, grain, grain

0.2

Sorghum, grain, stover

0.5

Soybean

0.02

Sugarcane, cane

0.02

Sweet potato, roots

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33710, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, 2008]

§ 180.272 Tribuphos; tolerances for residues.
top
(a) General. Tolerances are established for residues of the defoliant tribuphos ( S,S,S -tributyl
phosphorotrithioate) in or on food commodities as follows:

Commodity

Parts per million

Cattle, fat

0.15

Cattle, meat

0.02

Cattle, meat byproducts

0.02

Cotton, gin byproducts

40.0

Cotton, undelinted seed

4.0

Goat, fat

0.15

Goat, meat

0.02

Goat, meat byproducts

0.02

Hog, fat

0.15

Hog, meat

0.02

Hog, meat byproducts

0.02

Horse, fat

0.15

Horse, meat

0.02

Horse, meat byproducts

0.02

Milk

0.01

Sheep, fat

0.15

Sheep, meat

0.02

Sheep, meat byproducts

0.02

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33698, May 24, 2000, as amended at 67 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, 2007]

§ 180.274 Propanil; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the herbicide propanil (3', 4'dichloropropionanilide) and its metabolites convertible to 3, 4-dichloroaniline (3, 4-DCA) in or on the
following food commodities:

Commodity

Parts per million

Cattle, fat

0.10

Cattle, meat

0.05

Cattle, meat byproducts

1.0

Crayfish

0.05

Egg

0.30

Goat, fat

0.10

Goat, meat

0.05

Goat, meat byproducts

1.0

Hog, fat

0.10

Hog, meat

0.05

Hog, meat byproducts

1.0

Horse, fat

0.10

Horse, meat

0.05

Horse, meat byproducts

1.0

Milk

0.05

Poultry, fat

0.05

Poultry, meat

0.10

Poultry, meat byproducts

0.50

Rice, bran

40

Rice, grain

10

Rice, hulls

30

Rice, straw

75

Sheep, fat

0.10

Sheep, meat

0.05

Sheep, meat byproducts
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34827, June 26, 1998, as amended at 72 FR 28888, May 23, 2007]

§ 180.275 Chlorothalonil; tolerances for residues.
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(a) General. (1) Tolerances are established for the fungicide chlorothalonil (tetrachloroisophthalonitrile)
and its metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.

Commodity
Almond

Parts per million
0.05

Almond, hulls

1.0

Apricot

0.5

Asparagus

0.1

Banana (NMT 0.05 ppm in edible pulp)

0.5

Bean, dry, seed

0.1

Bean, snap, succulent

5

Blueberry

1.0

Brassica, head and stem, subgroup 5A

5.0

Carrot, roots
Celery

1
15

Cherry, sweet

0.5

Cherry, tart

0.5

Cocoa bean, dried bean

0.05

Coffee, bean, green

0.20

Corn, sweet, kernel plus cob with husks removed

1

Cranberry

5.0

Ginseng

4.0

Horseradish

4.0

Lentil

0.10

Lychee

15

Mango

1.0

Mushroom

1.0

Nectarine

0.5

Okra

6.0

Onion, bulb

0.5

Onion, green
Papaya

5
15

Parsnip, roots

1

Passionfruit

3

Pea, edible podded

5

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Peach

0.5

Peanut

0.3

Pistachio

0.2

Plum

0.2

Plum, prune

0.2

Potato

0.1

Rhubarb

4.0

Soybean

0.2

Starfruit

3.0

Tomato

5

Vegetable, cucurbit, group 9

5.0

Vegetable, fruiting, group 8, except tomato

6.0

Yam, true

0.10

(2) Tolerances are established for the metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the
following food commodities.

Commodity

Parts per million

Cattle, fat

0.1

Cattle, kidney

0.5

Cattle, meat byproducts, except kidney

0.05

Cattle, meat

0.03

Goat, fat

0.1

Goat, kidney

0.5

Goat, meat byproducts, except kidney

0.05

Goat, meat

0.03

Hog, fat

0.1

Hog, kidney

0.5

Hog, meat byproducts, except kidney

0.05

Hog, meat

0.03

Horse, fat

0.1

Horse, kidney

0.5

Horse, meat byproducts, except kidney

0.05

Horse, meat

0.03

Milk

0.1

Sheep, fat

0.1

Sheep, kidney

0.5

Sheep, meat byproducts, except kidney

0.05

Sheep, meat

0.03

(b) Section 18 emergency exemptions . [Reserved]

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(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for the combined residues of chlorothalonil and its metabolite in or on the following raw
agricultural commodities:

Commodity

Parts per million

Hazelnut

0.1

Mint hay

2

Persimmon

1.5

(d) Indirect or inadvertent residues. [Reserved]
[42 FR 56114, Oct. 21, 1977]
Editorial Note: ForFederal Registercitations affecting §180.275, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.276 Formetanate hydrochloride; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide formetanate hydrochloride (m[[dimethylamino)methylene]amino ]phenyl methylcarbamate hydrochloride) in or on raw agricultural
commodities as follows:

Commodity

Parts per million

Apple

0.50

Apple, wet pomace

1.5

Grapefruit

1.5

Lemon

0.60

Lime

0.03

Nectarine

0.40

Orange

1.5

Peach

0.40

Pear

0.50

Tangelo

0.03

Tangerine

0.03

(b) Section 18 emergency exemptions. A time-limited tolerance is established for residues of the
insecticide formetanate hydrochloride ( m -[[(dimethylamino) methylene]amino ]phenyl methylcarbamate
hydrochloride) in connection with use of the pesticide under section 18 emergency exemptions granted by
EPA. The tolerances in this paragraph will expire and are revoked on the date specified in the following
table.

Commodity
Onion, dry bulb

Parts per million

Expiration/revocation date

0.02

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34827, June 26, 1998, as amended at 69 FR 43924, July 23, 2004; 73 FR 9232, Feb. 20, 2008; 73
FR 52613, Sept. 10, 2008; 74 FR 636, Jan. 7, 2009]

§ 180.278 Phenmedipham; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the herbicide phenmedipham (3methoxycarbonylaminophenyl-3'-methylcarbanilate) in or on the following food commodities:

Commodity

Parts per million

Beet, garden, roots

0.2

Beet, garden, tops

0.2

Beet, sugar, dried pulp

0.5

Beet, sugar, molasses

0.2

Beet, sugar, roots

0.1

Beet, sugar, tops

0.1

Spinach

4.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 28888, May 23, 2007]

§ 180.284 Zinc phosphide; tolerances for residues.
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(a) General. Tolerances are established for residues of the phosphine resulting from the use of the
rodenticide zinc phosphide in or on the raw agricultural commodities as follows:

Commodity

Parts per million

Alfalfa, forage

0.2

Alfalfa, hay

0.2

Barley, grain

0.05

Barley, hay

0.2

Barley, straw

0.2

Bean, dry, seed

0.05

Beet, sugar, roots

0.05

Beet, sugar, tops

0.2

Grape
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Grass (rangeland)

0.1

Potato

0.05

Sugarcane, cane

0.01

Timothy, hay

0.5

Timothy, forage

0.5

Wheat, forage

0.05

Wheat, grain

0.05

Wheat, hay

0.05

Wheat, straw

0.05

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of phosphine
resulting from the use of the rodenticide zinc phosphide in connection with use of the pesticide under
FIFRA section 18 emergency exemptions granted by EPA. The tolerances are specified in the following
table. The tolerances expire on the date specified in the table.

Commodity

Parts per million

Expiration/Revocation Date

Alfalfa, forage

1.0

12/31/05

Alfalfa, hay

1.0

12/31/05

Clover, forage

0.1

12/31/05

Clover, hay

0.1

12/31/05

Timothy, seed

0.1

12/31/05

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for residues of phosphine resulting from the use of the rodenticide zinc phosphide in or on
the following raw agricultural commodities as follows:

Commodity

Parts per million

Artichoke, globe

0.01

Beet, sugar, roots

0.04

Beet, sugar, tops

0.02

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 45182, Aug. 25, 1998, as amended at 63 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, 1999; 64
FR 61791, Nov. 15, 1999; 65 FR 8874, Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR 62634, Oct.
19, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, 2003; 70 FR
7046, Feb. 10, 2005]

§ 180.287 Amitraz; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide amitraz (N'-[2,4-dimethylphenyl]-N[[(2,4-dimethylphenyl)imino] methyl]]- N-methylmethanimidamide) and its metabolites containing the 2,4dimethylaniline moiety (calculated as the parent) in or on the following food commodities:

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Commodity

Parts per million

Cattle, fat

0.1

Cattle, meat

0.02

Cattle, meat byproducts

0.2

Cotton, undelinted seed1

1.0

Hog, fat

0.1

Hog, kidney

0.1

Hog, liver

0.1

Hog, meat

0.05

Hog, meat byproducts

0.3

Milk

0.03

Milk, fat

0.2

Pear

3.0

1There

are no U.S. registrations on cottonseed as of May 3, 2006.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[44 FR 70145, Dec. 6, 1979, as amended at 51 FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57
FR 53568, Nov. 12, 1992; 58 FR 14316, Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31,
2002; 72 FR 53454, Sept. 19, 2007]

§ 180.288 2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.
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(a) General. Tolerances are established for residues of the fungicide 2-(thiocyanomethylthio)benzothiazole
in or on the following food commodities:

Commodity

Parts per million

Barley, grain

0.1(N)

Barley, straw

0.1(N)

Beet, sugar, roots

0.1(N)

Beet, sugar, tops

0.1(N)

Corn, field, forage

0.1(N)

Corn, grain

0.1(N)

Corn, stover

0.1(N)

Cotton, forage

0.1(N)

Cotton, undelinted seed

0.1(N)

Oat, forage

0.1(N)

Oat, grain

0.1(N)

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Oat, hay

0.1(N)

Oat, straw

0.1(N)

Rice, grain

0.1(N)

Rice, straw

0.1(N)

Safflower, seed

0.1(N)

Sorghum, grain, forage

0.1(N)

Sorghum, grain, grain

0.1(N)

Sorghum, grain, stover

0.1(N)

Wheat, forage

0.1(N)

Wheat, grain

0.1(N)

Wheat, hay

0.1(N)

Wheat, straw

0.1(N)

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003]

§ 180.289 Methanearsonic acid; tolerances for residues.
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(a) General. Tolerances are established for residues of the herbicide methanearsonic acid (calculated as
As2O3) from application of the disodium and monosodium salts of methanearsonic acid in or on raw
agricultural commodities as follows:

Commodity

Parts per million

Cotton, undelinted seed

0.7

Cotton, hulls

0.9

Fruit, citrus

0.35

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34828, June 26, 1998]

§ 180.291 Pentachloronitrobenzene; tolerance for residues.
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(a) A tolerance of 0.1 part per million is established for negligible residues of the fungicide
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pentachloronitrobenzene in or on the raw agricultural commodity cotton, undelinted seed.
(b) Tolerances with regional registration (refer to §180.1 (n)) are established for the combined residues of
the fungicides pentachloronitrobenzene (PCNB) and its metabolites pentachloroaniline (PCA) and methyl
pentachlorophenyl sulfide (MPCPS) in or on the following raw agricultural commodities:

Commodity

Parts per million

Collards

0.2

Kale

0.2

Mustard greens

0.2

[36 FR 22540, Nov. 25, 1971, as amended at 53 FR 9443, Mar. 23, 1988; 71 FR 74816, Dec. 13, 2006]

§ 180.292 Picloram; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the pesticide picloram (4-amino-3,5,6trichloropicolinic acid) from its application in the acid form or in the form of its potassium, triethylamine, or
triisopropanolamine salts expressed as picloram in or on the following raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.5

Barley, straw

1.0

Cattle, fat

0.2

Cattle, kidney

5.0

Cattle, liver

0.5

Cattle, meat

0.2

Cattle, meat byproducts, except kidney and liver

0.2

Egg

0.05

Goat, fat

0.2

Goat, kidney

5.0

Goat, liver

0.5

Goat, meat

0.2

Goat, meat byproducts, except kidney and liver

0.2

Grain, aspirated fractions

4.0

Grass, forage

80.0

Hog, fat

0.2

Hog, kidney

5.0

Hog, liver

0.5

Hog, meat

0.2

Hog, meat byproducts, except kidney and liver

0.2

Horse, fat

0.2

Horse, kidney

5.0

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Horse, liver

0.5

Horse, meat

0.2

Horse, meat byproducts, except kidney and liver

0.2

Milk

0.05

Oat, forage

1.0

Oat, grain

0.5

Oat, straw

1.0

Poultry, fat

0.05

Poultry, meat

0.05

Poultry, meat byproducts

0.05

Sheep, fat

0.2

Sheep, kidney

5.0

Sheep, liver

0.5

Sheep, meat

0.2

Sheep, meat byproducts, except kidney and liver

0.2

Wheat, forage

1.0

Wheat, grain

0.5

Wheat, straw

1.0

(2) Tolerances are established for residues of picloram [4-amino-3,5,6-trichloropicolinic acid] resulting from
the application of the pesticide to growing crops in the following:

Commodity

Parts per million

Barley, pearled barley

3.0

Oat, groats/rolled oats

3.0

Wheat, bran

3.0

Wheat, germ

3.0

Wheat, middlings

3.0

Wheat, shorts

3.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[41 FR 19221, May 11, 1976, as amended at 47 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; 64
FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, 2007]

§ 180.293 Endothall; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of endothall, 7-oxabicyclo [2, 2, 1]
heptane-2, 3-dicarboxylic acid and its monomethyl ester in or on the following food commodities:
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Commodity

Parts per million

Cotton, undelinted seed

0.1

Fish

0.1

Hop, dried cones

0.1

Potato

0.1

Rice, grain

0.05

Rice, straw

0.05

(2) An interim tolerance of 0.2 parts per million is established for residues of the herbicide endothall (7 oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in water, potable from use of its potassium, sodium, di- N,
N -dimethylalkylamine, and mono- N-N, -dimethylalkylamine salts as algicides or herbicides to control
aquatic plants in canals, lakes, ponds, and other potential sources of water, potable.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[41 FR 23717, June 11, 1976, as amended at 51 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, 1997; 63
FR 42249, Aug. 7, 1998; 67 FR 35048, May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR 74816, Dec.
13, 2006; 72 FR 52018, Sept. 12, 2007]

§ 180.294 Benomyl; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of the fungicide benomyl (methyl 1(butylcarbamoyl)-2-benzimidazolecarbamate) and its metabolites containing the benzimidazole moiety
(calculated as benomyl) in or on the following raw agricultural commodities:

Commodity

Parts per million Expiration/Revocation Date

Almond, hulls

1.0

1/1/07

Apple, postharvest

7.0

1/1/08

15.0

1/1/08

Banana, postharvest, not more than
0.2 ppm shall be present in the pulp
after peel is removed and discarded

1.0

1/1/08

Barley, grain

0.2

1/1/08

Barley, straw

0.2

1/1/08

Bean

2.0

1/1/07

Beet, sugar, roots

0.2

1/1/07

Beet, sugar, tops

15.0

1/1/07

Blackberry

7.0

1/1/08

Blueberry

7.0

1/1/08

Boysenberry

7.0

1/1/08

Apricot, postharvest

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Broccoli

0.2

1/1/06

15.0

1/1/06

0.2

1/1/06

Cabbage, chinese, bok choy

10.0

1/1/06

Cabbage, chinese, napa

10.0

1/1/06

Carrot, roots

0.2

1/1/07

Cattle, fat

0.1

1/1/08

Cattle, meat

0.1

1/1/08

Cattle, meat byproducts

0.1

1/1/08

Cauliflower

0.2

1/1/06

Celery

3.0

1/1/07

Cherry, postharvest

15.0

1/1/08

Citrus, dried pulp

50.0

1/1/08

Collards

0.2

1/1/06

Corn, sweet, forage

0.2

1/1/08

Corn, sweet, kernel plus cob with
husks removed

0.2

1/1/08

Corn, sweet, stover

0.2

1/1/08

Cucumber

1.0

1/1/07

Currant

7.0

1/1/08

Dewberry

7.0

1/1/08

Egg

0.1

1/1/08

Eggplant

0.2

1/1/09

10.0

1/1/08

Garlic

0.2

1/1/06

Goat, fat

0.1

1/1/08

Goat, meat

0.1

1/1/08

Goat, meat byproducts

0.1

1/1/08

Grape

10.0

1/1/08

Grape, raisin

50.0

1/1/08

Hog, fat

0.1

1/1/08

Hog, meat

0.1

1/1/08

Hog, meat byproducts

0.1

1/1/08

Horse, fat

0.1

1/1/08

Horse, meat

0.1

1/1/08

Horse, meat byproducts

0.1

1/1/08

Kale

0.2

1/1/06

Kohlrabi

0.2

1/1/06

Loganberry

7.0

1/1/08

Mango

3.0

1/1/08

Melon

1.0

1/1/07

Brussels sprouts
Cabbage

Fruit, citrus, postharvest

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Milk

0.1

1/1/08

10.0

1/1/08

0.2

1/1/06

15.0

1/1/08

Nut

0.2

1/1/07

Oat, grain

0.2

1/1/08

Oat, straw

0.2

1/1/08

15.0

1/1/08

0.2

1/1/08

15.0

1/1/08

Pear, postharvest

7.0

1/1/08

Pepper

0.2

1/1/09

35.0

1/1/08

0.2

1/1/07

Plum, postharvest

15.0

1/1/08

Plum, prune, fresh, postharvest

15.0

1/1/08

Poultry, fat

0.1

1/1/08

Poultry, liver

0.2

1/1/08

Poultry, meat

0.1

1/1/08

Poultry, meat byproducts, except
liver

0.1

1/1/08

Pumpkin

1.0

1/1/07

Raspberry

7.0

1/1/08

Rice, grain

5.0

1/1/08

Rice, hulls

20.0

1/1/08

Rice, straw

15.0

1/1/08

Rutabaga

0.2

1/1/07

Rye, grain

0.2

1/1/08

Rye, straw

0.2

1/1/08

Sheep, fat

0.1

1/1/08

Sheep, meat

0.1

1/1/08

Sheep, meat byproducts

0.1

1/1/08

Soybean

0.2

1/1/07

Spinach

0.2

1/1/07

Squash, summer

1.0

1/1/07

Squash, winter

1.0

1/1/07

Strawberry

5.0

1/1/08

Sweet potato, roots

0.2

1/1/07

Tomato

5.0

1/1/09

50.0

1/1/09

0.2

1/1/07

Mushroom, postharvest
Mustard greens
Nectarine, postharvest

Peach, postharvest
Peanut
Peanut, hay

Pineapple, postharvest
Pistachio

Tomato, concentrated products
Turnip, roots

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Wheat, grain

0.2

1/1/08

Wheat, straw

15.0

1/1/08

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for residues of the fungicide benomyl (methyl 1-[butylcarbamoyl]-2benzimidazolecarbamate) and its metabolites containing the benzimidazole moiety (calculated as
benomyl) in or on the raw agricultural commodities.

Commodity

Parts per million

Avocado

Expiration/Revocation Date

3.0

1/1/08

10.0

1/1/07

Papaya

3.0

1/1/08

Pistachio

0.2

1/1/07

Turnip, greens

6.0

1/1/07

10.0

1/1/07

Dandelion, leaves

Watercress
(d) Indirect or inadvertent residues. [Reserved]

[52 FR 58536, Dec. 23, 1987, as amended at 52 FR 58538, Dec. 23, 2987; 53 FR 9024, Mar. 18, 1988; 59
FR 46354, Sept. 8, 1994; 63 FR 2167, Jan. 14, 1998; 67 FR 46905, July 17, 2002]

§ 180.296 Dimethyl phosphate of 3-hydroxy- N
crotonamide; tolerances for residues.

-methyl- cis

-

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(a) General. Tolerances are established for residues of the insecticide Dimethyl phosphate of 3-hydroxy- N
-methyl- cis -crotonamide in or on the following raw agricultural commodities:

Commodity

Parts per million

Cotton, undelinted seed

Expiration/Revocation date

0.1

12/31/00

Peanut

0.05

12/31/00

Potato

0.1

12/31/00

Sugarcane, cane

0.1

12/31/00

Tomato

0.5

12/31/00

Tomato, concentrated products

2.0

12/31/00

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 19492, Apr. 21, 1999]

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§ 180.297

N

-1-Naphthyl phthalamicacid; tolerances for residues.

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(a) General. Tolerances are established for residues of the herbicide N -1-naphthyl phthalamic acid from
application of its sodium salt in or on the following raw agricultural commodities:

Commodity

Parts per million

Cantaloupe

0.1(N)

Cucumber

0.1(N)

Muskmelon

0.1(N)

Watermelon

0.1(N)

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 32306, May 16, 1980, as amended at 63 FR 57075, Oct. 26, 1998]

§ 180.298 Methidathion; tolerances for residues.
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(a) General. Tolerances are established for residues of the insecticide methidathion ( O,O -dimethyl
phosphorodithioate, S -ester with 4-(mercaptomethyl-2-methoxy-1,3,4-thiadiazolin-5-one) in or on the
following raw agricultural commodities:

Commodity
Almond, hulls
Artichoke, globe
Citrus, oil

Parts per million
6.0
0.05
420.0

Cotton, undelinted seed

0.2

Fruit, citrus, group 10, except tangerine

4.0

Fruit, pome, group 11

0.05

Fruit, stone, group 12

0.05

Mango

0.05

Nut, tree, group 14

0.05

Olive

0.05

Safflower, seed

0.5

Sorghum, forage, forage

2.0

Sorghum, grain, forage

2.0

Sorghum, grain, grain

0.2

Sorghum, grain, stover

2.0

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Sunflower, seed

0.5

Tangerine

6.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for residues of the insecticide methidathion (O,O-dimethyl phosphorodithioate, S-ester
with 4-(mercaptomethyl-2-methoxy-1,3,4-thiadiazolin-5-one), in or on the following raw agricultural
commodity:

Commodity

Parts per million

Expiration/Revocation Date

Alfalfa, forage

5.0

3/31/08

Alfalfa, hay

5.0

3/31/08

Kiwifruit

0.1

None

Longan

0.1

None

Starfruit

0.1

None

Sugar apple

0.2

None

Timothy, forage

5.0

3/31/08

Timothy, hay

5.0

3/31/08

(d) Indirect or inadvertent residues. [Reserved]
[43 FR 44845, Sept. 29, 1978, as amended at 43 FR 45363, Oct. 2, 1978; 46 FR 18314, Mar. 24, 1981; 50
FR 1054, Jan. 9, 1985; 50 FR 5070, Feb. 6, 1985; 53 FR 23391, June 22, 1988; 54 FR 20125, May 10,
1989; 55 FR 2377, Jan. 24, 1990; 55 FR 24083, June 14, 1990; 55 FR 49389, Nov. 28, 1990; 57 FR
31325, July 15, 1992; 63 FR 57075, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 72 FR 53460, Sept. 19,
2007]

§ 180.299 Dicrotophos; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide dicrotophos, dimethyl phosphate of
3-hydroxy- N , N -dimethyl-cis-crotonamide, in or on the following food commodities:

Commodity

Parts per million

Cotton, gin byproducts

2.0

Cotton, undelinted seed

0.2

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 52613, Sept. 10, 2008]

§ 180.300 Ethephon; tolerances for residues.

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(a) General. Tolerances are established for residues of the plant regulator ethephon [(2-chloroethyl)
phosphonic acid] in or on food commodities as follows:

Commodity
Apple

Parts per million
5.0

Apple, juice

10.0

Barley, bran

5.0

Barley, grain

2.0

Barley, straw

10.0

Blackberry

30.0

Blueberry

20.0

Cantaloupe
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Cherry
Coffee, bean, green
Cotton, gin byproducts

2.0
0.02
1.0
0.02
0.2
10.0
0.5
180.0

Cotton, undelinted seed

6.0

Cucumber

0.1

Egg
Goat, fat
Goat, kidney
Goat, meat

0.002
0.02
1.0
0.02

Goat, meat byproducts, except kidney

0.2

Grape

2.0

Grape, raisin

12.0

Hazelnut

0.80

Hog, fat

0.02

Hog, kidney
Hog, meat
Hog, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Milk
Nut, macadamia
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1.0
0.02
0.2
0.02
1.0
0.02
0.2
0.01
0.5

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Pepper

30.0

Pineapple

2.0

Poultry, fat

0.02

Poultry, liver

0.05

Poultry, meat

0.01

Poultry, meat byproducts, except liver

0.01

Sheep, fat

0.02

Sheep, kidney

1.0

Sheep, meat

0.02

Sheep, meat byproducts, except kidney

0.2

Sugarcane, molasses

1.5

Tomato

2.0

Walnut

0.5

Wheat, bran

5.0

Wheat, germ

5.0

Wheat, grain

2.0

Wheat, middlings

5.0

Wheat, shorts

5.0

Wheat, straw

10.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(n), of
0.1 part per million is established for residues of the plant regulator ethephon [(2-chloroethyl)phosphonic
acid] in or on the food commodity sugarcane.
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33710, May 24, 2000, as amended at 72 FR 53455, Sept. 19, 2007]

§ 180.301 Carboxin; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the fungicide carboxin (5,6-dihydro2-methyl-1,4-oxathiin-3-carboxanilide) and its metabolites determined as aniline and expressed as parent
compound, in or on food commodities as follows:

Commodity

Parts per million

Barley, grain

0.2

Barley, straw

0.2

Bean, dry, seed

0.2

Bean, succulent

0.2

Canola, seed

0.03

Cattle, fat

0.05

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Cattle, meat byproducts
Cattle, meat

0.1
0.05

Corn, field, forage

0.2

Corn, field, grain

0.2

Corn, field, stover

0.2

Corn, pop, grain

0.2

Corn, pop, stover

0.2

Corn, sweet, forage

0.2

Corn, sweet, kernel plus cob with husks removed

0.2

Corn, sweet, stover

0.2

Cotton, undelinted seed

0.2

Egg

0.05

Goat, fat

0.05

Goat, meat byproducts

0.1

Goat, meat

0.05

Hog, fat

0.05

Hog, meat byproducts

0.1

Hog, meat

0.05

Horse, fat

0.05

Horse, meat byproducts

0.1

Horse, meat

0.05

Milk

0.05

Oat, forage

0.5

Oat, grain

0.2

Oat, straw

0.2

Onion, bulb

0.2

Peanut

0.2

Peanut, hay

0.2

Poultry, fat

0.1

Poultry, meat byproducts

0.1

Poultry, meat

0.1

Rice, grain

0.2

Rice, straw

0.2

Safflower, seed

0.2

Sheep, fat
Sheep, meat byproducts
Sheep, meat

0.05
0.1
0.05

Soybean, seed

0.2

Wheat, forage

0.5

Wheat, grain

0.2

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Wheat, straw

0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 FR
4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Dec. 14,
2001; 67 FR 40218, June 12, 2002; 67 FR 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006]

§ 180.303 Oxamyl; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the insecticide oxamyl, methyl N,N dimethyl- N -[(methylcarbamoyl)-oxy]-1-thiooxamimidate, and its oxime metabolite methyl N,N -dimethyl- N
-hydroxy-1-thiooxamimidate calculated as oxamyl in or on the following food commodities:

Commodity
Apple

Parts per million
2

Banana

0.3

Cantaloupe

2.0

Carrot

0.1

Celery

10.0

Cotton, undelinted seed

0.2

Cucumber

2.0

Eggplant

2.0

Fruit, citrus, group 10

3

Garlic, bulb

0.2

Melon, honeydew

2.0

Onion, bulb

0.2

Peanut

0.05

Peanut, hay

2.0

Pear

2.0

Peppermint, tops

10.0

Pepper, bell

2.0

Pepper, nonbell

5.0

Pineapple

1

Pineapple, process residue

2.0

Pumpkin

2.0

Soybean, seed

0.1

Spearmint, tops

10.0

Squash, summer

2.0

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Squash, winter

2.0

Tomato

2

Vegetable, tuberous and corm, subgroup 1C

0.1

Watermelon

2.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54961, Sept. 24, 2008]

§ 180.304 Oryzalin; tolerances for residues.
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(a) General . Tolerances are established for residues of the herbicide oryzalin, 3,5-dinitro- N 4, N 4dipropylsulfanilamide, in or on the following raw agricultural commodities:

Commodity

Parts per million

Almond, hulls

0.05

Avocado

0.05

Berry group 13

0.05

Cranberry

0.05

Fig

0.05

Fruit, citrus, group 10

0.05

Fruit, pome, group 11

0.05

Fruit, stone, group 12

0.05

Grape

0.05

Kiwifruit

0.05

Nut, tree, group 14

0.05

Olive

0.05

Pistachio

0.05

Pomegranate

0.05

Strawberry

0.05

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(n),
are established for residues of oryzalin, 3,5-dinitro- N 4, N 4-dipropylsulfanilamide, in or on the following
raw agricultural commodities:

Commodity

Parts per million

Guava
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Papaya

0.05

(d) Indirect or inadvertent residues . [Reserved]
[71 FR 54434, Sept. 15, 2006]

§ 180.309 &b.alpha;-Naphthaleneacetamide; tolerances for residues.
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(a) General. Tolerances are established for combined negligible residues of the plant regulatorαnaphthaleneacetamide and its metabolite α-naphthaleneacetic acid (calculated asα-naphthaleneacetic
acid) in or on the following food commodities:

Commodity

Parts per million

Apple

0.1

Pear

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003]

§ 180.311 Cacodylic acid; tolerances for residues.
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(a) General. Tolerances are established for residues of the defoliant cacodylic acid (dimethylarsinic acid),
expressed as As2O3, in or on the following raw agricultural commodity as follows:

Commodity

Parts per million

Cotton, undelinted seed
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 6567, Feb. 11, 2004]

§ 180.312 4-Aminopyridine; tolerances for residues.
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(a) General . Tolerances are established for residues of the bird repellent 4-aminopyridine in or on the

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following food commodities:

Commodity

Parts per million Expiration/Revocation Date

Corn, field, forage

0.1

1/15/06

Corn, field, grain

0.1

1/15/06

Corn, field, stover

0.1

1/15/06

Corn, pop, grain

0.1

1/15/06

Corn, pop, stover

0.1

1/15/06

Corn, sweet, forage

0.1

1/15/06

Corn, sweet, kernel plus cob with
husks removed

0.1

1/15/06

Corn, sweet, stover

0.1

1/15/06

Sunflower, seed

0.1

1/15/06

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39441, July 1, 2003, as amended at 70 FR 55268, Sept. 21, 2005]

§ 180.314 Triallate; tolerances for residues.
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(a) General . Tolerances are established for residues of triallate, S-2,3,4-trichloroallyl
diisopropylthiocarbamate and its metabolite 2,3,3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the
following food commodity:

Commodity

Parts per million

Bermudagrass, hay

0.3

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with a regional registration, as defined in 180.1(m),
are established for residues of the herbicide (S-2, 3, 4-trichloroallyl diisopropylthiocarbamate) and its
metabolite 2, 3, 3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodities:

Commodity

Parts per million

Barley, grain

0.05

Barley, hay

1.0

Barley, straw

0.3

Beet, sugar, dried pulp

0.2

Beet, sugar, roots

0.1

Beet, sugar, tops

0.5

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Pea, dry

0.2

Pea, field, hay

1.0

Pea, field, vines

0.5

Pea, succulent

0.2

Wheat, forage

0.5

Wheat, grain

0.05

Wheat, hay

1.0

Wheat, straw

1.0

(d) Indirect or inadvertent residues . [Reserved]
[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, 2008; 74
FR 29963, June 24, 2009]

§ 180.315 Methamidophos; tolerances for residues.
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(a) Tolerances are established for residues of the insecticide methamidophos ( O,S -dimethyl
phosphoramidothioate) in or on the following raw agricultural commodities:

Commodity

Parts per million

Broccoli

1.0

Brussels sprouts

1.0

Cabbage

1.0

Cauliflower

1.0

Cotton, undelinted seed

0.1

Cucumber

1.0

Eggplant

1.0

Lettuce

1.0

Melon

0.5

Pepper

1.0

Potato

0.1

Tomato

1.0

(b) Tolerances with regional registration, as defined in §180.1(n), are established for residues of
methamidophos in or on the following raw agricultural commodities:

Commodity

Parts per million

Celery
[47 FR 13525, Mar. 31, 1982, as amended at 48 FR 44537, Sept. 29, 1983; 52 FR 33238, Sept. 2, 1987;
67 FR 49617, July 31, 2002]

§ 180.316 Pyrazon; tolerances for residues.
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(a) General. Tolerances are established for combined residues of the herbicide pyrazon (5-amino-4-chloro2-phenyl-3(2H)-pyridazinone) and its metabolites (calculated as pyrazon) in or on the following food
commodities:

Commodity

Parts per million

Beet, garden, roots

0.9

Beet, garden, tops

7.0

Beet, sugar, molasses

1.5

Beet, sugar, roots

0.2

Beet, sugar, tops

3.0

Cattle, fat

0.10

Cattle, liver

0.15

Cattle, meat

0.10

Cattle, meat byproducts, except liver

0.10

Goat, fat

0.10

Goat, liver

0.15

Goat, meat

0.10

Goat, meat byproducts, except liver

0.10

Horse, fat

0.10

Horse, liver

0.15

Horse, meat

0.10

Horse, meat byproducts, except liver

0.10

Milk

0.02

Sheep, fat

0.10

Sheep, liver

0.15

Sheep, meat

0.10

Sheep, meat byproducts, except liver

0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for combined residues of the herbicide
pyrazon, 5-amino-4-chloro-2-phenyl-3(2 H )-pyridazinone, and its metabolites (calculated as pyrazon), in
or on the following food commodities:

Commodity

Parts per million

Corn, field, forage

0.5

Corn, field, stover

0.5

Soybean, forage

0.5

Soybean, hay

0.5

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Wheat, forage

0.3

Wheat, hay

0.2

Wheat, straw

0.1

[68 FR 39441, July 1, 2003, as amended at 73 FR 52614, Sept. 10, 2008]

§ 180.317 Propyzamide; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the herbicide propyzamide and its
metabolites (containing the 3,5-dichlorobenzoyl moiety calculated as 3,5-dichloro-N-(1,1-dimethyl-2propynyl)benzamide) in or on the following food commodities:

Commodity

Parts per million

Alfalfa, seed

10.0

Animal feed, nongrass, group 18

10.0

Apple

0.1

Artichoke, globe

0.01

Blackberry

0.05

Blueberry

0.05

Boysenberry

0.05

Cattle, fat

0.2

Cattle, kidney

0.4

Cattle, liver

0.4

Cattle, meat

0.02

Cattle, meat byproducts, except kidney and liver

0.02

Egg

0.02

Endive

1.0

Fruit, stone, group 12

0.1

Goat, fat

0.2

Goat, kidney

0.4

Goat, liver

0.4

Goat, meat

0.02

Goat, meat byproducts, except kidney and liver

0.02

Grape

0.1

Hog, fat

0.2

Hog, kidney

0.4

Hog, liver

0.4

Hog, meat

0.02

Hog, meat byproducts, except kidney and liver

0.02

Horse, fat

0.2

Horse, kidney

0.4

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Horse, liver

0.4

Horse, meat

0.02

Horse, meat byproducts, except kidney and liver

0.02

Lettuce, head

1.0

Milk

0.02

Pear

0.1

Poultry, fat

0.02

Poultry, liver

0.2

Poultry, meat

0.02

Poultry, meat byproducts, except liver

0.02

Radicchio

2.0

Raspberry

0.05

Sheep, fat

0.2

Sheep, kidney

0.4

Sheep, liver

0.4

Sheep, meat

0.02

Sheep, meat byproducts, except kidney and liver

0.02

(b) Section 18 emergency exemptions . Time-limited tolerances are established for the combined residues
of the herbicide propyzamide and its metabolites (containing the 3,5-dichlorobenzoyl moiety calculated as
3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide) in or on the following food commodities:

Commodity

Parts per million

Cranberry

Expiration/Revocation Date

0.05

12/31/09

(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(m)
are established for the combined residues of the herbicide propyzamide and its metabolites (containing
the 3,5-dichlorobenzoyl moiety calculated as 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide) in or on
the following food commodities:

Commodity

Parts per million

Pea, field, seed

0.05

Rhubarb

0.1

(d) Indirect or inadvertent residues . Tolerances are established for the combined indirect or inadvertent
residues of the herbicide propyzamide and its metabolites (containing the 3,5-dichlorobenzoyl moiety
calculated as 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide) in or on the following food commodities:

Commodity

Parts per million

Grain, cereal, forage, group 16

0.6

Grain, cereal, hay, group 16

0.2

Grain, cereal, straw, group 16

0.3

[72 FR 52018, Sept. 12, 2007]

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§ 180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.
top
(a) General. (1) A tolerance is established for the herbicide 4-(2-methyl-4-chlorophenoxy) butyric acid in or
on the following food commodity:

Commodity

Parts per million

Pea

0.1(N)

(2) Tolerances are established for the combined residues, free and conjugated, of the herbicide MCPB, 4(4-chloro-2-methylphenoxy)butanoic acid, and its metabolite MCPA, (4-chloro-2-methylphenoxy)acetic
acid, in or on the following food commodities:

Commodity

Parts per million

Peppermint, tops

0.20

Spearmint, tops

0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39441, July 1, 2003, as amended at 73 FR 66785, Nov. 12, 2008]

§ 180.319 Interim tolerances.
top
While petitions for tolerances for negligible residues are pending and until action is completed on these
petitions, interim tolerances are established for residues of the listed pesticide chemicals in or on the
following raw agricultural commodities:

Substances

Uses

Tolerance in parts per
million

Raw
agricultural
commodity

Coordination product of zinc
ion and maneb

Fungicide 1.0 (Calculated as zinc
ethylenebisdithiocarbamate)

Potato

Endothall (7-oxabicyclo(2,2,1) heptane 2,3dicarboxylic acid)

Herbicide 0.2

Beet, sugar

Isopropyl carbanilate (IPC)

Herbicide 5.0

Alfalfa, hay;
clover, hay;
and grass, hay

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2.0

Alfalfa, forage;
clover, forage;
and grass,
forage

0.1

Flax, seed;
lentil; lettuce,
head and
lettuce, leaf;
pea;
safflower,
seed; spinach;
and beet,
sugar, roots
and beet,
sugar, tops

0.5

Egg; cattle,
fat; cattle
meat; cattle,
meat
byproducts;
goat, fat;
goat, meat;
goat, meat
byproducts;
hog, fat; hog,
meat; hog,
meat
byproducts;
horse, fat;
horse, meat;
horse, meat
byproducts;
milk; sheep,
fat; sheep
meat; sheep,
meat
byproducts;
poultry, fat;
poultry, meat;
poultry, meat
byproducts

Parathion (O,O-diethyl-O-p- Herbicide 0.5
nitrophenythiophosphate) or
its methyl homolog

Rye

Pentachloronitrobenzene

Peanut

Fungicide 1.0

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0.1

Bean, broccoli,
Brussels
sprouts,
cabbage,
cauliflower,
garlic, pepper,
potato, and
tomato

[71 FR 74816, Dec. 13, 2006, as amended at 72 FR 37654, July 11, 2007; 73 FR 52614, Sept. 10, 2008]

§ 180.324 Bromoxynil; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the herbicide bromoxynil (3,5-dibromo-4hydroxybenzonitrile) resulting from application of its octanoic and/or heptanoic acid ester in or on the
following commodities:

Commodity

Parts per million

Alfalfa, forage

0.1

Alfalfa, hay

0.5

Barley, grain

0.05

Barley, hay

9.0

Barley, straw

4.0

Corn, field, forage

0.3

Corn, field, grain

0.05

Corn, field, stover

0.2

Corn, pop, grain

0.05

Corn, pop, stover

0.2

Flax, seed

0.1

Garlic

0.1

Grain, aspirated fractions

0.3

Grass, forage

3.0

Grass, hay

3.0

Oat, forage

0.3

Oat, grain

0.05

Oat, hay

9.0

Oat, straw

4.0

Onion, bulb

0.1

Peppermint, hay

0.1

Rye, forage

1.0

Rye, grain

0.05

Rye, straw

2.0

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Sorghum, grain, forage

0.5

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.2

Spearmint, hay

0.1

Wheat, forage

1.0

Wheat, grain

0.05

Wheat, hay

4.0

Wheat, straw

2.0

(2) Tolerances are established for residues of the herbicide bromoxynil (3,5-dibromo-4hydroxybenzonitrile) and its metabolite 3,5-dibromo-4-hydroxybenzoic acid (DBHA) resulting from
application of its octanoic and/or heptanoic acid ester in or on the following commodities:

Commodity

Parts per million

Cattle, fat

1

Cattle, meat byproducts

3.5

Cattle, meat

0.5

Cotton, gin byproducts

7.0

Cotton, hulls

5.0

Cotton, undelinted seed

1.5

Egg
Goat, fat

0.05
1

Goat, meat byproducts

3.5

Goat, meat

0.5

Hog, fat

1

Hog, meat byproducts

3.5

Hog, meat

0.5

Horse, fat

1

Horse, meat byproducts

3.5

Horse, meat

0.5

Milk

0.1

Poultry, fat
Poultry, meat byproducts
Poultry, meat
Sheep, fat

0.05
0.3
0.05
1

Sheep, meat byproducts

3.5

Sheep, meat

0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
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[62 FR 33023, June 18, 1997, as amended at 63 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, 2001;
70 FR 7046, Feb. 10, 2005; 72 FR 35666, June 29, 2007; 72 FR 41930, Aug. 1, 2007]

§ 180.325 2-(m-Chlorophenoxy) propionic acid; tolerances for residues.
top
(a) General . A tolerance is established for negligible residues of the plant regulator 2-(m-chlorophenoxy)
propionic acid from application of the acid or of 2-(m-chlorophenoxy)propionamide in or on the following
raw agricultural commodity:

Commodity

Parts per million

Pineapple

Expiration/Revocation Date
0.3

2/1/07

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[69 FR 43924, July 23, 2004]

§ 180.328 Napropamide; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide napropamide, N , N -diethyl-2-(1napthalenyloxy) propionamide, in or on the following food commodities:

Commodity

Parts per million Expiration/revocation date

Almond, hulls

0.1

None

Artichoke, globe

0.1

4/26/09

Asparagus

0.1

None

Avocado

0.1

4/26/09

Basil

0.1

None

Berry group 13

0.1

None

Coffee, green bean

0.1

None

Cranberry

0.1

None

Fig

0.1

4/26/09

Fruit, citrus

0.1

4/26/09

Fruit, pome

0.1

4/26/09

Fruit, stone

0.1

4/26/09

Grape

0.1

None

Kiwifruit

0.1

None

Marjoram

0.1

None

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Nut, tree, group 14

0.1

None

Olive

0.1

4/26/09

Peppermint, tops

0.1

None

Persimmon

0.1

None

Pistachio

0.1

04/26/09

Rhubarb

0.1

None

Rosemary

0.1

None

Savory, summer

0.1

None

Savory, winter

0.1

None

Spearmint, tops

0.1

None

Strawberry

0.1

None

Sweet potato, roots

0.1

None

Vegetable, brassica, leafy, group 5

0.1

None

Vegetable, fruiting, group 8

0.1

None

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances are established for residues of the herbicide
napropamide, N , N -diethyl-2-(1-napthalenyloxy) propionamide, in or on the following food commodities:

Commodity

Parts per million

Pomegranate

Expiration/revocation date
0.1

4/26/09

(d) Indirect or inadvertent residues . [Reserved]
[73 FR 52614, Sept. 10, 2008]

§ 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for
residues.
top
(a) General . (1) Tolerances are established for the combined residues of the insecticide oxydemetonmethyl (S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl
sulfone in or on the following food commodities:

Commodity
Alfalfa, forage

Parts per million
5.0

Alfalfa, hay

11.0

Bean, lima

0.2

Beet, sugar, roots

0.3

Beet, sugar, tops

0.5

Broccoli

1.0

Brussels sprouts

1.0

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Cabbage

2.0

Cauliflower

1.0

Clover, forage

5.0

Clover, hay

10.0

Corn, sweet, forage

1.0

Corn, sweet, kernel plus cob with husks removed

0.5

Corn, sweet, stover

3.0

Cotton, undelinted seed

0.02

Cucumber

1.0

Eggplant

1.0

Grapefruit

1.0

Hazelnut

0.05

Lemon

1.0

Lettuce, head

2.0

Melon

0.2

Onion, bulb

0.05

Orange

1.0

Pepper

0.75

Peppermint, tops

12.5

Pumpkin

0.2

Safflower, seed

1.0

Sorghum, forage, forage

2.0

Sorghum, grain, forage

2.0

Sorghum, grain, grain

0.75

Spearmint, tops

12.5

Squash, summer

1.0

Squash, winter

0.3

Strawberry

2.0

Walnut

0.05

(2) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its cholinesterase-inhibiting metabolites in or on
the following food commodities:

Commodity

Parts per million

Cattle, fat

0.01

Cattle, meat

0.01

Cattle, meat byproducts

0.01

Egg

0.01

Goat, fat

0.01

Goat, meat

0.01

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Goat, meat byproducts

0.01

Hog, fat

0.01

Hog, meat

0.01

Hog, meat byproducts

0.01

Horse, fat

0.01

Horse, meat

0.01

Horse, meat byproducts

0.01

Milk

0.01

Poultry, fat

0.01

Poultry, meat

0.01

Poultry, meat byproducts

0.01

Sheep, fat

0.01

Sheep, meat

0.01

Sheep, meat byproducts

0.01

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registrations, as defined in §180.1(m),
are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)-ethyl)
O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food
commodities:

Commodity

Parts per million

Broccoli raab

2.0

(d) Indirect or inadvertent residues . [Reserved]
[72 FR 54578, Sept. 26, 2007]

§ 180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide 4-(2,4-dichlorophenoxy) butyric acid
(2,4-DB), both free and conjugated, determined as the acid, in or on food commodities, as follows:

Commodity

Parts per million

Alfalfa, forage

0.7

Alfalfa, hay

2.0

Cattle, meat byproducts
Clover

0.05
0.2

Goat, meat byproducts

0.05

Hog, meat byproducts

0.05

Horse, meat byproducts

0.05

Peanut
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Peppermint, tops

0.2

Sheep, meat byproducts

0.05

Soybean, forage

0.7

Soybean, hay

2.0

Soybean, seed

0.5

Spearmint, tops

0.2

Trefoil, forage

0.7

Trefoil, hay

2.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54961, Sept. 24, 2008]

§ 180.332 Metribuzin; tolerances for residues.
top
(a) General. Tolerances are established for combined residues of the herbicide metribuzin (4-amino-6-(1,1dimethyl- ethyl)-3-(methylthio)-;1,2,4-triazin-5(4 H )-one) and its triazinone metabolites in or on food
commodities:

Commodity

Parts per million

Alfalfa, forage

2.0

Alfalfa, hay

7.0

Asparagus

0.1

Barley, grain

0.75

Barley, hay

7.0

Barley, pearled barley

3.0

Barley, straw

1.0

Carrot, roots

0.3

Cattle, fat

0.7

Cattle, meat

0.7

Cattle, meat byproducts

0.7

Corn, field, forage

0.1

Corn, field, grain

0.05

Corn, field, stover

0.1

Corn, pop, grain
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
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0.05
0.1
0.05
0.1

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Egg

0.01

Goat, fat

0.7

Goat, meat

0.7

Goat, meat byproducts

0.7

Grass, forage

2.0

Grass, hay

7.0

Hog, fat

0.7

Hog, meat

0.7

Hog, meat byproducts

0.7

Horse, fat

0.7

Horse, meat

0.7

Horse, meat byproducts

0.7

Lentil

0.05

Milk

0.05

Pea, dry, seed

0.05

Pea, field, hay

4.0

Pea, field, vines

0.5

Pea, succulent

0.1

Potato

0.6

Potato, chips

3.0

Potato, processed potato waste

3.0

Poultry, fat

0.7

Poultry, meat

0.7

Poultry, meat byproducts

0.7

Sainfoin, forage

2.0

Sainfoin, hay

7.0

Sheep, fat

0.7

Sheep, meat

0.7

Sheep, meat byproducts

0.7

Soybean, seed

0.3

Soybean, forage

4.0

Soybean, hay

4.0

Sugarcane, cane

0.1

Sugarcane, molasses

2.0

Tomato

0.1

Wheat, bran

3.0

Wheat, forage

2.0

Wheat, germ

3.0

Wheat, grain

0.75

Wheat, hay

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7.0

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Wheat, middlings

3.0

Wheat, shorts

3.0

Wheat, straw

1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, 1979;
44 FR 45387, Aug. 2, 1979; 52 FR 23654, June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR 66024,
66025, Dec. 17, 1997; 65 FR 33698, May 24, 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, July 31,
2002]

§ 180.337 Oxytetracycline; tolerance for residues.
top
Tolerances are established for residues of the pesticide oxytetracycline in or on the following raw
agricultural commodities:

Commodity

Parts per million

Apple

0.35

Peach

0.35

Pear

0.35

[60 FR 34871, July 5, 1995, as amended at 72 FR 62794, Nov. 7, 2007]

§ 180.339 MCPA; tolerances for residues.
top
(a) General . (1) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2methylphenoxy)acetic acid), both free and conjugated, resulting from the direct application of MCPA or its
sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the following food commodities:

Commodity

Parts per million

Alfalfa, forage

0.5

Alfalfa, hay

2.0

Barley, grain

1.0

Barley, hay

40

Barley, straw

25

Clover, forage

0.5

Clover, hay

2.0

Flax, seed

0.1

Grain, aspirated fractions

3.0

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Grass, forage

300

Grass, hay

20

Lespedeza, forage

0.5

Lespedeza, hay

2.0

Oat, forage

20

Oat, grain

1.0

Oat, hay

115

Oat, straw

25

Pea, dry

0.1

Pea, field, hay

0.1

Pea, succulent

0.1

Pea, field, vines

0.1

Rye, forage

20

Rye, grain

1.0

Rye, straw

25

Trefoil, forage

0.5

Trefoil, hay

2.0

Vetch, forage

0.5

Vetch, hay

2.0

Wheat, forage

20

Wheat, grain

1.0

Wheat, hay

115

Wheat, straw

25

(2) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic
acid) resulting from the direct application of MCPA or its sodium or dimethylamine salts, or its 2-ethylhexyl
ester in or on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.1

Cattle, meat

0.1

Cattle, meat byproducts

0.1

Goat, fat

0.1

Goat, meat

0.1

Goat, meat byproducts

0.1

Hog, fat

0.1

Hog, meat

0.1

Hog, meat byproducts

0.1

Horse, fat

0.1

Horse, meat

0.1

Horse, meat byproducts

0.1

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Milk

0.1

Sheep, fat

0.1

Sheep meat

0.1

Sheep meat byproducts

0.1

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008]

§ 180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl
crotonate; tolerances for residues.
top
(a) General . Tolerances are established for combined negligible residues of a fungicide and insecticide
that is a mixture of 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate in or on raw
agricultural commodities as follows:

Commodity

Parts per million

Apple1

0.1

Grape1

0.1

1There

are no U.S. registrations on apple and grape as of October 24, 2002.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[40 FR 29715, July 15, 1975, as amended at 63 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, 2004]

§ 180.342 Chlorpyrifos; tolerances for residues.
top
(a) General . (1) Tolerances are established for residues of the pesticide chlorpyrifos per se ( O,O -diethylO -(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

Commodity
Alfalfa, forage
Alfalfa, hay
Almond
Almond, hulls
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Parts per million
3.0
13
0.2
12

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Apple

0.01

Apple, wet pomace

0.02

Banana

0.1

Beet, sugar, dried pulp

5.0

Beet, sugar, molasses

15

Beet, sugar, roots

1.0

Beet, sugar, tops

8.0

Cattle, fat

0.3

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Cherry, sweet

1.0

Cherry, tart

1.0

Citrus, dried pulp

5.0

Citrus, oil

20

Corn, field, forage

8.0

Corn, field, grain

0.05

Corn, field, refined oil

0.25

Corn, field, stover

8.0

Corn, sweet, forage

8.0

Corn, sweet, kernel plus cob with husk removed

0.05

Corn, sweet, stover

8.0

Cotton, undelinted seed

0.2

Cranberry

1.0

Cucumber

0.05

Egg

0.01

Fig

0.01

Fruit, citrus, group 10

1.0

Goat, fat

0.2

Goat, meat

0.05

Goat, meat byproducts

0.05

Hazelnut

0.2

Hog, fat

0.2

Hog, meat

0.05

Hog, meat byproducts

0.05

Horse, fat

0.25

Horse, meat

0.25

Horse, meat byproducts

0.25

Kiwifruit

2.0

Lettuce

1.0

Milk, fat (Reflecting 0.01 ppm in whole milk)

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Nectarine
Onion, bulb

0.05
0.5

Peach

0.05

Peanut

0.2

Peanut, refined oil

0.2

Pear

0.05

Pecan

0.2

Pepper

1.0

Peppermint, tops

0.8

Peppermint, oil

8.0

Plum, prune, fresh

0.05

Poultry, fat

0.1

Poultry, meat

0.1

Poultry, meat byproducts

0.1

Pumpkin

0.05

Radish

2.0

Rutabaga

0.5

Sheep, fat

0.2

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Spearmint, tops

0.8

Spearmint, oil

8.0

Sorghum, grain, forage

0.5

Sorghum, grain, grain

0.5

Sorghum, grain, stover

2.0

Soybean, seed

0.3

Strawberry

0.2

Sunflower, seed

0.1

Sweet potato, roots

0.05

Turnip, roots

1.0

Turnip, tops

0.3

Vegetable, brassica, leafy, group 5

1.0

Vegetable, legume, group 6. except soybean

0.05

Walnut

0.2

Wheat, forage

3.0

Wheat, grain

0.5

Wheat, straw

6.0

(2) Chlorpyrifos [ O,O- diethyl O- (3,5,6-trichloro-2-pyridyl) phosphorothioate] may be safely used in
accordance with the following prescribed conditions.
(i) Application shall be limited solely to spot and/or crack and crevice treatment in food handling
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establishments where food and food products are held, processed, prepared or served. Contamination of
food or food contact surfaces shall be avoided. Food must be removed or covered during treatment.
(ii) Spray concentration for spot treatment shall be limited to a maximum of 0.5 percent of the active
ingredient by weight. A course, low-pressure spray shall be used to avoid atomization or splashing of the
spray.
(iii) Paint-on application for spot treatment shall be limited to a maximum of 2 percent of the active
ingredient by weight.
(iv) Crack and crevice treatment shall be limited to a maximum of 2 percent of the active ingredient by
weight. Equipment capable of delivering a pin-stream of insecticide shall be used.
(v) Application via adhesive strips shall contain a maximum of 10% by weight of the controlled-release
product in food-handling establishments where food and food products are held, processed, prepared, or
served. A maximum of 36 strips (or 5.15 grams of chlorpyrifos) is to be used per 100 square feet of floor
space. The strips are not to be placed in exposed areas where direct contact with food, utensils, and foodcontact surfaces would be likely to occur.
(vi) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(3) A tolerance of 0.1 part per million is established for residues of chlorpyrifos, per se, in or on food
commodities (other than those already covered by a higher tolerance as a result of use on growing crops)
in food service establishments where food and food products are prepared and served, as a result of the
application of chlorpyrifos in microencapsulated form.
(i) Application of a microencapsulated product shall be limited solely to spot and/or crack and crevice
treatment in food handling establishments where food and food products are prepared and served. All
treatments shall be applied in such a manner as to avoid contamination of food or food contact surfaces.
(ii) Spray concentrations shall be limited to a maximum of 0.5 percent of the active ingredient by weight.
(iii) For crack and crevice treatment, equipment capable of delivering a pin stream of spray directly into
cracks and crevices or capable of applying small amounts of insecticide into cracks and crevices shall be
used.
(iv) For spot treatment, an individual spot shall not exceed 2 square feet.
(v) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in 180.1(m),
are established for residues of the pesticide chlorpyrifos per se ( O,O -diethyl- O -(3,5,6-trichloro-2-pyridyl)
phosphorothioate) in or on the following food commodities:

Commodity

Parts per million

Asparagus
Grape

5.0
0.01

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33711, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006;
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73 FR 53739, Sept. 17, 2008]

§ 180.345 Ethofumesate; tolerances for residues.
top
(a) General . Tolerances for the combined residues of the herbicide ethofumesate (2-ethoxy-2,3-dihydro3,3-dimethyl-5-benzofuranyl methanesulfonate) and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5benzofuranyl methanesulfonate and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranyl methanesulfonate
both calculated as parent compound in or on the following food commodities:

Commodity

Parts per million

Beet, garden, roots

0.5

Beet, garden, tops

5.0

Beet, sugar, molasses

0.5

Beet, sugar, refined sugar

0.2

Beet, sugar, roots

0.3

Beet, sugar, tops

4.0

Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Garlic

0.25

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Grass, straw

1.0

Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Onion, bulb

0.25

Shallot, bulb

0.25

Shallot, fresh leaves

0.25

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. Tolerances with regional registration as defined in 40 CFR 180.1
(m) are established for the combined residues of ethofumesate,(2-ethoxy -2, 3-dihydro-3, 3-dimethyl-5benzofuranyl methanesulfonate) and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl
methanesulfonate and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranyl methanesulfonate (both calculated
as the parent compound) in or on the raw agricultural commodities:

Commodity

Parts per million

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Carrot, roots

7.0

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34828, June 26, 1998, as amended at 71 FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007]

§ 180.349 Fenamiphos; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the nematocide fenaminphos, (ethyl
3-methyl-4-(methylthio)phenyl (1-methylethyl)phosphoramidate, and its cholinesterase inhibiting
metabolites ethyl 3-methyl-4-(methylsulfinyl)phenyl (1-methylethyl)phosphoramidate and ethyl 3-methyl-4(methylsulfonyl)phenyl (1-methylethyl)phosporamidate in or on the following food commodities:

Commodity

Parts per million

Expiration/Revocation Date

Apple

0.25

12/31/09

Banana1

0.10

None

Brussels sprouts

0.05

12/31/09

Cabbage

0.10

12/31/09

Cherry, sweet

0.25

12/31/09

Cherry, tart

0.25

12/31/09

2.5

None

Citrus, oil

25.0

None

Eggplant

0.05

12/31/09

Fruit, citrus, group 101

0.50

None

Garlic1

0.50

None

Grape1

0.10

None

Grape, raisin

0.30

None

Okra

0.30

12/31/09

Peach

0.25

12/31/09

Peanut

1.0

12/31/09

Pineapple1

0.30

None

Raspberry

0.10

12/31/09

Strawberry

0.60

12/31/09

Citrus, dried pulp

1There

are no U.S. registrations as of December 31, 2009.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for the combined residues of Fenamiphos (ethyl 3-methyl-4-(methylthio)phenyl (1methylethyl) phosphoramidate) and its cholinesterase-inhibiting metabolites ethyl 3-methyl-4(methylsulfinyl)phenyl (1-methylethyl) phosphoramidate and ethyl 3-methyl-4-(methylsulfonyl)phenyl (1methylethyl) phosphoramidate in or on the following raw agricultural commodities:

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Commodity

Parts per million

Asparagus

Expiration/Revocation Date

0.02

12/31/09

Beet, garden roots

1.5

12/31/09

Beet, garden, tops

1.0

12/31/09

Cabbage, Chinese, bok choy

0.50

12/31/09

Kiwifruit

0.10

12/31/09

Pepper, nonbell

0.60

12/31/09

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33712, May 24, 2000, as amended at 73 FR 53739, Sept. 17, 2008]

§ 180.350 Nitrapyrin; tolerances forresidues.
top
(a) General. Tolerances are established for the combined residues of the soil microbiocide nitrapyrin [2chloro-6-(trichloromethyl) pyridine] and its metabolite, 6-chloropicolinic acid in or on the following raw
agricultural commodities:

Commodity

Parts per million

Corn, field, forage

1.0

Corn, field, grain

0.1

Corn, field, milled byproducts

0.2

Corn, field, stover

1.0

Corn, pop, grain

0.1

Corn, pop, stover

1.0

Corn, sweet, forage

1.0

Corn, sweet, kernel plus cob with husks removed

0.1

Corn, sweet, stover

1.0

Sorghum, forage, forage

0.5

Sorghum, grain, forage

0.5

Sorghum, grain, grain

0.1

Sorghum, grain, stover

0.5

Wheat, bran

3.0

Wheat, forage

2.0

Wheat, grain

0.5

Wheat, milled byproducts, except flour

2.0

Wheat, straw

6.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[46 FR 58315, Dec. 1, 1981, as amended at 47 FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, 1987; 58
FR 32304, June 9, 1993; 63 FR 57076, Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007]

§ 180.352 Terbufos; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the insecticide terbufos
(phosphorodithioic acid, S -(t-butylthio)methyl O,O -diethyl ester) and its phosphorylated (cholinesteraseinhibiting) metabolites (phosphorothioic acid, S -(t-butylthio)methyl O,O -diethyl ester; phosphorothioic
acid, S -(t-butylsulfinyl)methyl O,O -diethyl ester; phosphorothioic acid, S -(t-butylsulfonyl)methyl O,O diethyl ester; phosphorodithioic acid, S -(t-butylsulfinyl)methyl O,O -diethyl ester; and phosphorodithioic
acid, S -(t-butylsulfonyl)methyl O,O -diethyl ester) in or on food commodities:

Commodity

Parts per million

Banana

0.025

Beet, sugar, roots

0.05

Beet, sugar, tops

0.1

Coffee, green bean1

0.05

Corn, field, forage

0.5

Corn, field, grain

0.5

Corn, field, stover

0.5

Corn, pop, grain

0.5

Corn, pop, stover

0.5

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, forage

0.5

Corn, sweet, stover

0.5

Sorghum, grain, forage

0.5

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.5

1There

are no U. S. registrations as of August 2, 1995, for the use of terbufos on the growing crop, coffee.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 53740, Sept. 17, 2008]

§ 180.353 Desmedipham; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide desmedipham, (ethyl- m http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c...&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (224 of 651) [9/8/2009 3:02:20 PM]

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hydroxycarbanilate carbanilate) in or on the following raw agricultural commodities in the table that follows:

Commodity

Parts per million

Beet, garden, roots

0.05

Beet, garden, tops

1.0

Beet, sugar, roots

0.1

Beet, sugar, tops

5.0

Spinach

6.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[40 FR 4658, Jan. 31, 1975, as amended at 62 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, 1998;
64 FR 46292, Aug. 25, 1999; 65 FR 82293, Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 37764,
June 25, 2003; 69 FR 71717, Dec. 10, 2004; 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. 17, 2008]

§ 180.355 Bentazon; tolerances for residues.
top
(a) General. (1) Tolerances are established for the combined residues of the herbicide bentazon (3isopropyl-1 H -2,1,3-benzothiadiazin-4(3 H )-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on
the following food commodities:

Commodity

Parts per million

Bean, dry, seed

0.05

Bean, succulent

0.5

Corn, field, forage

3.0

Corn, field, grain

0.05

Corn, field, stover

3.0

Corn, pop, grain

0.05

Corn, sweet, kernel plus cob with husks removed

0.05

Cowpea, forage

10.0

Cowpea, hay

3.0

Flax, seed

1.0

Pea, dry, seed

1.0

Pea, field, hay

8.0

Pea, field, vines

3.0

Pea, succulent

3.0

Peanut
Peanut, hay
Pepper, nonbell
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0.05
3.0
0.05

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Peppermint, tops

1.0

Rice, grain

0.05

Rice, hulls

0.25

Rice, straw

3.0

Sorghum, forage

0.20

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.05

Soybean, forage

8.0

Soybean, hay

8.0

Soybean, seed

0.05

Spearmint, tops

1.0

(2) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl-1 H -2,1,3benzothiadiazin-4(3 H )-one-2,2-dioxide) and its metabolite 2-amino- N -isopropyl benzamide (AIBA) in or
on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.05

Cattle, meat byproducts

0.05

Cattle, meat

0.05

Egg

0.05

Goat, fat

0.05

Goat, meat byproducts

0.05

Goat, meat

0.05

Hog, fat

0.05

Hog, meat byproducts

0.05

Hog, meat

0.05

Milk

0.02

Poultry, fat

0.05

Poultry, meat byproducts

0.05

Poultry, meat

0.05

Sheep, fat

0.05

Sheep, meat byproducts

0.05

Sheep, meat

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(n),
are established for combined residues of the herbicide, bentazon (3-isopropyl-1H-2, 1,3-benzothiadiazin-4
(3H)-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food commodities:

Commodity

Parts per million

Clover, forage
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1.0

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Clover, hay

2.0

(d) Indirect or inadvertent residues. [Reserved]
[42 FR 26979, May 26, 1977]
Editorial Note: ForFederal Registercitations affecting §180.355, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.356 Norflurazon; tolerances for residues.
top
(a) General. Tolerances are established for the combined residues of the herbicide norflurazon (4-chloro-5(methylamino)-2-(alpha, alpha, alpha-trifluoro- m -tolyl)-3-(2 H )-pyridazinone) and its desmethyl
metabolite 4-chloro-5-(amino)-2-alpha, alpha, alpha-trifluoro- m -tolyl)-3(2 H )-pyridazinone in or on the
following raw agricultural commodities:

Commodity

Parts per million

Alfalfa, forage

3.0

Alfalfa, hay

5.0

Alfalfa, seed

0.1

Almond, hulls

1.0

Almond

0.1

Apple

0.1

Apricot

0.1

Asparagus

0.05

Avocado

0.20

Blackberry

0.1

Blueberry

0.2

Cattle, fat

0.1

Cattle, liver

0.50

Cattle, meat

0.1

Cattle, meat byproducts, except liver

0.1

Cherry

0.1

Citrus, dried pulp

0.4

Citrus, molasses

1.0

Cotton, undelinted seed

0.1

Cranberry

0.1

Fruit, citrus

0.2

Goat, fat

0.1

Goat, liver

0.50

Goat, meat

0.1

Goat, meat byproducts, except liver

0.1

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Grape

0.1

Hazelnut

0.1

Hog, fat

0.1

Hog, liver

0.50

Hog, meat

0.1

Hog, meat byproducts, except liver

0.1

Hop, dried cones

3.0

Hop, vines

1.0

Horse, fat

0.1

Horse, liver

0.50

Horse, meat

0.1

Horse, meat byproducts, except liver

0.1

Milk

0.1

Nectarine

0.1

Peach

0.1

Peanut

0.05

Peanut, hay

5.50

Peanut, hay

1.5

Pear

0.1

Pecan

0.1

Plum, prune, fresh

0.1

Poultry, fat

0.1

Poultry, meat

0.1

Poultry, meat byproducts

0.1

Raspberry

0.2

Sheep, fat

0.1

Sheep, liver

0.50

Sheep, meat

0.1

Sheep, meat byproducts, except liver

0.1

Soybean

0.1

Soybean, forage

1.0

Soybean, hay

1.0

Walnut

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 14909, Apr. 7, 1982]
Editorial Note: ForFederal Registercitations affecting §180.356, see the List of CFR Sections Affected,
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which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.360 Asulam; tolerance for residues.
top
(a) General . Tolerances are established for the combined residues of asulam (methyl sulfanilylcarbamate)
and its sulfanilamide containing metabolites in or on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.2

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.2

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.2

Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.2

Milk

0.05

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.2

Sugarcane, cane

1.0

Sugarcane, molasses

30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39441, July 1, 2003, as amended at 72 FR 37654, July 11, 2007]

§ 180.361 Pendimethalin; tolerances for residues.
top
(a) General. Tolerances are established for the combined residues of the herbicide pendimethalin [ N- (1ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine] and its metabolite 4-[(1-ethylpropyl)amino]-2-methyl-3,5dinitrobenzyl alcohol in or on the following raw agricultural commodities:

Commodity
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Parts per million

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Alfalfa, forage

3.0

Alfalfa, hay

4.0

Alfalfa, seed

0.10

Almond, hulls

0.4

Apple, wet pomace
Artichoke, globe

0.20
0.1

Asparagus

0.15

Beans

0.10

Beans, forage

0.10

Beans, hay

0.10

Brassica head and stem, subgroup 5-A

0.1

Carrot

0.5

Citrus, oil

0.5

Corn, field, forage

0.1

Corn, field, grain

0.1

Corn, field, stover

0.1

Corn, pop, grain

0.1

Corn, sweet, forage

0.1

Corn, sweet, kernel plus cob with husks removed

0.1

Corn, sweet, stover

0.1

Cotton, gin byproducts

3.0

Cotton, undelinted seed

0.1

Crayfish

0.05

Fruit, citrus, group 10

0.1

Fruit, pome, group 11

0.10

Fruit, stone, group 12

0.10

Garlic

0.1

Grape

0.1

Juneberry

0.10

Leek

0.20

Nut, tree, group 14

0.1

Onion, bulb

0.1

Onion, green

0.20

Onion, welsh

0.20

Peanut

0.1

Peanut, hay

0.1

Peas (except field peas)

0.10

Peppermint, oil

1.0

Peppermint, tops

0.2

Pistachio

0.1

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Pomegranate

0.10

Potato

0.1

Rice, grain

0.1

Rice, straw

0.1

Shallot

0.2

Sorghum, forage

0.1

Sorghum, grain, grain

0.1

Sorghum, grain, stover

0.1

Soybean, forage

0.1

Soybean, hay

0.1

Soybean, seed

0.1

Spearmint, oil

1.0

Spearmint, tops

0.2

Strawberry

0.10

Sugarcane, cane

0.1

Sunflower, seed

0.1

Vegetable, fruiting, group 8

0.10

Wheat, grain

0.10

Wheat, forage

3.0

Wheat, hay

0.60

Wheat, straw

0.30

(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for combined residues of the herbicide pendimethalin, [ N -(1-ethylpropyl)-3,4-dimethyl-2,6dinitrobenzenamine], and its metabolite 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, in or
on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18
emergency exemptions. The tolerances expire and are revoked on the date specified in the table.

Commodity

Parts per million

Expiration/revocation date

Bermuda grass, forage

25

12/31/09

Bermuda grass, hay

60

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[49 FR 15293, Apr. 18, 1984]
Editorial Note: ForFederal Registercitations affecting §180.361, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.362 Hexakis (2-methyl-2-phenylpropyl)distannoxane; tolerances for residues.
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(a) General . (1) Tolerances are established for residues of hexakis (2-methyl-2-phenylpropyl)
distannoxane in or on the following raw agricultural commodities:

Commodity

Parts per million

Almond, hulls

80.0

Apple

15.0

Apple, wet pomace

100.0

Cherry, sweet

6.0

Cherry, tart

6.0

Citrus, dried pulp

100.0

Citrus, oil

140.0

Cucumber

4.0

Eggplant

6.0

Fruit, citrus, group 10

20.0

Grape

5.0

Grape, raisin

20.0

Nut, tree, group 14

0.5

Papaya

2.0

Peach

10.0

Pear

15.0

Pistachio

0.5

Plum, prune, fresh

4.0

Plum, prune, dried

20.0

Strawberry

10.0

(2) Tolerances are established for the combined residues of hexakis (2-methyl-2-phenylpropyl)
distannoxane and its organotin metabolites dihydroxybis(2-methyl-2-phenylpropyl)stannane, and 2-methyl2phenylpropylstannoic acid in or on the following raw agricultural commodities:

Commodity

Parts per million

Cattle, fat

0.5

Cattle, meat

0.5

Cattle, meat byproducts

0.5

Egg

0.1

Goat, fat

0.5

Goat, meat

0.5

Goat, meat byproducts

0.5

Hog, fat

0.5

Hog, meat

0.5

Hog, meat byproducts

0.5

Horse, fat

0.5

Horse, meat

0.5

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Horse, meat byproducts

0.5

Milk, fat

0.1

Poultry, fat

0.1

Poultry, meat

0.1

Poultry, meat byproducts

0.1

Sheep, fat

0.5

Sheep, meat

0.5

Sheep, meat byproducts

0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for
residues of the insecticide hexakis [2-methyl-2-phenylpropyl] distannoxane and its organotin metabolites
calculated as hexakis [2-methyl-2-phenylpropyl] distannoxane in or on the food commodities:

Commodity

Parts per million

Raspberry

10.0

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33713, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, 2008]

§ 180.364 Glyphosate; tolerances for residues.
top
(a) General . (1) Tolerances are established for residues of glyphosate N -(phosphonomethyl)glycine
resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the ethanolamine salt
of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the potassium
salt of glyphosate in or on the following food commodities:

Commodity

Parts per million

Acerola

0.2

Alfalfa, seed

0.5

Almond, hulls

25

Aloe vera

0.5

Ambarella

0.2

Animal feed, nongrass, group 18

400

Artichoke, globe

0.2

Asparagus

0.5

Atemoya

0.2

Avocado

0.2

Bamboo, shoots

0.2

Banana

0.2

Barley, bran
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30

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Beet, sugar, dried pulp

25

Beet, sugar, roots

10

Beet, sugar, tops

10

Berry group 13

0.2

Betelnut

1.0

Biriba

0.2

Blimbe

0.2

Borage, seed

0.1

Breadfruit

0.2

Cacao bean, bean

0.2

Cactus, fruit

0.5

Cactus, pads

0.5

Canistel

0.2

Canola, seed

20

Chaya

1.0

Cherimoya

0.2

Citrus, dried pulp

1.5

Coconut

0.1

Coffee, bean, green

1.0

Corn, field, forage

6.0

Corn, field, grain

5.0

Corn, pop, grain

0.1

Corn, sweet, grain

0.1

Cotton, gin byproducts

210

Cotton, undelinted seed

40

Cranberry

0.2

Crambe, seed

0.1

Custard apple

0.2

Date, dried fruit

0.2

Dokudami

2.0

Durian

0.2

Epazote

1.3

Feijoa

0.2

Fig

0.2

Fish

0.25

Flax, meal

8.0

Flax, seed

4.0

Fruit, citrus, group 10

0.5

Fruit, pome, group 11

0.2

Fruit, stone, group 12

0.2

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Galangal, roots

0.2

Ginger, white, flower

0.2

Gourd, buffalo, seed

0.1

Governor's plum

0.2

Gow kee, leaves

0.2

Grain, cereal, forage, fodder and straw, group 16, except field corn,
forage

100

Grain, cereal, group 15 except field corn, popcorn, rice, sweet corn,
and wild rice

30

Grape

0.2

Grass, forage, fodder and hay, group 17

300

Guava

0.2

Herbs subgroup 19A

0.2

Hop, dried cones

7.0

Ilama

0.2

Imbe

0.2

Imbu

0.2

Jaboticaba

0.2

Jackfruit

0.2

Jojoba, seed

0.1

Juneberry

0.2

Kava, roots

0.2

Kenaf, forage

200

Kiwifruit

0.2

Lesquerella, seed

0.1

Leucaena, forage

200

Lingonberry

0.2

Longan

0.2

Lychee

0.2

Mamey apple

0.2

Mango

0.2

Mangosteen

0.2

Marmaladebox

0.2

Meadowfoam, seed

0.1

Mioga, flower

0.2

Mustard, seed

0.1

Noni

0.20

Nut, pine

1.0

Nut, tree, group 14

1.0

Okra

0.5

Olive

0.2

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Oregano, Mexican, leaves

2.0

Palm heart

0.2

Palm heart, leaves

0.2

Palm, oil

0.1

Papaya

0.2

Papaya, mountain

0.2

Passionfruit

0.2

Pawpaw

0.2

Pea, dry

8.0

Peanut

0.1

Peanut, hay

0.5

Pepper leaf, fresh leaves

0.2

Peppermint, tops

200

Perilla, tops

1.8

Persimmon

0.2

Pineapple

0.1

Pistachio

1.0

Pomegranate

0.2

Pulasan

0.2

Quinoa, grain

5.0

Rambutan

0.2

Rapeseed, seed

20

Rice, grain

0.1

Rice, wild, grain

0.1

Rose apple

0.2

Safflower, seed

85

Salal

0.2

Sapodilla

0.2

Sapote, black

0.2

Sapote, mamey

0.2

Sapote, white

0.2

Sesame, seed

0.1

Shellfish

3.0

Soursop

0.2

Spanish lime

0.2

Spearmint, tops

200

Spice subgroup 19B

7.0

Star apple

0.2

Starfruit

0.2

Stevia, dried leaves

1.0

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Strawberry

0.2

Sugar apple

0.2

Sugarcane, cane

2.0

Sugarcane, molasses

30

Sunflower, seed

85

Surinam cherry

0.2

Tamarind

0.2

Tea, dried

1.0

Tea, instant

7.0

Teff, grain

5.0

Ti, leaves

0.2

Ti, roots

0.2

Ugli fruit

0.5

Vegetable, bulb, group 3

0.2

Vegetable, cucurbit, group 9

0.5

Vegetable, foliage of legume, subgroup 7A, except soybean

0.2

Vegetable, fruiting, group 8

0.1

Vegetable, leafy, brassica, group 5

0.2

Vegetable, leafy, except brassica, group 4

0.2

Vegetable, leaves of root and tuber, group 2, except sugar beet tops

0.2

Vegetable, legume, group 6 except soybean and dry pea

5.0

Vegetable, root and tuber, group 1, except sugar beet

0.2

Wasabi, roots

0.2

Water spinach, tops

0.2

Watercress, upland

0.2

Wax jambu

0.2

Yacon, tuber

0.2

(2) Tolerances are established for combined residues of glyphosate, N -(phosphonomethyl)glycine and its
metabolite N -acetyl-glyphosate (expressed as glyphosate) resulting from the application of glyphosate,
the isopropylamine salt of glyphosate, the ethanolamine salt of glyphosate, the dimethylamine salt of
glyphosate, the ammonium salt of glyphosate, and the potassium salt of glyphosate on the food
commodities:

Commodity

Parts per Million

Cattle, meat byproducts
Egg
Goat, meat byproducts
Grain aspirated fractions

5.0
0.05
5.0
310.0

Hog, meat byproducts

5.0

Horse, meat byproducts

5.0

Poultry, meat

4.0

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Poultry, meat byproducts

1.0

Sheep, meat byproducts

5.0

Soybean, forage

100.0

Soybean, hay

200.0

Soybean, hulls

120.0

Soybean, seed

20.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 64911, Oct. 1, 1980]
Editorial Note: ForFederal Registercitations affecting §180.364, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.367

n

-Octyl bicycloheptenedicarboximide; tolerances for residues.

top
(a) General. (1) Tolerances are established for residues of the insecticide n -octyl bicycloheptenedicarboximide, resulting from dermal application, in food commodities as follows:

Commodity

Parts per million

Cattle, fat

0.3

Goat, fat

0.3

Hog, fat

0.3

Horse, fat

0.3

Milk, fat

0.3

Sheep, fat

0.3

(2) N -octylbicycloheptene dicarboximide may be safely used in accordance with the following prescribed
conditions:
(i) It is used in combination with piperonyl butoxide and pyrethrins for insect control in food-processing and
food-storage areas, provided that the food is removed or covered prior to such use.
(ii) Residues in food resulting from the use described in paragraph (a)(2)(i) of this section shall not exceed
10 parts per million of N- octylbicycloheptene dicarboximide, 10 parts per million of piperonyl butoxide, and
1 part per million of pyrethrins.
(iii) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
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(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33713, May 24, 2000]

§ 180.368 Metolachlor; tolerances for residues.
top
(a) General . (1) Tolerances are established for the combined residues (free and bound) of the herbicide
metolachlor, 2-chloro- N -(2- ethyl-6-methylphenyl)- N -(2-methoxy-1-methylethyl)acetamide, and its
metabolites, determined as the derivatives, 2- [(2-ethyl-6- methylphenyl)amino]-1-propanol and 4-(2-ethyl6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the
following raw agricultural commodities:

Commodity
Almond, hulls
Animal feed, nongrass, group 18

Parts per million
0.30
1.0

Cattle, fat

0.04

Cattle, kidney

0.20

Cattle, liver

0.10

Cattle, meat

0.04

Cattle, meat byproducts, except kidney and liver

0.04

Corn, field, forage

6.0

Corn, field, grain

0.10

Corn, field, stover

6.0

Corn, sweet, forage

6.0

Corn, sweet, kernel plus cob with husks removed

0.10

Corn, sweet, stover

6.0

Cotton, gin byproducts

4.0

Cotton, undelinted seed

0.10

Dill

0.50

Egg

0.04

Goat, fat

0.04

Goat, kidney

0.20

Goat, liver

0.10

Goat, meat

0.04

Goat, meat byproducts, except kidney and liver

0.04

Grass, forage

10

Grass, hay

0.20

Horse, fat

0.04

Horse, kidney

0.20

Horse, liver

0.10

Horse, meat

0.04

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Horse, meat byproducts, except kidney and liver

0.04

Milk

0.02

Nut, tree, group 14

0.10

Okra

0.50

Pea and bean, dried shelled, except soybean, subgroup 6C

0.10

Pea and bean, succulent shelled, subgroup 6B

0.30

Peanut

0.20

Peanut, hay

20

Peanut, meal

0.40

Potato

0.20

Poultry, fat

0.04

Poultry, meat

0.04

Poultry, meat byproducts

0.04

Safflower, seed

0.10

Sheep, fat

0.04

Sheep, kidney

0.20

Sheep, liver

0.10

Sheep, meat

0.04

Sheep, meat byproducts, except kidney and liver

0.04

Sorghum, grain, forage

1.0

Sorghum, grain, grain

0.30

Sorghum, grain, stover

4.0

Soybean, forage

5.0

Soybean, hay

8.0

Soybean, seed

0.20

Spinach

0.50

Tomato

0.10

Vegetable, foliage of legume, subgroup 7A, except soybean

15.0

Vegetable, legume, edible podded, subgroup 6A

0.50

(2) Tolerances are established for the combined residues (free and bound) of the herbicide S -metolachlor
S -2-chloro- N -(2-ethyl-6-methylphenyl)- N -(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and
its metabolites, determined as the derivatives, 2-[2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound, in or on
the following raw agricultural commodities:

Commodity
Asparagus

Parts per million
0.10

Beet, sugar, molasses

2.0

Beet, sugar, roots

0.5

Beet, sugar, tops

15.0

Brassica, head and stem, subgroup 5A

0.60

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Cattle, fat

0.04

Cattle, kidney

0.20

Cattle, liver

0.05

Cattle, meat

0.02

Cattle, meat byproducts, except kidney and liver

0.04

Corn, field, grain

0.10

Corn, field, forage

6.0

Corn, field, stover

6.0

Corn, pop, grain

0.10

Corn, pop, stover

6.0

Corn, sweet, forage

6.0

Corn, sweet, kernel plus cob with husks removed

0.10

Corn, sweet, stover

6.0

Cotton, gin byproducts

4.0

Cotton, undelinted seed

0.10

Egg

0.02

Garlic

0.10

Goat, fat

0.04

Goat, kidney

0.20

Goat, liver

0.05

Goat, meat

0.02

Goat, meat byproducts, except kidney and liver

0.04

Grass, forage

10.0

Grass, hay

0.20

Horse, fat

0.04

Horse, kidney

0.20

Horse, liver

0.05

Horse, meat

0.02

Horse, meat byproducts, except kidney and liver

0.04

Milk

0.02

Onion, bulb

0.10

Onion, green

2.0

Peanut

0.20

Pea and bean, dried shelled, except soybean, subgroup 6C

0.10

Peanut, hay

20.0

Peanut, meal

0.40

Poultry, fat

0.04

Poultry, meat

0.02

Poultry, meat byproducts

0.04

Pumpkin

0.10

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Safflower, seed

0.10

Shallot, bulb

0.10

Sheep, fat

0.04

Sheep, kidney

0.20

Sheep, liver

0.05

Sheep, meat

0.02

Sheep, meat byproducts, except kidney and liver

0.04

Sorghum, grain, forage

1.0

Sorghum, grain, grain

0.3

Sorghum, grain, stover

4.0

Soybean, forage

5.0

Soybean, hay

8.0

Soybean, seed

0.20

Spinach

0.50

Squash, winter

0.10

Sunflower, seed

0.50

Sunflower, meal

1.0

Tomato, paste

0.30

Vegetable, foliage of legume, except soybean, subgroup 7A

15.0

Vegetable, fruiting, except tabasco pepper, group 8

0.10

Vegetable, leaf petioles, subgroup 4B

0.10

Vegetable, legume, edible podded, subgroup 6A

0.50

Vegetable, root, except sugar beet, subgroup 1B

0.30

Vegetable, tuberous and corm, subgroup 1C

0.20

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . (1) Tolerances with regional registration as defined in 180.1(m)
are established for the combined residues (free and bound) of the herbicide metolachlor [2-chloro- N -(2ethyl-6-methylphenyl)- N -(2-methoxy-1-methylethyl)acetamide] and its metabolites, determined as the
derivatives, 2-[2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5methyl-3-morpholinone, each expressed as the parent compound, in or on the following raw agricultural
commodities:

Commodity

Parts per million

Pepper, nonbell

0.50

(2) Tolerances with regional registration as defined in 180.1(m) are established for the combined residues
(free and bound) of the herbicide S -metolachlor, S -2-chloro- N -(2-ethyl-6-methylphenyl)- N -(2- methoxy1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-[(2-ethyl6-methylphenyl)amino]-1- propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3- morpholinone,
each expressed as the parent compound, in or on the following raw agricultural commodities:

Commodity

Parts per million

Pepper, tabasco
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0.50

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(d) Indirect or inadvertent residues . (1) Tolerances are established for the indirect or inadvertent
combined residues (free and bound) of the herbicide metolachlor, 2-chloro- N -(2-ethyl-6- methylphenyl)N -(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the derivatives, 2-[(2-ethyl-6methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone,
each expressed as the parent compound in the following raw agricultural commodities:

Commodity

Parts per million

Animal feed, nongrass, group 18

1.0

Barley, grain

0.10

Barley, straw

0.50

Buckwheat, grain

0.10

Millet, forage

0.50

Millet, grain

0.10

Millet, straw

0.50

Oat, forage

0.50

Oat, grain

0.10

Oat, straw

0.50

Rice, grain

0.10

Rice, straw

0.50

Rye, forage

0.50

Rye, grain

0.10

Rye, straw

0.50

Wheat, forage

0.50

Wheat, grain

0.10

Wheat, straw

0.50

(2) Tolerances are established for the indirect or inadvertent combined residues (free and bound) of the
herbicide S -metolachlor, S -2- chloro- N -(2-ethyl-6-methylphenyl)- N -(2-methoxy-1-methylethyl)
acetamide, its R-enantiomer, and its metabolites determined as the derivatives, 2-[(2-ethyl-6-methylphenyl)
amino]-1-propanol and 4-(2-ethyl-6- methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, each expressed
as the parent compound in or on the following food commodities:

Commodity

Parts per million

Animal feed, nongrass, group 18
Barley, grain
Barley, hay

1.0
0.10
1.0

Barley, straw

0.50

Buckwheat, grain

0.10

Oat, forage

0.50

Oat, grain

0.10

Oat, hay

1.0

Oat, straw

0.50

Rice, grain

0.10

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Rice, straw

0.50

Rye, forage

0.50

Rye, grain

0.10

Rye, straw

0.50

Wheat, forage

0.50

Wheat, grain

0.10

Wheat, hay

1.0

Wheat, straw

0.50

[73 FR 53740, Sept. 17, 2008]

§ 180.369 Difenzoquat; tolerances for residues.
top
(a) General . Tolerances are established for residues of difenzoquat (1,2-dimethyl-3,5-diphenyl-1 H pyrazolium ion), derived from application of the methyl sulfate salt and calculated as the cation, in or on
the following raw agricultural commodities:

Commodity

Parts per million

Barley, bran

0.25

Barley, grain

0.05

Barley, straw

5.0

Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.05

Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Poultry, fat

0.05

Poultry, meat

0.05

Poultry, meat byproducts

0.05

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Wheat, bran

0.25

Wheat, grain

0.05

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Wheat, shorts

0.25

Wheat, straw

5.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 56399, Sept. 27, 2006]

§ 180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.
top
(a) General. Tolerances are established for residues of the fungicide 5-ethoxy-3-(trichloromethyl)-1,2,4thiadiazole and its monoacid metabolite 3-carboxy-5-ethoxy-1,2,4-thiadiazole in or on the following raw
agricultural commodities:

Commodity

Parts per million

Barley, grain

0.1

Barley, hay

0.1

Corn, field, forage

0.1

Corn, field, grain

0.1

Corn, field, stover

0.1

Corn, sweet, forage

0.1

Corn, sweet, stover

0.1

Cotton, gin byproducts

0.1

Cotton, undelinted seed

0.1

Peanut

0.1

Peanut, hay

0.1

Safflower, seed

0.1

Sorghum, grain, forage

0.1

Sorghum, grain, grain

0.1

Tomato

0.15

Vegetable, foliage of legume, group 7

0.1

Vegetable, legume, group 6

0.1

Wheat, forage

0.1

Wheat, grain

0.1

Wheat, straw

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[47 FR 49845, Nov. 3, 1982, as amended at 48 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, 1998; 72
FR 41931, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008]

§ 180.371 Thiophanate-methyl; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of thiophanate-methyl (dimethyl [(1,2phenylene) bis (iminocarbonothioyl)] bis(carbamate)) and its metabolite methyl 2-benzimidazoyl
carbamate (MBC), calculated as thiophanate-methyl in or on the following commodities:

Commodity

Parts per million

Almond

0.1

Almond, hulls

0.5

Apple

2.0

Apricot

15.0

Banana

2.0

Bean, dry, seed

0.2

Bean, snap, succulent

0.2

Beet, sugar, roots

0.2

Beet, sugar, tops

15.0

Cattle, fat

0.15

Cattle, meat

0.15

Cattle, meat byproducts

0.15

Cherry, sweet

20.0

Cherry, tart

20.0

Goat, fat

0.15

Goat, meat

0.15

Goat, meat byproducts

0.15

Grape

5.0

Horse, fat

0.15

Horse, meat

0.15

Horse, meat byproducts

0.15

Milk

0.15

Onion, bulb

0.5

Onion, green

3.0

Peach

3.0

Peanut

0.1

Peanut, hay

5.0

Pear

3.0

Pecan

0.1

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Pistachio

0.1

Plum

0.5

Potato

0.1

Sheep, fat

0.15

Sheep, meat

0.15

Sheep, meat byproducts

0.15

Soybean, seed

0.2

Soybean, hulls

1.5

Strawberry

7.0

Sugarcane, cane

0.1

Vegetable, cucurbit, group 9

1.0

Wheat, grain

0.1

Wheat, hay

0.1

Wheat, straw

0.1

(b) Section 18 emergency exemptions . Tolerances are established for the combined residues of
thiophanate-methyl (dimethyl [(1,2-phenylene) bis (iminocarbonothioyl)] bis(carbamate)) and its metabolite
methyl 2-benzimidazoyl carbamate (MBC), calculated as thiophanate-methyl in or on the following
commodities:

Commodity

Parts per million

Expiration/Revocation Date

Blueberry

1.5

6/30/09

Citrus

0.5

12/31/09

Cotton, gin byproducts

5.0

12/31/08

Cotton, undelinted seed

0.05

12/31/08

Mushroom

0.01

12/31/09

0.5

12/31/09

Vegetable, fruiting, group 8

(c) Tolerances with regional registrations . Tolerances with a regional registration, as defined in 180.1(m),
are established for the combined residues of thiophanate-methyl(dimethyl[(1,2- phenylene)bis
(iminocarbonothioyl) ]bis(carbamate)) and its metabolite methyl 2-benzimidazoyl carbamate (MBC),
calculated as thiophanate-methyl in or on the following commodities:

Commodity

Parts per million

Canola, seed

0.1

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33699, May 24, 2000, as amended at 67 FR 55150, Aug. 28, 2002; 67 FR 57753, Sept. 12, 2002;
72 FR 37654, July 11, 2007; 72 FR 71801, Dec. 19, 2007; 74 FR 636, Jan. 7, 2009]

§ 180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.
top
(a) General . A tolerance is established for residues of the fungicide 2,6-dimethyl-4-tridecylmorpholine in
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or on the following food commodity:

Commodity

Parts per million
1.0

Banana1
1There

are no U.S. registrations.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54961, Sept. 24, 2008]

§ 180.373 [Reserved]
top

§ 180.377 Diflubenzuron; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide diflubenzuron ( N -[[(4chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide) in or on the following food commodities:

Commodity

Parts per million

Artichoke, globe

6.0

Cattle, fat

0.05

Cattle, meat

0.05

Cotton, undelinted seed

0.2

Egg

0.05

Goat, fat

0.05

Goat, meat

0.05

Grapefruit

0.5

Hog, fat

0.05

Hog, meat

0.05

Horse, fat

0.05

Horse, meat

0.05

Milk

0.05

Mushroom

0.2

Orange, sweet

0.5

Poultry, fat

0.05

Poultry, meat byproducts

0.05

Poultry, meat

0.05

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Sheep, fat

0.05

Sheep, meat

0.05

Soybean

0.05

Soybean, hulls

0.5

Tangerine

0.5

(2) Tolerances are established for combined residues of the insecticide diflubenzuron and its metabolites
4-chlorophenlyurea and 4-chloroaniline in or on the following food commodities:

Commodity

Parts per million

Almond, hulls

6.0

Barley, grain

0.06

Barley, hay

3.0

Barley, straw

1.8

Brassica, leafy greens, subgroup 5B

9.0

Cattle, meat byproducts

0.15

Fruit, stone, group 12, except cherry

0.07

Goat, meat byproducts

0.15

Grain, aspirated fractions
Grass, forage, fodder, and hay, group 17

11
6.0

Hog, meat byproducts

0.15

Horse, meat byproducts

0.15

Nut, tree, group 14

0.06

Oat, forage

7.0

Oat, grain

0.06

Oat, hay

6.0

Oat, straw

3.5

Peanut
Peanut, hay

0.10
55

Peanut, refined oil

0.20

Pear

0.50

Pepper

1.0

Pistachio

0.06

Pummelo

0.50

Rice, grain

0.02

Rice, straw

0.8

Sheep, meat byproducts

0.15

Turnip greens

9.0

Wheat, forage

7.0

Wheat, grain

0.06

Wheat, hay

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6.0

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Wheat, straw

3.5

(b) Section 18 emergency exemptions . Time-limited tolerances are established for of the insecticide
diflubenzuron, (N-[[(4-chlorophenyl)amino]carbonyl]-2,6- difluorobenzamide and its metabolites 4chlorophenylurea and 4-chloroaniline, in connection with use of the pesticide under section 18 emergency
exemptions granted by EPA. The tolerances are specified in the following table, and will expire and are
revoked on the dates specified.

Commodity

Parts per million

Expiration/revocation date

Alfalfa, forage

6.0

12/31/11

Alfalfa, hay

6.0

12/31/11

Lemon

0.8

12/31/10

30

12/31/08

0.10

12/31/08

Wheat, aspirated grain fractions
Wheat, milled byproducts
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33699, May 24, 2000, as amended at 65 FR 47882, Aug. 4, 2000; 66 FR 16144, Mar. 23, 2001; 67
FR 7092, Feb. 15, 2002; 67 FR 35048, May 17, 2002; 67 FR 59017, Sept. 19, 2002; 67 FR 59181, Sept.
20, 2002; 68 FR 51484, Aug. 27, 2003; 69 FR 29459, May 24, 2004; 70 FR 75739, Dec. 21, 2005; 71 FR
69033, Nov. 29, 2006; 72 FR 40758, July 25, 2007; 73 FR 72357, Nov. 28, 2008]

§ 180.378 Permethrin; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the insecticide cis- and transpermethrin isomers [cis-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane
carboxylate] and [trans-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane
carboxylate] in/on the following food commodities:

Commodity

Parts per million

Alfalfa, forage

20

Alfalfa, hay

45

Almond
Almond, hulls

0.05
20

Artichoke, globe

5.0

Asparagus

2.0

Avocado

1.0

Broccoli

2.0

Brussels sprouts

1.0

Cabbage

6.0

Cattle, fat

1.5

Cattle, meat

0.10

Cattle, meat byproducts

0.10

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Cauliflower

0.5

Cherry, sweet

4.0

Cherry, tart

4.0

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain

50
0.05
30
0.05

Corn, pop, stover

30

Corn, sweet, forage

50

Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.10
30

Egg

0.10

Eggplant

0.50

Fruit, pome, group 11

0.05

Garlic, bulb

0.10

Grain, aspirated fractions

0.50

Goat, fat

1.5

Goat, meat

0.10

Goat, meat byproducts

0.10

Hazelnut

0.05

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.05

Horse, fat

1.5

Horse, meat

0.10

Horse, meat byproducts

0.10

Horseradish

0.50

Kiwifruit

2.0

Leaf petioles subgroup 4B

5.0

Leafy greens subgroup 4A

20

Lettuce, head

20

Milk, fat (reflecting 0.88 ppm in whole milk)

3.0

Mushroom

5.0

Onion, bulb

0.10

Peach

1.0

Pepper, bell

0.50

Pistachio

0.10

Potato

0.05

Poultry, fat

0.15

Poultry, meat

0.05

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Poultry, meat byproducts

0.05

Sheep, fat

1.5

Sheep, meat

0.10

Sheep, meat byproducts

0.10

Soybean, seed

0.05

Spinach

20

Tomato

2.0

Vegetable, cucurbit, group 9

1.5

Walnut

0.05

Watercress

5.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(m)
are established for the combined residues of the insecticide cis- and trans-permethrin isomers [cis-(3phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] and [trans-(3phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] in/on the following
food commodities:

Commodity

Parts per million

Collards

15

Grass, forage

15

Grass, hay

15

Papaya

1.0

Turnip, tops

10

Turnip, roots

0.20

(d) Indirect or inadvertent residues . [Reserved]
[72 FR 52019, Sept. 12, 2007]

§ 180.379 Cyano(3-phenoxyphenyl)methyl-4-chloro-&b.alpha;-(1-methylethyl)
benzeneacetate; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide Cyano(3-phenoxyphenyl)methyl4-chloro-α-(1-methylethyl)benzeneacetate in or on the following raw agricultural commodities:

Commodity
Almond, hulls

Parts per million
15.0

Almond

0.2

Apple

2.0

Artichoke, globe

0.2

Bean, dry, seed

0.25

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Bean, snap, succulent

2.0

Broccoli

2.0

Blueberry

3.0

Cabbage

10.0

Caneberry subgroup 13A

3.0

Cantaloupe

1.0

Carrot, roots

0.5

Cattle, fat

1.5

Cattle, meat byproducts

1.5

Cattle, meat

1.5

Cauliflower

0.5

Collards

10.0

Corn, grain

0.02

Corn, forage

50.0

Corn, stover

50.0

Corn, sweet, kernel plus cob with husks removed

0.1

Cotton, undelinted seed

0.2

Cucumber

0.5

Currant

3.0

Eggplant

1.0

Elderberry

3.0

Fruit, stone

10.0

Goat, fat

1.5

Goat, meat byproducts

1.5

Goat, meat

1.5

Gooseberry

3.0

Hazelnut

0.2

Hog, fat

1.5

Hog, meat byproducts

1.5

Hog, meat

1.5

Horse, fat

1.5

Horse, meat byproducts

1.5

Horse, meat

1.5

Huckleberry

3.0

Melon, honeydew

1.0

Milk

0.3

Milk, fat

7.0

Muskmelon

1.0

Peanut
Pear

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0.02
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Pea
Pea, dry, seed

1.0
0.25

Pecan

0.2

Pepper

1.0

Potato

0.02

Pumpkin

1.0

Radish, roots

0.3

Radish, tops

8.0

Sheep, fat

1.5

Sheep, meat byproducts

1.5

Sheep, meat

1.5

Soybean

0.05

Squash, summer

0.5

Squash, winter

1.0

Sugarcane, cane

2.0

Sunflower, seed

1.0

Tomato

1.0

Turnip, greens

20.0

Turnip, roots

0.5

Walnut

0.2

Watermelon

1.0

(2) A food additive tolerance of 0.05 parts per million is established for residues of the insecticide cyano
(37phenoxyphenyl)methyl-4-chloro-alpha-(1-methylethyl)benzeneacetate and an isomer, (S)-cyano(3phenoxyphenyl)methyl-(S)-4-chloro-alpha-(1-methylethyl)-benzeneacetate, as follows:
(i) In or on food commodities (other than those already covered by a higher tolerance as a result of use on
growing crops) in food-handling establishments where food products are held, processed, or prepared.
(ii) Application of cyano(3-phenoxyphenyl)methyl-4-chloro-alpha-(1-methylethyl)benzeneacetate shall be
limited to space treatment with a maximum of 0.5 fluid ounce of a 0.05-percent active ingredient solution
per 1,000 cubic feet of space, or as a contact spray applied as a coarse wet spray at a maximum of 1
gallon of a 0.2-percent active ingredient solution per 1,000 square feet of surface. Food must be removed
or covered during treatment. Spray should not be applied directly to surfaces or utensils that may come
into contact with food. Food-contact surfaces and equipment should be thoroughly cleaned with an
effective cleaning compound and rinsed with potable water before using.
(iii) Application of (S)-cyano(3-phenoxyphenyl) methyl-(S)-4-chloro-alpha-(1-methylethyl)benzeneacetate
shall be limited to space treatment with a maximum of 1.0 fluid ounce of a 0.25-percent active ingredient
solution per 1,000 cubic feet of space, or as a contact spray applied as a coarse wet spray at a maximum
of 1 gallon of a 0.05-percent active ingredient solution per 1,000 square feet of surface, or as a
pressurized spot/crack and crevice spray of a 0.25-percent solution. Food must be removed or covered
during treatment. Spray should not be applied directly to surfaces or utensils that may come into contact
with food. Food-contact surfaces and equipment should be thoroughly cleaned with an effective cleaning
compound and rinsed with potable water before using.
(iv) To assure safe use of the additive, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

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(3) A regulation is established permitting residues of the insecticide 4-cyano(3-phenoxyphenyl)methyl 4chloro-alpha-(1-methylethyl)benzeneacetate in or on the following commodities:

Commodity

Parts per million

Soybean, hulls

1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for
residues of the insecticide cyano(3-phenoxyphenyl)methyl-4-chloro-alpha-(1-methylethyl)benzeneacetate
in or on the following raw agricultural commodities:

Commodity

Parts per million

Okra

0.1

(d) Indirect or inadvertent residues. [Reserved]
[44 FR 6099, Jan. 31, 1979. Redesignated and amended at 44 FR 37919, June 29, 1979; further
amended at 55 FR 26440, June 28, 1990]
Editorial Note: ForFederal Registercitations affecting §180.379, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.380 Vinclozolin; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the fungicide vinclozolin (3-(3,5dichlorophenyl)-5-ethenyl-5-methyl-2,4-oxazolidinedione) and its metabolites containing the 3,5dichloroaniline moiety in or on the food commodities in the table below. There are no U.S. registrations for
grape (wine) as of July 30, 1997.

Commodity

Parts per million

Expiration/Revocation Date

Bean, succulent

2.0

11/30/05

Canola, seed

1.0

11/30/08

Cattle, fat

0.05

11/30/08

Cattle, meat

0.05

11/30/08

Cattle, meat byproducts

0.05

11/30/08

Egg

0.05

11/30/08

Goat, fat

0.05

11/30/08

Goat, meat

0.05

11/30/08

Goat, meat byproducts

0.05

11/30/08

Grape, wine

6. 0

None

Hog, fat

0.05

11/30/08

Hog, meat

0.05

11/30/08

Hog, meat byproducts

0.05

11/30/08

Horse, fat

0.05

11/30/08

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Horse, meat

0.05

11/30/08

Horse, meat byproducts

0.05

11/30/08

Lettuce, head

10.0

11/30/05

Lettuce, leaf

10.0

11/30/05

Milk

0.05

11/30/08

Poultry, fat

0.1

11/30/08

Poultry, meat

0.1

11/30/08

Poultry, meat byproducts

0.1

11/30/08

Sheep, fat

0.05

11/30/08

Sheep, meat

0.05

11/30/08

Sheep, meat byproducts

0.05

11/30/08

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
(e) Revoked tolerances subject to the channel of trade provisions. The following table lists commodities
with residues of vinclozolin resulting from lawful use are subject to the channels of trade provisions of
section 408(l)(5) of the FFDCA:

Commodity

Parts per million

Cucumber

1.0

Fruit, stone, except plum, prune, fresh

25.0

Pepper, bell

3.0

Strawberry

10.0

[62 FR 38474, July 18, 1997, as amended at 63 FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, 2000; 67
FR 40189, June 12, 2002; 68 FR 56189, Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR 55268, Sept.
21, 2005]

§ 180.381 Oxyfluorfen; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

Commodity

Parts per million

Almond, hulls

0.1

Artichoke, globe

0.05

Avocado

0.05

Banana

0.05

Broccoli

0.05

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Cabbage

0.05

Cacao bean, dried bean

0.05

Cattle, fat

0.01

Cattle, meat

0.01

Cattle, meat byproducts

0.01

Cauliflower

0.05

Coffee, bean, green

0.05

Corn, field, grain

0.05

Cotton, undelinted seed

0.05

Date, dried fruit

0.05

Egg

0.03

Feijoa

0.05

Fig

0.05

Fruit, pome, group 11

0.05

Fruit, stone, group 12

0.05

Goat, fat

0.01

Goat, meat

0.01

Goat, meat byproducts

0.01

Grape

0.05

Hog, fat

0.01

Hog, meat

0.01

Hog, meat byproducts

0.01

Horse, fat

0.01

Horse, meat

0.01

Horse, meat byproducts

0.01

Horseradish

0.05

Kiwifruit

0.05

Milk

0.01

Nut, tree, group 14

0.05

Olive

0.05

Onion, bulb

0.05

Peppermint, tops

0.05

Persimmon

0.05

Pistachio

0.05

Pomegranate

0.05

Poultry, fat

0.2

Poultry, meat

0.01

Poultry, meat byproducts

0.01

Sheep, fat

0.01

Sheep, meat

0.01

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Sheep, meat byproducts

0.01

Soybean

0.05

Spearmint, tops

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for
residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in
or on the following food commodities:

Commodity

Parts per million

Blackberry

0.05

Chickpea, seed

0.05

Grass, forage

0.05

Grass, hay

0.05

Grass, seed screenings

0.05

Guava

0.05

Papaya

0.05

Raspberry

0.05

Taro, corm

0.05

Taro, leaves

0.05

(d) Indirect or inadvertent residues. [Reserved]
[45 FR 85022, Dec. 24, 1980]
Editorial Note: ForFederal Registercitations affecting §180.381, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.383 Sodium salt of acifluorfen; tolerances for residues.
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(a) General . Tolerances are established for combined residues of the herbicide sodium salt of acifluorfen,
sodium 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, and its metabolites (the corresponding
acid, methyl ester, and amino analogues) in or on the following raw agricultural commodities:

Commodity

Parts per million

Peanut

0.1

Rice, grain

0.1

Rice, straw

0.2

Soybean, seed

0.1

Strawberry
(b) Section 18 emergency exemptions. [Reserved]

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0.05

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(c) Tolerances with regional restrictions. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 24877, Apr. 11, 1980, as amended at 46 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982;
61 FR 30165, June 14, 1996; 62 FR 39974, July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb.
11, 2004; 71 FR 54434, Sept. 15, 2006]

§ 180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the plant growth regulator mepiquat (N,Ndimethylpiperidinium) in or on the following commodities:

Commodity

Parts per million

Cattle, meat byproducts

0.1

Cotton, gin byproducts

6.0

Cotton, undelinted seed

2.0

Goat, meat byproducts

0.1

Hog, meat byproducts

0.1

Horse, meat byproducts

0.1

Sheep, meat byproducts

0.1

(2) Tolerances are established for residues of the plant growth regulator mepiquat chloride (N,Ndimethylpiperidinium chloride) in or on the following commodities:

Commodity

Parts per million

Cattle, fat

0.1

Cattle, meat

0.1

Goat, fat

0.1

Goat, meat

0.1

Grape

1.0

Grape, raisin

5.0

Hog, fat

0.1

Hog, meat

0.1

Horse, fat

0.1

Horse, meat

0.1

Sheep, fat

0.1

Sheep, meat

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
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[67 FR 3118, Jan. 23, 2002]

§ 180.385 Diclofop-methyl; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of the herbicide diclofop-methyl (methyl
2-[4-(2,4-dichlorophenoxy)phenoxy]propanoate) and its metabolites, 2-[4-(2,4-dichlorophenoxy)phenoxy]
propanoic acid and 2-[4-(2,4-dichloro-5-hydroxyphenoxy)phenoxy]propanoic acid, in or on the following
raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.1

Barley, straw

0.1

Wheat, grain

0.1

Wheat, straw

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, 1986; 51
FR 19176, May 28, 1986; 63 FR 57077, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007]

§§ 180.388-180.389 [Reserved]
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§ 180.390 Tebuthiuron; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(2-hydroxy-1,1dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-Nmethylurea, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the
following raw agricultural commodities:

Commodity

Parts per million

Grass, forage

10.0

Grass, hay

10.0

(2) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, 2-dimethylethyl-5-amino1,3,4-thiadiazole, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or
on the following raw agricultural commodities:

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Commodity

Parts per million

Cattle, fat

1.0

Cattle, meat

1.0

Cattle, meat byproducts

5.0

Goat, fat

1.0

Goat, meat

1.0

Goat, meat byproducts

5.0

Horse, fat

1.0

Horse, meat

1.0

Horse, meat byproducts

5.0

Sheep, fat

1.0

Sheep, meat

1.0

Sheep, meat byproducts

5.0

(3) A tolerance is established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4thiadiazol-2-yl)-N-methylurea, N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'hydroxymethyl-N-methylurea, and N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity

Parts per million

Milk

0.8

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 53461, Sept. 19, 2007]

§ 180.395 Hydramethylnon; tolerances for residues.
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(a) General. Tolerances are established for residues of the insecticide tetrahydro-5,5-dimethyl-2(1 H )pyrimidinone(3-(4-(trifluoromethyl)phenyl)-1-(2-(4-(trifluoromethyl)phenyl)ethenyl)-2-propenylidene)
hydrazone in or on the following raw agricultural commodities:

Commodity

Parts per million

Grass, forage

2.0

Grass, hay

2.0

Pineapple

0.05

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 55198, Aug. 19, 1980, as amended at 63 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, 1998; 66
FR 28672, May 24, 2001; 68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR 41931, Aug.
1, 2007]

§ 180.396 Hexazinone; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of hexazinone (3-cyclohexyl-6(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione) and its plant metabolites; A [3-(4hydroxycyclohexyl)-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione], B [3-cyclohexyl-6(methylamino)-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione], C [3-(4-hydroxycyclohexyl)-6-(methylamino)1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione], D [3-cyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1 H ,3 H ,5
H )-trione], and E [3-(4-hydroxycyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1 H ,3 H ,5 H )-trione] (calculated
as hexazinone) in the following commodities:

Commodity

Parts per million

Alfalfa, forage

2.0

Alfalfa, hay

8.0

Alfalfa, seed

2.0

Blueberry

0.6

Grass, forage

10.0

Pineapple

0.6

(2) Tolerances are established for the combined residues of hexazinone (3-cyclohexyl-6-(dimethylamino)1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione) and its animal tissue metabolites; B [3-cyclohexyl-6(methylamino)-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione], and F (3-cyclohexyl-6-amino-1-methyl-1,3,5triazine-2,4-(1 H ,3 H )-dione) (calculated as hexazinone) in the following food commodities:

Commodity

Parts per million

Cattle, fat

0.1

Cattle, meat

0.1

Cattle, meat byproducts

0.1

Goat, fat

0.1

Goat, meat

0.1

Goat, meat byproducts

0.1

Hog, fat

0.1

Hog, meat

0.1

Hog, meat byproducts

0.1

Horse, fat

0.1

Horse, meat

0.1

Horse, meat byproducts

0.1

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Sheep, fat

0.1

Sheep, meat

0.1

Sheep, meat byproducts

0.1

(3) Tolerances are established for the combined residues of hexazinone (3-cyclohexyl-6-(dimethylamino)1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione) and its metabolites; B [3-cyclohexyl-6-(methylamino)-1methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione], C [3-(4-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5triazine-2,4-(1 H ,3 H )-dione], C-2 [3-(3-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1
H ,3 H )-dione] and F (3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione) (calculated as
hexazinone) in milk:

Commodity

Parts per million

Milk

0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(n)
and which excludes use of hexazinone on sugarcane in Florida, are established for the combined residues
of hexazinone (3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione and its plant
metabolites; A [3-(4-hydroxycyclohexyl)-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4(1 H ,3 H )-dione], B
[3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione], C [3-(4-hydroxycyclohexyl)-6(methylamino)-1-methyl-1,3,5-triazine-2,4-(1 H ,3 H )-dione], D [(3-cyclohexyl)-1-methyl-1,3,5-triazine2,4,6-(1 H ,3 H ,5 H )-trione], and E [3-(4-hydroxycyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1 H ,3 H ,5 H )trione] (calculated as hexazinone) in the following commodities:

Commodity

Parts per milliom

Sugarcane, cane

0.6

Sugarcane, molasses

4.0

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33713, May 24, 2000, as amended at 71 FR 56399, Sept. 27, 2006]

§ 180.399 Iprodione; tolerances for residues.
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(a) General. (1) Tolerances are established for the combined residues of the fungicide iprodione [3-(3,5dichlorophenyl)- N -(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer 3-(1-methylethyl)- N (3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolite 3-(3,5-dichlorophenyl)-2,4dioxo-1-imidazolidine-carboxamide in or on the following food commodities:

Commodity

Parts per million

Almond, hulls

2.0

Almond

0.3

Apricot

20.0

Bean, dry, seed
Bean, forage
Bean, succulent
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2.0
90.0
2.0

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Blueberry

15.0

Boysenberry

15.0

Broccoli

25.0

Caneberry subgroup 13A

25.0

Carrot, roots

5.0

Cherry, sweet, postharvest

20.0

Cherry, tart

20.0

Cotton, undelinted seed

0.10

Cowpea, hay

90.0

Currant

15.0

Garlic

0.1

Ginseng

2.0

Ginseng, dried root

4.0

Grape

60.0

Grape, raisin

300

Kiwifruit

10.0

Lettuce

25.0

Nectarine, postharvest

20.0

Onion, bulb

0.5

Peach, postharvest

20.0

Peanut

0.5

Peanut, hay

150.0

Plum, postharvest

20.0

Plum, prune

20.0

Potato

0.5

Raspberry

15.0

Rice, bran

30.0

Rice, grain

10.0

Rice, hulls

50.0

Rice, straw

20.0

Strawberry

15.0

(2) Tolerances are established for the combined residues of iprodione [3-(3,5-dichlorophenyl)- N -(1methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)- N -(3,5-dichlorophenyl)2,4-dioxo-1-imidazolidinecarboxamide, and its metabolites [3-(3,5-dichlorophenyl)-2,4-dioxo-1imidazolidine-carboxamide] and [ N -(3,5-dichloro-4-hydroxyphenyl)-ureido-carboxamide], all expressed as
iprodione equivalents in or on the following food commodities of animal origin:

Commodity

Parts per million

Cattle, fat

0.5

Cattle, kidney

3.0

Cattle, liver

3.0

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Cattle, meat

0.5

Cattle, meat byproducts, except kidney and liver

0.5

Egg

1.5

Goat, fat

0.5

Goat, kidney

3.0

Goat, liver

3.0

Goat, meat

0.5

Goat, meat byproducts, except kidney and liver

0.5

Hog, fat

0.5

Hog, kidney

3.0

Hog, liver

3.0

Hog, meat

0.5

Hog, meat byproducts, except kidney and liver

0.5

Horse, fat

0.5

Horse, kidney

3.0

Horse, liver

3.0

Horse, meat

0.5

Horse, meat byproducts, except kidney and liver

0.5

Milk

0.5

Poultry, fat

3.5

Poultry, liver

5.0

Poultry, meat

1.0

Poultry, meat byproducts, except liver

1.0

Sheep, fat

0.5

Sheep, kidney

3.0

Sheep, liver

3.0

Sheep, meat

0.5

Sheep, meat byproducts, except kidney and liver

0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)2,4-dioxo-1-imidazolidinecarboxamide], and its metabolite [3-(3,5-dichlorophenyl)-2,4-dioxo-1imidazolidinecarboxamide] in or on the following food commodity:

Commodity

Parts per million

Mustard greens
(d) Indirect or inadvertent residues. [Reserved]
[48 FR 40385, Sept. 7, 1983]

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15.0

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Editorial Note: ForFederal Registercitations affecting §180.399, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.401 Thiobencarb; tolerances for residues.
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(a) Tolerances are established for the combined residues of the herbicide thiobencarb ( S -[(4chlorophenyl)methyl]diethyl-carbamothioate) and its chlorobenzyl and chlorophenyl moiety-containing
metabolites in or on the following raw agricultural commodities:

Commodity

Part per million

Cattle, fat

0.2

Cattle, meat byproducts

0.2

Cattle, meat

0.2

Egg

0.2

Goat, fat

0.2

Goat, meat byproducts

0.2

Goat, meat

0.2

Hog, fat

0.2

Hog, meat byproducts

0.2

Hog, meat

0.2

Horse, fat

0.2

Horse, meat byproducts

0.2

Horse, meat

0.2

Milk

0.05

Poultry, fat

0.2

Poultry, meat byproducts

0.2

Poultry, meat

0.2

Rice, grain

0.2

Rice, straw

1.0

Sheep, fat

0.2

Sheep, meat byproducts

0.2

Sheep, meat

0.2

(b) Tolerances with regional registration, as defined in §180.1(n), are established for residues of the
herbicide thiobencarb (S-[(4-chloro-phenyl)methyl]diethylcarbamothioate) and its chlorobenzyl and
chlorophenyl moiety-containing metabolites in or on the following raw agricultural commodities:

Commodity

Parts per million

Celery

0.2

Endive

0.2

Lettuce

0.2

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[47 FR 6833, Feb. 17, 1982, as amended at 56 FR 2440, Jan. 23, 1991]

§ 180.403 Thidiazuron; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of the defoliant thidiazuron (N-phenylN-1,2,3-thiadiazol-5-ylurea) and its aniline containing metabolites in or on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.4

Cattle, meat

0.4

Cattle, meat byproducts

0.4

Cotton, gin byproducts

24.0

Cotton, undelinted seed

0.3

Goat, fat

0.4

Goat, meat

0.4

Goat, meat byproducts

0.4

Hog, fat

0.4

Hog, meat

0.4

Hog, meat byproducts

0.4

Horse, fat

0.4

Horse, meat

0.4

Horse, meat byproducts

0.4

Milk

0.05

Sheep, fat

0.4

Sheep, meat

0.4

Sheep, meat byproducts

0.4

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33700, May 24, 2000, as amended at 72 FR 53462, Sept. 19, 2007]

§ 180.404 Profenofos; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide profenofos (O-(4-bromo-2chlorophenyl)-O-ethyl-S-propyl phosphorothioate) in or on the following food commodities:

Commodity

Parts per million

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Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Cotton, gin byproducts

55.0

Cotton, undelinted seed

2.0

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Milk

0.01

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, 2002; 72
FR 54579, Sept. 26, 2007]

§ 180.405 Chlorsulfuron; tolerances for residues.
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(a) General. (1) Tolerances are established for the combined residues of chlorsulfuron (2-chloro- N- [(4methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl]benzenesulfonamide) and its metabolite, 2-chloro-5hydroxy- N- [(4-methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl] benzenesulfonamide in or on the
following raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.1

Barley, straw

0.5

Oat, forage

20.0

Oat, grain

0.1

Oat, straw

0.5

Wheat, forage

20.0

Wheat, grain

0.1

Wheat, straw

0.5

(2) Tolerances are established for residues of chlorsulfuron (2-chloro- N- [(4-methoxy-6-methyl-1,3,5-

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triazin-2- yl)aminocarbonyl] benzenesulfonamide) in or on the following raw agricultural commodities.

Commodity

Parts per million

Cattle, fat

0.3

Cattle, meat

0.3

Cattle, meat byproducts

0.3

Goat, fat

0.3

Goat, meat

0.3

Goat, meat byproducts

0.3

Grass, forage

11.0

Grass, hay

19.0

Hog, fat

0.3

Hog, meat

0.3

Hog, meat byproducts

0.3

Horse, fat

0.3

Horse, meat

0.3

Horse, meat byproducts

0.3

Milk

0.1

Sheep, fat

0.3

Sheep, meat

0.3

Sheep, meat byproducts

0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 52873, Aug. 14, 2002]

§ 180.406 Dimethipin; tolerances for residues.
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(a) General. Tolerances are established for residues of the harvest growth regulant dimethipin (2,3dihydro-5,6-dimethyl-1,4-dithiin 1,1,4,4-tetraoxide; CAS Reg. No. 55290–64–7) in or on the following food
commodities:

Commodity

Parts per million

Expiration/Revocation Date

Cattle, meat

0.01

5/31/10

Cattle, meat byproducts

0.01

5/31/10

Cotton, undelinted seed

0.50

5/31/10

Goat, meat

0.01

5/31/10

Goat, meat byproducts

0.01

5/31/10

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Hog, meat

0.01

5/31/10

Hog, meat byproducts

0.01

5/31/10

Horse, meat

0.01

5/31/10

Horse, meat byproducts

0.01

5/31/10

Sheep, meat

0.01

5/31/10

Sheep, meat byproducts

0.01

5/31/10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33700, May 24, 2000, as amended at 72 FR 52019, Sept. 12, 2007; 73 FR 54962, Sept. 24, 2008]

§ 180.407 Thiodicarb; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of the insecticide thiodicarb (dimethyl
N , N ′-[thiobis[[(methylimino)carbonyloxy]] bis[ethanimidothioate]) and its metabolite methomyl ( S methyl N -[(methylcarbamoyl) oxy]thioacetimidate) in or on the following food commodities or groups.
The time-limited tolerances expire and are revoked on the dates listed in the following table:

Commodity

Parts per million Expiration/revocation date

Broccoli

7.0

None

Cabbage

7.0

None

Cauliflower

7.0

None

Corn, sweet, kernel plus cob with
husks removed

2.0

None

Cotton, undelinted seed

0.4

None

Cotton, hulls

0.8

None

Soybean, hulls

0.8

None

Soybean

0.2

None

35

None

Vegetable, leafy, except brassica,
group 4
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 44595, Aug. 22, 1997]

§ 180.408 Metalaxyl; tolerances for residues.

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(a) General. Tolerances are established for the combined residues of the fungicide metalaxyl [ N -(2,6dmethylphyenyl)- N -(methoxyacetyl) alanine methylester] and its metabolites containing the 2,6dimethylaniline moiety, and N -(2-hydroxy methyl-6-methylphenyl)- N -(methoxyacetyl)-alanine methyl
ester, each expressed as metalaxyl equivalents, in or on the following food commodities:

Commodity
Alfalfa, forage
Alfalfa, hay
Almond
Almond, hulls

Parts per million
6.0
20.0
0.5
10.0

Apple

0.2

Apple, wet pomace

0.4

Apricot, dried

4.0

Asparagus

7.0

Avocado

4.0

Beet, garden, roots

0.1

Beet, garden, tops

0.1

Beet, sugar

0.1

Beet, sugar, molasses

1.0

Beet, sugar, roots

0.5

Beet, sugar, tops

10.0

Blueberry

2.0

Broccoli

2.0

Brussels sprouts

2.0

Cabbage

1.0

Cattle, fat

0.4

Cattle, kidney

0.4

Cattle, liver

0.4

Cattle, meat

0.05

Cattle, meat byproducts, except kidney and liver

0.05

Cauliflower

1.0

Citrus, oil

7.0

Citrus, dried pulp

7.0

Clover, forage

1.0

Clover, hay

2.5

Cotton, undelinted seed

0.1

Cranberry

4.0

Egg

0.05

Fruit, citrus

1.0

Fruit, stone, group 12

1.0

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Ginseng

3.0

Goat, fat

0.4

Goat, kidney

0.4

Goat, liver

0.4

Goat, meat

0.05

Goat, meat byproducts, except kidney and liver

0.05

Grain, cereal, group 15, except barley, oat and wheat

0.1

Grain, crop

0.1

Grape

2.0

Grape, raisin

6.0

Grass, forage

10.0

Grass, hay

25.0

Hog, fat

0.4

Hog, kidney

0.4

Hog, liver

0.4

Hog, meat

0.05

Hog, meat byproducts, except kidney and liver

0.05

Hop, dried cones

20

Hop, vines

2.0

Horse, fat

0.4

Horse, kidney

0.4

Horse, liver

0.4

Horse, meat

0.05

Horse, meat byproducts, except kidney and liver

0.05

Lettuce, head
Milk

5.0
0.02

Mustard greens

5.0

Onion, bulb

3.0

Onion, green
Peanut

10.0
0.2

Peanut, hay

20.0

Peanut, meal

1.0

Peanut, hulls

2.0

Pineapple

0.1

Pineapple, fodder

0.1

Pineapple, forage

0.1

Plum, prune, dried

4.0

Potato, processed (including potato, chips)

4.0

Potato, processed potato waste

4.0

Poultry, fat

0.4

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Poultry, kidney

0.4

Poultry, liver

0.4

Poultry, meat

0.05

Poultry, meat byproducts, except kidney and liver

0.05

Potato

0.5

Raspberry

0.5

Sheep, fat

0.4

Sheep, kidney

0.4

Sheep, liver

0.4

Sheep, meat

0.05

Sheep, meat byproducts, except kidney and liver

0.05

Soybean, hulls

2.0

Soybean, meal

2.0

Soybean, seed

1.0

Spinach

10.0

Strawberry

10.0

Sunflower, seed

0.1

Sunflower, forage

0.1

Tomato, processed

3.0

Vegetable, brassica, leafy, group 5, except broccoli, cabbage,
cauliflower, brussels sprouts, and mustard greens

0.1

Vegetable, cucurbit, group 9

1.0

Vegetable, foilage of legume, group 7

8.0

Vegetable, fruiting, group 8

1.0

Vegetable, leafy, except brassica, group 4, except spinach

5.0

Vegetable, leaves of root and tuber, group 2

15.0

Vegetable, legume, cannery waste

5.0

Vegetable, legume, group 6

0.2

Vegetable, root and tuber, group 1

0.5

Walnut

0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration (refer to §180.1(n)) are
established for the combined residues of the fungicide metalaxyl [ N -(2,6-dimethylphenyl)- N (methoxyacetyl) alanine methyl ester] and its metabolites containing the 2,6-dimethylaniline moiety, and N (2-hydroxy methyl-6-methyl)- N -(methoxyacetyl)-alanine methylester, each expressed as metalaxyl, in or
on the following raw agricultural commodity:

Commodity

Parts per million

Papaya

0.1

(d) Indirect or inadvertent tolerances. Tolerances are established for indirect or inadvertent residues of
metalaxyl in or on the food commodities when present therein as a result of the application of metalaxyl to
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growing crops listed in paragraph (a) of this section and other non-food crops to read as follows:

Commodity

Part per million

Barley, grain

0.2

Barley, milling fractions

1.0

Barley, straw

2.0

Grain, cereal, forage, fodder and straw, group 16, except barley, oat,
and wheat; forage

1.0

Grain, cereal, forage, fodder and straw, group 16, except barley, oat,
and wheat; stover

1.0

Grain, cereal, forage, fodder and straw, group 16, except barley, oat,
and wheat; straw

1.0

Oat, forage

2.0

Oat, grain

0.2

Oat milling fractions

1.0

Oat, straw

2.0

Wheat, forage

2.0

Wheat, grain

0.2

Wheat, milling fractions

1.0

Wheat, straw

2.0

[65 FR 33700, May 24, 2000, as amended at 72 FR 35666, June 29, 2007]

§ 180.409 Pirimiphos-methyl; tolerances for residues.
top
(a) General . Tolerances are established for residues of the insecticide pirimiphos-methyl (O-(2diethylamino-6-methyl-4-pyrimidinyl) O,O-dimethyl phosphorothioate) in or on the following raw agricultural
commodities:

Commodity

Parts per million

Cattle, fat

0.02

Cattle, meat byproducts

0.02

Corn, field, grain

8.0

Corn, pop, grain

8.0

Goat, fat

0.02

Goat, meat byproducts

0.02

Grain, aspirated fractions

20.0

Hog, fat

0.02

Hog, meat byproducts

0.02

Horse, fat

0.02

Horse, meat byproducts

0.02

Poultry, fat

0.02

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Sheep, fat

0.02

Sheep, meat byproducts

0.02

Sorghum, grain, grain

8.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33714, May 24, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 49617, July 31, 2002;
70 FR 44492, Aug. 3, 2005; 72 FR 53462, Sept. 19, 2007]

§ 180.410 Triadimefon; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the fungicide triadimefon, 1-(4chlorophenoxy)-3,3-dimethyl-1-(1 H -1,2,4-triazol-1-yl)-2-butanone, and triadimenol, β-(4-chlorophenoxy)-α(1,1-dimethylethyl)-1 H -1,2,4-triazole-1-ethanol, expressed as triadimefon, in or on the following food
commodities:

Commodity

Parts per million

Expiration/Revocation Date

Apple

1.0

7/25/10

Apple, wet pomace

4.0

7/25/10

Grape

1.0

7/25/10

Pear

1.0

7/25/10

Pineapple

2.0

None

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registrations, as defined in § 180.1(m),
are established for the combined residues of the fungicide triadimefon, 1-(4-chlorophenoxy)-3,3-dimethyl-1(1 H -1,2,4-triazol-1-yl)-2-butanone, and triadimenol, β-(4-chlorophenoxy)-α-(1,1-dimethylethyl)-1 H -1,2,4triazole-1-ethanol, expressed as triadimefon, in or on the following food commodities:

Commodity

Parts per million

Raspberry

Expiration/Revocation Date
2.0

7/25/10

(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54962, Sept. 24, 2008]

§ 180.411 Fluazifop-P-butyl; tolerances for residues.
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(a) General . Tolerances are established for residues of the herbicide, fluazifop-P-butyl, butyl(R)-2-[4-[[5(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, and the free and conjugated forms of the resolved
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isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, expressed as
fluazifop, in or on the following commodities:

Commodity

Parts per million

Beans, dry, seed
Carrot, roots

50
2.0

Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Cotton, oil

0.2

Cotton, undelinted seed

0.1

Egg
Endive

0.05
6.0

Fruit, stone

0.05

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.05

Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Milk

0.05

Nut, macadamia

0.1

Onion, bulb

0.5

Peanut

1.5

Peanut, meal

2.2

Pecans

0.05

Poultry, fat

0.05

Poultry, meat

0.05

Poultry, meat byproducts

0.05

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Soybean, seed

2.5

Spinach

6.0

Sweet potato, roots
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registrations are established for

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0.05

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residues of the herbicide, fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]
propanoate, and the free and conjugated forms of the resolved isomer of fluazifop, (R)-2-[4-[[5(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, expressed as fluazifop, in or on the following
commodities:

Commodity

Parts per million

Asparagus

3.0

Coffee, bean

0.1

Pepper, tabasco

1.0

Rhubarb

0.5

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33714, May 24, 2000, as amended at 74 FR 9372, Mar. 4, 2009]

§ 180.412 Sethoxydim; tolerances for residues.
top
(a) General . Tolerances are established for combined residues of the herbicide 2-[1-(ethoxyimino)butyl]-5[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one (CAS Reg. No. 74051–80–2) and its metabolites
containing the 2-cyclohexen-1-one moiety (calculated as the herbicide) in or on the following commodities:

Commodity

Parts per million

Alfalfa, forage

40

Alfalfa, hay

40

Almond, hulls

2.0

Apricot

0.2

Apple, wet pomace

0.8

Asparagus

4.0

Bean, succulent

15

Beet, sugar, molasses

10

Beet, sugar, tops

3.0

Blueberry

4.0

Borage, meal

10

Borage, seed

6.0

Buckwheat, flour

25

Buckwheat, grain

19

Caneberry subgroup 13 A

5.0

Canola, meal

40

Canola, seed

35

Cattle, fat

0.2

Cattle, meat

0.2

Cattle, meat byproducts

1.0

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Cherry, sweet

0.2

Cherry, tart

0.2

Citrus, dried pulp

1.5

Clover, forage

35

Clover, hay

55

Coriander, leaves

4.0

Corn, field, forage

2.0

Corn, field, grain

0.5

Corn, field, stover

2.5

Corn, sweet, forage

3.0

Corn, sweet, kernel plus cob with husk removed

0.4

Corn, sweet, stover

3.5

Cotton, undelinted seed

5.0

Cowpea, forage

15

Cowpea, hay

50

Crambe, meal

40.0

Crambe, seed

35.0

Cranberry
Cuphea, seed
Dillweed, fresh leaves
Echium, seed

2.5
35.0
10
35.0

Egg

2.0

Flax, seed

5.0

Fruit, citrus, group 10

0.5

Fruit, pome, group 11

0.2

Goat, fat

0.2

Goat, meat

0.2

Goat, meat byproducts

1.0

Gold of pleasure, meal

40.0

Gold of pleasure, seed

35.0

Grape

1.0

Grape, raisin

2.0

Hare's ear mustard, seed

35.0

Hog, fat

0.2

Hog, meat

0.2

Hog, meat byproducts

1.0

Horse, fat

0.2

Horse, meat

0.2

Horse, meat byproducts

1.0

Juneberry

5.0

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Lesquerella, seed
Lingonberry

35.0
5.0

Lunaria, seed

35.0

Meadowfoam, seed

35.0

Milk

0.5

Milkweed, seed

35.0

Mustard, seed

35.0

Nectarine

0.2

Nut, tree, group 14

0.2

Oil radish, seed
Okra

35.0
2.5

Pea and bean, dried shelled, except soybean, subgroup 6C

25

Pea, field, hay

40

Pea, field, vines

20

Pea, succulent

10

Peach

0.2

Peanut

25

Peppermint, tops

30

Pistachio
Poppy, seed

0.2
35.0

Potato granules/flakes

8.0

Potato waste, processed

8.0

Poultry, fat

0.2

Poultry, meat

0.2

Poultry, meat byproducts

2.0

Radish, tops

4.5

Rapeseed, meal

40

Rapeseed, seed

35

Safflower, seed

15

Salal
Sesame, seed

5.0
35.0

Sheep, fat

0.2

Sheep, meat

0.2

Sheep, meat byproducts

1.0

Soybean, hay

10

Soybean, seed

16

Spearmint, tops

30

Strawberry

10

Sunflower, meal

20

Sunflower, seed

7.0

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Sweet rocket, seed

35.0

Turnip, tops

5.0

Vegetable, brassica, leafy, group 5

5.0

Vegetable, bulb, group 3

1.0

Vegetable, cucurbit, group 9

4.0

Vegetable, fruiting, group 8

4.0

Vegetable, leafy, except brassica, group 4

4.0

Vegetable, root and tuber, group 1

4.0

(b) Section 18 emergency exemptions.
(c) Tolerances with regional registration. Tolerances with regional registration, as defined in §180.1(m),
are established for the combined residues of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]3-hydroxy-2-cyclohexen-1-one) and its metabolites containing the 2-cyclohexen-1-one moiety (calculated
as the herbicide) in or on the following commodities:

Commodity

Parts per million

Expiration/Revocation Date

Artichoke, globe

5.0

None

Rhubarb

0.3

None

(d) Indirect and inadvertent residues. [Reserved]
[62 FR 17740, Apr. 11, 1997]
Editorial Note: ForFederal Registercitations affecting §180.412, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.413 Imazalil; tolerances for residues.
top
(a) General . (1) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4dichlorophenyl)-2-(2-propenyloxy)ethyl]-1 H -imidazole, and its metabolite, 1-(2,4-dichlorophenyl)-2-(1 H imidazole-1-yl)-1-ethanol, in or on the following food commodities:

Commodity

Parts per million

Banana

3.0

Barley, grain

0.1

Barley, hay

0.5

Barley, straw

0.5

Citrus, dried pulp
Citrus, oil
Fruit, citrus, postharvest

25.0
200.0
10.0

Wheat, forage

0.5

Wheat, grain

0.1

Wheat, hay

0.5

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Wheat, straw

0.5

(2) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4dichlorophenyl)-2-(2-propenyloxy)ethyl]-1 H -imidazole, and its metabolites, 3-[2-(2,4-dichlorophenyl)-2(2,3-dihydroxypropoxy)ethyl]-2,4-imidazolidinedione (FK772) and 3-[2-(2,4-dichlorophenyl)-2-(hydroxy)]2,4-imidazolidinedione (FK284), in or on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.01

Cattle, meat

0.01

Cattle, meat byproducts

0.2

Goat, fat

0.01

Goat, meat

0.01

Goat, meat byproducts

0.2

Horse, fat

0.01

Horse, meat

0.01

Horse, meat byproducts

0.2

Milk

0.02

Sheep, fat

0.01

Sheep, meat

0.01

Sheep, meat byproducts

0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33715, May 24, 2000, as amended at 67 FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006]

§ 180.414 Cyromazine; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide cyromazine ( N -cyclopropyl1,3,5-triazine-2,4,6-triamine) in or on the following raw agricultural commodities:

Commodity

Parts per million

Bean, dry, except cowpea

3.0

Bean, lima

1.0

Broccoli

1.0

Cabbage, abyssinian

10.0

Cabbage, seakale

10.0

Cattle, fat

0.05

Cattle, kidney
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Cattle, meat

0.05

Cattle, meat byproducts, except kidney

0.05

Egg

0.25

Garlic

0.2

Garlic, great-headed, bulb

0.2

Goat, fat
Goat, kidney

0.05
0.2

Goat, meat

0.05

Goat, meat byproducts, except kidney

0.05

Hanover salad, leaves

10.0

Hog, fat

0.05

Hog, kidney

0.2

Hog, meat

0.05

Hog, meat byproducts, except kidney

0.05

Horse, fat

0.05

Horse, kidney

0.2

Horse, meat

0.05

Horse, meat byproducts, except kidney

0.05

Leek

3.0

Mango1

0.3

Milk

0.05

Mushroom

1.0

Onion, bulb

0.2

Onion, green

3.0

Onion, potato

3.0

Onion, tree

3.0

Onion, welsh

3.0

Pepper

1.0

Potato

0.8

Poultry, fat (from chicken layer hens and chicken breeder hens only)

0.05

Poultry, meat (from chicken layer hens and chicken breeder hens
only)

0.05

Poultry, meat byproducts (from chicken layer hens and chicken
breeder hens only)

0.05

Rakkyo, bulb

0.2

Shallot, bulb

0.2

Shallot, fresh leaves

3.0

Sheep, fat
Sheep, kidney

0.05
0.2

Sheep, meat

0.05

Sheep, meat byproducts, except kidney

0.05

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Tomato

0.5

Turnip, greens

10.0

Vegetable, brassica, leafy, group 5, except broccoli

10.0

Vegetable, leafy, except brassica, group 4

7.0

Vegetable, cucurbit, group 9

1.0

1There

are no U.S. registrations on mango as of May 4, 2000.

(2) The additive cyromazine ( N -cyclopropyl-1,3,5-triazine-2,4,6-triamine) may be safely used in
accordance with the following prescribed conditions:
(i) It is used as a feed additive only in feed for chicken layer hens and chicken breeder hens at the rate of
not more than 0.01 pound of cyromazine per ton of poultry feed.
(ii) It is used for control of flies in manure of treated chicken layer hens and chicken breeder hens.
(iii) Feeding of cyromazine-treated feed must stop at least 3 days (72 hours) before slaughter. If the feed is
formulated by any person other than the end user, the formulator must inform the end user, in writing, of
the 3–day (72 hours) preslaughter interval.
(iv) To ensure safe use of the additive, the labeling of the pesticide formulation containing the feed additive
shall conform to the labeling which is registered by the U.S. Environmental Protection Agency, and the
additive shall be used in accordance with this registered labeling.
(v) Residues of cyromazine are not to exceed 5.0 parts per million (ppm) in poultry feed.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of
cyromazine ( N -cyclopropyl-1,3,5-triazine-2,4,6-triamine), in or on the raw agricultural commodities when
present therein as a result of the application of cyromazine to growing crops listed in paragraph (a)(1) of
this section.

Commodity

Parts per million

Cotton, undelinted seed

0.1

Corn, sweet, kernel plus cob with husks removed

0.5

Corn, sweet, forage

0.5

Corn, sweet, stover

0.5

Radish, roots

0.5

Radish, tops

0.5

[65 FR 25860, May 4, 2000, as amended at 67 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, 2003]

§ 180.415 Aluminum tris ( O

-ethylphosphonate); tolerances for residues.

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(a) General. Tolerances are established for residues of the fungicide aluminum tris( O -ethylphosphonate)
in or on the following food commodities:

Commodity

Parts per million Expiration/Revocation Date

Avocado

25

None

Banana

3.0

None

Blueberry

40

12/31/00

Bushberry subgroup 13B

40

None

Caneberry subgroup 13A

0.1

None

Cranberry

0.5

None

Fruit, citrus, group 10

5.0

None

10

None

0.1

None

Hop, dried cones

45

None

Juneberry

40

None

Lingonberry

40

None

Nut, macadamia

0.20

None

Onion, green

10.0

None

Pea, succulent

0.3

None

Pineapple

0.1

None

Pineapple, fodder

0.1

None

Pineapple, forage

0.1

None

Onion, bulb

0.5

None

Salal

40

None

Strawberry

75

None

3

None

Turnip, greens

40

None

Turnip, roots

15

None

Vegetable, brassica, leafy, group 5

60

None

Vegetable, cucurbit, group 9

15

None

100

None

Fruit, pome
Ginseng

Tomato

Vegetable, leafy, except brassica,
group 4
(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for residues of the fungicide aluminum tris ( O -ethylphosphonate) in or on the following
raw agricultural commodities:

Commodity

Parts per million

Asparagus
Grape

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0.1
10

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(d) Indirect or inadvertent residues. [Reserved]
[64 FR 36801, July 8, 1999, as amended at 64 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, 2000; 67
FR 55346, Aug. 29, 2002; 68 FR 11335, Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005]

§ 180.416 Ethalfluralin; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide ethalfluralin [ N -ethyl- N -(2-methyl-2propenyl)-2,6-dinitro-4-(trifluoromethyl)benzenamine] in or on the following raw agricultural commodities:

Commodity

Parts per million

Bean, dry, seed

0.05

Dill, dried leaves

0.05

Dill, fresh leaves

0.05

Mustard, seed

0.05

Peanut

0.05

Pea, dry, seed

0.05

Potato

0.05

Rapeseed, seed

0.05

Safflower, seed

0.05

Soybean

0.05

Sunflower, seed

0.05

Vegetable, cucurbit, group 9

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[49 FR 391, Jan. 4, 1984, as amended at 50 FR 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 FR
66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, July 19, 2001;
66 FR 41454, Aug. 8, 2001; 67 FR 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; 72 FR 68534, Dec.
5, 2007]

§ 180.417 Triclopyr; tolerances for residues.
top
(a) General . (1) Tolerances for residues of the herbicide triclopyr per se, as a result of the application/use
of butoxyethyl ester of triclopyr and triethyylamine salt of triclopyr, are established in or on the following
raw agricultural commodities:

Commodity

Parts per million

Egg

0.05

Fish

3.0

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Grass, forage

700.0

Grass, hay

200.0

Milk

0.01

Poultry, fat

0.1

Poultry, meat

0.1

Poultry, meat byproducts, except kidney

0.1

Rice, grain

0.3

Rice, straw

10.0

Shellfish

3.5

(2) Tolerances for the combined residues of the herbicide triclopyr ((3,5,6-trichloro-2-pyridinyl)oxy) acetic
acid and its metabolite 3,5,6-trichloro-2-pyridinol (TCP), as a result of the application/use of butoxyethyl
ester of triclopyr or the triethylamine salt of triclopyr, are established in or on the following raw agricultural
commodities:

Commodity
Cattle, fat

Parts per million
0.05

Cattle, kidney

0.5

Cattle, liver

0.5

Cattle, meat

0.05

Cattle, meat byproducts, except kidney and liver

0.05

Goat, fat

0.05

Goat, kidney

0.5

Goat, liver

0.5

Goat, meat

0.05

Goat, meat byproducts, except kidney and liver

0.05

Hog, fat

0.05

Hog, kidney

0.5

Hog, liver

0.5

Hog, meat

0.05

Hog, meat byproducts, except kidney and liver

0.05

Horse, fat

0.05

Horse, kidney

0.5

Horse, liver

0.5

Horse, meat

0.05

Horse, meat byproducts, except kidney and liver

0.05

Sheep, fat

0.05

Sheep, kidney

0.5

Sheep, liver

0.5

Sheep, meat

0.05

Sheep, meat byproducts, except kidney and liver

0.05

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[50 FR 18486, May 1, 1985, as amended at 55 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, 1995; 62
FR 46894, Sept. 5, 1997; 63 FR 45406, Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR 58725, Sept.
18, 2002; 72 FR 41931, Aug. 1, 2007]

§ 180.418 Cypermethrin and an isomer zeta-cypermethrin; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide cypermethrin (±)alpha cyano-(3phenoxyphenyl)methyl(±)cis,trans-3(2,2-dichloroethenyl-2,2-dimethylcyclopropanecarboxylate in or on the
following commodities:

Commodity
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

Parts per million
2.0
14.0

Cattle, fat

1.0

Cattle, meat

0.2

Cattle, meat byproducts

0.05

Cotton, gin byproducts

11.0

Cotton, undelinted seed

0.5

Egg

0.05

Goat, fat

1.0

Goat, meat

0.2

Goat, meat byproducts
Hog, fat

0.05
0.1

Hog, meat

0.05

Horse, fat

1.0

Horse, meat

0.2

Horse, meat byproducts

0.05

Lettuce, head

4.0

Milk, fat (reflecting 0.10 in whole milk)

2.5

Onion, bulb

0.1

Onion, green

6.0

Pecan

0.05

Poultry, fat

0.05

Poultry, meat

0.05

Sheep, fat

1.0

Sheep, meat

0.2

Sheep, meat byproducts
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(2) Tolerances are established for residues of the insecticide Z-cypermethrin (S-cyano(3-phenoxyphenyl)
methyl (±))(cis-trans 3-(2,2-dichloroethenyl)-2,2 dimethylcyclopropanecarboxylate and its inactive Risomers in or on the following raw agricultural commodities:

Commodity
Alfalfa, hay

Parts per million
15.00

Alfalfa, forage

5.00

Alfalfa, seed

0.50

Almond, hulls

6

Animal feed, nongrass, group 18, forage

8

Animal feed, nongrass, group 18, hay

40

Beet, sugar, roots

0.05

Beet, sugar, tops

0.20

Berry group 13

0.8

Borage, seed

0.2

Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Cabbage

2.00
14.00
2.00

Castor oil plant, refined oil

0.4

Castor oil plant, seed

0.2

Cattle, fat
Cattle, meat
Cattle, meat byproducts

1.00
0.2
0.05

Chinese tallowtree, refined oil

0.4

Chinese tallowtree, seed

0.2

Cilantro, leaves

10

Citrus, dried pulp

1.8

Citrus, oil

4.0

Corn, field, forage

0.20

Corn, field, grain

0.05

Corn, field, stover

3.00

Corn, pop, grain

0.05

Corn, pop, stover

3.00

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

15.00
0.05
15.00

Cotton, undelinted seed

0.5

Crambe, seed

0.2

Cuphea, seed

0.2

Echium, seed

0.2

Egg
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Euphorbia, refined oil

0.4

Euphorbia, seed

0.2

Evening primrose, refined oil

0.4

Evening primrose, seed

0.2

Flax, seed

0.2

Food commodities/feed commodities (other than those covered by a
higher tolerance as a result of use on growing crops) in food/feed
handling establishments

0.05

Fruit, citrus, group 10

0.35

Fruit, pome, group 11

2

Fruit, stone, group 12

1

Goat, fat
Goat, meat

1.00
0.2

Goat, meat byproducts

0.05

Gold of pleasure, seed

0.2

Grain, aspirated fractions
Grape

10.0
2

Grass, forage, fodder, and hay, group 17, forage

10

Grass, forage, fodder and hay, group 17, hay

35

Hare's-ear mustard, seed

0.2

Hog, fat

0.1

Hog, meat

0.05

Horse, fat

1.00

Horse, meat
Horse, meat byproducts

0.2
0.05

Jojoba, refined oil

0.4

Jojoba, seed

0.2

Lesquerella, seed

0.2

Lunaria, seed

0.2

Meadowfoam, seed

0.2

Milk, fat (reflecting 0.10 in whole milk)

2.50

Milkweed, seed

0.2

Mustard, seed

0.2

Niger seed, refined oil

0.4

Niger seed, seed

0.2

Nut, tree, group 14

0.05

Oil radish, seed

0.2

Okra

0.2

Onion, bulb

0.10

Onion, green

3.00

Pea and bean, dried shelled, except soybean, subgroup 6C

0.05

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Pea and bean, succulent shelled, subgroup 6B

0.1

Peanut

0.05

Pecan

0.05

Poppy, seed

0.2

Poultry, fat

0.05

Poultry, meat

0.05

Rapeseed

0.2

Rice, grain

1.50

Rice, hulls

6.00

Rice, straw

2.00

Rice, wild, grain

1.5

Rose hip, refined oil

0.4

Rose hip, seed

0.2

Safflower, seed

0.2

Sesame, seed

0.2

Sheep, fat
Sheep, meat

1.00
0.2

Sheep, meat byproducts

0.05

Sorghum, grain, forage

0.1

Sorghum, grain, grain

0.5

Sorghum, grain, stover

5.0

Soybean, seed

0.05

Stokes aster, refined oil

0.4

Stokes aster, seed

0.2

Sugarcane, cane

0.60

Sunflower, refined oil

0.5

Sunflower, seed

0.2

Sweet rocket, seed

0.2

Tallowwood, refined oil

0.4

Tallowwood, seed

0.2

Tea oil plant, refined oil

0.4

Tea oil plant, seed

0.2

Turnip, greens

14

Vegetable, cucurbit, group 9

0.2

Vegetable, fruiting, group 8

0.2

Vegetable, leafy, except brassica, group 4

10.00

Vegetable, legume, edible podded, subgroup 6A

0.5

Vegetable, root and tuber, group 1, except sugar beet

0.1

Vernonia, refined oil

0.4

Vernonia, seed

0.2

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Wheat, forage

3.0

Wheat, grain

0.2

Wheat, hay

6.0

Wheat, straw

7.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63235, 63243, Nov. 26, 1997, as amended at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, Sept.
17, 2001; 67 FR 6430, Feb. 12, 2002; 67 FR 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; 71 FR
78382, Dec. 29, 2006; 72 FR 53462, Sept. 19, 2007; 72 FR 71801, Dec. 19, 2007; 73 FR 1525, Jan. 9,
2008]

§ 180.419 Chlorpyrifos-methyl; tolerances for residues.
top
(a) General. (1) Tolerances are established for the combined residues of the insecticide chlorpyrifosmethyl [ O,-O,- dimethyl O -(3,5,6-trichloro-2-pyridyl)] phosphorothioate and its metabolite (3,5,6-trichloro2-pyridinol) in or on the following food commodities:

Commodity

Parts per million

Barley, grain

6.0

Cattle, fat

0.5

Cattle, meat

0.5

Cattle, meat byproducts

0.5

Egg

0.1

Goat, fat

0.5

Goat, meat

0.5

Goat, meat byproducts

0.5

Hog, fat

0.5

Hog, meat

0.5

Hog, meat byproducts

0.5

Horse, fat

0.5

Horse, meat

0.5

Horse, meat byproducts

0.5

Milk, fat (0.05 ppm (N) in whole milk

1.25

Oat, grain

6.0

Poultry, fat

0.5

Poultry, meat

.5

Poultry, meat byproducts

.5

Rice, grain
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Sheep, fat

0.5

Sheep, meat

0.5

Sheep, meat byproducts

0.5

Sorghum, grain

6.0

Wheat, grain

6.0

(2) Tolerances are established for the combined residues of the insecticide chlorpyrifos-methyl ( O,-Odimethyl- O- (3,5,6-trichloro-2-pyridyl) phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or
on the following food commodities when present therein as a result of application to stored grains:

Food

Parts per million

Barley milling fractions (except flour)

90

Oat, groats/rolled oats

130

Rice milling fractions (except flour)

30

Sorghum, grain, bran

90

Wheat milling fractions (except flour)

30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33715, May 24, 2000]

§ 180.420 Fluridone; tolerances for residues.
top
(a) Tolerances are established for the combined residues (free and bound) of the herbicide fluridone (1methyl-3-phenyl-5-[3-trifluoromethyl)phenyl]-4(1 H )-5-[3-(trifluoromethyl)phenyl]-4(1 H )-pyridinone) in fish
and crayfish at 0.5 part per million.
(b) Tolerances are established for residues of the herbicide fluridone in the following raw agricultural
commodities:

Commodity

Parts per million

Cattle, fat

0.05

Cattle, kidney

.1

Cattle, liver

.1

Cattle, meat

.05

Cattle, meat byproducts

.05

Egg

.05

Goat, fat

.05

Goat, kidney

.1

Goat, liver

.1

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Goat, meat

.05

Goat, meat byproducts

.05

Hog, fat

.05

Hog, kidney

.1

Hog, liver

.1

Hog, meat

.05

Hog, meat byproducts

.05

Horse, fat

.05

Horse, kidney

.1

Horse, liver

.1

Horse, meat

.05

Horse, meat byproducts

.05

Milk

.05

Poultry, fat

.05

Poultry, kidney

.01

Poultry, liver

.01

Poultry, meat

.05

Poultry, meat byproducts

.05

Sheep, fat

.05

Sheep, kidney

.1

Sheep, liver

.1

Sheep, meat

.05

Sheep, meat byproducts

.05

(c) Tolerances are established in the following irrigated crops and crop groupings for residues of the
herbicide fluridone resulting from use of irrigation water containing residues of 0.15 ppm following
applications on or around aquatic sites. Where tolerances are established at higher levels from other uses
of fluridone on the following crops, the higher tolerance also applies to residues in the irrigated commodity.
The tolerances follow:

Commodity

Parts per million

Avocado

0.1

Citrus

.1

Cotton, undelinted seed

.1

Cucurbits

.1

Fruit, pome

.1

Fruit, small

.1

Fruit, stone

.1

Grain, crop

.1

Grass, forage

.15

Hop, dried cones

.1

Legume, forage

.15

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Nut

.1

Vegetable, fruiting

.1

Vegetable, leafy

.1

Vegetable, root crop

.1

Vegetable, seed and pod

.1

[51 FR 12146, Apr. 9, 1986, as amended at 55 FR 29829, July 20, 1990]

§ 180.421 Fenarimol; tolerances for residues.
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(a) General . Tolerances are established for residues of the fungicide fenarimol, alpha-(2-chlorophenyl)alpha-(4-chlorophenyl)-5-pyrimidinemethanol, in or on the following raw agricultural commodities:

Commodity

Parts per million

Apple

0.1

Apple, wet pomace

0.3

Banana

0.25

Cattle, fat

0.01

Cattle, kidney

0.01

Cattle, meat

0.01

Cattle, meat byproducts, except kidney

0.05

Cherry, sweet

1.0

Cherry, tart

1.0

Goat, fat

0.01

Goat, kidney

0.01

Goat, meat

0.01

Goat, meat byproducts, except kidney

0.05

Grape

0.1.

Hazelnut

0.02

Horse, fat

0.01

Horse, kidney

0.01

Horse, meat

0.01

Horse, meat byproducts, except kidney

0.05

Pear

0.1

Pecan

0.02

Sheep, fat

0.01

Sheep, kidney

0.01

Sheep, meat

0.01

Sheep, meat byproducts, except kidney

0.05

(b) Section 18 emergency exemptions. [Reserved]
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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[51 FR 39662, Oct. 30, 1986, as amended at 53 FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, 1988; 54
FR 45734, Oct. 31, 1989; 60 FR 33354, June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR 61447, Nov.
18, 1997; 67 FR 35048, May 17, 2002; 67 FR 41807, June 19, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR
32846, June 7, 2006; 71 FR 54434, Sept. 15, 2006]

§ 180.422 Tralomethrin; tolerances for residues.
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(a) General. (1) Tolerances are established for the combined residues of the pesticide chemical
tralomethrin (( S )- alpha -cyano-3-phenoxybenzyl (1 R ,3 S )-2,2-dimethyl-3-[( RS )-1,2,2,2tetrabromoethyl]-cyclopropanecarboxylate) and its metabolites ( S )- alpha -cyano-3-phenoxybenzyl (1
R ,3 R )-3(2,2-dibromovinyl)-2,2-dimethyl-cyclopropanecarboxylate and ( S )- alpha -cyano-3phenoxybenzyl(1 S ,3 R )-3-(2,2-dibromovinyl)-2,2-dimethyl-cyclopropanecarboxylate calculated as the
parent in or on the following food commodities:

Commodity

Parts per million

Broccoli

0.5

Cotton, undelinted seed

0.02

Cotton, oil

0.20

Lettuce, head

1.00

Lettuce, leaf

3.00

Soybean

0.05

Sunflower, seed

0.05

(2) A tolerance of 0.02 part per million is established for the combined residues of the insecticide
tralomethrin (( S )- alpha -cyano-3-phenoxybenzyl-(1 R ,3 S )-2,2-dimethyl-3-[(RS)-1,2,2,2tetrabromoethyl] cyclopropanecarboxylate) and its metabolites cis -deltamethrin [( S-alpha -cyano-3phenoxybenzyl-(1 R ,3 R )-3-[2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate] and transdeltamethrin [( S )- alpha -cyano-3-phenoxybenzyl (1 S ,3 R )-3-(2,2-dibromovinyl)-2,2dimethylcyclopropanecarboxylate] as follows:
(i) In or on food commodities (other than those covered by a higher tolerance as a result of use on growing
crops) in food-handling establishments.
(ii) The insecticide may be present as a residue from application of tralomethrin in food-handling
establishments, including food service, manufacturing, and processing establishments, such as
restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants,
and canneries in accordance with the following prescribed conditions:
(A) Application shall be limited to a general surface and spot and/or crack and crevice treatment in foodhandling establishments where food and food products are held, processed, prepared, and served.
General surface application may be used only when the facility is not in operation provided exposed food
has been covered or removed from the area being treated. All food-contact surfaces and equipment must
be thoroughly cleaned after general surface applications. Spot and/or crack and crevice application may
be used while the facility is in operation provided exposed food is covered or removed from the area being
treated prior to application. Spray concentration shall be limited to a maximum of 0.06 percent active
ingredient. Contamination of food and food-contact surfaces shall be avoided.
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(B) To assure safe use of the insecticide, its label and labelling shall conform to that registered with the U.
S. Environmental Protection Agency and shall be used in accordance with such label and labelling.
(3) A tolerance of 0.02 part per million is established for the combined residues of the insecticide
tralomethrin (( S )- alpha -cyano-3-phenoxybenzyl-(1 R ,3 S )-2,2-dimethyl-3-[( RS )-1,2,2,2tetrabromoethyl] cyclopropanecarboxylate) and its metabolites cis -deltamethrin [( S )- alpha -cyano-3phenoxybenzyl-(1 R ,3 R )-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate] and trans deltamethrin [( S )- alpha -cyano-3-phenoxybenzyl (1 S ,3 R )-3-(2,2-dibromovinyl)-2,2dimethylcyclopropanecarboxylate as follows:
(i) In or on all feed items (other than those covered by a higher tolerance as a result of use on growing
crops) in feed-handling establishments.
(ii) The insecticide may be present as a residue from application of tralomethrin in feed-handling
establishments, including feed manufacturing and processing establishments in accordance with the
following prescribed conditions:
(A) Application shall be limited to a general surface and spot and/or crack and crevice treatment in feedhandling establishments where feed and feed products are held or processed. General surface application
may be used only when the facility is not in operation provided exposed feed has been covered or
removed from the area being treated. All feed-contact surfaces and equipment must be thoroughly
cleaned after general surface applications. Spot and/or crack and crevice application may be used while
the facility is in operation provided exposed feed is covered or removed from the area being treated prior
to application. Spray concentration shall be limited to a maximum of 0.06 percent active ingredient.
Contamination of feed and feed- contact surfaces shall be avoided.
(B) To assure safe use of the insecticide, its label and labelling shall conform to that registered with the U.
S. Environmental Protection Agency and shall be used in accordance with such label and labelling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63001, Nov. 26, 1997, as amended at 62 FR 66025, Dec. 17, 1997; 65 FR 33701, May 24, 2000;
71 FR 74817, Dec. 13, 2006]

§ 180.425 Clomazone; tolerances for residues.
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(a) General. Tolerances are established for residues of the herbicide clomazone, 2-(2-chlorophenyl)methyl4,4-dimethyl-3-isoxazolidinone, in or on the following raw agricultural commodities:

Commodity
Bean, snap, succulent
Cabbage
Cotton, undelinted seed
Cucumber

Parts per million
0.05
0.1
0.05
0.1

Pea, succulent

0.05

Pepper

0.05

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Peppermint, tops

0.05

Pumpkin

0.1

Rice, grain

0.02

Rice, straw

0.02

Soybean

0.05

Spearmint, tops

0.05

Squash, summer

0.1

Squash, winter

0.1

Sugarcane, cane

0.05

Sweet potato, roots

0.05

Vegetable, cucurbit, group 9

0.05

Vegetable, tuberous and corm, except potato, subgroup 1D

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[51 FR 9446, Mar. 19, 1986]
Editorial Note: ForFederal Registercitations affecting §180.425, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.426 2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1 H
yl]-3-quinoline carboxylic acid; tolerance for residues.

-imidazol-2-

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A tolerance is established for residues of the herbicide 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1
H -imidazol-2-yl]-3-quinoline carboxylic acid, in or on the raw agricultural commodity soybean at 0.05 part
per million.
[51 FR 13309, Apr. 2, 1986]

§ 180.427 Tau-Fluvalinate; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide tau-fluvalinate, cyano-(3phenoxyphenyl)methyl N -[2-chloro-4-(trifluoromethyl)phenyl]- D -valinate, in or on the following food
commodities:

Commodity

Parts per million

Honey
(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertent residues. [Reserved]
[65 FR 33701, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, 2008]

§ 180.428 Metsulfuron methyl; tolerances for residues.
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(a) General. (1) Tolerances are established for the combined residues of the herbicide metsulfuron methyl
(methyl 2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- 2-yl)amino]carbonyl]amino] sulfonyl] benzoate) and its
metabolite methyl 2-[[[[(4-methoxy-6-methyl-1-,3,5- triazin-2-yl)amino]carbonyl]amino] sulfonyl]-4hydroxybenzoate in or on the following raw material agricultural commodities:

Commodity

Parts per million

Barley, grain

0.1

Barley, hay

20.0

Barley, straw

0.3

Grass, forage

15.0

Grass, hay

15.0

Grass, straw

15.0

Sorghum, grain, forage

0.2

Sorghum, grain, grain

0.1

Sorghum, grain, stover

0.2

Sugarcane, cane

0.05

Wheat, forage

5.0

Wheat, grain

0.1

Wheat, hay

20.0

Wheat, straw

0.3

(2) Tolerances are established for residues of metsulfuron methyl (methyl-2[[[[(4-methoxy- 6-methyl-1,3,5triazin-2- yl)amino]carbonyl]amino] sulfonyl] benzoate) in or on the following raw agricultural commodities:

Commodity

Parts per million

Cattle, fat

0.1

Cattle, kidney

0.5

Cattle, meat

0.1

Cattle, meat byproducts

0.1

Goat, fat

0.1

Goat, kidney

0.5

Goat, meat

0.1

Goat, meat byproducts

0.1

Hog, fat

0.1

Hog, kidney

0.5

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Hog, meat

0.1

Hog, meat byproducts

0.1

Horse, fat

0.1

Horse, kidney

0.5

Horse, meat

0.1

Horse, meat byproducts

0.1

Milk

0.05

Sheep, fat

0.1

Sheep, kidney

0.5

Sheep, meat

0.1

Sheep, meat byproducts

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 70191, Dec. 16, 1999, as amended at 66 FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, 2002]

§ 180.429 Chlorimuron ethyl; tolerances for residues.
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(a) General. Tolerances are established for residues of the herbicide chlorimuron ethyl, ethyl 2-[[[[(4-chloro6-methoxypyrimidin-2yl) amino]carbonyl]sulfonyl]benzoate], in or on the following raw agricultural
commodities:

Commodity

Parts per million

Berry, low growing, except strawberry, subgroup 13–07H

0.02

Peanut

0.02

Soybean

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[74 FR 10494, Mar. 11, 2009]

§ 180.430 Fenoxaprop-ethyl; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of the herbicide fenoxaprop-ethyl [(±)ethyl 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoate] and its metabolites [2-[4-](6-chloro-2benzoxazoly)oxy]phenoxy]propanoic acid and 6-chloro- 2,3-dihydrobenzoxazol-2-one], each expressed as
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fenoxaprop-ethyl, in or on the following raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.05

Barley, straw

0.1

Cattle, fat

0.05

Cattle, meat byproducts

0.05

Cattle, meat

0.05

Cotton, undelinted seed

0.05

Goat, fat

0.05

Goat, meat byproducts

0.05

Goat, meat

0.05

Hog, fat

0.05

Hog, meat byproducts

0.05

Hog, meat

0.05

Horse, fat

0.05

Horse, meat byproducts

0.05

Horse, meat

0.05

Milk

0.02

Peanut

0.05

Peanut, hulls

0.05

Rice, grain

0.05

Sheep, fat

0.05

Sheep, meat byproducts

0.05

Sheep, meat

0.05

Soybean

0.05

Wheat, grain

0.05

Wheat, straw

0.50

(b) Section 18 emergency exemptions. Time-limited tolerances are established for combined residues of
the herbicide fenoxaprop-ethyl, [(±)-ethyl 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoic acid], and
its metabolites (2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoic acid and 6-chloro-2,3dihydrobenzoxazol-2-one), each expressed as fenoxaprop-ethyl, in connection with use of the pesticide
under section 18 emergency exemptions granted by EPA, in or on the food commodities in the following
table. The tolerances expire and are revoked on the dates specified in the following table.

Commodity

Expiration/
revocation date

Parts per million

Grass, forage

0.05

12/31/10

Grass, hay

0.05

12/31/10

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
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[63 FR 1377, Jan. 9, 1998, as amended at 63 FR 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008]

§ 180.431 Clopyralid; tolerances for residues.
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(a) General. Tolerances are established for combined residues of the herbicide clopyralid (3,6-dichloro-2pyridinecarboxylic acid) in or on the following commodities:

Commodity

Parts per million

Asparagus

1.0

Barley, grain

3.0

Barley, hay

9.0

Barley, milled fractions (except flour)

12

Barley, straw

9.0

Beet, garden, tops

3.0

Beet, garden, roots

4.0

Beet, sugar, molasses

10

Beet, sugar, roots

2.0

Beet, sugar, tops

3.0

Brassica, head and stem, subgroup 5A

2.0

Canola, meal

6.0

Canola, seed

3.0

Cattle, fat

1.0

Cattle, liver

3.0

Cattle, meat

1.0

Cattle, meat byproducts, except liver

36.0

Corn, field, forage

3.0

Corn, field, stover

10.0

Corn, field, grain

1.0

Corn, field, milled byproducts

1.5

Corn, pop, grain

1.0

Corn, pop, stover

10.0

Corn, sweet, forage

7.0

Corn, sweet, kernel plus cob with husks removed

1.0

Corn, sweet, stover

10.0

Crambe, seed

3.0

Cranberry

4.0

Egg

0.1

Flax, meal

6.0

Flax, seed

3.0

Fruit, stone, group 12

0.5

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Goat, fat

1.0

Goat, liver

3.0

Goat, meat

1.0

Goat, meat byproducts, except liver
Grass, forage and hay

36.0
500.0

Hog, fat

0.2

Hog, meat

0.2

Hog, meat byproducts

0.2

Hop, dried cones

5.0

Horse, fat

1.0

Horse, liver

3.0

Horse, meat

1.0

Horse, meat byproducts, except liver

36.0

Milk

0.2

Mint, hay

3.0

Mustard greens

5.0

Mustard, seed

3.0

Oat, forage

9.0

Oat, grain

3.0

Oat, groats/rolled oats

12

Oat, straw

9.0

Plum, prune, dried

1.5

Poultry, fat

0.2

Poultry, meat

0.2

Poultry, meat byproducts

0.2

Rapeseed, seed

3.0

Rapeseed, forage

3.0

Sheep, fat

1.0

Sheep, liver

3.0

Sheep, meat

1.0

Sheep, meat byproducts, except liver

36.0

Spinach

5.0

Strawberry

1.0

Turnip, greens

4.0

Turnip, roots

1.0

Wheat, forage

9.0

Wheat, grain

3.0

Wheat, milled fractions (except flour)
Wheat, straw
(b) Section 18 emergency exemptions. [Reserved]
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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[52 FR 10566, Apr. 2, 1987]
Editorial Note: ForFederal Registercitations affecting §180.431, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.432 Lactofen; tolerances for residues.
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(a) Tolerances are established for residues of the herbicide lactofen, 1-(carboethoxy)ethyl 5-[2-chloro-4(trifluoromethyl)phenoxy]-2- nitrobenzoate, in or on the following raw agricultural commodities:

Commodity

Parts per million

Beans, snap, succulent, except lima bean

0.01

Cotton, gin byproducts

0.02

Cotton, undelinted seed

0.01

Peanut

0.01

Soybean, seed

0.01

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registrations, as defined in 180.1(n)
are established for residues of the herbicide, lactofen, 1-(carboethoxy)ethyl 5-[2-chloro-4-(trifluoromethyl)
phenoxy]-2- nitrobenzoate, in or on the following food commodities:

Commodity

Parts per million

Okra

0.02

Vegetables, fruiting, group 08

0.02

(d) Indirect or inadvertent residues . [Reserved]
[69 FR 57216, Sept. 24, 2004, as amended at 72 FR 33906, June 20, 2007]

§ 180.433 Fomesafen; tolerances for residues.
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(a) General . Tolerances are established for the residues of fomesafen 5-[2-chloro-4-(trifluoromethyl)
phenoxy]- N -(methylsulfonyl)-2-nitrobenzamide from the application of its sodium salt in or on the
following commodities:

Commodity

Parts per million

Bean, dry

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Bean, snap, succulent

0.05

Cotton, gin byproducts

0.025

Cotton, undelinted seed

0.025

Soybean

0.05

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 25951, May 3, 2006, as amended at 72 FR 52020, Sept. 12, 2007]

§ 180.434 Propiconazole; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the fungicide 1-[[2-(2,4dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole and its metabolites determined as 2,4dichlorobenzoic acid and expressed as parent compound in or on the following commodities:

Commodity

Parts per million

Almond, hulls

7.0

Banana

0.2

Barley, bran

0.6

Barley, grain

0.3

Barley, hay

1.4

Barley, straw

10

Beet, garden, roots

0.30

Beet, garden, tops

5.5

Beet, sugar, dried pulp

1.0

Beet, sugar, molasses

1.5

Beet, sugar, roots

0.3

Beet, sugar, tops

10

Berry group 13

1.0

Carrot, roots

0.25

Cattle, fat

0.05

Cattle, kidney

2.0

Cattle, liver

2.0

Cattle, meat

0.05

Cattle, meat byproducts, except liver and kidney

0.05

Cilantro, leaves

13

Corn, field, forage

12

Corn, field, grain

0.2

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Corn, field, stover

30

Corn, pop, grain

0.2

Corn, pop, stover

30

Corn, sweet, forage

6.0

Corn, sweet, kernel plus cob with husks removed

0.1

Corn, sweet, stover
Fruit, stone, group 12
Goat, fat

30
1.0
0.05

Goat, kidney

2.0

Goat, liver

2.0

Goat, meat

0.05

Goat, meat byproducts, except liver and kidney

0.05

Grain, aspirated fractions

30

Grass, forage

0.5

Grass, hay

0.5

Grass, straw

40

Hog, kidney

0.2

Hog, liver

0.2

Horse, fat

0.05

Horse, kidney

2.0

Horse, liver

2.0

Horse, meat

0.05

Horse, meat byproducts, except liver and kidney

0.05

Leaf petioles subgroup 4B
Milk

5.0
0.05

Mushroom

0.1

Nut, tree, group 14

0.1

Oat, forage

1.7

Oat, grain

0.3

Oat, hay

1.4

Oat, straw

10

Onion, bulb

0.2

Onion, green

9.0

Parsley, fresh leaves

13

Parsley, dried leaves

35

Peanut
Peanut, hay

0.2
20

Peppermint, tops

3.5

Pineapple

4.5

Pineapple, process residue

7.0

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Pistachio

0.1

Rice, bran

15

Rice, grain

7.0

Rice, hulls

20

Rice, straw

18

Rye, bran

0.6

Rye, forage

1.7

Rye, grain

0.3

Rye, straw

10

Sheep, fat

0.05

Sheep, kidney

2.0

Sheep, liver

2.0

Sheep, meat

0.05

Sheep, meat byproducts, except liver and kidney

0.05

Sorghum, grain, forage

12

Sorghum, grain, grain

3.5

Sorghum, grain, stover

15

Soybean, forage

11

Soybean, hay

30

Soybean, seed

2.0

Spearmint, tops

3.5

Strawberry

1.3

Wheat, bran

0.6

Wheat, forage

1.7

Wheat, grain

0.3

Wheat, hay

1.4

Wheat, straw

10

(b) Section 18 emergency exemptions . Time-limited tolerances are established for residues of
propiconazole (1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole) and its
metabolites determined as 2,4-dichlorobenzoic acid and expressed as parent compound, in connection
with use of the pesticide under section 18 emergency exemptions granted by EPA. The tolerances will
expire and are revoked on the dates specified in the following table:

Commodity

Parts per million

Expiration/revocation date

Nectarine

2.0

12/31/10

Peach

2.0

12/31/10

(c) Tolerances with regional registrations . A tolerance with regional registration, as defined in §180.1(m),
is established for residues of 1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl]methyl]-1H-1,2,4-triazole
and its metabolites determined as 2,4-dichlorobenzoic acid and expressed as parent compound, in or on
the following commodities:

Commodity

Parts per million

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Cranberry

1.0

Rice, wild, grain

0.5

(d) Indirect or inadvertent residues . Tolerances are established for the combined residues of the fungicide
1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole and its metabolites
determined as 2,4-dichlorobenzoic acid and expressed as parent compound in or on the following
commodities when present therein as a result of application of propiconazole to growing crops in
paragraphs (a) and (c) of this section:

Commodity

Parts per million

Alfalfa, forage

0.1

Alfalfa, hay

0.1

[71 FR 55306, Sept. 22, 2006, as amended at 72 FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, 2009]

§ 180.435 Deltamethrin; tolerances for residues.
top
(a) General. (1) Tolerances are established for the combined residues of the pesticide chemical
deltamethrin [(1 R ,3 R )-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylic acid ( S )- alpha -cyano3-phenoxybenzyl ester and its major metabolites, trans deltamethrin [( S )- alpha -cyano- m phenoxybenzyl(1R,3S)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate] and alpha-R deltamethrin [( R )- alpha -cyano- m -phenoxybenzyl-(1 R ,3 R )-3-(2,2-dibromovinyl)-2,2dimethylcyclopropanecarboxylate] in or on the following agricultural commodities:

Commodity

Parts per million

Almond, hulls

2.5

Apple, wet pomace

1.0

Artichoke, globe

0.5

Barley, bran

5.0

Cattle, fat

0.05

Cattle, meat

0.02

Cattle, meat byproducts

0.05

Corn, field, forage

0.7

Corn, field, refined oil

2.5

Corn, field, stover

5.0

Corn, pop, stover

5.0

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, refined oil

10
0.03
15
0.2

Cotton, undelinted seed

0.04

Egg

0.02

Fruit, pome, Group 11

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Goat, fat

0.05

Goat, meat

0.02

Goat, meat byproducts

0.05

Grain, aspirated fractions
Grain, cereal, Group 15, except sweet corn

65
1.0

Hog, fat

0.05

Horse, fat

0.05

Horse, meat

0.02

Horse, meat byproducts

0.05

Lychee*

0.2

Milk, fat (reflecting 0.02 ppm in whole milk)

0.1

Nut, tree, Group 14

0.1

Onion, bulb

0.1

Onion, green

1.5

Poultry, fat

0.05

Poultry, meat

0.02

Poultry, meat byproducts

0.02

Radish, tops

4.0

Rapeseed

0.2

Rice, hulls

2.5

Rye, bran

5.0

Sheep, fat

0.05

Sheep, meat

0.02

Sheep, meat byproducts

0.05

Sorghum, grain, forage

0.5

Sorghum, grain, stover

1.0

Soybean, seed

0.1

Soybean, hulls

0.2

Starfruit*

0.2

Sunflower, seed

0.1

Tomato

0.2

Tomato, concentrated products

1.0

Vegetable, cucurbit, Group 9

0.2

Vegetable, fruiting, Group 8

0.3

Vegetable, root, except sugar beet, Subgroup IB

0.2

Vegetable, tuberous and corm, Subgroup IC
Wheat, bran

0.04
5.0

*There are no U.S. registrations for use of deltamethrin on starfruit and lychee.
(2) A tolerance of 0.05 ppm is established for residues of the insecticide deltamethrin (1 R ,3 R )-3-(2,2dibromovinyl)-2,2-dimethylcyclopropanecarboxylic acid ( S )-alpha-cyano-3-phenoxybenzyl ester and its
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major metabolites, trans deltamethrin ( S )-alpha-cyano- m -phenoxybenzyl-(1 R ,3 R )-3-(2,2dibromovinyl)-2,2-dimethylcyclopropanecarboxylate and alpha- R -deltamethrin[( R )-alpha-cyano- m phenoxybenzyl-(1 R ,3 R )-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate] as follows:
(i) In or on all food/feed items (other than those covered by a higher tolerance as a result of use on
growing crops) in food/feed handling establishments.
(ii) The insecticide may be present as a residue from application of deltamethrin in food handling
establishments, including food service, manufacturing and processing establishments, such as
restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants,
and canneries, feed handling establishments including feed manufacturing and processing
establishments, in accordance with the following prescribed conditions:
(A) Application shall be limited to general surface and spot and/or crack and crevice treatment in food/feed
handling establishments where food/feed and food/feed products are held, processed, prepared and
served. General surface application may be used only when the facility is not in operation provided
exposed food/feed has been covered or removed from the area being treated. Spot and/or crack and
crevice application may be used while the facility is in operation provided exposed food/feed is covered or
removed from the area being treated prior to application. Spray concentration shall be limited to a
maximum of 0.06 percent active ingredient. Contamination of food/feed or food/feed contact surfaces shall
be avoided.
(B) To assure safe use of the insecticide, its label and labeling shall conform to that registered with the U.
S. Environmental Protection Agency and shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63001, Nov. 26, 1997, as amended at 63 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, 2004]

§ 180.436 Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2dimethyl-cyclopropane-carboxylate; CAS No. 68359–37–
5) in or on the following raw agricultural commodities:

Commodity

Parts per million

Alfalfa

5.0

Alfalfa, forage

5.0

Alfalfa, hay

13

Almond, hulls

0.5

Barley, bran

0.5

Barley, grain

0.15

Beet, sugar, dried pulp
Beet, sugar, roots
Brassica, head and stem, subgroup 5A

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1.0
0.10
2.5

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Brassica, leafy greens, subgroup 5B

7.0

Buckwheat, grain

0.15

Carrot, roots

0.20

Cattle, fat

2.0

Cattle, meat

0.10

Cattle, meat byproducts

0.10

Citrus, dried pulp

0.3

Citrus, oil

0.3

Corn, field, grain

0.05

Corn, pop, grain

0.05

Corn, sweet, kernel plus cob with husks removed

0.05

Cotton, hulls

2.0

Cotton, refined oil

2.0

Cotton, undelinted seed

1.0

Egg

0.01

Fruit, citrus, group 10

0.2

Fruit, pome, group 11

0.5

Fruit, stone, group 12

0.3

Goat, fat

2.0

Goat, meat

0.05

Goat, meat byproducts

0.05

Grain, aspirated fractions
Grain, cereal, forage, fodder and hay, group 16, forage, except rice
Grain, cereal, forage, fodder and hay, group 16, hay, except rice

150
25
6.0

Grain, cereal, forage, fodder and hay, group 16, stover, except rice

30

Grain, cereal, forage, fodder and hay, group 16, straw, except rice

7.0

Grape

1.0

Grape, raisin

3.5

Grass, forage, fodder and hay, group 17, forage

12

Grass, forage, fodder and hay, group 17, hay

50

Hog, fat

0.5

Hog, meat

0.01

Hog, meat byproducts

0.01

Hop, dried cones

20.0

Hop, vines

4.0

Horse, fat

2.0

Horse, meat

0.05

Horse, meat byproducts

0.05

Lettuce, head

2.0

Lettuce, leaf

3.0

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Milk

0.2

Milk, fat

5.0

Millet, grain
Mustard greens
Nut, tree, group 14

0.15
7.0
0.01

Oat, bran

0.5

Oat, grain

0.15

Pea and bean, dried shelled, except soybean, subgroup 6C

0.15

Pea, dry, seed

0.15

Pea, southern, succulent

0.25

Peanut

0.01

Peanut, hay

6.0

Pepper

0.50

Pistachio

0.01

Poultry, fat

0.01

Poultry, meat

0.01

Poultry, meat byproducts

0.01

Radish, roots

1.0

Rye, bran

0.5

Rye, grain

0.15

Sheep, fat

2.0

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Sorghum, grain, grain

3.5

Soybean, forage

8.0

Soybean, hay

4.0

Soybean, seed

0.03

Sugarcane, cane

0.05

Sugarcane, molasses

0.20

Sunflower, forage

5.0

Sunflower, seed

0.02

Teosinte, grain

0.05

Tomato

0.20

Tomato, paste

0.5

Tomato, pomace

5.0

Triticale, grain

0.15

Turnip, greens

7.0

Vegetable, cucurbit, group 9

0.1

Vegetable, fruiting, group 8

0.5

Vegetable, leafy, except brassica, group 4

6.0

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Vegetable, tuberous and corm, subgroup 1C

0.01

Wheat, bran

0.5

Wheat, grain

0.15

Wheat, shorts

0.5

(2) A tolerance of 0.05 ppm is established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate; CAS Reg. No.
69359–37–5) in food commodities exposed to the insecticide during treatment of food-handling
establishments where food and food products are held, processed, prepared, or served. Treatments may
be made by general surface, spot, and/or crack and crevice applications.
(i) General surface treatments shall be limited to a maximum of 3.8 grams of active ingredient per 1,000
square feet, applying to walls, floors, and ceilings with a low-pressure system. Cover or remove all food
processing and/or handling equipment during application. Do not apply directly to food products.
Reapplications may be made at 10-day intervals.
(ii) Crack and crevice or spot treatments shall be limited to a maximum of 0.1 percent of the active
ingredient weight, applied with a low-pressure system with a pinpoint or variable-pattern nozzle. Dust
formulation shall be limited to a maximum of 0.1 percent of the active ingredient by weight, applied using a
hand duster, power duster, or other equipment capable of applying dust insecticide directly into voids and
cracks and crevices. Dust applications should be made in a manner to avoid deposits on exposed
surfaces or introducing the material into the air. Cover exposed food or remove food from premises. Do
not apply directly to food. Reapplications may be made at 10-day intervals.
(iii) To ensure safe use of the insecticide, its label and labeling shall conform to that registered by the
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(3) A tolerance of 0.05 part per million is established for residues of the insecticide cyfluthrin (cyano(4fluoro-3-phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate; CAS Reg.
No. 68359–37–5) in feed commodities exposed to the insecticide during treatment of feed-handling
establishments where feed and feed products are held, processed, prepared, or served. Treatments may
be made by general surface, spot, and/or crack and crevice applications.
(i) General surface tratments shall be limited to a maximum of 3.8 grams of active ingredient per 1,000
square feet, applying to walls, floors, and ceilings with a low-pressure system. Cover or remove all feed
processing and/or handling equipment during application. Do not apply directly to feed products.
Reapplications may be made at 10-day intervals.
(ii) Crack and crevice or spot treatments shall be limited to a maximum of 0.1 percent of the active
ingredient by weight, applied with a low-pressure system with a pinpoint or variable-pattern nozzle. Dust
formulation shall be limited to a maximum of 0.1 percent of the active ingredient by weight, applied using a
hand duster, power duster, or other equipment capable of applying dust insecticide directly into voids and
cracks and crevices. Dust applications should be made in a manner to avoid deposits on exposed
surfaces or introducing the material into the air. Cover exposed feed or remove feed from premises. Do
not apply directly to feed. Reapplications may be made at 10-day intervals.
(iii) To ensure safe use of the insecticide, its label and labeling shall conform to that registered by EPA,
and it shall be used in accordance with such label and labeling.
(4) Tolerances are established for residues of the isomer, beta-cyfluthrin, cyano(4-fluoro-3-phenoxyphenyl)
methyl-3-(2,2-dichloroethenyl)-2,2-dimethyl-cyclopropanecarboxylate [mixture comprising the enantiomeric
pair ( R )-α-cyano-4-fluoro-3-phenoxybenzyl (1 S ,3 S )-3-(2,2-dichlorovinyl)-2,2dimethylcyclopropanecarboxylate and (S)-α-cyano-4-fluoro-3-phenoxybenzyl (1 R ,3 R )-3-(2,2dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate with the enantiomeric pair ( R )-α-cyano-4-fluoro-3phenoxybenzyl (1 S ,3 R )-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate and ( S )-α-cyano-4fluoro-3-phenoxybenzyl (1 R ,3 S )-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate], in or on the
following raw agricultural commodities:
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Commodity

Parts per million

Alfalfa

5.0

Alfalfa, forage

5.0

Alfalfa, hay

13

Almond, hulls

0.5

Barley, bran

0.5

Barley, grain

0.15

Beet, sugar, dried pulp
Beet, sugar, roots

1.0
0.10

Brassica, head and stem, subgroup 5A

2.5

Brassica, leafy greens, subgroup 5B

7.0

Buckwheat, grain

0.15

Carrot, roots

0.20

Cattle, fat

2.0

Cattle, meat

0.10

Cattle, meat byproducts

0.10

Citrus, dried pulp

0.3

Citrus, oil

0.3

Corn, field, grain

0.05

Corn, pop, grain

0.05

Corn, sweet, kernel plus cob with husks removed

0.05

Cotton, hulls

2.0

Cotton, refined oil

2.0

Cotton, undelinted seed

1.0

Egg

0.01

Fruit, citrus, group 10

0.2

Fruit, pome, group 11

0.5

Fruit, stone, group 12

0.3

Goat, fat

2.0

Goat, meat

0.05

Goat, meat byproducts

0.05

Grain, aspirated fractions
Grain, cereal, forage, fodder and hay, group 16, forage, except rice
Grain, cereal, forage, fodder and hay, group 16, hay, except rice

150
25
6.0

Grain, cereal, forage, fodder and hay, group 16, stover, except rice

30

Grain, cereal, forage, fodder and hay, group 16, straw, except rice

7.0

Grape

1.0

Grape, raisin

3.5

Grass, forage, fodder and hay, group 17, forage

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Grass, forage, fodder and hay, group 17, hay
Hog, fat

50
0.5

Hog, meat

0.01

Hog, meat byproducts

0.01

Hop, dried cones

20.0

Hop, vines

4.0

Horse, fat

2.0

Horse, meat

0.05

Horse, meat byproducts

0.05

Lettuce, head

2.0

Lettuce, leaf

3.0

Milk

0.2

Milk, fat

5.0

Millet, grain
Mustard greens
Nut, tree, group 14

0.15
7.0
0.01

Oat, bran

0.5

Oat, grain

0.15

Pea and bean, dried shelled, except soybean, subgroup 6C

0.15

Pea, dry, seed

0.15

Pea, southern, succulent

0.25

Peanut

0.01

Peanut, hay

6.0

Pepper

0.50

Pistachio

0.01

Poultry, fat

0.01

Poultry, meat

0.01

Poultry, meat byproducts

0.01

Radish, roots

1.0

Rye, bran

0.5

Rye, grain

0.15

Sheep, fat

2.0

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Sorghum, grain, grain

3.5

Soybean, forage

8.0

Soybean, hay

4.0

Soybean, seed

0.03

Sugarcane, cane

0.05

Sugarcane, molasses

0.20

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Sunflower, forage

5.0

Sunflower, seed

0.02

Teosinte, grain

0.05

Tomato

0.20

Tomato, paste

0.5

Tomato, pomace

5.0

Triticale, grain

0.15

Turnip, greens

7.0

Vegetable, cucurbit, group 9

0.1

Vegetable, fruiting, group 8

0.5

Vegetable, leafy greens, except Brassica, group 4

6.0

Vegetable, tuberous and corm, subgroup 1C

0.01

Wheat, bran

0.5

Wheat, grain

0.15

Wheat, shorts

0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[53 FR 1924, Jan. 25, 1988]
Editorial Note: ForFederal Registercitations affecting §180.436, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.437 Methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)- p
-toluate
and methyl 6-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)- m
-toluate;
tolerances for residues.
top
Tolerances are established for the combined residues of the herbicide methyl 2-(4-isopropyl-4-methyl-5oxo-2-imidazolin-2-yl)- p -toluate and methyl 6-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)- m -toluate in
or on the following raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.10

Barley, straw

2.00

Sunflower, seed

0.10

Wheat, grain

0.10

Wheat, straw

2.00

[53 FR 24069, June 27, 1988]

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§ 180.438 Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for
residues.
top
(a) General . (1) Tolerances are established for the combined residues of the pyrethroid lambdacyhalothrin, 1:1 mixture of ( S )-α-cyano-3-phenoxybenzyl-( Z )-(1 R ,3 R )-3-(2-chloro-3,3,3-trifluoroprop-1enyl)-2,2-dimethylcyclopropanecarboxylate and ( R )-α-cyano-3-phenoxybenzyl-( Z )-(1 S ,3 S )-3-(2chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and its epimer expressed as
epimer of lambda-cyhalothrin, a 1:1 mixture of ( S )-α-cyano-3-phenoxybenzyl-( Z )-(1 S ,3 S )-3-(2-chloro3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and ( R )-α-cyano-3-phenoxybenzyl-( Z )(1 R ,3 R )-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate, on plants and
livestocks, as indicated in the following table.

Commodity

Parts per million

Alfalfa, forage

5.0

Alfalfa, hay

6.0

Almond, hulls

1.5

Apple, wet pomace

2.50

Avocado, imported

0.20

Barley, bran

0.2

Barley, grain

0.05

Barley, hay

2.0

Barley, straw

2.0

Brassica, head and stem, subgroup 5A

0.4

Buckwheat, grain

0.05

Canola, refined oil

2.0

Canola, seed

1.0

Cattle, fat

3.0

Cattle, meat

0.2

Cattle, meat byproducts

0.2

Corn, field, flour

0.15

Corn, field, forage

6.0

Corn, field, grain

0.05

Corn, field, stover

1.0

Corn, pop, grain

0.05

Corn, pop, grain, flour

0.05

Corn, pop, stover

1.0

Corn, sweet, forage

6.0

Corn, sweet, stover

1.0

Corn, sweet, kernel plus cob with husks removed

0.05

Cotton, undelinted seed

0.05

Egg

0.01

Fruit, pome, group 11

0.30

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Fruit, stone, group 12

0.50

Garlic

0.1

Goat, fat

3.0

Goat, meat

0.2

Goat, meat byproducts

0.2

Grain, aspirated fractions

2.0

Grass, forage, fodder and hay, group 17

7.0

Hog, fat

0.2

Hog, meat

0.01

Hog, meat byproducts

0.02

Hop, dried cones

10.0

Horse, fat

3.0

Horse, meat

0.2

Horse, meat byproducts

0.2

Lettuce, head

2.0

Lettuce, leaf

2.0

Milk, fat (reflecting 0.4 ppm in whole milk)

10.0

Nut, tree, group 14

0.05

Oat, grain

0.05

Oat, forage

2.0

Oat, hay

2.0

Oat, straw

2.0

Onion, bulb

0.1

Pea and bean, dried shelled, except soybean, subgroup 6C

0.10

Pea and bean, succulent shelled, subgroup 6B

0.01

Peanut

0.05

Peanut, hay

3.0

Pistachio

0.05

Poultry, fat

0.03

Poultry, meat

0.01

Poultry, meat byproducts

0.01

Rice, grain

1.0

Rice, hulls

5.0

Rice, straw

1.8

Rice, wild, grain

1.0

Rye, bran

0.2

Rye, grain

0.05

Rye, forage

2.0

Rye, straw

2.0

Sheep, fat

3.0

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Sheep, meat

0.2

Sheep, meat byproducts

0.2

Soybean

0.01

Sorghum, grain, grain

0.2

Sorghum, grain, forage

0.30

Sorghum, grain, stover

0.50

Sugarcane, cane

0.05

Sunflower, forage

0.2

Sunflower, seed, hulls

0.50

Sunflower, refined oil

0.30

Sunflower, seed

0.2

Tomato

0.1

Tomato, dry pomace

6.0

Tomato, wet pomace

6.0

Vegetable, cucurbit, group 9

0.05

Vegetable, fruiting, group 8

0.20

Vegetable, legume, edible podded, subgroup 6A

0.20

Vegetable, tuberous and corm, subgroup 1C

0.02

Wheat, grain

0.05

Wheat, forage

2.0

Wheat, hay

2.0

Wheat, straw

2.0

Wheat, bran

0.2

(2) Tolerances1 are established for the combined residues of the pyrethroid [gamma-cyhalothrin (the
isolated active isomer of lambda-cyhalothrin) ( S )-'-cyano-3-phenoxybenzyl ( Z )-(1 R ,3 R )-3-(2-chloro3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate)) and its epimer ( R )-'-cyano-3phenoxybenzyl ( Z )-(1 R ,3 R )-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2dimethylcyclopropanecarboxylate in/on the following commodities:

Commodity

Parts per million

Alfalfa, forage

5

Alfalfa, hay

6

Almond, hulls

1.5

Apple, pomace, wet

2.50

Avocado, imported

0.20

Brassica, head and stem, subgroup 5A
Canola, seed
Cattle, fat

0.4
0.15
3

Cattle, meat

0.2

Cattle, meat byproducts

0.2

Corn, field, flour

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Corn, field, forage

6.0

Corn, field, grain

0.05

Corn, field, stover

1.0

Corn, pop, grain

0.05

Corn, pop, stover

1.0

Corn, sweet, forage

6.0

Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.05
1.0

Cotton, undelinted seed

0.05

Egg

0.01

Fruit, pome, group 11

0.30

Fruit, stone, group 12

0.50

Garlic

0.10

Goat, fat

3.0

Goat, meat

0.2

Goat, meat byproducts

0.2

Grain, aspirated fractions

2.0

Hog, fat

3.0

Hog, meat

0.2

Hog, meat byproducts

0.2

Horse, fat

3.0

Horse, meat

0.2

Horse, meat byproducts

0.2

Lettuce, head

2.0

Lettuce, leaf

2.0

Milk, fat (reflecting 0.20 ppm in whole milk)

5.0

Nut, tree, group 14

0.05

Okra

0.20

Onion, bulb

0.1

Pea and bean, dried shelled, except soybean, subgroup 6C

0.10

Pea and bean, succulent shelled, subgroup 6B

0.01

Peanut

0.05

Peanut, hay

3.0

Pistachio

0.05

Poultry, fat

0.03

Poultry, meat

0.01

Poultry, meat byproducts

0.01

Rice, grain

1.0

Rice, hulls

5.0

Rice, straw

1.8

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Sheep, fat

3.0

Sheep, meat

0.2

Sheep, meat byproducts

0.2

Sorghum, grain, forage

0.30

Sorghum, grain, grain

0.20

Sorghum, grain, stover

0.50

Soybean

0.01

Sugarcane

0.05

Sunflower, forage

0.20

Sunflower, refined oil

0.30

Sunflower, seed

0.20

Sunflower, seed, hulls

0.50

Tomato

0.10

Tomato, dry pomace

6.0

Tomato, wet pomace

6.0

Vegetables, fruiting, group 8

0.20

Vegetable, legume, edible podded, subgroup 6A

0.20

Wheat, bran

2.0

Wheat, forage

2.0

Wheat, grain

0.05

Wheat, hay

2.0

Wheat, straw

2.0

1 The analytical enforcement methods for lambda-cyhalothrin are applicable for determination of gammacyhalothrin residues in plant and animal commodities.

(3) A tolerance of 0.01 part per million is established for residues of the insecticide lamba-cyhalothrin and
an isomer gamma-cyhalothrin in or on all food commodities (other than those already covered by a higher
tolerance as a result of use on growing crops) in food-handling establishments where food products are
held, processed, or prepared.
(b) Section 18 emergency exemptions . Time-limited tolerances are established for combined residues of
the insecticide lambda-cyhalothrin (a 1:1 mixture of ( S )-α-cyano-3-phenoxybenzyl-( Z )-(1 R ,3 R )-3-(2chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and (R)-α-cyano-3-phenoxybenzyl( Z )-(1 S ,3 S )-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and its epimer
a 1:1 mixture of ( S )-α-cyano-3-phenoxybenzyl-( Z )-(1 S ,3 S )-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2dimethylcyclopropanecarboxylate and ( R )-α-cyano-3-phenoxybenzyl -( Z )-(1 R ,3 R )-3-(2-chloro-3,3,3trifluoroprop-1-enyl)-2,2-dimethylcyclo-propanecarboxylate in connection with use of the pesticide under
section 18 emergency exemptions granted by EPA. The tolerances will expire and are revoked on the
dates specified in the following table:

Commodity

Parts per million

Expiration/revocation date

Barley, bran

0.2

12/31/08

Barley, grain

0.05

12/31/08

Barley, hay

2.0

12/31/08

Barley, straw

2.0

12/31/08

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Clover, forage

5.0

12/31/08

Clover, hay

6.0

12/31/08

Grass, forage

5.0

12/31/08

Grass, hay

6.0

12/31/08

Rice, wild, grain

1.0

12/31/08

(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 74817, Dec. 13, 2006, as amended at 72 FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, 2008]

§ 180.439 Thifensulfuron methyl; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide thifensulfuron methyl (methyl-3-[[[[(4methoxy-6-methyl-1,3,5-triazin-2-yl)amino] carbonyl] amino] sulfonyl]-2-thiophene carboxylate) in or on the
following raw agricultural commodities:

Commodity

Parts per million

Barley, grain
Barley, hay

0.05
0.8

Barley, straw

0.10

Canola, seed

0.02

Corn, field, forage

0.10

Corn, field, grain

0.05

Corn, field, stover

0.10

Cotton, gin byproducts

0.02

Cotton, undelinted seed

0.02

Flax, seed

0.02

Oat, forage

0.2

Oat, grain

0.05

Oat, hay

0.05

Oat, straw

0.10

Rice, grain

0.05

Rice, straw

0.05

Sorghum, grain, forage.

0.05

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.05

Soybean

0.10

Wheat, forage

2.5

Wheat, grain

0.05

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Wheat, hay

0.7

Wheat, straw

0.10

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 55982, Sept. 17, 2004, as amended at 69 FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, 2007;
73 FR 47075, Aug. 13, 2008]

§ 180.440 Tefluthrin; tolerances for residues.
top
(a) General. Tolerances are established for the combined residues of the insecticide tefluthrin (2,3,5,6
tetrafluroro-4-methylphenyl)methyl-(1 alpha, 3 alpha)-( Z )-(±)-3(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2diemthylcyclopropanecarboxylate) and its metabolite ( Z )-3-(2-chloro-3,3,3-trifluroro-1-propenyl)-2,2dimethylcyclopropanecarboxylic acid in or on the following commodities:

Commodity

Parts per million

Corn, field, fodder and forage, pop and sweet

0.06

Corn, field, grain and pop

0.06

Corn, sweet, kernel plus cob with husks removed

0.06

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 62961, Nov. 26, 1997]

§ 180.441 Quizalofop ethyl; tolerances for residues.
top
(a) General. (1) Tolerances are established for the combined residues of the herbicide quizalofop (2-[4-(6chloroquinoxalin-2-yl oxy)phenoxy]propanoic acid) and quizalofop ethyl (ethyl-2-[4-(6-chloroquinoxalin-2-yl
oxy)phenoxy]propanoate), all expressed as quizalofop ethyl, in or on the following agricultural
commodities:

Commodity

Parts per million

Bean, dry
Bean, succulent

0.4
0.25

Beet, sugar, roots

0.1

Beet, sugar, tops

0.5

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Cowpea, forage

3.0

Cowpea, hay

3.0

Pea, dry

0.25

Pea, field, hay

3.0

Pea, field, vines

3.0>

Pea, succulent

0.3

Soybean, flour

0.5

Soybean, hulls

0.02

Soybean, meal

0.5

Soybean, soapstock

1.0

Soybean

0.05

(2) Tolerances are established for the combined residues of the herbicide quizalofop (2-[4-(6chloroquinoxalin-2-yl oxy)phenoxy]propanoic acid), quizalop-ethyl (ethyl-2-[4-(6-chloroquinoxalin-2-yl oxy)
phenoxy]propanoate), and quizalofop-methyl (methyl 2-[4-(6-chloroquinoxalin-2-yl-oxy)phenoxy]
propanoate, all expressed as quizalofop ethyl, as follows:

Commodity

Parts per million

Cattle, fat

0.05

Cattle, meat

0.02

Cattle, meat byproducts

0.05

Egg

0.02

Goat, fat

0.05

Goat, meat

0.02

Goat, meat byproducts

0.05

Hog, fat

0.05

Hog, meat

0.02

Hog, meat byproducts

0.05

Horse, fat

0.05

Horse, meat

0.02

Horse, meat byproducts

0.05

Milk

0.01

Milk, fat

0.25

Poultry, fat

0.05

Poultry, meat

0.02

Poultry, meat byproducts

0.05

Sheep, fat

0.05

Sheep, meat

0.02

Sheep, meat byproducts

0.05

(3) Tolerances are established for the combined residues of the herbicide quizalofop-p ethyl ester [ethyl
( R )-(2-[4-((6-chloroquinoxalin-2-yl)oxy)phenoxy)propanoate], and its acid metabolite quizalofop-p [ R -(2(4-((6-quinoxalin-2-yl)oxy)phenoxy)propanoic acid], and the S enantiomers of both the ester and the acid,
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all expressed as quizalofop-p-ethyl ester, in or on the following raw agricultural commodities;

Commodity

Parts per million

Barley, grain

0.05

Barley, hay

0.05

Barley, straw

0.05

Beet, sugar, molasses

0.2

Canola, meal

1.5

Canola, seed

1.0

Cotton, undelinted seed

0.1

Flax, seed

0.05

Lentil, seed

0.05

Peppermint, tops

2.0

Spearmint, tops

2.0

Sunflower, seed

1.9

Wheat, forage

0.05

Wheat, grain

0.05

Wheat, hay

0.05

Wheat, straw

0.05

(4) Time limited tolerances to expire on June 14, 1999 are established for the combined residues of the
herbicide quizalofop-p ethyl ester (ethyl ( R )-(2-(4-((6-chloroquinoxalin-2-yl)oxy)phenoxy)propanoate) and
it acid metabolite quizalofop-p [ R -(2-(4-((6-chloroquinoxalin-2-yl)oxy)phenoxy)propanoic acid), and the S
enantiomers of both the ester and the acid, all expressed as quizalofop-p-ethyl ester in or on the following
raw agricultural commodities:

Commodities

Parts per million

Beet, sugar, molasses

0.2

Beet, sugar, roots

0.1

Beet, sugar, tops

0.5

Vegetable, foliage of legume, except soybean, subgroup 7A

3.0

Vegetable, legume, group 6

0.25

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n),
are established for the combined residues of the herbicide quizalofop -p ethyl ester [ethyl ( R )-2-[4-((6chloroquinoxalin-2-yl)oxy)phenoxy] propionate], its acid metabolite quizalofop -p [ R -(2-[4-((6chloroquinoxalin-2-yl)oxy)phenoxy]) propanoic acid], and the S enantiomers of both the ester and the acid,
all expressed as quizalofop -p ethyl ester, in or the raw agricultural commodities, as follows:

Commodity

Parts per million

Pineapple
(d) Indirect or inadvertent residues. [Reserved]

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0.1

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[63 FR 32759, June 16, 1998, as amended at 70 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, 2006]

§ 180.442 Bifenthrin; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide bifenthrin (2-methyl [1,1′biphenyl]-3-yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate in or on
the following food commodities:

Commodity

Parts per million

Almond, hulls

2.0

Artichoke, globe

1.0

Banana1

0.1

Beet, garden, roots
Beet, garden, tops

0.45
15

Brassica, head and stem, subgroup 5A, except cabbage

0.6

Brassica, leafy greens, subgroup 5B

3.5

Bushberry subgroup 13-07B

1.8

Cabbage

4.0

Caneberry subgroup 13A

1.0

Cattle, fat

1.0

Cattle, meat byproducts
Cattle, meat
Coriander, dried leaves

0.10
0.5
25

Coriander, leaves

6.0

Coriander, seed

5.0

Corn, forage

3.0

Corn, grain (field, seed, and pop)
Corn, stover
Corn, sweet, kernel plus cob with husk removed
Cotton, undelinted seed

0.05
5.0
0.05
0.5

Eggplant

0.05

Egg

0.05

Fruit, citrus, group 10

0.05

Goat, fat
Goat, meat byproducts
Goat, meat
Grain, aspirated fractions

1.0
0.10
0.5
70

Grape

0.2

Groundcherry

0.5

Herb subgroup 19A

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0.05

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Hog, fat
Hog, meat byproducts
Hog, meat
Hop, dried cones
Horse, fat
Horse, meat byproducts

1.0
0.10
0.5
10.0
1.0
0.10

Horse, meat

0.5

Leafy petioles subgroup 4B

3.0

Lettuce, head

3.0

Mayhaw

1.4

Milk, fat (reflecting 0.1 ppm in whole milk)

1.0

Nut, tree, group 14

0.05

Okra

0.50

Pea and bean, dried shelled, expect soybean, subgroup 6C

0.15

Pea and bean, succulent shelled, subgroup 6B

0.05

Peanut

0.05

Pear

0.5

Pepino

0.5

Pepper, bell

0.5

Pepper, nonbell

0.5

Pistachio

0.05

Poultry, fat

0.05

Poultry, meat byproducts

0.05

Poultry, meat

0.05

Radish, tops

4.5

Rapeseed, seed

0.05

Sheep, fat

1.0

Sheep, meat byproducts

0.1

Sheep, meat

0.5

Soybean, hulls

0.50

Soybean, refined oil

0.30

Soybean, seed

0.2

Spinach

0.2

Strawberry

3.0

Tomato

0.15

Turnip, greens

3.5

Vegetable, cucurbit, group 9

0.4

Vegetable, legume, edible podded, subgroup 6A

0.6

Vegetable, root, subgroup 1B except sugar beet and garden beet

0.10

Vegetable, tuberous and corm, subgroup 1C

0.05

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1There

are no U.S. registrations as of April 30, 2003.

(2) A tolerance of 0.05 ppm is established for residues of the insecticide bifenthrin, (2-methyl[1,1′-biphenyl]3-yl)methyl-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropane-carboxylate, as follows:
(i) In or on all food/feed items (other than those covered by a higher tolerance as a result of use on
growing crops) in food/feed handling establishments.
(ii) The insecticide may be present as a residue from application of bifenthrin in food handling
establishments, including food service, manufacturing and processing establishments, such as
restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants,
and canneries, feed handling establishments including feed manufacturing and processing
establishments, in accordance with the following prescribed conditions:
(A) Application shall be limited to general surface and spot and/or crack and crevice treatment in food/feed
handling establishments where food/feed and food/feed products are held, processed, prepared and
served. General surface application may be used only when the facility is not in operation provided
exposed food/feed has been covered or removed from the area being treated. Spot and/or crack and
crevice application may be used while the facility is in operation provided exposed food/feed is covered or
removed from the area being treated prior to application. Spray concentration shall be limited to a
maximum of 0.06 percent active ingredient. Contamination of food/feed or food/feed contact surfaces shall
be avoided.
(B) To assure safe use of the insecticide, its label and labeling shall conform to that registered with the U.
S. Environmental Protection Agency and shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. A time-limited tolerance is established for the residues of the
insecticide bifenthrin ((2-methyl [1,1'-biphenyl]-3-yl)methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)-2,2dimethylcyclopropanecarboxylate) in connection with use of the pesticide under a section 18 emergency
exemption granted by EPA. This tolerance will expire and is revoked on the date specified in the following
table.

Commodity

Parts per million

Expiration/Revocation Date

Orchardgrass, forage

2.5

12/31/09

Orchardgrass, hay

4.5

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 31002, June 6, 1997]
Editorial Note: ForFederal Registercitations affecting §180.442, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.443 Myclobutanil; tolerances for residues.
top
(a) General. Tolerances are established for combined residues of the fungicide myclobutanil alpha-butylalpha-(4-chlorophenyl)-1 H -1,2,4-triazole-1-propanenitrile and its alcohol metabolite (alpha-(3hydroxybutyl)-alpha-(4-chlorophenyl)-1 H -1,2,4-triazole-1-propanenitrile (free and bound), in or on the
following food commodities:

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Commodity

Parts per million

Almond

0.1

Almond, hulls

2.0

Apple

0.5

Apple, dry pomace

5.0

Apple, wet pomace

5.0

Artichoke, globe

0.90

Asparagus

0.02

Banana, postharvest

4.0

Bean, snap, succulent

1.0

Caneberry subgroup 13A

2.0

Canistel

3.0

Cattle, fat

0.05

Cattle, liver

1.0

Cattle, meat

0.1

Cattle, meat byproducts, except liver

0.2

Cherry, sweet

5.0

Cherry, tart

5.0

Cilantro, leaves

9.0

Cotton, undelinted seed
Currant
Egg
Fruit, stone, except cherry
Goat, fat

0.02
3.0
0.02
2.0
0.05

Goat, liver

1.0

Goat, meat

0.1

Goat, meat byproducts, except liver

0.2

Gooseberry

2.0

Grain, aspirated fractions
Grape pomace (wet and dry)
Grape

35
10.0
1.0

Grape, raisin

10.0

Grape, raisin, waste

25.0

Hog, fat

0.05

Hog, liver

1.0

Hog, meat

0.1

Hog, meat byproducts, except liver

0.2

Hop, dried cones
Horse, fat
Horse, liver

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10
0.05
1.0

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Horse, meat

0.1

Horse, meat byproducts, except liver

0.2

Leafy greens, subgroup 4A, except spinach

9.0

Mango

3.0

Mayhaw

0.70

Milk

0.2

Okra

4.0

Papaya

3.0

Peppermint, tops

3.0

Plum, prune, dried

8.0

Poultry, fat

0.02

Poultry, meat

0.02

Poultry, meat byproducts

0.02

Sapodilla

3.0

Sapote, black

3.0

Sapote, mamey

3.0

Sheep, fat

0.05

Sheep, liver

1.0

Sheep, meat

0.1

Sheep, meat byproducts, except liver

0.2

Soybean, forage

3.5

Soybean, hay

15

Soybean, refined oil

0.40

Soybean, seed

0.25

Spearmint, tops

3.0

Star apple

3.0

Strawberry

0.50

Tomato

0.30

Tomato, puree

0.50

Tomato, paste

1.0

Vegetable, cucurbit, group 9

0.20

Vegetable, fruiting, group 8, except tomato

4.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the
fungicide myclobutanil in connection with use of the pesticide under section 18 emergency exemptions
granted by EPA. These tolerances will expire and are revoked on the dates specified in the following table.

Commodity

Parts per million Expiration/revocation date

Vegetable, foliage of legume, group
07

1.0

12/31/09

Vegetable, legume, group 06

1.0

12/31/09

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide myclobutanil
alpha-butyl-alpha-(4-chlorophenyl)-1 H -1,2,4-triazole-1-propanenitrile in or on the following food
commodities:

Commodity

Parts per million

Animal feed, nongrass, group 18

0.03

Grain, cereal, forage, fodder and straw, group 16

0.03

Grain, cereal, group 15

0.03

Vegetable, brassica, leafy, group 5

0.03

Vegetable, foliage of legume, group 7

0.03

Vegetable, fruiting, group 8

0.03

Vegetable, leafy, except brassica, group 4

0.03

Vegetable, leaves of root and tuber, group 2

0.03

Vegetable, legume, group 6

0.03

Vegetable, root and tuber, group 1

0.03

[54 FR 6131, Feb. 8, 1989]
Editorial Note: ForFederal Registercitations affecting §180.443, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.444 Sulfur dioxide; tolerances for residues.
top
A tolerance is established as follows for sulfite residues of the fungicide sulfur dioxide (determined as
(SO2)) in or on the following raw agricultural commodity(ies):

Commodity

Parts per million

Grape, postharvest

10.0

[54 FR 20126, May 10, 1989]

§ 180.445 Bensulfuron methyl; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide bensulfuron methyl (methyl-2[[[[[(4,6dimethoxy-pyrimidin-2-yl) amino] carbonyl] amino] sulfonyl] methyl] benzoate) in or on the following raw
agricultural commodities:

Commodity

Parts per million

Crayfish

0.05

Rice, grain

0.02

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Rice, straw

0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 9435, Feb. 25, 1998]

§ 180.446 Clofentezine; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide clofentezine (3,6-bis(2chlorophenyl)-1,2,4,5-tetrazine) in or on the following raw agricultural commodities:

Commodity

Parts per million

Almond, hulls

5.0

Almond

0.5

Apple, pomace

3.0

Apple

0.5

Apricot

1.0

Cherry

1.0

Grape

1.0

Nectarine

1.0

Peach

1.0

Pear

0.5

Persimmon

0.05

Walnut

0.02

(2) Tolerances are established for the combined residues of clofentezine and the 3-(2-chloro-4hydroxyphenyl)-6-(2-chlorophenyl)-1,2,4,5-tetrazine metabolite in or on the following commodities:

Commodity

Parts per million

Cattle, fat

0.05

Cattle, liver

0.4

Cattle, meat

0.05

Cattle, meat byproducts, except liver

0.05

Goat, fat

0.05

Goat, liver

0.4

Goat, meat

0.05

Goat, meat byproducts, except liver

0.05

Hog, fat

0.05

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Hog, liver

0.4

Hog, meat

0.05

Hog, meat byproducts, except liver

0.05

Horse, fat

0.05

Horse, liver

0.4

Horse, meat

0.05

Horse, meat byproducts, except liver

0.05

Milk

0.01

Sheep, fat

0.05

Sheep, liver

0.4

Sheep, meat

0.05

Sheep, meat byproducts, except liver

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[56 FR 15503, Apr. 17, 1991, as amended at 56 FR 22335, May 15, 1991; 59 FR 26947, May 25, 1994; 60
FR 12709, Mar. 8, 1995; 64 FR 19050, Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005]

§ 180.447 Imazethapyr; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the herbicide imazethapyr, 2-[4,5-dihydro-4methyl-4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, applied as its acid or
ammonium salt, in or on the following raw agricultural commodities:

Commodity

Parts per million
0.10

Canola, seed1
Soybean

0.1

Vegetable, legume, group 6

0.1

1 There are no U.S. registrations for canola as of March 21, 2003.
(2) Tolerances are established for the sum of the residues of the herbicide imazethapyr, 2-[4,5-dihydro-4methyl-4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid; its metabolite CL
288511, 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine
carboxylic acid; and its metabolite CL 182704, 5-[1-(beta-D-glucopyranosyloxy)ethyl]-2-[4,5-dihydro-4methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-pyridinecarboxylic acid, applied as its acid or
ammonium salt, in or on the following commodities:

Commodity

Parts per million

Alfalfa, seed

0.15

Alfalfa, seed screenings

0.15

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Animal feed, nongrass, group 18, forage

3.0

Animal feed, nongrass, group 18, hay

5.5

Peanut

0.1

Rice, bran

1.2

Rice, grain

0.3

Rice, straw

0.4

(3) A tolerance is established for the sum of residues of the herbicide imazethapyr, 2-[4,5-dihydro-4methyl-4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, and its metabolite CL
288511, 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine
carboxylic acid, applied as its acid or ammonium salt, in or on the following commodities:

Commodity

Parts per million

Cattle, meat byproducts

0.10

Corn, field, forage

0.1

Corn, field, grain

0.1

Corn, field, stover

0.1

Crayfish

0.15

Goat, meat byproducts

0.10

Hog, meat byproducts

0.10

Horse, meat byproducts

0.10

Sheep, meat byproducts

0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n) of
this chapter, are established for the sum of residues of the herbicide imazethapyr, 2- [4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-ethyl- 3-pyridine carboxylic acid, as its ammonium salt, and its
metabolite, 2- [4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1- hydroxyethyl)-3pyridine carboxylic acid, both free and conjugated, applied as its acid or ammonium salt, in or on the
following raw agricultural commodities:

Commodity

Parts per million

Endive

0.1

Lettuce, head

0.1

Lettuce, leaf

0.1

(d) Indirect or inadvertent residues. [Reserved]
[67 FR 55331, Aug. 29, 2002, as amended at 68 FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, 2006]

§ 180.448 Hexythiazox; tolerance for residues.
top
(a) General. Tolerances are established for the combined residues of the miticide hexythiazox, trans-5-(4chlorophenyl) -N -cyclohexyl-4-methyl-2-oxothiazolidine-3-carboxamide and its metabolites containing the
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(4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety (expressed as parts per million of the parent
compound) in or on the following commodities:

Commodity

Parts per million

Almond, hulls

10

Apple, wet pomace

0.40

Caneberry subgroup 13A

1.0

Cattle, fat

0.02

Cattle, meat byproducts

0.02

Citrus, dried pulp

0.60

Citrus, oil

24

Date, dried fruit

1.0

Fruit, pome, group 11

0.25

Fruit, stone, group 12, except plum

1.0

Goat, fat

0.02

Goat, meat byproducts

0.02

Grape

0.75

Hog, fat

0.02

Hog, meat byproducts

0.02

Hop, dried cones

2.0

Horse, fat

0.02

Horse, meat byproducts

0.02

Milk

0.02

Nut, tree, group 14

0.30

Peppermint, tops

2.0

Pistachio

0.30

Plum

0.10

Plum, prune, dried

0.40

Plum, prune, fresh

0.10

Sheep, fat

0.02

Sheep, meat byproducts

0.02

Spearmint, tops

2.0

Strawberry

3.0

(b) Section 18 emergency exemptions . Time-limited tolerances are established for the combined residues
of the insecticide hexythiazox and its metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3thiazolidine moiety in connection with use of the pesticide under section 18 emergency exemptions
granted by EPA. These tolerances will expire and are revoked on the dates specified in the following table.

Commodity

Parts per million

Expiration/revocation date

Corn, field, forage

2.0

12/31/10

Corn, field, grain

0.05

12/31/10

Corn, field, stover

2.0

12/31/10

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(c) Tolerances with regional registrations. Tolerances with regional registrations as defined 40 CFR 180.1
(n), are established for the combined residues of the ovicide/miticide hexythiazox (trans-5-(4chlorophenyl)- N -cyclohexyl-4-methyl-2-oxothiazolidine-3-carboxamide) and its metabolites containing the
(4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety (expressed as parent) in or on the following
commodities:

Commodity

Parts per million

Corn, field, forage

6.0

Corn, field, grain

0.02

Corn, field, stover

2.5

Cotton, gin byproducts, CA only

3.0

Cotton, undelinted seed, CA only

0.20

Fruit, citrus group 10 (CA, AZ, TX only)

0.35

(d) Indirect or inadvertent residues. [Reserved]
[54 FR 17948, Apr. 26, 1989]
Editorial Note: ForFederal Registercitations affecting §180.448, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.449 Avermectin B1 and its delta-8,9-isomer; tolerances for residues.
top
(a) General. Tolerances are established for the combined residues of the insecticide avermectin B1(a
mixture of avermectins containing greater than or equal to 80% avermectin B1a(5- O- demethyl avermectin
A1) and less than or equal to 20% avermectin B1b(5- O -demethyl-25-de(1-methylpropyl)-25-(1methylethyl) avermectin A1)) and its delta-8,9-isomer in or on the following commodities:

Commodity
Almond, hulls
Apple
Apple, wet pomace
Avocado

Parts per million
0.10
0.020
0.10
0.020

Cattle, fat

0.03

Cattle, meat

0.02

Cattle, meat byproducts

0.06

Celeriac, roots

0.05

Celeriac, tops

0.05

Citrus, dried pulp

0.10

Citrus, oil

0.10

Citrus

0.02

Cotton, gin byproducts

0.15

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Cotton, undelinted seed

0.005

Food products in food handling establishments (other than those
already covered by higher tolerances as a result of use on growing
crops, and other than those already covered by tolerances on milk,
meat, and meat byproducts)

0.01

Fruit, stone, group 12

0.09

Goat, fat

0.01

Goat, meat

0.02

Goat, meat byproducts

0.02

Grape

0.02

Herb subgroup 19A, except chive

0.030

Hog, fat

0.01

Hog, meat

0.02

Hog, meat byproducts

0.02

Hop, dried cones

0.20

Horse, fat

0.01

Horse, meat

0.02

Horse, meat byproducts

0.02

Milk

0.005

Nut, tree, group 14

0.01

Pear

0.02

Peppermint, tops

0.010

Pistachio

0.01

Plum, prune, dried

0.025

Poultry, meat

0.02

Poultry, meat byproducts

0.02

Sheep, fat

0.01

Sheep, meat

0.02

Sheep, meat byproducts

0.02

Spearmint, tops

0.010

Vegetable, tuberous and corm, subgroup 01C

0.01

Strawberry

0.02

Vegetable, cucurbit, group 9

0.005

Vegetable, fruiting, group 8

0.020

Vegetable, leafy, except brassica, group 4

0.10

(b) Section 18 emergency exemptions. Time-limited tolerances are established for the residues of
avermectin B1and it delta-8,9-isomer, in connection with use of the pesticide under section 18 emergency
exemptions granted by EPA. The tolerances are specified in the following table. The tolerances will expire
on the dates specified in the table.

Commodity

Parts per million

Expiration/revocation date

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Bean, lima, seed

0.005

12/31/10

Onion, bulb

0.005

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 44095, Aug. 19, 1997]
Editorial Note: ForFederal Registercitations affecting §180.449, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1ethanol; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the fungicide β-(4-chlorophenoxy)-α(1,1-dimethylethyl)-1 H -1,2,4-triazole-1-ethanol (triadimenol) and its butanediol metabolite, 4-(4chlorophenoxy)-2,2-dimethyl-4-(1 H -1,2,4-triazol-l-yl)-1,3-butanediol, calculated as triadimenol, in or on
the following commodities:

Commodity
Banana 1

Parts per million
0.2

Barley, grain

0.05

Barley, straw

0.2

Corn, field, forage

0.05

Corn, field, grain

0.05

Corn, field, stover

0.05

Corn, pop, grain

0.05

Corn, pop, stover

0.05

Corn, sweet, forage

0.05

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, stover

0.05

Cotton, undelinted seed

0.02

Oat, forage

2.5

Oat, grain

0.05

Oat, straw

0.2

Rye, forage

2.5

Rye, grain

0.05

Rye, straw

0.1

Sorghum, forage

0.05

Sorghum, grain, grain

0.01

Sorghum, grain, stover

0.01

Wheat, forage
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Wheat, grain

0.05

Wheat, straw

0.2

1There

are no U.S. registrations for banana (whole) as of September 22, 1993.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54962, Sept. 24, 2008]

§ 180.451 Tribenuron methyl; tolerances for residues.
top
(a) General . Tolerances are established for the residues of the herbicide tribenuron methyl (methyl-2-[[[[N(4-methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino] carbonyl]amino]sulfonyl] benzoate) in or on the
following raw agricultural commodities:

Commodity

Parts per million

Barley, grain
Barley, hay

0.05
0.4

Barley, straw

0.10

Canola, seed

0.02

Corn, field, forage

0.05

Corn, field, grain

0.05

Corn, field, stover

0.05

Cotton, gin byproducts

0.02

Cotton, undelinted seed

0.02

Flax, seed

0.02

Oat, forage

0.05

Oat, grain

0.05

Oat, hay

0.05

Oat, straw

0.10

Rice, grain

0.05

Rice, straw

0.05

Sorghum, grain, forage

0.05

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.05

Soybean, seed

0.05

Sunflower, seed

0.05

Wheat, forage

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Wheat, grain

0.05

Wheat, hay

0.5

Wheat, straw

0.10

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration, as defined in §180.1(n)
are established for residues of the herbicide tribenuron methyl (methyl-2-[[[[N-(4-methoxy-6-methyl-1,3,5triazin-2-yl) methylamino] carbonyl]amino]sulfonyl] benzoate) in or on the following raw agricultural
commodities:

Commodity

Parts per million

Grass, forage, fodder and hay, group 17, except bermudagrass;
forage

0.10

Grass, forage, fodder and hay, group 17, except bermudagrass; hay

0.10

(d) Indirect or inadvertent residues . [Reserved]
[69 FR 56718, Sept. 22, 2004, as amended at 72 FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, 2008]

§ 180.452 Primisulfuron-methyl; tolerances for residues.
top
(a) General. Tolerances are established for residues of primisulfuron-methyl (3-[4,6-bis-(difluoromethoxy)pyrimidin-2-yl]-1-(2-methoxycarbonylphenylsulfonyl) urea) in or on the following raw agricultural
commodities.

Commodity

Parts per million

Cattle, fat

0.10

Cattle, meat

0.10

Cattle, meat byproducts

0.10

Corn, forage

0.10

Corn, grain

0.02

Corn, stover

0.10

Corn, sweet, kernel plus cob with husks removed

0.10

Egg

0.10

Goat, fat

0.10

Goat, meat

0.10

Goat, meat byproducts

0.10

Hog, fat

0.10

Hog, meat

0.10

Hog, meat byproducts

0.10

Horse, fat

0.10

Horse, meat

0.10

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Horse, meat byproducts

0.10

Milk

0.02

Poultry, fat

0.10

Poultry, meat

0.10

Poultry, meat byproducts

0.10

Sheep, fat

0.10

Sheep, meat

0.10

Sheep, meat byproducts

0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[55 FR 21548, May 25, 1990, as amended at 62 FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, 1998; 67
FR 35049, May 17, 2002]

§ 180.454 Nicosulfuron, [3-pyridinecarboxamide, 2-((((4,6-dimethoxypyrimidin-2-yl)
aminocarbonyl)aminosulfonyl))-N,N-dimethyl]; tolerances for residues.
top
Tolerances are established for the residues of the herbicide nicosulfuron [3-pyridinecarboxamide, 2-((((4,6dimethoxypyrimidin-2-yl)aminocarbonyl)aminosulfonyl))-N,N-dimethyl] in or on the following raw
agricultural commodities:

Commodity

Parts per million

Corn, field, forage

0.1

Corn, forage

0.1

Corn, grain

0.1

Corn, stover

0.1

Corn, sweet, forage

0.1

Corn, sweet, kernel plus cob with husks removed

0.1

Corn, sweet, stover

0.1

[55 FR 28621, July 12, 1990, as amended at 61 FR 7734, Feb. 29, 1996]

§ 180.455 Procymidone; tolerances for residues.
top
A tolerance is established for the residues of the fungicide procymidone, N -(3,5-dichlorophenyl)-1,2dimethylcyclopropane-1,2 dicarboximide, in or on the following raw agricultural commodity:

Commodity

Parts per million

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Grape, wine

5.0

[59 FR 42514, Aug. 18, 1994]

§ 180.456 Oxadixyl; tolerances for residues.
top
(a) General. Tolerances are established for the combined residues of the fungicide oxadixyl [2-methoxy-N(2-oxo-1,3-oxazolidin-3-yl)-acet-2′,6′-xylidide] and its desmethyl (M-3) metabolite (2-hydroxy-N-(2-oxo-1,3oxazolidin-3-yl)-acet-2′,6′-xylidide), calculated as oxadixyl in or on the following raw agricultural
commodities:

Commodity

Parts per million Expiration/Revocation Date

Animal feed, nongrass, group, 18

0.1

9/27/03

Cotton, undelinted seed

0.1

9/27/03

Grain, cereal, group 15, except
wheat

0.1

9/27/03

Grass, forage, fodder and hay,
group 17

0.1

9/27/03

Pea

0.1

9/27/03

Soybean

0.1

9/27/03

Sunflower, seed

0.1

9/27/03

Vegetable, brassica, leafy, group 5

0.1

9/27/03

Vegetable, cucurbit, group 9

0.1

9/27/03

Vegetable, fruiting, group 8

0.1

9/27/03

Vegetable, leafy, except brassica,
group 4

0.1

9/27/03

Vegetable, root and tuber, group 1

0.1

9/27/03

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 45642, July 10, 2002]

§ 180.457 Beta-([1,1′-biphenyl]-4-yloxy)-alpha-(1,1-dimethylethyl)-1 H
triazole-1-ethanol; tolerances for residues.

-1,2,4-

top
A tolerance is established for the residues of the fungicide beta-([1,1′-biphenyl]-4-yloxy)-alpha-(1,1dimethylethyl)-1 H -1,2,4-triazole-1-ethanol in or on the following raw agricultural commodity:

Commodity

Parts per million

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Banana

0.2

There are no U.S. registrations as of April 1, 1992.
[57 FR 29032, June 30, 1992]

§ 180.458 Clethodim; tolerances for residues.
top
(a) General. (1) Tolerances are established for the combined residues of the herbicide clethodim ((E)-(±)-2[1-[[(3-chloro-2-propenyl)oxy]imino]propyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one) and its
metabolites containing the 2-cyclohexen-1-one moiety in or on the following raw agricultural commodities.

Commodity

Parts per million

Cattle, fat

0.2

Cattle, meat

0.2

Cattle, meat byproducts

0.2

Cotton, undelinted seed

1.0

Egg

0.2

Goat, fat

0.2

Goat, meat

0.2

Goat, meat byproducts

0.2

Hog, fat

0.2

Hog, meat

0.2

Hog, meat byproducts

0.2

Horse, fat

0.2

Horse, meat

0.2

Horse, meat byproducts

0.2

Milk

0.05

Potato

0.5

Poultry, fat

0.2

Poultry, meat

0.2

Poultry, meat byproducts

0.2

Sheep, fat

0.2

Sheep, meat

0.2

Sheep, meat byproducts

0.2

Soybean

10.0

(2) Time limited tolerances are established for the combined residues of clethodim, ((E)-(±)-2-[1-[[(3-chloro2-propenyl)oxy]imino]propyl]-5-[2-ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one) and its metabolites
containing the 5-(2-ethylthiopropyl)cyclohexene-3-one and 5-(2-(ethylthiopropyl)-5-hydroxycyclohexene-3one moieties and their sulphoxides and sulphones, expressed as clethodim in or on the following raw
agricultural commodities:

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Commodity

Parts per million

Expiration/Revocation Date

Tomato, paste

3

4/30/03

Tomato, puree

2

4/30/03

(3) Tolerances are established for the combined residues of the herbicide clethodim [(E)-(±)-2-[1-[[(3chloro-2-propenyl)oxy]imino]propyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one] and its
metabolites containing the 5-(2-ethylthiopropyl)cyclohexen-3-one and 5-(2-ethylthiopropyl)-5hydroxycyclohexen-3-one moieties and their sulphoxides and sulphones, expressed as clethodim
tolerance residues for the following commodities.

Commodity
Alfalfa, forage

Parts per million
6.0

Alfalfa, hay

10

Asparagus

1.7

Bean, dry, seed

2.5

Beet, sugar, molasses

1.0

Beet, sugar, roots

0.20

Beet, sugar, tops

1.0

Brassica, head and stem, subgroup 5A

3.0

Brassica, leafy greens, subgroup 5B

3.0

Canola, meal

1.0

Canola, seed

0.50

Corn, field, forage

0.2

Corn, field, grain

0.2

Corn, field, stover

0.2

Cranberry

0.50

Clover, forage

10.0

Clover, hay

20.0

Flax, meal

1.0

Flax, seed

0.50

Flax seed

0.6

Herb subgroup 19A
Hop, dried cones

12.0
0.5

Leaf petioles subgroup 4B

0.60

Leafy greens subgroup 4A

2.0

Lettuce, leaf

2.0

Melon subgroup 9A

2.0

Mustard, seed

0.50

Onion, bulb

0.20

Onion, green

2.0

Peanut

3.0

Peanut, hay

3.0

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Peanut, meal

5.0

Peppermint, tops

5.0

Potato, granules/flakes

2.0

Radish, tops

0.70

Safflower, meal

10.0

Safflower, seed

5.0

Sesame, seed

0.35

Spearmint, tops

5.0

Spinach

2.0

Squash/cucumber subgroup 9B

0.50

Strawberry

3.0

Sunflower, meal

10.0

Sunflower, seed

5.0

Turnip, greens

3.0

Vegetable, fruiting, group 8

1.0

Vegetable, legume group 6, except soybean

3.5

Vegetable, root, except sugar beet, subgroup 1B

1.0

Vegetable, tuberous and corm, subgroup 1C

1.0

(4) Tolerances are established for residues of the herbicide clethodim ((E)-(±)-2-[1-[[(3-chloro-2-propenyl)
oxy]imino]propyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one) and its metabolites containing the
2-cyclohexen-1-one moiety in or on the following feeds.

Feed

Parts per million

Cotton, meal
Soybean, soapstock

2.0
15.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[59 FR 4835, Feb. 2, 1994, as amended at 60 FR 33360, June 28, 1995; 60 FR 40505, Aug. 9, 1995; 63
FR 17108, Apr. 8, 1998; 66 FR 14837, Mar. 14, 2001; 66 FR 30080, June 5, 2001; 66 FR 30333, June 6,
2001; 66 FR 47979, Sept. 17, 2001; 66 FR 67493, Dec. 31, 2001; 67 FR 46900, July 17, 2002; 70 FR
7047, Feb. 10, 2005; 72 FR 26316, May 9, 2007; 72 FR 71082, Dec. 14, 2007]

§ 180.459 Triasulfuron; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide triasulfuron [3-(6-methoxy-4-methyl1,3,5-triazin-2-yl)-1-(2-(2-chloroethoxy)phenylsulfonyl)urea] in or on the following raw agricultural
commodities:

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Commodity

Parts per million

Barley, grain

0.02

Barley, straw

2.0

Cattle, fat

0.1

Cattle, kidney

0.5

Cattle, meat byproducts, except kidney

0.1

Cattle, meat

0.1

Goat, fat

0.1

Goat, kidney

0.5

Goat, meat byproducts, except kidney

0.1

Goat, meat

0.1

Grass, forage

7.0

Grass, hay

2.0

Hog, fat

0.1

Hog, kidney

0.5

Hog, meat byproducts

0.1

Hog, meat

0.1

Horse, fat

0.1

Horse, kidney

0.5

Horse, meat byproducts, except kidney

0.1

Horse, meat

0.1

Milk

0.02

Sheep, fat

0.1

Sheep, kidney

0.5

Sheep, meat byproducts, except kidney

0.1

Sheep, meat

0.1

Wheat, forage

5.0

Wheat, grain

0.02

Wheat, straw

2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[60 FR 36731, July 18, 1995, as amended at 63 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, 1998]

§ 180.460 Benoxacor; tolerances for residues.
top
(a) General . Tolerances are established for residues of the inert ingredient (safener) benoxacor (4(dichloroacetyl)-3,4-dihydro-3-methyl-2H-1, 4-benzoxazine) at 0.01 parts per million (ppm) when used in
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pesticide formulations containing metolachlor or S-metolachlor in or on raw agricultural commodities for
which tolerances have been established for metolachlor or S-metolachlor.
(b) Section 18 energency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 7305, Feb. 13, 1998, as amended at 70 FR 21631, Apr. 27, 2005]

§ 180.461 Cadusafos; tolerances for residues.
top
A tolerance is established for the residues of the nematicide/insecticide cadusafos, O -ethyl S,S -di- sec butyl phosphorodithioate, in or on the following raw agricultural commodity:

Commodity

Parts per million

Banana

0.01

There are no U.S. registrations as of May 10, 1994, for the nematicide/insecticid cadusafos.
[59 FR 39467, Aug. 3, 1994]

§ 180.462 Pyridate; tolerances for residues.
top
(a) General. Tolerances are established for the combined residues of the herbicide pyridate ( O -(6-chloro3-phenyl-4-pyridazinyl)- S -octyl-carbonothioate), the metabolite 6-chloro-3-phenyl-pyridazine-4-ol and
conjugates of 6-chloro-3-phenyl-pyridazine-4-ol, expressed as pyridate, in or on the following raw
agricultural commodities:

Commodity

Parts per million

Brassica, head and stem, subgroup 5A

0.03

Cabbage

0.03

Chickpea, seed

0.1

Collards

0.03

Corn, field, forage

0.03

Corn, grain

0.03

Corn, stover

0.03

Peanut

0.03

Peppermint, tops

0.20

Spearmint, tops

0.20

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[57 FR 54303, Nov. 18, 1992, as amended at 62 FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, 1998; 64
FR 46298, Aug. 25, 1999; 65 FR 25652, May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR 35665, June
29, 2007]

§ 180.463 Quinclorac; tolerances for residues.
top
(a) General. Tolerances are established for residues of quinclorac (3,7-dichloro-8-quinoline carboxylic
acid) in or the following food commodities:

Commodity

Parts per million

Barley, grain

2.0

Cattle, fat

0.7

Cattle, meat byproducts

1.5

Cattle, meat

0.05

Egg

0.05

Goat, fat

0.7

Goat, meat byproducts

1.5

Goat, meat

0.05

Grain, aspirated fractions

1200

Hog, fat

0.7

Hog, meat byproducts

1.5

Hog, meat

0.05

Horse, fat

0.7

Horse, meat byproducts

1.5

Horse, meat

0.05

Milk

0.05

Poultry, fat

0.05

Poultry, meat byproducts

0.1

Poultry, meat

0.05

Rice, bran

15.0

Rice, grain

5.0

Rice, straw

12.0

Sheep, fat

0.7

Sheep, meat byproducts

1.5

Sheep, meat

0.05

Sorghum, grain, forage

3.0

Sorghum, grain, grain

6.0

Sorghum, grain, stover

1.0

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Wheat, forage

1.0

Wheat, germ

0.75

Wheat, grain

0.5

Wheat, hay

0.5

Wheat, straw

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[57 FR 47996, Oct. 21, 1992, as amended at 64 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. 26,
1999; 65 FR 33701, May 24, 2000; 67 FR 35049, May 17, 2002; 72 FR 55073, Sept. 28, 2007]

§ 180.464 Dimethenamid; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide dimethenamid, 1(R,S)-2-chloro- N [(1-methyl-2-methoxy)ethyl]- N -(2,4-dimethylthien-3-yl)-acetamide, applied as either the 90:10 or 50:50 S:
R isomers, in or on the following food commodities:

Commodity

Parts per million

Bean, dry, seed

0.01

Beet, garden, roots

0.01

Beet, garden, tops

0.01

Beet, sugar, dried pulp

0.01

Beet, sugar, molasses

0.01

Beet, sugar, roots

0.01

Beet, sugar, tops

0.01

Corn, field, forage

0.01

Corn, field, grain

0.01

Corn, field, stover

0.01

Corn, pop, forage

0.01

Corn, pop, grain

0.01

Corn, pop, stover

0.01

Corn, sweet, forage

0.01

Corn, sweet, kernel plus cob with husks removed

0.01

Corn, sweet, stover

0.01

Garlic

0.01

Grass, forage

0.15

Grass, hay
Grass, seed screenings

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2.5
0.01

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Grass, straw

0.01

Hop, dried cones

0.05

Horseradish

0.01

Leek

0.01

Onion, bulb

0.01

Onion, green

0.01

Onion, Welsh

0.01

Peanut

0.01

Peanut, hay

0.01

Radish, roots

0.01

Radish, tops

0.01

Rutabaga, roots

0.01

Rutabaga, tops

0.1

Shallot, bulb

0.01

Shallot, fresh leaves

0.01

Sorghum, grain, forage

0.01

Sorghum, grain, grain

0.01

Sorghum, grain, stover

0.01

Soybean, seed

0.01

Turnip, greens

0.1

Turnip, roots

0.01

Turnip, tops

0.1

Vegetable, tuberous and corm, subgroup 1C

0.01

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registration are established for
residues of dimethenamid, 1 (R,S)-2-chloro-N-[(1-methyl-2-methoxy) ethyl]-N-(2,4-dimethylthien-3-yl)acetamide) in or on the following raw agricultural commodities:

Commodity

Parts per million

Pumpkin

0.01

Squash, winter

0.01

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 51551, Aug. 24, 2000, as amended at 67 FR 46884, July 17, 2002; 69 FR 29459, May 24, 2004;
69 FR 57207, Sept. 24, 2004; 70 FR 24712, May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR 49354,
Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; 72 FR 73630, Dec. 28, 2007]

§ 180.465 4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.
top
(a) General. Tolerances are established for the residues of 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]
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decane, (CAS No. 71526–07–3) when used as an inert ingredient (safener) in or on the following raw
agricultural commodities:

Commodity1

Parts per million

Corn, field, forage

0.005

Corn, field, grain

0.005

Corn, field, stover

0.005

Corn, pop, grain

0.005

Corn, pop, stover

0.005

1There

are no U.S. registered products containing 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of
June 17, 2002.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 4392, Jan. 29, 2003]

§ 180.466 Fenpropathrin; tolerances for residues.
top
(a) General. Tolerances are established for residues of the pesticide chemical fenpropathrin (alpha-cyano3-phenoxy-benzyl 2,2,3,3-tetramethylcyclopropanecarboxylate) in or on the following agricultural
commodities:

Commodity

Parts per million

Almond, hulls

4.5

Avocado

1.0

Brassica, head and stem, subgroup 5A

3.0

Bushberry subgroup 13B

3.0

Caneberry subgroup 13-07A

12

Canistel

1.0

Cattle, fat

1.0

Cattle, meat byproducts

0.1

Cattle, meat

0.1

Cherry, sweet

5.0

Cherry, tart

5.0

Citrus, dried pulp

4.0

Citrus, oil

75

Cotton, refined oil

3.0

Cotton, undelinted seed

1.0

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Egg

0.05

Fruit, citrus, group 10

2.0

Fruit, pome, group 11

5.0

Fruit, stone, crop group 12, except cherry

1.4

Goat, fat

1.0

Goat, meat byproducts

0.1

Goat, meat

0.1

Grape

5.0

Grape, raisin

10.0

Hog, fat

1.0

Hog, meat byproducts

0.1

Hog, meat

0.1

Horse, fat

1.0

Horse, meat byproducts

0.1

Horse, meat

0.1

Juneberry

3.0

Lingonberry

3.0

Mango

1.0

Melon subgroup 9A

0.5

Milk, fat (reflecting 0.08 ppm in whole milk)

2.0

Nut, tree, crop group 14

0.10

Olive

5.0

Papaya

1.0

Pea, succulent

0.02

Peanut, hay

20.0

Peanut

0.01

Pistachio

0.10

Poultry, fat

0.05

Poultry, meat byproducts

0.05

Poultry, meat

0.05

Salal

3.0

Sapodilla

1.0

Sapote, black

1.0

Sapote, mamey

1.0

Sheep, fat

1.0

Sheep, meat byproducts

0.1

Sheep, meat

0.1

Squash/Cucumber subgroup 9B

0.5

Star apple

1.0

Strawberry

2.0

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Vegetable, fruiting, group 8

1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63034, Nov. 26, 1997, as amended at 63 FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, 1999; 65
FR 11242, Mar. 2, 2000; 65 FR 24397, Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR 64774, Dec. 14,
2001; 67 FR 35049, May 17, 2002; 70 FR 38789, July 6, 2005; 70 FR 55747, Sept. 23, 2005; 74 FR
12606, Mar. 25, 2009]

§ 180.467 Carbon disulfide; tolerances for residues.
top
Tolerances are established for the nematicide, insecticide, and fungicide carbon disulfide, from the
application of sodium tetrathiocarbonate, in or on the following raw agricultural commodities:

Commodity

Parts per million

Almond

0.1

Almond, hulls

0.1

Grapefruit

0.1

Grape

0.1

Lemon

0.1

Orange, sweet

0.1

Peach

0.1

Plum, prune, fresh

0.1

[58 FR 33771, June 21, 1993, as amended at 62 FR 26949, May 16, 1997]

§ 180.468 Flumetsulam; tolerances for residues.
top
Tolerances are established for residues of the herbicide flumetsulam, N -(2,6-difluorophenyl)-5-methyl(1,2,4)-triazolo-[1,5a]-pyrimidine-2-sulfonamide, in or on the following raw agricultural commodities:

Commodity

Parts per million

Bean, dry

0.05

Corn, field, grain

0.05

Corn, field, forage

0.05

Corn, field, stover

0.05

Soybean

0.05

[58 FR 57967, Oct. 28, 1993, as amended at 71 FR 58518, Oct. 4, 2006]
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§ 180.469 Dichlormid; tolerances for residues.
top
(a) General . Tolerances are established for residues of dichormid; (Acetamide, 2,2-dichloro- N,N -di-2propenyl-) (CAS Reg. No. 37764–25–3) when used as an inert ingredient (herbicide safener) in pesticide
formulations in or on the following food commodities:

Commodity

Parts per million Expiration/revocation date

Corn, field, forage

0.05

12/31/10

Corn, field, grain

0.05

12/31/10

Corn, field, stover

0.05

12/31/10

Corn, pop, grain

0.05

12/31/10

Corn, pop, stover

0.05

12/31/10

Corn, sweet, forage

0.05

12/31/10

Corn, sweet, kernel plus cob with
husks removed

0.05

12/31/10

Corn, sweet, stover

0.05

12/31/10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 16149, Mar. 27, 2000, as amended at 67 FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, 2004;
70 FR 76699, Dec. 28, 2005; 74 FR 37623, July 29, 2009]

§ 180.470 Acetochlor; tolerances for residues.
top
(a) General . Tolerances are established for residues of acetochlor; 2-chloro-2'-methyl-6-ethyl- N ethoxymethylacetanilide, and its metabolites containing the ethyl methyl aniline (EMA) moiety and the
hydroxyethyl methyl aniline (HEMA) moiety, to be analyzed as acetochlor and expressed as acetochlor
equivalents, in or on the following raw agricultural commodities.

Commodity

Parts per million

Corn, field, forage

4.5

Corn, field, grain

0.05

Corn, field, stover

2.5

Corn, pop, grain

0.05

Corn, pop, stover

2.5

Corn, sweet, forage

1.5

Corn, sweet, kernels plus cob with husks removed
Corn, sweet, stover
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0.05
1.0

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Sorghum, grain, forage

1.6

Sorghum, grain, grain

0.05

Sorghum, grain, stover

1.7

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for indirect or inadvertent residues of
acetochlor; 2-chloro-2'-methyl-6-ethyl- N -ethoxymethylacetanilide, and its metabolites containing the ethyl
methyl aniline (EMA) moiety and the hydroxyethyl methyl aniline (HEMA) moiety, to be analyzed as
acetochlor and expressed as acetochlor equivalents, in or on the following raw agricultural commodities
when present therein as a result of application of acetochlor to the growing crops in paragraph (a) of this
section:

Commodity

Parts per million

Animal feed, nongrass, group 18, forage

1.3

Animal feed, nongrass, group 18, hay

3.5

Beet, sugar, root

0.05

Beet, sugar, tops

0.05

Grain, cereal, forage, fodder and straw, group 16, except corn, grain
sorghum, rice and wheat, forage

0.5

Grain, cereal, forage, fodder and straw, group 16, except corn, grain
sorghum, rice and wheat, hay

2.0

Grain, cereal, forage, fodder and straw, group 16, except corn, grain
sorghum, rice and wheat, stover

0.1

Grain, cereal, forage, fodder and straw, group 16, except corn, grain
sorghum, rice and wheat, straw

0.3

Grain, cereal, group 15, except corn, grain sorghum, rice, and wheat,
grain

0.05

Pea and bean, dried shelled, except soybean, subgroup 6C

0.05

Potato

0.05

Soybean, forage

0.7

Soybean, hay

1.0

Soybean, seed

0.1

Sunflower, seed

0.05

Wheat, forage

0.5

Wheat, grain

0.02

Wheat, hay

2.0

Wheat, straw

0.1

[72 FR 27468, May 16, 2007, as amended at 74 FR 29969, June 24, 2009]

§ 180.471 Furilazole; tolerances for residues.
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(a) General . Tolerances are established for residues of furilazole; 3-dichloroacetyl-5-(2-furanyl)-2, 2dimethyloxazolidine (CAS Reg. No. 121776–33–8) when used as an inert ingredient (safener) in pesticide
formulations in or on the following raw agricultural commodities:

Commodity

Parts per million

Corn, field, forage

0.01

Corn, field, grain

0.01

Corn, field, stover

0.01

Corn, pop, grain

0.01

Corn, pop, stover

0.01

Sorghum, forage

0.01

Sorghum, grain

0.01

Sorghum, stover

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 8867, Feb. 23, 2000, as amended at 67 FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, 2007]

§ 180.472 Imidacloprid; tolerances for residues.
top
(a) General . Tolerances are established permitting the combined residues of the insecticide imidacloprid
(1-[6-chloro-3-pyridinyl) methyl]- N -nitro-2-imidazolidinimine) and its metabolites containing the 6chloropyridinyl moiety, all expressed as 1-[(6-chloro-3-pyridinyl)methyl]- N -nitro-2-imidazolidinimine, in or
on the following food commodities:

Commodity

Parts Per Million

Acerola

1.0

Almond, hulls

4.0

Apple

0.5

Apple, wet pomace

3.0

Aspirated grain fractions

240

Atemoya

0.30

Artichoke, globe

2.5

Avocado

1.0

Banana

0.50

Barley, grain

0.05

Barley, hay

0.5

Barley, straw

0.5

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Beet, sugar, roots

0.05

Beet, sugar, tops

0.5

Beet, sugar, molasses

0.3

Biriba
Blueberry
Borage, seed

0.30
3.5
0.05

Caneberry, subgroup 13-A

2.5

Canistel

1.0

Canola, seed

0.05

Cattle, fat

0.3

Cattle, meat byproducts

0.3

Cattle, meat

0.3

Cherimoya

0.3

Citrus, dried pulp

5.0

Coffee, bean, green

0.80

Corn, field, forage

0.10

Corn, field, grain

0.05

Corn, field, stover

0.20

Corn, pop, grain

0.05

Corn, pop, stover

0.20

Corn, sweet, forage

0.10

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, stover

0.20

Cotton, gin byproducts

4.0

Cotton, undelinted seed

6.0

Cotton, meal

8.0

Crambe, seed

0.05

Cranberry

0.05

Currant

3.5

Custard apple

0.30

Egg

0.02

Elderberry

3.5

Feijoa

1.0

Flax, seed

0.05

Fruit, citrus, group 10

0.7

Fruit, pome, group 11

0.6

Fruit, stone, group 12

3.0

Goat, fat

0.3

Goat, meat byproducts

0.3

Goat, meat

0.3

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Gooseberry

3.5

Grape, juice

1.5

Grape, pomace (wet or dried)

5.0

Grape, raisin

1.5

Grape, raisin, waste

15.0

Grape

1.0

Guava

1.0

Herbs subgroup 19A, dried herbs

48.0

Herbs subgroup 19-A, fresh herbs

8.0

Hog, fat

0.3

Hog, meat byproducts

0.3

Hog, meat

0.3

Hop, dried cones

6.0

Horse, fat

0.3

Horse, meat byproducts

0.3

Horse, meat

0.3

Huckleberry

3.5

Ilama

0.30

Jaboticaba

1.0

Juneberry

3.5

Kava, leaves

4.0

Kava, roots

0.40

Leaf petioles subgroup 4B

6.0

Leafy greens subgroup 4A

3.5

Lettuce, head and leaf

3.5

Lingonberry

3.5

Longan

3.0

Lychee

3.0

Mango

1.0

Milk

0.1

Millet, pearl, forage

2.0

Millet, pearl, grain

0.05

Millet, pearl, hay

6.0

Millet, pearl, straw

3.0

Millet, proso, forage

2.0

Millet, proso, grain

0.05

Millet, proso, hay

6.0

Millet, proso, straw

3.0

Mustard, black, seed

0.05

Mustard, field, seed

0.05

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Mustard, Indian, seed

0.05

Mustard, rapeseed, seed

0.05

Mustard, seed

0.05

Nut, tree, group 14

0.05

Oat, forage

2.0

Oat, grain

0.05

Oat, hay

6.0

Oat, straw

3.0

Okra

1.0

Passionfruit

1.0

Papaya

1.0

Peanut

0.45

Peanut, hay

35

Peanut, meal

0.75

Pecan

0.05

Persimmon

3.0

Pistachio

0.05

Pomegranate

0.90

Potato, chip

0.4

Potato, processed potato waste

0.9

Poultry, fat

0.05

Poultry, meat byproducts

0.05

Poultry, meat

0.05

Pulasan

3.0

Rambutan

3.0

Rapeseed, seed

0.05

Raspberry, wild

2.5

Rye, forage

2.0

Rye, grain

0.05

Rye, hay

6.0

Rye, straw

3.0

Safflower, seed

0.05

Salal

3.5

Sapodilla

1.0

Sapote, black

1.0

Sapote, mamey

1.0

Sheep, fat

0.3

Sheep, meat byproducts

0.3

Sheep, meat

0.3

Sorghum, forage

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0.10

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Sorghum, grain, grain

0.05

Sorgum, grain, stover

0.10

Soursop

0.30

Soybean, forage

8.0

Soybean, hay

35

Soybean, meal

4.0

Soybean, seed

3.5

Spanish lime

3.0

Star apple

1.0

Starfruit

1.0

Strawberry

0.50

Sugar apple

0.30

Sunflower, seed

0.05

Tomato, paste

6.0

Tomato, pomace (wet or dried)

4.O

Tomato, puree

3.0

Vegetable, brassica leafy, group 5

3.5

Vegetable, cucurbit, group 9

0.5

Vegetable, fruiting, group 8

1.0

Vegetable, leaves of root and tuber, group 2

4.0

Vegetable, legume, group 6, except soybean

4.0

Vegetable, root and tuber, group 1, except sugar beet

0.40

Watercress

3.5

Watercress, upland

3.5

Wax jambu

1.0

Wheat, forage

7.0

Wheat, grain

0.05

Wheat, hay

0.5

Wheat, straw

0.5

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for indirect or inadvertent combined
residues of the insecticide imidacloprid (1-[(6-chloro-3-pyridinyl)methyl]- N -nitro-2-imidazolidinimine) and
its metabolites containing the 6-chloropyridinyl moiety, all expressed as 1-[(6-chloro-3-pyridinyl)methyl]- N nitro-2-imidazolidinimine, when present therein as a result of the application of the pesticide to growing
crops listed in this section and other non-food crops as follows:

Commodity
Corn, sweet, kernel plus cob with husks removed
Grain, cereal, forage, fodder and straw, group 16; forage

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Parts Per Million
0.05
2.0

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Grain, cereal, forage, fodder and straw, group 16; hay

6.0

Grain, cereal, forage, fodder and straw, group 16; stover

0.3

Grain, cereal, forage, fodder and straw, group 16; straw

3.0

Grain, cereal, group 15

0.05

Vegetable, foliage of legume, group 7

2.5

Vegetable, legume, group 6

0.3

[71 FR 46116, Aug. 11, 2006, as amended at 72 FR 33912, June 20, 2007]

§ 180.473 Glufosinate ammonium; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide glufosinate-ammonium (butanoic
acid, 2-amino-4-(hydroxymethylphosphinyl)-monoammonium salt) and its metabolites, 2-acetamido-4methylphosphinico-butanoic acid and 3-methylphosphinico-propionic acid, expressed as 2-amino-4(hydroxymethylphosphinyl)butanoic acid equivalents, in or on the following food commodities:

Commodity

Parts per million

Almond, hulls

0.50

Apple

0.05

Banana

0.30

Banana, pulp

0.20

Beet, sugar, molasses

5.0

Beet, sugar, roots

0.9

Beet, sugar, tops (leaves)

1.5

Bushberry subgroup 13B

0.15

Canola, meal

1.1

Canola, seed

0.40

Cattle, fat

0.40

Cattle, meat

0.15

Cattle, meat byproducts

6.0

Corn, field forage

4.0

Corn, field, grain

0.20

Corn, field, stover

6.0

Cotton, gin byproducts

15

Cotton, undelinted seed

4.0

Egg

0.15

Goat, fat

0.40

Goat, meat

0.15

Goat, meat byproducts
Grain aspirated fractions
Grape
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6.0
25
0.05

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Hog, fat

0.40

Hog, meat

0.15

Hog, meat byproducts

6.0

Horse, fat

0.40

Horse, meat

0.15

Horse, meat byproducts

6.0

Juneberry

0.10

Lingonberry

0.10

Milk

0.15

Nut, tree, group 14

0.10

Pistachio

0.10

Potato

0.80

Potato, chips

1.6

Potato granules/flakes

2.0

Poultry, fat

0.15

Poultry, meat

0.15

Poultry, meat byproducts

0.60

Rice, grain

1.0

Rice, hull

2.0

Rice, straw

2.0

Salal

0.10

Sheep, fat

0.40

Sheep, meat

0.15

Sheep, meat byproducts

6.0

Soybean

2.0

Soybean, hulls

5.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional restrictions. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the
herbicide glufosinate ammonium, butanoic acid, 2-amino-4-(hydroxymethylphosphinyl)-, monoammonium
salt and its metabolite, 3-methylphosphinicopropionic acid in or on the following raw agricultural
commodities when present therein as a result of the application of glufosinate ammonium to crops listed in
paragraph (a) of this section:

Commodity

Parts per million

Barley, hay

0.40

Barley, straw

0.40

Buckwheat, fodder

0.40

Buckwheat, forage

0.40

Oat, forage

0.40

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Oat, hay

0.40

Oat, straw

0.40

Rye, forage

0.40

Rye, straw

0.40

Teosinte

0.40

Triticale

0.40

Wheat, forage

0.40

Wheat, hay

0.40

Wheat, straw

0.40

[68 FR 55849, Sept. 29, 2003, as amended at 71 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, 2007]

§ 180.474 Tebuconazole; tolerances for residues.
top
(a) General . (1) Tolerances are established for the residues of the fungicide, tebuconazole, alpha-[2-(4Chlorophenyl)ethyl]-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol in or on the following
commodities:

Commodity

Parts per million

Almond, hulls

6.0

Apple, wet pomace

0.1

Asparagus

0.05

Banana

0.05

Barley, grain

0.15

Barley, hay

7.0

Barley, straw

3.5

Bean, dry seed

0.1

Bean, succulent

0.1

Beet, garden, roots

0.70

Beet, garden, tops

7.0

Brassica, leafy greens, subgroup 5B

2.5

Cherry, sweet, pre- and post-harvest

5.0

Cherry, tart, pre- and post-harvest

5.0

Coffee, green bean1

0.15

Coffee, roasted bean1

0.3

Corn, field, forage

4.0

Corn, field, grain

0.05

Corn, field, stover

3.5

Corn, pop, grain

0.05

Corn, pop, stover

3.5

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Corn, sweet, forage

7.0

Corn, sweet, kernel plus cob with husks removed

0.5

Corn, sweet, stover

6.0

Cotton, gin byproducts

25.0

Cotton, undelinted seed

2.0

Fruit, pome, group 11
Fruit, stone, group 12, except cherry
Grain, aspirated fractions

0.05
1.0
16.0

Grape

5.0

Grass, forage

8.0

Grass, hay

25.0

Grass, seed screenings

55.0

Grass, straw

30.0

Hop, dried cones

35.0

Lychee

1.6

Mango, postharvest

0.15

Nut, tree, group 14

0.05

Oat, forage

0.10

Oat, grain

0.05

Oat, hay

0.10

Oat, straw

0.10

Okra

1.2

Onion, bulb, subgroup 3-07A

0.2

Onion, green, subgroup 3-07B

1.3

Peach

1.0

Peanut

0.1

Pistachio
Plum, pre- and post-harvest

0.05
1.0

Soybean, forage

25

Soybean, hay

50

Soybean, seed

0.08

Sunflower, seed

0.05

Sunflower, meal

0.2

Sunflower, refined oil

0.2

Vegetable, cucurbit, group 9

0.09

Wheat, forage

3.0

Wheat, grain

0.05

Wheat, hay

7.0

Wheat, straw

1.5

1There

are no U.S. registrations as of 7/31/2008.

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(2) Tolerances are established for the combined residues of the fungicide, tebuconazole and its 1-(4chlorophenyl)-4,4-dimethyl-3-(1 H -1,2,4-triazole-1-yl-methyl)-pentane-3,5-diol metabolite.

Commodity

Parts per million

Cattle, meat byproducts

0.2

Goat, meat byproducts

0.2

Horse, meat byproducts

0.2

Milk

0.1

Sheep, meat byproducts

0.2

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations for the residues of the
fungicide, tebuconazole, alpha-[2-(4-Chlorophenyl)ethyl]-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1ethanol in or on the following commodities:

Commodity

Parts per million

Turnip, roots

0.5

Turnip, tops

7.0

(d) Indirect or inadvertent residues. [Reserved]
[59 FR 39464, Aug. 3, 1994]
Editorial Note: ForFederal Registercitations affecting §180.474, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.475 Difenoconazole; tolerances for residues.
top
(a) General . (1) Tolerances are established for residues of the fungicide difenoconazole, 1-[2-[2-chloro-4(4-chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]-1 H -1,2,4-triazole, in or on the following
commodities:

Commodity

Parts per million

Apple, wet pomace

4.5

Banana1

0.2

Barley, grain

0.1

Barley, hay

0.05

Barley, straw

0.05

Beet, sugar

0.01

Beet, sugar, dried pulp

1.9

Canola, seed

0.01

Corn, sweet, forage

0.01

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Corn, sweet, kernel plus cob with husks removed

0.01

Corn, sweet, stover

0.01

Cotton, gin byproducts

0.05

Cotton, undelinted seed

0.05

Fruit, pome group 11

1.0

Grape1

0.10

Papaya1

0.30

Potato, processed waste

0.04
0.1

Rye, grain1
Vegetable, fruiting, group 8

0.60

Vegetable, tuberous and corm, subgroup 1C

0.01

1There

are no U.S. registrations.

(2) Tolerances are established for residues of the fungicide difenoconazole, 1-[2-[2-chloro-4-(4chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]-1 H -1,2,4-triazole, and its metabolite, CGA205375, 1-[2-chloro-4-(4-chloro-phenoxy)phenyl]-2-[1,2,4]triazol-1-yl-ethanol, in or on the following
commodities:

Commodity

Parts per million

Cattle, fat

0.10

Cattle, liver

0.20

Cattle, meat

0.05

Cattle, meat byproduct (except liver)

0.10

Eggs

0.10

Goat, fat

0.10

Goat, liver

0.20

Goat, meat

0.05

Goat, meat byproduct (except liver)

0.10

Hog, fat

0.10

Hog, liver

0.20

Hog, meat

0.05

Hog, meat byproduct (except liver)

0.10

Horse, fat

0.10

Horse, liver

0.20

Horse, meat

0.05

Horse, meat byproduct (except liver)

0.10

Milk

0.01

Sheep, fat

0.10

Sheep, liver

0.20

Sheep, meat

0.05

Sheep, meat byproduct (except liver)

0.10

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(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are
established for residues of the fungicide difenoconazole in or on the specified agricultural commodities,
resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances
expire and are revoked on the date specified in the table.

Commodity

Parts per million

Almond

Expiration/revocation date

0.05

12/31/11

Almond, hulls

5.0

12/31/11

Cantaloupe

1.0

12/31/11

Cucumber

1.0

12/31/11

Watermelon

1.0

12/31/11

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 36254, July 6, 1999, as amended at 64 FR 47687, Sept. 1, 1999; 65 FR 55921, Sept. 15, 2000; 65
FR 82940, Dec. 29, 2000; 66 FR 64774, Dec. 14, 2001; 68 FR 37765, June 25, 2003; 70 FR 75739, Dec.
21, 2005; 71 FR 53984, Sept. 13, 2006; 73 FR 1508, Jan. 9, 2008; 73 FR 45629, Aug. 6, 2008]

§ 180.476 Triflumizole; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the fungicide triflumizole, including its
metabolites and degradates, in or on the commodities listed in the table below. Compliance with the
tolerance levels specified below is to be determined by measuring only the parent compound triflumizole,
1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2-propoxyethyl )-1 H -imidazole, and its metabolites
containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as stoichiometric equivalent of the
parent compound.

Commodity

Parts per million

Apple, pomace

2.0

Apple

0.5

Brassica, head and stem, subgroup 5A

8.0

Brassica, leafy greens, subgroup 5B

40

Canistel

2.5

Cherry, sweet

1.5

Cherry, tart

1.5

Cilantro, leaves
Grape

35
2.5

Grape pomace

15.0

Grape, raisin, waste

10.0

Hazelnut

0.05

Hop, dried cones

50

Leafy greens subgroup 4A, except spinach

35

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Mango

2.5

Papaya

2.5

Pear

0.5

Pineapple

4.0

Sapodilla

2.5

Sapote, black

2.5

Sapote, mamey

2.5

Star apple

2.5

Strawberry

2.0

Swiss chard

18

Turnip, greens

40

Vegetable, cucurbit, Group 9

0.5

(2) Tolerances are established for residues of the fungicide triflumizole, including its metabolites and
degradates, in or on the commodities of animal origin listed in the table below. Compliance with the
tolerance levels specified below is to be determined by measuring only the parent compound triflumizole,
1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2-propoxyethyl )-1 H -imidazole, the metabolite 4-chloro-2hydroxy-6-trifluoromethylaniline sulfate, and other metabolites containing the 4-chloro-2trifluoromethylaniline moiety, calculated as the parent compound.

Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat

0.5
0.05
0.5
0.05
0.5
0.05

Goat, meat byproducts

0.5

Hog, fat

0.5

Hog, meat

0.05

Hog, meat byproducts

0.5

Horse, fat

0.5

Horse, meat
Horse, meat byproducts

0.05
0.5

Milk

0.05

Poultry, fat

0.05

Poultry, meat

0.05

Poultry, meat byproducts

0.1

Sheep, fat

0.5

Sheep, meat
Sheep, meat byproducts
(b) Section 18 emergency exemptions . Time limited tolerances are established for the residues
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0.05
0.5

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triflumizole (1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2-propoxyethyl)-1H-imidazole) and its
metabolites containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as the parent in connection
with use of the pesticide under section 18 emergency exemptions granted by EPA. The tolerances are
specified in the following table, and will expire and are revoked on the dates specified.

Commodity

Parts per million

Expiration/revocation date

Cabbage, chinese, napa

20

12/31/09

Kohlrabi

20

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33702, May 24, 2000, as amended at 67 FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, 2002;
70 FR 7047, Feb. 10, 2005; 70 FR 17915, Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR 49358, Aug.
23, 2006; 74 FR 26543, June 3, 2009]

§ 180.477 Flumiclorac pentyl; tolerances for residues.
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(a) General . Tolerances are established for residues of the herbicide flumiclorac pentyl, [2-chloro-4-fluoro5-(1,3,4,5,6,7-hexahydro-1,3-dioxo-2H-isoindol-2-yl)phenoxy]-acetate, in or on the raw agricultural
commodities listed below.

Commodity

Parts per million

Corn, field, forage

0.01

Corn, field, grain

0.01

Corn, field, stover

0.01

Cotton, gin byproducts

3.0

Cotton, undelinted seed

0.2

Soybean, hulls

0.02

Soybean, seed

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33702, May 24, 2000, as amended at 71 FR 11533, Mar. 8, 2006]

§ 180.478 Rimsulfuron; tolerances for residues
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(a) General. Tolerances are established for residues of the herbicide rimsulfuron ( N -((4,6dimethoxypyrimidin-2-yl)aminocarbonyl)-3-(ethylsulfonyl)-2-pyridinesulfonamide in or on the following raw
agricultural commodities:

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Commodity

Parts per million

Almond, hulls

0.09

Corn, field, forage

0.1

Corn, field, grain

0.1

Corn, field, stover

0.1

Fruit, citrus, group 10

0.01

Fruit, pome, group 11

0.01

Fruit, stone, group 12

0.01

Grape

0.01

Nut, tree, group 14

0.01

Pistachio

0.01

Potato

0.1

Tomato

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 16696, Apr. 6, 1998, as amended at 72 FR 41913, Aug. 1, 2007]

§ 180.479 Halosulfuron-methyl; tolerances for residues.
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(a) General . (1) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl 5[(4,6-dimethoxy-2-pyrimidiny)amino] carbonylaminosulfonyl-3-chloro-1-methyl-1 H -pyrazole-4-caboxylate,
and its metabolites determined as 3-chloro-1-methyl-5-sulfamoylpyrazole-4-carboxylic acid, expressed as
halosulfuron-methyl equivalent in or on the raw agricultural commodities listed in the table in this unit.

Commodity

Parts per million

Cattle, meat byproducts

0.1

Goat, meat byproducts

0.1

Hog, meat byproducts

0.1

Horse, meat byproducts

0.1

Sheep, meat byproducts

0.1

(2) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy2-pyrimidinyl) amino]carbonylaminosulfonyl-3-chloro-1-methyl-1 H -pyrazole- 4-carboxylate, in or on the
raw agricultural commodities listed below.

Commodity

Parts per million

Alfalfa, forage

1.0

Alfalfa, hay

2.0

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Almond, hulls

0.2

Asparagus

0.8

Bean, dry, seed

0.05

Bean, snap, succulent

0.05

Corn, field, forage

0.2

Corn, field, grain

0.05

Corn, field, stover

0.8

Corn, pop, grain

0.05

Corn, pop, stover

0.8

Corn, sweet, forage

0.2

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, stover

0.8

Cotton, gin byproducts

0.05

Cotton, undelinted seed

0.05

Melon subgroup 9A

0.1

Nut, tree, group 14

0.05

Pistachio

0.05

Rice, grain

0.05

Rice, straw

0.2

Sorghum, grain, forage

0.05

Sorghum, grain, grain

0.05

Sorghum, grain, stover

0.1

Squash/Cucumber subgroup 9B

0.5

Sugarcane, cane

0.05

Vegetable, fruiting, group 8

0.05

(b) Section 18 emergency exemptions . Time-limited tolerances are established for residues of
halosulfuron methyl, methyl 5-[(4,6-dimethoxy-2-pyrimidinyl)amino] carbonylaminosulfonyl-3-chloro-1methyl-1 H -pyrazole-4-carboxylate, in connection with use of the pesticide under FIFRA section 18
emergency exemptions granted by EPA in or on the following commodity:

Commodity

Parts per million

Sweet potato

Expiration/revocation date
1.0

12/31/08

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 25448, May 12, 1999, as amended at 65 FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, 2001;
66 FR 66786, Dec. 27, 2001; 67 FR 45649, July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR 51622,
Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007]

§ 180.480 Fenbuconazole; tolerances for residues.

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(a) General . Tolerances are established for combined residues of the fungicide fenbuconazole, alpha–[2–
(4–chlorophenyl)– ethyl]–alpha–phenyl–3–(1H–1,2,4–triazole)– 1–propanenitrile, and its metabolites RH–
9129, cis–5–(4–chlorophenyl)– dihydro–3–phenyl–3–(1H–1,2,4– triazole–1–ylmethyl)–2–3 H–furanone,
and RH–9130, trans–5–(4– chlorophenyl)dihydro–3–phenyl–3– (1H–1,2,4–triazole–1–ylmethyl)–2–3 H–
furanone, expressed as fenbuconazole in or on the following agricultural commodities.

Commodity

Parts per million

Almond

0.05

Almond, hulls

1.0

Apple

0.4

Apple, wet pomace

1.0

Banana

0.3

Beet, sugar, dried pulp

1.0

Beet, sugar, molasses

0.4

Beet, sugar, roots

0.3

Beet, sugar, tops

9.0

Bushberry subgroup 13B

0.3

Cattle, meat byproducts

0.05

Citrus, dried pulp

5.0

Citrus, oil

40.0

Cranberry

0.5

Fruit, citrus, group 10

1.0

Fruit, stone, group 12

1.0

Goat, meat byproducts

0.05

Grain, aspirated fractions

6.0

Grape1

1.0

Horse, meat byproducts

0.05

Peanut

0.1

Pecan

0.05

Pepper

0.40

Sheep, meat byproducts

0.05

Wheat, forage

4.0

Wheat, grain

0.1

Wheat, hay

8.0

Wheat, straw

8.0

1There

are no United States registrations for grape as of August 2006.

(b) Section 18 emergency exemptions . Time-limited tolerances are established for fenbuconazole (alpha[2-4-chlorophenyl)-ethyl]alpha-phenyl-3-(1 H -1,2,4-triazole)-1-propanenitrile] and its metabolites, cis-5-(4chlorophenyl)-dihydro-3-phenyl-3-(1 H -1,2,4-triazole-1-ylmethyl)-2-3 H -furanone and trans-5-(4chlorophenyl)dihydro-3-phenyl-3-(1 H 1,2,4-triazole-1-ylmethyl-2-3 H -furanone, expressed as

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fenbuconazole in or on the following raw agricultural commodities in connection with use of the pesticide
under a section 18 exemption granted by EPA. The time-limited tolerances will expire on the date
specified in the following table.

Commodity

Parts per million

Expiration/revocation date

Cattle, fat

0.01

12/31/08

Cattle, meat

0.01

12/31/08

Goat, fat

0.01

12/31/08

Goat, meat

0.01

12/31/08

Hog, fat

0.01

12/31/08

Hog, meat

0.01

12/31/08

Hog, meat byproducts

0.01

12/31/08

Horse, fat

0.01

12/31/08

Horse, meat

0.01

12/31/08

Sheep, fat

0.01

12/31/08

Sheep, meat

0.01

12/31/08

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[60 FR 11032, Mar. 1, 1995]
Editorial Note: ForFederal Registercitations affecting §180.480, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.481 Prosulfuron; tolerances for residues.
top
Tolerances that expire as indicated in the table below are established for residues of the herbicide
prosulfuron 1-(4-methoxy-6-methyl-triazin-2-yl)-3-[2-(3,3,3-trifluoropropyl)-phenylsulfonyl]-urea in or on the
following raw agricultural commodities:

Commodity

Parts per million Expiration date

Cattle, fat

0.05

12/31/99

Cattle, kidney

0.05

Do.

Cattle, liver

0.05

Do.

Cattle, meat

0.05

Do.

Cattle, meat byproducts

0.05

Do.

Corn, forage

0.01

Do.

Corn, grain and fresh (including sweet kernels plus
cobs with husks removed)

0.01

Do.

Corn, stover

0.01

Do.

Goat, fat

0.05

Do.

Goat, kidney

0.05

Do.

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Goat, liver

0.05

Do.

Goat, meat

0.05

Do.

Goat, meat byproducts

0.05

Do.

Grain, cereal, forage, fodder and straw, group 16,
except rice and wild rice; forage

0.10

Do.

Grain, cereal, forage, fodder and straw, group 16,
except rice and wild rice; hay

0.20

Do.

Grain, cereal, forage, fodder and straw, group 16,
except rice and wild rice; stover

0.01

Do.

Grain, cereal, forage, fodder and straw, group 16,
except rice and wild rice; straw

0.02

Do.

Grain, cereal, group 15, except rice and wild rice

0.01

Do.

Hog, fat

0.05

Do.

Hog, kidney

0.05

Do.

Hog, liver

0.05

Do.

Hog, meat

0.05

Do.

Hog, meat byproducts

0.05

Do.

Horse, fat

0.05

Do.

Horse, kidney

0.05

Do.

Horse, liver

0.05

Do.

Horse, meat

0.05

Do.

Horse, meat byproducts

0.05

Do.

Milk

0.01

Do.

Sheep, fat

0.05

Do.

Sheep, kidney

0.05

Do.

Sheep, liver

0.05

Do.

Sheep, meat

0.05

Do.

Sheep, meat byproducts

0.05

Do.

[61 FR 26842, May 29, 1996, as amended at 61 FR 26844, May 29, 1996]

§ 180.482 Tebufenozide; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the insecticide tebufenozide, benzoic acid, 3,5dimethyl-1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, in or on the following raw agricultural
commodities:

Commodity

Parts per million

Almond, hulls

25

Apple, pomace

3.0

Apple

1.0

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Berry group 13

3.0

Brassica, head and stem, subgroup 5A

5.0

Brassica, leafy greens, subgroup 5B

10.0

Canola, refined oil

4.0

Canola, seed

2.0

Citrus, oil

15.0

Cotton

1.5

Cotton, gin byproducts

30

Cranberry

1.0

Fruit, citrus, group 10

0.80

Fruit, pome

1.5

Grape

3.0

Kiwifruit1

0.5

Leaf petioles subgroup 4B

2.0

Leafy greens subgroup 4A

10.0

Peppermint, tops

10.0

Spearmint, tops

10.0

Tree nut crop group including pistachio

0.1

Turnip, greens

9.0

Turnip, roots

0.3

Vegetable, fruiting, group 8

1.0

Vegetable, tuberous and corm, except potato, subgroup 1D

0.015

Walnut
1There

0.1

are no U.S. registrations on kiwifruit as of June 15, 1999.

(2) Tolerances are established for the combined residues of tebufenozide and its metabolites benzoic
acid, 3,5-dimethyl-1-(1,1-dimethylethyl)-2-((4-carboxymethyl)benzoyl)hydrazide), benzoic acid, 3hydroxymethyl,5-methyl-1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, the stearic acid conjugate of
benzoic acid, 3-hydroxymethyl,5-methyl-1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide and benzoic
acid, 3-hydroxymethyl-5-methyl-1-(1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide.

Commodity

Parts per million

Fat of cattle, goat, hog, horse, and sheep

0.1

Meat of cattle, goat, hog, horse and sheep

0.08

Meat byproducts of cattle, goat, hog, horse and sheep

0.08

Milk

0.04

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the
insecticide benzoic acid in connection with use of the pesticide under section 18 emergency exemptions
granted by EPA. The tolerances will expire and are revoked on the dates specified in the following table.

Commodity
Beet, garden, roots

Parts per million

Expiration/revocation date

0.3

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Beet, garden, tops

9.0

12/31/05

Grape

3.0

12/31/05

0.25

12/31/05

Sweet potato, roots
(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues . Tolerances are established for the indirect or inadvertent combined
residues of tebufenozide, benzoic acid, 3,5-dimethyl-1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide and
its metabolite benzoic acid, 3,5-dimethyl-1-(1,1dimethylethyl)-2-[4-(1-hydroxyethyl)benzoyl]hydrazide in or
on the raw agricultural commodities when present therein as a result of the application of tebufenozide to
growing crops listed in paragraph (a) of this section to read as follows:

Commodity

Parts per million

Animal feed, nongrass, group 18

1.0

Grain, cereal, forage, fodder and straw, group 16

1.0

Grass, forage, fodder and hay, group 17

1.0

Vegetable, foliage of legume, group 7

0.20

[60 FR 29347, May 31, 1995]
Editorial Note: ForFederal Registercitations affecting §180.482, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.483 O
-[2-(1,1-Dimethylethyl)-5-pyrimidinyl] O
methylethyl) phosphorothioate; tolerances for residues.

-ethyl- O

-(1-

top
Time-limited tolerances are established for residues of the insecticide O -[2-(1,1-dimethylethyl)-5pyrimidinyl] O -ethyl- O -(1-methylethyl) phosphorothioate in or on the following raw agricultural
commodities:

Commodity

Parts per million Expiration date

Corn, forage and fodder, field, pop, and sweet

0.01

7/6/99

Corn, grain, field and pop

0.01

Do.

Corn, sweet, kernel plus cob with husks removed

0.01

Do.

[60 FR 34873, July 5, 1995]

§ 180.484 Flutolanil ( N
-(3-(1-methylethoxy)phenyl)-2-(trifluoromethyl)
benzamide); tolerances for residues.
top
(a) General. Tolerances are established for residues of flutolanil, N -(3-(1-methylethoxy)phenyl)-2(trifluoromethyl)benzamide, and its metabolites converted to 2-(trifluoromethyl) benzoic acid and
calculated as flutolanil in or on the following raw agricultural commodities:

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Commodity

Parts per million

Cattle, fat

0.10

Cattle, kidney

1.00

Cattle, liver

2.00

Cattle, meat byproducts

0.05

Cattle, meat

0.05

Egg

0.05

Goat, fat

0.10

Goat, kidney

1.00

Goat, liver

2.00

Goat, meat byproducts

0.05

Goat, meat

0.05

Hog, fat

0.10

Hog, kidney

1.00

Hog, liver

2.00

Hog, meat byproducts

0.05

Hog, meat

0.05

Horse, fat

0.10

Horse, kidney

1.00

Horse, liver

2.00

Horse, meat byproducts

0.05

Horse, meat

0.05

Milk

0.05

Peanut

0.5

Peanut, hay

15.0

Peanut, meal

1.0

Potato

0.20

Potato, wet peel

0.30

Poultry, fat

0.05

Poultry, meat

0.05

Poultry, meat byproducts

0.05

Rice, bran

10.0

Rice, grain

7.0

Rice, hulls

25.0

Rice, straw

10.0

Sheep, fat

0.10

Sheep, kidney

1.00

Sheep, liver

2.00

Sheep, meat

0.05

Sheep, meat byproducts

0.05

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for the indirect or inadvertent residues of
the fungicide flutolanil, N -(3-(1-methylethoxy)phenyl)-2-(trifluoromethyl)benzamide, and its metabolites
converted to 2-(trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the following commodities:

Commodity

Parts per million

Soybean, forage

8.0

Soybean, hay

2.5

Soybean, seed

0.20

Wheat, bran

0.20

Wheat, forage

2.5

Wheat, grain

0.05

Wheat, hay

1.2

Wheat, straw

0.20

[60 FR 42458, Aug. 16, 1995, as amended at 61 FR 33044, June 26, 1996; 63 FR 42256, 42257, Aug. 7,
1998; 66 FR 10825, Feb. 20, 2001; 71 FR 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; 73 FR
33017, June 11, 2008]

§ 180.485 Cyproconazole; tolerances for residues.
top
(a) General . (1) Tolerances are established for the free and conjugated residues of the fungicide
cyproconazole, α-(4-chlorophenyl)-α-(1-cyclopropylethyl)-1 H -1,2,4-triazole-1-ethanol, in or on the
following food commodities:

Commodity
Aspirated grain fractions

Parts per million
2.5

Cattle, fat

0.01

Cattle, meat byproducts (except liver)

0.01

Coffee bean, green (Imported)1

0.1

Corn, field, forage

0.60

Corn, field, grain

0.01

Corn, field, stover

1.2

Goat, fat

0.01

Goat, meat byproducts (except liver)

0.01

Horse, fat

0.01

Horse, meat byproducts (except liver)

0.01

Sheep, fat

0.01

Sheep, meat byproducts (except liver)

0.01

Soybean, forage

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Soybean, hay

3.0

Soybean, oil

0.10

Soybean, seed

0.05

Wheat, forage

0.80

Wheat, grain

0.05

Wheat, grain, milled byproducts

0.10

Wheat, hay

1.3

Wheat, straw
1There

0.90

are no U.S. registrations as of February 15, 2008 for use on coffee bean.

(2) A tolerance is established for the combined free and conjugated residues of cyproconazole α-(4chlorophenyl)-α-(1-cyclopropylethyl)-1 H -1,2,4-triazole-1-ethanol] and its metabolite [δ-(4-chlorophenyl)-β,
δ-dihydroxy-γ-methyl-1 H -1,2,4-triazole-1-hexenoic acid in or on the following commodity:

Commodity

Parts per million

Milk

0.02

(3) Tolerances are established for the combined free and conjugated residues of cyproconazole α-(4chlorophenyl)-α-(1-cyclopropylethyl)-1 H -1,2,4-triazole-1-ethanol and its metabolite 2-(4-chlorophenyl)-3cyclopropyl-1-[1,2,4]triazol-1-yl-butane-2,3-diol in or on the following commodities:

Commodity

Parts per million

Cattle, liver

0.50

Goat, liver

0.50

Hog, liver

0.01

Horse, liver

0.50

Sheep, liver

0.50

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 53835, Oct. 7, 1998, as amended at 71 FR 71058, Dec. 8, 2006; 73 FR 27760, May 14, 2008]

§ 180.486 Phosphorothioic acid, 0,0
tetrachloroethyl) ester; tolerances for residues.

-diethyl 0

-(1,2,2,2-

top
Tolerances are established permitting the residue of the insecticide phosphorothioic acid, 0,0 -diethyl 0 (1,2,2,2-tetrachloroethyl) ester in or on the following raw agricultural commodities:

Commodity

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Parts per million

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Corn, field, forage

0.01

Corn, field, grain

0.01

Corn, field, stover

0.01

Corn, pop, grain

0.01

Corn, pop, stover

0.01

Corn, sweet, forage

0.01

Corn, sweet, kernel plus cob with husks removed

0.01

Corn, sweet, stover

0.01

[60 FR 49792, Sept. 27, 1995]

§ 180.487 Pyrithiobac sodium; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide, pyrithiobac sodium, (sodium 2chloro-6-[(4,6-dimethoxypyrimidin-2-yl)thio]benzoate), resulting from the application of the pesticide
chemical in or on the following foods/feeds:

Commodity

Parts per million

Cotton, gin byproducts

0.15

Cotton, undelinted seed

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 54783, Oct. 22, 1997, as amended at 64 FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, 2002]

§ 180.490 Imazapic-ammonium; tolerances for residues.
top
(a) General. (1) Tolerances are established for combined residues of the herbicide imazapic, (±)-2-[4,5dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1 H -imidazol-2-yl]-5-methyl-3-pyridinecarboxylic acid and its
metabolite (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1 H -imidazol-2-yl]-5-hydroxymethyl-3pyridinecarboxylic acid, both free and conjugated, in or on the following food commodities:

Commodity

Parts per million

Grass, forage

15

Grass, hay

30

Peanut

0.1

(2) Tolerances are also established for the combined residues of the herbicide imazapic, (±)-2-[4,5-dihydro4-methyl-4-(1-methylethyl)-5-oxo-1 H -imidazol-2-yl]-5-methyl-3-pyridinecarboxylic acid and its free

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metabolite (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1 H -imidazol-2-yl]-5-hydroxymethyl-3pyridinecarboxylic acid, in or on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.10

Cattle, kidney

1.0

Cattle, meat byproducts, except kidney

0.1

Cattle, meat

0.1

Goat, fat

0.1

Goat, kidney

1.0

Goat, meat byproducts, except kidney

0.1

Goat, meat

0.1

Horse, fat

0.1

Horse, kidney

1.0

Horse, meat byproducts, except kidney

0.1

Horse, meat

0.1

Milk

0.1

Sheep, fat

0.1

Sheep, kidney

1.0

Sheep, meat byproducts, except kidney

0.1

Sheep, meat

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with reginal registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 54224, Oct. 6, 1999, as amended at 66 FR 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001]

§ 180.491 Propylene oxide; tolerances for residues.
top
(a) General . (1) Tolerances are established for residues of propylene oxide when used as a postharvest
fumigant in or on the following food commodities:

Commodity

Parts per million

Cacao bean, dried bean

200

Cacao bean, cocoa powder

200

Fig

3.0

Garlic, dried

300

Grape, raisin

1.0

Herbs and spices, group 19, dried

300

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Nut, tree, group 14

300

Onion, dried

300

Plum, prune, dried

2.0

(2) Tolerances are established for the reaction product, propylene chlorohydrin, from use of propylene
oxide as a postharverst fumigant, in or on the following food commodities:

Commodity

Parts per million

Basil, dried leaves

6000

Cacao bean, dried bean

20.0

Cacao bean, cocoa powder

20.0

Fig

3.0

Garlic, dried

6000

Grape, raisin

4.0

Herbs and spices, group 19, dried, except basil

1500

Nut, tree, group 14

10.0

Onion, dried

6000

Plum, prune, dried

2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33702, May 24, 2000, as amended at 68 FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, 2007; 73
FR 54963, Sept. 24, 2008]

§ 180.492 Triflusulfuron methyl; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide, triflusulfuron methyl 2-[[[[[4(dimethylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino]carbonyl]amino]sulfonyl]-3methylbenzoate in or on the raw agricultural commodities:

Commodity

Parts per million

Beet, sugar, roots

0.05

Beet, sugar, tops

0.05

Chicory, roots

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[67 FR 40196, June 12, 2002]

§ 180.493 Dimethomorph; tolerances for residues.
top
(a) General . Tolerances are established for the residues of the fungicide dimethomorph, ( E,Z ) 4-[3-(4chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propenyl]morpholine, in or on the following commodities:

Commodity

Parts per million

Brassica, head and stem, subgroup 5A

2.0

Brassica, leafy greens, subgroup 5B

20.0

Ginseng

0.90
6.0

Grape, raisin1
Hop, dried cones

60

Lettuce, head

10

Lettuce, leaf

10

Potato

0.05

Potato, wet peel

0.20

Taro, corm

0.5

Taro, leaves

6.0

Turnip, greens

20.0

Vegetable, bulb, group 3

2.0

Vegetable, cucurbit, group 9

0.5

Vegetable, fruiting, group 8

1.5

1There

are no U.S. registrations as of March 4, 2009, for the use of dimethomorph on grapes grown for
raisin production.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances with regional registrations are established for
residues of the fungicide dimethomorph, ( E,Z ) 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2propenyl]morpholine, in or on the following commodities:

Commodity

Parts per million

Bean, lima, succulent

0.60

Grape

3.5

(d) Indirect or inadvertent residues. Time-limited tolerances are established for inadvertent or indirect
residues of the fungicide dimethomorph in or on the following raw agricultural commodities when present
therein as a result of the application of dimethomorph to growing crops. The tolerances will expire and are
revoked on the dates specified in the following table.

Commodity

Parts per million Expiration/revocation date

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Grain, cereal, forage, fodder and
straw, group 16, forage

0.05

5/12/04

Grain, cereal, forage, fodder and
straw, group 16, hay

0.10

5/12/04

Grain, cereal, forage, fodder and
straw, group 16, stover

0.15

5/12/04

Grain, cereal, forage, fodder and
straw, group 16, straw

0.15

5/12/04

Grain, cereal, group 15

0.05

5/12/04

[62 FR 26416, May 14, 1997, as amended at 62 FR 39961, July 25, 1997; 63 FR 8139, Feb. 18, 1998; 63
FR 32140, June 12, 1998; 64 FR 18369, Apr. 14, 1999; 64 FR 25455, May 12, 1999; 65 FR 58390, Sept.
29, 2000; 66 FR 37598, July 19, 2001; 67 FR 35049, May 17, 2002; 67 FR 60923, Sept. 27, 2002; 68 FR
55833, Sept. 29, 2003; 70 FR 7047, Feb. 10, 2005; 71 FR 76177, Dec. 20, 2006; 74 FR 9356, Mar. 4,
2009]

§ 180.494 Pyridaben; tolerance for residues.
top
(a) General. Tolerances are established for residues of the insecticide pyridaben [2-tert-butyl-5-(4-tertbutylbenzylthio)-4-chloropyridazin-3(2H)-one] on the following plants, and of the insecticide pyridaben and
its metabolites (2-tert-butyl-5-(4-(1-carboxy-1-methylethyl)benzylthio)-4-chloropyridazin-3(2H)-one] and (2tert-butyl-5-[4(-1,1-dimethyl-2-hypdroxyethyl)benzylthio-4-chloropyridazinn-3(2H)-one) on animals, as
indicated in the following table.

Commodity

Parts per million

Revocation/expiration date

Almond, hulls

4.0

None

Apple

0.5

None

Apple, wet pomace

0.75

None

Canistel

0.10

None

Cattle, fat

0.05

None

Cattle, meat

0.05

None

Cattle, meat byproducts

0.05

None

Citrus

0.5

None

Citrus, dried pulp

1.5

None

10.0

None

Fruit, stone, group 12

2.5

None

Goat, fat

0.0

None

Goat, meat

0.05

None

Goat, meat byproducts

0.05

None

1.5

None

Hog, fat

0.05

None

Hog, meat

0.05

None

Hog, meat byproducts

0.05

None

Citrus, oil

Grape

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Hop, dried cones

10.0

None

Horse, fat

0.05

None

Horse, meat

0.05

None

Horse, meat byproducts

0.05

None

Mango

0.10

None

Milk

0.01

None

Nut, tree, group 14

0.05

None

Papaya

0.10

None

Pear

0.75

None

Pistachio

0.05

None

Sapodilla

0.10

None

Sapote, black

0.10

None

Sapote, mamey

0.10

None

Sheep, fat

0.05

None

Sheep, meat

0.05

None

Sheep, meat byproduct

0.05

None

Star apple

0.10

None

Strawberry

2.5

None

0.15

None

Tomato
(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(n)
are established for residues of the insecticide pyridaben [2-tert-butyl-5(4-tert-butylbenzylthio)-4chloropyridazin-3(2H)-one] in or on the following raw agricultural commodity:

Commodity

Parts per million

Cranberry

Expiration Date
0.5

None

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 43712, July 14, 2000, as amended at 66 FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, 2005]

§ 180.495 Spinosad; tolerances for residues.
top
(a) General . Tolerances are established for residues of the insecticide spinosad in or on the food
commodities in the table to this paragraph. Spinosad is a fermentation product of Saccharopolyspora
spinosa . The product consists of two related active ingredients: Spinosyn A (Factor A: CAS # 131929–60–
7) or 2-[(6-deoxy-2,3,4-tri- O -methyl-α- L -manno-pyranosyl)oxy]-13-[[5-(dimethylamino)-tetrahydro-6methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b-tetradecahydro-14-methyl-1Has-Indaceno[3,2-d]oxacyclododecin-7,15-dione; and Spinosyn D (Factor D; CAS # 131929–63–0) or 2-[(6deoxy-2,3,4-tri- O -methyl-α- L -manno-pyranosyl)oxy]-13-[[5-(dimethyl-amino)-tetrahydro-6-methyl-2Hpyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b-tetradecahydro-4,14-methyl-1H-asIndaceno[3,2-d]oxacyclododecin-7,15-dione.

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Commodity
Acerola
Alfalfa, seed

Parts per million
1.5
0.15

Alfalfa, seed screenings

2.0

Almond, hulls

2.0

Amaranth, grain, grain

1.0

Amaranth, grain, stover

10

Animal feed, nongrass, group, 18

0.02

Animal feed, nongrass, group, 18, forage

35.0

Animal feed, nongrass, group, 18, hay

30.0

Apple pomace

0.5

Artichoke, globe

0.3

Asparagus

0.2

Atemoya

0.3

Avocado

0.3

Banana

0.25

Beet, sugar, molasses

0.75

Biriba

0.3

Brassica, head and stem, subgroup 5A

2.0

Brassica, leafy greens, subgroup 5B

10.0

Bushberry subgroup 13B

0.250

Caneberry subgroup 13A

0.7

Canistel

0.3

Cattle, fat

50

Cattle, liver

10

Cattle, meat

2.0

Cattle, meat byproducts, except liver

5.0

Cherimoya

0.3

Citrus, oil

3.0

Citrus, dried pulp

0.5

Coriander, leaves

8.0

Corn, sweet, kernel plus cob with husks removed

0.02

Cotton, gin byproducts

1.5

Cotton, undelinted seed

0.02

Cranberry

0.01

Custard apple
Egg
Feijoa

0.3
0.30
.05

Fig

0.10

Fish

4.0

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Fish-shellfish, crustacean

4.0

Fish-shellfish, mollusc

4.0

Food commodities

0.02

Fruit, citrus, group 10

0.3

Fruit, pome, group 11

0.20

Fruit, stone, group 12

0.20

Goat, fat

50

Goat, liver

10

Goat, meat

2.0

Goat, meat byproducts, except liver

5.0

Grain, aspirated fractions

200

Grain, cereal, group 15

1.5

Grain, cereal, group 16, forage, except rice

2.5

Grain, cereal, group 16, hay, except rice

10.0

Grain, cereal, group, 16, stover, except rice

10.0

Grain, cereal, group, 16, straw, except rice

1.0

Grape

0.50

Grape, raisin

0.70

Grass, forage, fodder and hay, group 17, forage

10.0

Grass, forage, fodder and hay, group 17, hay

5.0

Guava

0.3

Herb subgroup 19A, dried

22

Herb subgroup 19A, fresh

3.0

Hog, fat

33

Hog, meat byproducts

8.0

Hog, meat

1.5

Hop, dried cones

22

Horse, fat

50

Horse, liver

10

Horse, meat

2.0

Horse, meat byproducts, except liver

5.0

Ilama

0.3

Jaboticaba

0.3

Juneberry

0.25

Lingonberry

0.250

Longan

0.3

Lychee

0.3

Mango

0.3

Milk

7.0

Milk, fat

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Nut, tree, group 14

0.02

Okra

0.40

Onion, green

2.0

Papaya

0.3

Passionfruit

0.3

Pea and bean, dried shelled, except soybean, subgroup 6C

0.02

Pea and bean, succulent shelled, subgroup 6B

0.02

Peanut

0.02

Peanut, hay

11.0

Peppermint, tops

3.5

Pineapple

0.02

Pineapple, process residue

0.08

Pistachio
Poultry, fat

0.020
1.3

Poultry, meat

0.10

Poultry, meat byproducts

0.10

Pulasan

0.3

Rambutan

0.3

Rice, hulls

4.0

Salal

0.250

Sapodilla

0.3

Sapote, black

0.3

Sapote, mamey

0.3

Sapote, white

0.3

Sheep, fat

50

Sheep, liver

10

Sheep, meat

2.0

Sheep, meat byproducts, except liver

5.0

Soursop

0.3

Soybean

0.02

Spanish lime

0.3

Spearmint, tops

3.5

Spice, subgroup 19B, except black pepper

1.7

Star apple

0.3

Starfruit

0.3

Strawberry

1.0

Sugar apple

0.3

Ti, leaves

10.0

Vegetable, bulb, group 3, except green onion

0.10

Vegetable, cucurbit, group 9

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Vegetable, foliage of legume, group 7

8.0

Vegetable, fruiting, group 8

0.4

Vegetable, leafy, except brassica, group 4

8.0

Vegetable, leaves of root and tuber, group 2

10.0

Vegetable, legume, edible podded, subgroup 6A

0.30

Vegetable, root and tuber, group 1

0.10

Watercress

8.0

Wax jambu

0.3

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertant residues . [Reserved]
[72 FR 68540, Dec. 5, 2007]

§ 180.496 Thiazopyr; tolerances for residues.
top
Tolerances are established for combined residues of the herbicide thiazopyr (3-pyridinecaroxylic acid, 2(difluoromethyl)-5-(4,5-dihydro-2-thiazolyl)-4-(2-methylpropyl)-6-(trifluoromethyl)-, methyl ester) and its
metabolites determined as 2-(difluoromethyl)-6-(trifluoromethyl)-3,4,5-pyridinetricarboxylic acid, all
expressed as the parent equivalents in or on the following raw agricultural commodities:

Commodities

Parts per million

Grapefruit

0.05

Orange, sweet

0.05

[62 FR 9978, Mar. 5, 1997]

§ 180.497 Clofencet; tolerances for residues.
top
(a) Tolerances—general. Tolerances are established for the plant growth regulator (hybridizing agent)
clofencet, [2-(4-chlorophenyl)-3-ethyl-2,5 dihydro-5-oxo-4-pyridazinecarboxylic acid, potassium salt]
expressed as the free acid in or on the following raw agricultural commodities:

Commodities

Parts per million

Cattle, fat

0.04

Cattle, kidney

10.0

Cattle, meat byproducts, except kidney
Cattle, meat
Egg

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0.5
0.15
1.0

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Goat, fat

0.04

Goat, kidney

10.0

Goat, meat byproducts, except kidney

0.5

Goat, meat

0.15

Hog, fat

0.04

Hog, kidney

10.0

Hog, meat byproducts, except kidney

0.5

Hog, meat

0.15

Horse, fat

0.04

Horse, kidney

10.0

Horse, meat byproducts, except kidney

0.5

Horse, meat

0.15

Milk

0.02

Poultry, fat

0.04

Poultry, meat byproducts

0.20

Poultry, meat

0.15

Sheep, fat

0.04

Sheep, kidney

10.0

Sheep, meat byproducts, except kidney

0.5

Sheep, meat

0.15

Wheat, forage

10.0

Wheat, grain

250.0

Wheat, hay

40.0

Wheat, straw

50.0

(b) Tolerances for indirect or inadvertent residues. Tolerances are established for indirect or inadvertent
residues of the plant growth regulator (hybridizing agent) clofencet, [2-(4-chlorophenyl)-3-ethyl-2,5-dihydro5-oxo-4-pyridazinecarboxylic acid, potassium salt] expressed as the free acid in or on the following raw
agricultural commodities when present therein as a result of the application of clofencet to the growing
crops in paragraph (a) of this section:

Commodities

Parts per million

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet
corn, wheat, and wild rice; forage

4.0

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet
corn, wheat, and wild rice; hay

15.0

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet
corn, wheat, and wild rice; stover

1.0

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet
corn, wheat, and wild rice; straw

4.0

Grain, cereal group 15, except rice, sweet corn, wheat, and wild rice

20.0

Soybean

30.0

Soybean, forage

10.0

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Soybean, hay

10.0

[62 FR 9983, Mar. 5, 1997]

§ 180.498 Sulfentrazone; tolerances for residues.
top
(a)(1) General. A tolerance is established for combined residues of the herbicide sulfentrazone N-[2,4dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide
and its major metabolite 3-hydroxymethyl sulfentrazone N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide in or on the following raw
agricultural commodity:

Commodity

Parts per million

Soybean, seed

0.05

(2) Tolerances are established for combined residues of the herbicide sulfentrazone and its metabolites
HMS ( N -(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1 H -1,2,4-triazol- 1-yl)
phenyl)methanesulfonamide) and DMS ( N -(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxo-1 H 1,2,4-triazol-1-yl)phenyl)methanesulfonamide in or on the following food commodities:

Commodity

Parts per million

Asparagus

0.15

Bean, lima, succulent

0.15

Cabbage

0.20

Corn, field, forage

0.20

Corn, field, grain

0.15

Corn, field, stover

0.30

Horseradish

0.20

Pea and bean, dried shelled, except soybean, subgroup 6C

0.15

Peanut

0.20

Peanut, meal

0.40

Peppermint, tops

0.30

Potato

0.15

Spearmint, tops

0.30

Sugarcane, cane

0.15

Sugarcane, molasses

0.20

Sunflower, seed

0.20

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the
herbicide N -[2,4-dichloro-5-[4- (difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1 H -1,2,4-triazol-1-y-l]phenyl]
methanesulfonamide and its metabolites 3-hydroxymethyl sulfentrazone and 3-desmethyl sulfentrazone, in
connection with use of the pesticide under section 18 emergency exemptions granted by EPA. The
tolerance is specified in the following table. The tolerances expire and will be revoked by EPA on the date
specified in the table.

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Commodity

Parts per million Expiration/revocation date

Bean, succulent seed without pod
(lima bean & cowpea)

0.1

12/31/07

Flax, seed

0.20

12/31/10

Strawberry

0.60

12/31/10

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for inadvertent and indirect combined
residues of the herbicide sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolites 3-hydroxymethyl sulfentrazone (N[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]
methanesulfonamide) and 3-desmethyl sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-5oxo-1H-1,2,4-triazol-l-yl]phenyl]methanesulfonamide) in or on the following raw agricultural commodities
when present therein as a result of the application of sulfentrazone to growing crops.

Commodity

Parts per million

Grain, cereal (excluding sweet corn), Hulls

0.30

Grain, cereal, forage, fodder and atraw, group 16, except sweet corn;
forage

0.2

Grain, cereal, forage, fodder and atraw, group 16, except sweet corn;
hay

0.2

Grain, cereal, forage, fodder and atraw, group 16, except sweet corn;
stover

0.1

Grain, cereal, forage, fodder and atraw, group 16, except sweet corn;
straw

0.6

Grain, cereal, group 15, except sweet corn

0.1

Grain, cereal, group 15, except sweet corn; bran

0.15

[62 FR 10708, Mar. 10, 1997, as amended at 64 FR 51067, Sept. 21, 1999; 65 FR 67279, Nov. 9, 2000;
65 FR 82940, Dec. 29, 2000; 66 FR 39658, Aug. 1, 2001; 67 FR 46884, July 17, 2002; 67 FR 54118, Aug.
21, 2002; 68 FR 2247, Jan. 16, 2003; 68 FR 55280, Sept. 24, 2003; 69 FR 29459, May 24, 2004; 69 FR
71717, Dec. 10, 2004; 70 FR 7047, Feb. 10, 2005; 72 FR 71802, Dec. 19, 2007]

§ 180.499 Propamocarb hydrochloride, tolerances for residues.
top
(a) General. Tolerances are established for the residues of propyl[3-(dimethylamino)propyl]carbamate
monohydrochloride also known as propamocarb hydrochloride in or on the following raw agricultural
commodity:

Commodity

Parts per million

Lettuce, head

50

Lettuce, leaf

90

Potato

0.06

Tomato, paste

5.0

Vegetable, cucurbit, group 9

1.5

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Vegetable, fruiting, group 8

2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerance with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 15620, Apr. 2, 1997, as amended at 62 FR 26966, May 16, 1997; 63 FR 32136, June 12, 1998; 64
FR 16843, Apr. 7, 1999; 65 FR 58399, Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR 48585, Sept.
21, 2001; 67 FR 35049, May 17, 2002; 69 FR 47022, Aug. 4, 2004; 70 FR 7047, Feb. 10, 2005]

§ 180.500 Imazapyr; tolerances for residues.
top
(a) General. Tolerances are being established for residues of the herbicide imazapyr, [2-[4,5-dihydro-4methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-pyridinecarboxylic acid], applied as the acid or
ammonium salt, in or on the following raw agricultural commodities:

Commodity

Parts per million

Cattle, fat

0.05

Cattle, kidney

0.20

Cattle, meat

0.05

Cattle, meat byproducts, except kidney

0.05

Corn, field, forage

0.05

Corn, field, grain

0.05

Corn, field, stover

0.05

Fish

1.0

Goat, fat

0.05

Goat, kidney

0.20

Goat, meat

0.05

Goats, meat byproducts, except kidney

0.05

Grass, forage

100

Grass, hay

30

Horse, fat

0.05

Horse, kidney

0.20

Horse, meat

0.05

Horse, meat byproducts, except kidney

0.05

Milk

0.01

Sheep, fat

0.05

Sheep, kidney

0.20

Sheep, meat

0.05

Sheep, meat byproducts, except kidney

0.05

Shellfish

0.10

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55484, Sept. 26, 2003]

§ 180.501 Hydroprene; tolerances for residues.
top
(a) General. A tolerance of 0.2 part per million is established for residues of hydroprene [(S)-(Ethyl
(2E,4E,7S)-3,7,11-trimrthyl-2,4-dodecadienoate)], (CAS Reg. No. 65733–18–8) on food commodities in
food-handling establishments in accordance with the following prescribed conditions:
(1) Application shall be limited to spot, crack and crevice, perimeter and ultra low volume (ULV) fogging
treatment in food storage or food-handling establishments, including warehouses, food service,
manufacturing, and processing establishments such as restaurants, cafeterias, supermarkets, bakeries,
breweries, dairies, meat slaughtering and packing plants, and canneries where food and food products are
held, processed, and served: Provided that the food is removed or covered prior to such use, and foodprocessing surfaces are covered during treatment or thoroughly cleaned before using, or in the case of
point-source device treatments, devices must not come into direct contact with food preparation surfaces
and must be in a minimum distance of 3 feet from exposed foods.
(2) To assure safe use of the insect growth regulator, the label and labeling shall conform to that
registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such
label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 61647, Nov. 19, 1997, as amended at 71 FR 74818, Dec. 13, 2006]

§ 180.502 Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for
residues.
top
(a) General. Tolerances are established for residues of aminoethoxyvinylglycine hydrochloride (aviglycine
HCl) in or on the following food commodities:

Commodity

Parts per million

Apple
Fruit, stone, group 12, except cherry
Pear
(b) Section 18 emergency exemptions. [Reserved]

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0.08
0.170
0.08

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 24838, May 7, 1997, as amended at 64 FR 31129, June 10, 1999; 66 FR 36481, 36484, July 12,
2001; 69 FR 7606, Feb. 18, 2004]

§ 180.503 Cymoxanil, tolerance for residues.
top
(a) General . Tolerances are established for residues of the fungicide, cymoxanil, 2-cyano -N- [(ethylamino)
carbonyl]-2-(methoxyimino) acetamide, in or on the following food commodities:

Commodity

Parts per million

Caneberry, subgroup 13A-07

4.0

Cilantro, leaves

19

Hop, dried cones

7.0

Leafy greens, subgroup 4A

19

Leaf petioles, subgroup 4B

6.0

Lychee1

1.0

Onion, bulb, subgroup 3-07A

0.05

Onion, green, subgroup 3-07B

1.1

Potato

0.05

Vegetable, cucurbit, group 9

0.05

Vegetable, fruiting, group 8

0.2

1

There is no U.S. registration for lychee.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with a regional registration . Tolerances with a regional registration as defined in §180.1(n)
are established for the residues of the fungicide cymoxanil, 2-cyano - N - [(ethylamino)carbonyl]-2(methoxyimino) acetamide) in or on the raw agricultural commodities:

Commodity

Parts per million

Grape

0.10

(d) Indirect or inadvertent residues. [Reserved]
[62 FR 26411, May 14, 1997, as amended at 62 FR 39956, July 25, 1997; 63 FR 24949, May 6, 1998; 63
FR 66464, Dec. 2, 1998; 64 FR 6539, Feb. 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, July 19,
2001; 67 FR 35049, May 17, 2002; 68 FR 41936, July 16, 2003; 70 FR 7047, Feb. 10, 2005; 72 FR
37646, July 11, 2007; 73 FR 58885, Oct. 8, 2008]

§ 180.504 [Reserved]

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§ 180.505 Emamectin; tolerances for residues.
top
(a) General . (1) Tolerances are established for combined residues of emamectin (a mixture of a minimum
of 90% 4'-epi-methylamino-4'-deoxyavermectin B1aand maximum of 10% 4'-epi-methylamino-4'deoxyavermectin B1b) and its metabolites 8,9-isomer of the B1aand B1bcomponent of the parent (8,9ZMA), or 4'-deoxy-4'-epi-amino-avermectin B1aand 4'-deoxy-4'-epi-amino-avermectin B1b; 4'-deoxy-4'-epiamino avermectin B1a(AB1a); 4'-deoxy-4'-epi-(N-formyl-N-methyl)amino-avermectin (MFB1a); and 4'-deoxy4'-epi-(N-formyl)amino-avermectin B1a(FAB1a) in or on the following commodities:

Commodity

Parts per million

Almond, hulls

0.20

Apple, wet pomace

0.075

Cotton, gin byproducts

0.050

Cotton, undelinted seed

0.025

Fruit, pome, group 11

0.025

Nut, tree, group 14

0.02

Pistachio

0.02

Tomato, paste

0.150

Turnip, greens

0.050

Vegetable, Brassica, leafy, group 5

0.050

Vegetable, fruiting, group 8

0.020

Vegetable, leafy, except Brassica, group 4

0.100

(2) Tolerances are also established for combined residues of emamectin (MAB1a+ MAB1bisomers) and the
associated 8,9-Z isomers (8,9-ZB1a+ 8,9-ZB1b) in/on the following commodities when present therein as a
result of the application of emamectin to crops listed in the table in paragraph (a)(1) of this section:

Commodity

Parts per million

Cattle, fat

0.010

Cattle, liver

0.050

Cattle, meat

0.003

Cattle, meat byproducts, except liver

0.020

Goat, fat

0.010

Goat, liver

0.050

Goat, meat

0.003

Goat, meat byproducts, except liver

0.020

Hog, fat

0.003

Hog, liver

0.020

Hog, meat

0.002

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Hog, meat byproducts (except liver)

0.005

Horse, fat

0.010

Horse, liver

0.050

Horse, meat

0.003

Horse, meat byproducts, except liver

0.020

Milk

0.003

Sheep, fat

0.010

Sheep, liver

0.050

Sheep, meat

0.003

Sheep, meat byproducts, except liver

0.020

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. [Reserved]
[71 FR 18649, Apr. 12, 2006, as amended at 74 FR 2873, Jan. 16, 2009]

§ 180.506 Cyclanilide; tolerances for residues.
top
(a) General. Tolerances are established for residues of the plant growth regulator, cyclanilide, [1-(2,4dichlorophenylaminocarbonyl)-cyclopropane carboxylic acid] determined as 2,4-dichloroaniline (calculated
as cyclanilide) in or on the following food commodities and processed feed:

Commodity

Parts Per Million

Cattle, fat

0.10

Cattle, meat

0.02

Cattle, meat byproducts, except kidney

0.2

Cattle, kidney

2.0

Cotton, undelinted seed

0.60

Cotton, gin byproducts

25.0

Goat, fat

0.10

Goat, meat

0.02

Goat, meat byproducts, except kidney

0.20

Goat, kidney

2.0

Horse, fat

0.10

Horse, meat

0.02

Horse, meat byproducts, except kidney

0.20

Horse, kidney

2.0

Hog, fat

0.10

Hog, meat

0.02

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Hog, meat byproducts, except kidney

0.20

Hog, kidney

2.0

Milk

0.04

Sheep, fat

0.10

Sheep, meat

0.20

Sheep, meat byproducts, except kidney

0.20

Sheep, kidney

2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 28355, May 23, 1997; 62 FR 34182, June 25, 1997]

§ 180.507 Azoxystrobin; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the fungicide, azoxystrobin, [methyl( E )-2-(2-(6(2-cyanophenoxy) pyrimidin-4-yloxy)phenyl)-3-methoxyacrylate] and the Z-isomer of azoxystrobin, [methyl
( Z )-2-(2-(6-(2-cyanophenoxy)pyrimidin-4-yloxy)phenyl)-3 methoxyacrylate] in or on the following food
commodities and processed food:

Commodity

Parts per million

Acerola

2.0

Almond, hulls

4.0

Animal feed, nongrass, forage, group 18

45

Animal feed, nongrass, hay, group 18

120

Artichoke, globe

4.0

Asparagus

0.04

Atemoya

2.0

Avocado

2.0

Banana (pre-harvest and post harvest)

2.0 (of which not more than 0.1 is
contained in the pulp)

Barley, bran

0.2

Barley, forage

25

Barley, grain

0.1

Barley, hay

15.0

Barley, straw

4.0

Biriba

2.0

Brassica, head and stem, subgroup 5A

3.0

Brassica, leafy greens, subgroup 5B

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25

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Bushberry subgroup 13B

3.0

Caneberry subgroup 13A

5.0

Canistel

2.0

Canola, seed

1.0

Citrus, dried pulp

20.0

Citrus, oil

40.0

Cherimoya

2.0

Coriander, leaves

30.0

Corn, field, forage

12.0

Corn, field, grain

0.05

Corn, field, refined oil

0.3

Corn, field, stover

25.0

Corn, pop, grain

0.05

Corn, pop, stover

25.0

Corn, sweet, forage

12.0

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, stover

25.0

Cotton, gin byproducts

45

Cotton, undelinted seed

0.6

Crambe, seed

0.5

Cranberry

0.50

Cucurbits

0.3

Custard apple

2.0

Feijoa

2.0

Flax, seed

0.5

Fruit, citrus, group 10

10.0

Fruit, stone

1.5

Grain, aspirated fractions

420

Grape

1.0

Grass, forage1

15

Grass, hay1

20

Guava

2.0

Herb Subgroup 19A, dried leaves

260

Herb Subgroup 19A, fresh leaves

50

Hop, dried cones

20.0

Ilama

2.0

Jaboticaba

2.0

Jackfruit

2.0

Juneberry

3.0

Lingonberry

3.0

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Longan

2.0

Loquat

2.0

Lychee

2.0

Mango

2.0

Mustard, field, seed

0.5

Mustard, Indian, seed

0.5

Mustard, seed

0.5

Nut, tree, group 14

0.02

Okra

2.0

Onion, bulb

1.0

Onion, green

7.5

Passionfruit

2.0

Pawpaw

2.0

Papaya

2.0

Pea and bean, dried shelled, except soybean,
subgroup 6C

0.5

Pea and bean, succulent shelled, subgroup 6B

0.5

Peanut

0.2

Peanut, refined oil

0.6

Peanut, hay

15.0

Pecan

0.01

Peppermint, tops
Persimmon

30
2.0

Pistachio

0.50

Potato

0.03

Pulasan

2.0

Rambutan

2.0

Rapeseed, Indian

0.5

Rapeseed, seed

0.5

Rice, grain

5.0

Rice, hulls

20

Rice, straw

12

Rice, wild, grain

5.0

Safflower, seed

0.5

Salal

3.0

Sapodilla

2.0

Sapote, black

2.0

Sapote, mamey

2.0

Sapote, white

2.0

Sorghum, forage

25

Sorghum, grain

11

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Sorghum, stover

40

Soursop

2.0

Soybean, hay

55.0

Soybean, hulls

1.0

Soybean, seed

0.5

Spanish lime

2.0

Spearmint, tops

30

Spice Subgroup 19B, except black pepper

38

Star apple

2.0

Starfruit

2.0

Strawberry

10

Sugar apple

2.0

Sunflower, seed

0.5

Tamarind

2.0

Tomato

0.2

Tomato, paste

0.6

Turnip, greens

25

Vegetable, foliage of legume, group 7

30.0

Vegetable, fruiting, group 8, except tomato

2.0

Vegetable, leafy, except brassica, group 4

30.0

Vegetable, leaves of root and tuber, group 2

50.0

Vegetable, legume, edible podded, subgroup 6A,
except soybean

3.0

Vegetable, root, subgroup 1A

0.5

Vegetable, tuberous and corm, subgroup 1C

0.03

Watercress

3.0

Wax jambu

2.0

Wheat, bran

0.20

Wheat, forage

25

Wheat, grain

0.10

Wheat, hay

15

Wheat, straw

4.0

(2) Tolerances are established for residues of the fungicide, azoxystrobin [methyl( E )-2-(2-(6-(2cyanophenoxy)pyrimidin-4-yloxy)phenyl)-3-methoxyacrylate] in or on the following food commodities.

Commodity

Parts per million

Cattle, fat

0.03

Cattle, meat

0.01

Cattle, meat byproducts

0.07

Goat, fat

0.03

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Goat, meat

0.01

Goat, meat byproducts

0.07

Hog, fat

0.010

Hog, meat

0.01

Hog, meat byproducts

0.010

Horse, fat

0.03

Horse, meat

0.01

Horse, meat byproducts

0.07

Milk.

0.006

Sheep, fat

0.03

Sheep, meat

0.01

Sheep, meat byproducts

0.07

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 32235, June 13, 1997]
Editorial Note: ForFederal Registercitations affecting §180.507, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.509 Mefenpyr-diethyl; tolerance for residues.
top
(a) General. Tolerances are established for residues of the herbicide safener, mefenpyr-diethyl, 1-(2,4dichlorophenyl)-4,5-dihydro-5-methyl-1H-pyrazole-3,5-dicarboxylic acid, diethyl ester and its 2,4dichlorophenyl-pyrazoline metabolites, when applied at a rate no greater than 0.053 pound safener per
acre per growing season in or on the following raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.05

Barley, hay

0.2

Barley, straw

0.5

Canola, seed

0.02

Cattle, meat byproducts

0.1

Goat, meat byproducts

0.1

Hog, meat byproducts

0.1

Horse, meat byproducts

0.1

Sheep, meat byproducts

0.1

Wheat, forage

0.2

Wheat, grain

0.05

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Wheat, hay

0.2

Wheat, straw

0.5

Soybean, forage

0.1

Soybean, hay

0.1

Soybean, seed

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[73 FR 74977, Dec. 10, 2008]

§ 180.510 Pyriproxyfen; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide pyriproxyfen 2-[1-methyl-2-(4phenoxyphenoxy)ethoxypyridine in or on the following food commodities:

Commodity
Acerola
Almond, hulls
Animal feed, nongrass, group 18, forage

Parts per million
0.10
2.0
0.70

Animal feed, nongrass, group 18, hay

1.1

Animal feed, nongrass, group 18, seed

2.0

Apple, wet pomace

0.8

Atemoya

0.20

Avocado

1.0

Banana

0.20

Beet, sugar, dried pulp

3.0

Biriba

0.20

Brassica, head and stem, subgroup 5A

0.70

Brassica, leafy greens, subgroup 5B

2.0

Bushberry subgroup 13B

1.0

Cacao bean, dried

0.02

Caneberry, subgroup 13-A

1.0

Canistel

1.0

Canola, seed

0.20

Cherimoya

0.20

Citrus, oil
Citrus, dried pulp
Citrus hybrids
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2.0
0.30

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Coffee, instant

0.10

Coffee, green bean

0.02

Cotton, gin byproducts

2.0

Cotton, undelinted seed

0.05

Cranberry

1.0

Custard apple

0.20

Date

0.30

Feijoa

0.10

Fig

0.30

Fig, dried fruit

1.0

Fruit, citrus

0.3

Fruit, pome

0.2

Fruit, stone, group 12

1.0

Grain, cereal, group 15

1.1

Grain, cereal, forage, fodder and straw, group 16

1.1

Grape

2.5

Grass, forage, fodder, and hay, group 17, forage
Grass, forage, fodder, and hay, group 17, hay

0.70
1.1

Guava

0.10

Ilama

0.20

Jaboticaba

0.10

Juneberry

1.0

Lingonberry

1.0

Loganberry

0.30

Lychee

0.30

Mango

1.0

Nut, tree, group 14

0.02

Okra

0.02

Olive

1.0

Olive, oil

2.0

Onion, bulb
Papaya
Passionfruit

0.15
1.0
0.10

Pawpaw

1.0

Peanut

0.20

Pineapple

0.30

Pineapple, process residue

1.1

Pistachio

0.02

Pomegranate

0.20

Potato, chips

0.75

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Potato, granules/flakes

0.75

Potato, wet peel

0.75

Pulasan

0.30

Rambutan

0.30

Rice, hulls

5.5

Safflower, seed

0.20

Salal

1.0

Sapodilla

1.0

Sapote, black

1.0

Sapote, mamey

1.0

Sapote, white

0.30

Sesame, seed

0.02

Soursop

0.20

Spanish lime

0.30

Star apple

1.0

Starfruit

0.10

Strawberry

0.30

Sugar apple

0.20

Sugarcane

1.1

Tea

0.02

Vegetable, bulb, group 3, except onion, bulb

0.70

Vegetable, cucurbit, group 9

0.10

Vegetable, fruiting, group 8

0.2

Vegetable, legume, group 6

0.20

Vegetable, root and tuber, group 1

0.15

Walnut

0.02

Wax jambu

0.10

(2) A tolerance of 0.10 parts per million is established for all food commodities as a result of the proposed
use of NYLAR in food handling establishments where food and food products are held, prepared,
processed or served. Application is limited to space, general surface, spot, and/or crack and crevice
treatment in food handling establishments where food and food products are held, processed, prepared
and served. Space and general surface application may be used only when the facility is not in operation
provided exposed food is covered or removed from the area being treated prior to application. Spot, and/or
crack and crevice treatment may be used while the facility is in operation provided exposed food is
covered or removed from the area being treated prior to application. Food contact surfaces should be
thoroughly washed with an effective cleaning compound and rinced with potable water after use of the
product. To assure safe use of this additive, its label and labeling shall conform to that registered with the
U.S. Environmental Protection Agency, and shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. Time-limited tolerances are established for the residues of the
insect growth regulator pyriproxyfen, in connection with the use of the pesticide under section 18
emergency exemptions granted by EPA. The tolerances will expire on the dates specified in the following
table.

Commodity

Parts per million

Expiration/revocation date

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Bean, succulent

0.10

6/30/08

Celery

2.50

6/30/07

Strawberry

0.30

12/31/07

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 10233, Mar. 3, 1999]
Editorial Note: ForFederal Registercitations affecting §180.510, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.511 Buprofezin; tolerances for residues.
top
(a) General . Tolerances are established for residues of buprofezin, including its metabolites and
degradates in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only the buprofezin, 2-[(1,1-dimethylethyl)imino]tetrahydro-3(1methylethyl)-5-phenyl-4 H -1,3,5-thiadiazin-4-one, in the commodity.

Commodity

Parts per million

Acerola

0.30

Almond

0.05

Almond, hulls

2.0

Apricot

9.0

Atemoya

0.30

Avocado

0.30

Banana

0.20

Bean, snap, succulent

0.02

Berry, low growing, subgroup 13-07G

2.5

Birida

0.30

Brassica, head and stem, subgroup 5A

12.0

Canistel

0.90

Cattle, fat

0.05

Cattle, kidney

0.05

Cattle, liver

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Cherimoya

0.30

Citrus, dried pulp
Citrus, oil

7.5
80

Coffee, green bean

0.35

Cotton, gin byproducts

20.0

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Cotton, undelinted seed

0.35

Custard apple

0.30

Feijoa

0.30

Fruit, citrus, group 10

2.5

Fruit, pome, group 11

4.0

Fruit, stone, group 12, except apricot and peach

1.9

Goat, fat

0.05

Goat, kidney

0.05

Goat, liver

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Grape

2.5

Guave

0.30

Hog, fat

0.05

Hog, kidney

0.05

Hog, liver

0.05

Hog, meat

0.05

Hog, meat byproducts

0.05

Horse, fat

0.05

Horse, kidney

0.05

Horse, liver

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Llama

0.30

Jaboticaba

0.30

Lettuce, head

6.0

Loganberry

0.30

Lychee

0.30

Mango

0.90

Milk

0.01

Okra

4.0

Olive

3.5

Olive, oil

4.8

Papaya

0.90

Passionfruit

0.30

Peach

9.0

Pepper, nonbell

4.0

Pistachio
Pomegranate
Pulasan

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0.05
1.9
0.30

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Radicchio

6.0

Rambutan

0.30

Sapodilla

0.90

Sapote, black

0.90

Sapote, mamey

0.90

Sheep, fat

0.05

Sheep, kidney

0.05

Sheep, liver

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Soursop

0.30

Spanish lime

0.30

Star apple

0.90

Starfruit

0.30

Sugar apple

0.30

Vegetable, cucurbit, group 9

0.50

Vegetable, fruiting, group 8, except nonbell pepper

1.3

Vegetable, leafy, except Brassica, group 4, except head lettuce and
radicchio
Wax jambu

35
0.30

(b) Section 18 emergency exemption. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 40741, July 30, 1997, as amended at 63 FR 33585, June 19, 1998; 63 FR 41727, Aug. 5, 1998; 64
FR 45887, Aug. 23, 1999; 64 FR 59655, Nov. 3, 1999; 65 FR 52947, Aug. 31, 2000; 66 FR 46389, Sept.
5, 2001; 68 FR 37771, June 25, 2003; 70 FR 17907, Apr. 8, 2005; 71 FR 55313, Sept. 22, 2006; 72 FR
35187, June 27, 2007; 73 FR 19161, Apr. 9, 2008; 74 FR 33158, July 10, 2009]

§ 180.512 [Reserved]
top

§ 180.513 Chlorfenapyr; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide chlorfenapyr [4-bromo-2-(4chlorophenyl)-1-(ethoxymethyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile] in or on the following raw
agricultural commodities:

Commodity

Parts per million

Vegetable, fruiting, group 8
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1.0

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(2) A tolerance of 0.01 parts per million is established for residues of chlorfenapyr in or on all food
commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/
feed handling areas where food/feed products are prepared, held, processed, or served and in
accordance with the following prescribed conditions:
(i) Application shall be no greater than a 0.5% active ingredient solution for spot crack and crevice use in
food/feed handling establishments, where food and food products are held, processed, prepared and/or
served.
(ii) Application may only be undertaken when the facility is not in operation, and provided exposed food
has been covered, or removed from the area being treated prior to application.
(iii) Food contact surfaces and equipment should be throughly washed with an effective cleaning
compound, and rinsed with potable water after each use of the product.
(iv) Contamination of food or food contact surfaces shall be avoided. Application excludes any direct
application to any food, food packaging, or any food contact surfaces.
(v) To assure safe use, the label and labeling shall conform to that registered by the U.S. Environmental
Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55527, Sept. 26, 2003, as amended at 70 FR 3654, Jan. 26, 2005]

§ 180.514 Cloransulam-methyl; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide, cloransulam-methyl, N -(2carboxymethyl-6-chlorophenyl)-5-ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-pyrimidine-2-sulfonamide, plus its
acid, cloransulam, calculated as parent ester in or on the following raw agricultural commodities:

Commodity

Parts per million

Soybean, forage

0.1

Soybean, hay

0.2

Soybean, seed

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 49163, Sept. 19, 1997]

§ 180.515 Carfentrazone-ethyl; tolerances for residues.

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(a) General. Tolerances are established for combined residues of the herbicide carfentrazone-ethyl (ethylalpha-2-dichloro-5-[-4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1 H -1,2,4-triazol-1-yl]-4-fluorobenzene
propanoate) and its metabolite: carfentrazone-chloropropionic acid (alpha, 2-dichloro-5-[-4-difluoromethyl)4,5-dihydro-3-methyl-5-oxo-1 H -1,2,4-triazol-1-yl]-4-fluorobenzenepropanoic acid) in or on the following
raw agricultural commodities:

Commodity

Parts per million

Acerola

0.10

Almond, hulls

0.20

Atemoya

0.10

Avocado

0.10

Banana

0.20

Barley, bran

0.80

Barley, flour

0.80

Berry group 13

0.10

Birida

0.10

Borage

0.10

Cacao bean, bean

0.10

Cactus

0.10

Caneberry subgroup 13A

0.1

Canistel

0.10

Canola

0.10

Cherimoya

0.10

Coconut

0.10

Coffee, bean, green

0.10

Corn, field, forage

0.20

Corn, sweet, forage

0.20

Corn, sweet, kernel plus cob with husk removed

0.10

Cotton, gin byproducts

10

Cotton, undelinted seed

0.20

Cotton, hulls

0.60

Cotton, meal

0.35

Cotton, refined oil

1.0

Crambe, seed

0.10

Custard apple

0.10

Date, dried fruit

0.10

Fat (cattle, goat, horse, and sheep)

0.10

Feijoa

0.10

Fig

0.10

Fish

0.30

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Flax, seed

0.10

Fruit, citrus, group 10

0.10

Fruit, pome, group 11

0.10

Fruit, stone, group 12

0.10

Grain, aspirated grain fractions

1.8

Grain, cereal, forage, fodder and straw group 16, except corn and
sorghum; forage

1.0

Grain, cereal, forage, fodder and straw, group 16, hay

0.30

Grain, cereal, forage, fodder and straw, group 16, stover

0.30

Grain, cereal, forage, fodder and straw, group 16, except rice; straw

0.10

Grain, cereal, group 15

0.10

Grain, cereal, group 15 (except rice grain and sorghum grain)

0.10

Grain, cereal, stover

0.80

Grain, cereal, straw

3.0

Grape

0.10

Grass, forage

5.0

Grass, hay

8.0

Guava
Herbs and spices group 19

0.10
2.0

Hog, fat

0.10

Hog, meat

0.10

Hog, meat byproducts

0.10

Hop, dried cones

0.10

Horseradish

0.10

Ilama

0.10

Jaboticaba

0.10

Juneberry

0.10

Kava, roots

0.10

Kiwifruit

0.10

Lingonberry

0.10

Longan

0.10

Lychee

0.10

Mango

0.10

Meat, (cattle, goat, horse, and sheep)

0.10

Meat, byproducts, cattle, goat, horse, and sheep)

0.10

Milk

0.05

Millet, flour

0.80

Mustard, seed

0.10

Noni

0.10

Nut, tree, group 14

0.10

Oat, flour

0.80

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Okra

0.10

Olive

0.10

Palm heart

0.10

Palm heart, leaves

0.10

Papaya

0.10

Passionfruit

0.10

Pawpaw

0.10

Peanut

0.10

Peanut, hay

0.10

Persimmon

0.10

Pistachio

0.10

Pomegranate

0.10

Poultry, meat byproducts

0.10

Pulasan

0.10

Pummelo

0.10

Rambutan

0.10

Rapeseed, forage

0.10

Rapeseed, seed

0.10

Rice, grain

1.3

Rice, hulls

3.5

Rice, straw

1.0

Rye, bran

0.80

Rye, flour

0.80

Safflower, seed

0.10

Salal

0.10

Sapodilla

0.10

Sapote, black

0.10

Sapote, mamey

0.10

Shellfish

0.30

Sorghum, forage

0.20

Sorghum, grain

0.25

Sorghum, sweet

0.10

Soursop

0.10

Soybean, seed

0.10

Spanish lime

0.10

Star apple

0.10

Starfruit

0.10

Stevia

0.10

Strawberry

0.10

Strawberrypear

0.10

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Sugar apple

0.10

Sugarcane

0.15

Sunflower, seed

0.10

Tea, dried

0.10

Ti, leaves

0.10

Ti, roots

0.10

Vanilla

0.10

Vegetable, brassica, leafy, group 5

0.10

Vegetable, bulb, group 3

0.10

Vegetable, cucurbit, group 9

0.10

Vegetable, foliage of legume, except soybean, subgroup 7A

0.10

Vegetable, fruiting, group 8

0.10

Vegetable, leafy, except brassica, group 4

0.10

Vegetable, leaves of root and tuber, group 2

0.10

Vegetable, legume, group 6

0.10

Vegetable, root and tuber, group 1

0.10

Wasaba, roots

0.10

Wax jambu

0.10

Wheat, bran

0.80

Wheat, flour

0.80

Wheat, germ

0.80

Wheat, middlings

0.80

Wheat, shorts

0.80

(b) Section 18 emergency exemptions. Time-limited tolerances are established for combined residues of
the herbicide carfentrazone-ethyl and its chloropropionic acid metabolite in connection with use of the
pesticide under section 18 emergency exemptions granted by EPA. These tolerances will expire and are
revoked on the dates specified in the following table.

Commodity

Parts per million

Expiration/Revocation Date

Hop, dried cones

0.30

6/30/05

Tomato, paste

0.60

6/30/07

Tomato, puree

0.60

6/30/07

Vegetable, fruiting, group 8

0.10

6/30/07

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 52180, Sept. 30, 1998, as amended at 63 FR 65078, Nov. 25, 1998; 64 FR 45890, Aug. 23, 1999;
65 FR 48626, Aug. 9, 2000; 66 FR 39647, 39682, Aug. 1, 2001; 67 FR 35050, May 17, 2002; 67 FR
40211, June 12, 2002; 68 FR 37765, June 25, 2003; 69 FR 29459, May 24, 2004; 69 FR 58078, Sept. 29,
2004; 73 FR 9221, Feb. 20, 2008]

§ 180.516 Fludioxonil; tolerances for residues.
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(a) General. Tolerances are established for residues of the fungicide fludioxonil (4-(2,2-difluoro-1,3benzodioxol-4-yl)-1 H -pyrrole-3-carbonitrile) in or on the following commodities:

Commodity

Parts per million

Animal feed, nongrass, group 18

0.01

Avocado

0.45

Bean, dry

0.4

Bean, succulent

0.4

Brassica, head and stem, subgroup 5A

2.0

Brassica, leafy greens, subgroup 5B

10

Bushberry subgroup 13B

2.0

Caneberry subgroup 13A

5.0

Canistel
Citrus, oil

0.45
500

Cotton, gin byproducts

0.05

Cotton, undelinted seed

0.05

Flax, seed

0.05

Fruit, citrus, group 10

10

Fruit, pome, group 11

5.0

Fruit, stone, group 12

5.0

Grain, cereal

0.02

Grain, cereal, forage, fodder, and straw, group 16

0.01

Grape
Grass, forage, fodder and hay, group 17

1.0
0.01

Herb subgroup 19A, dried

65

Herb subgroup 19A, fresh

10

Herbs and spices group 19
Juneberry

0.02
2.0

Kiwifruit

20

Leafy greens subgroup 4A, except spinach

30

Lingonberry

2.0

Longan

1.0

Lychee

1.0

Mango

0.45

Melon subgroup 9A

0.03

Onion, bulb

0.20

Onion, green
Papaya

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7.0
0.45

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Peanut

0.01

Peanut, hay

0.01

Pistachio

0.10

Pomegranate

5.0

Pulasan

1.0

Rambutan

1.0

Rapeseed, forage

0.01

Rapeseed, seed

0.01

Safflower, seed

0.01

Salal

2.0

Sapodilla

0.45

Sapote, black

0.45

Sapote, mamey

0.45

Spanish lime

1.0

Star apple

0.45

Strawberry

2.0

Sunflower, seed

0.01

Tomatillo

0.50

Tomato

0.50

Turnip, greens

10

Vegetable, bulb, group 3

0.02

Vegetable, cucurbit, crop group 9

0.45

Vegetable, foliage of legume, group 7

0.01

Vegetable, fruiting, group 8

0.01

Vegetable, leafy, except brassica, group 4

0.01

Vegetable, leaves of root and tuber, crop group 2

30

Vegetable, legume, group 6

0.01

Vegetable, root and tuber, group 1

0.02

Vegetable, root, except sugar beet, subgroup 1B

0.75

Vegetable, tuberous and corn, except potato, subgroup 1D

3.5

Watercress

7.0

Yam, true, tuber

8.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the
fungicide fludioxonil (4-(2,2-difluoro-1,3-benzodioxol-4-yl)-1 H -pyrrole-3-carbonitrile) in connection with
use of the pesticide under section 18 emergency exemptions granted by EPA. The tolerances will expire
and are revoked on the dates specified in the following table:

Commodity
Starfruit

Parts per million

Expiration/revocation date
10

(c) Tolerances with regional registrations. [Reserved]

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12/31/10

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(d) Indirect or inadvertent residues. [Reserved]
[62 FR 56082, Oct. 29, 1997]
Editorial Note: ForFederal Registercitations affecting §180.516, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.517 Fipronil; tolerances for residues.
top
(a) General. Therefore, tolerances are established for combined residues of the insecticide fipronil (5amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)sulfinyl]-1H-pyrazole-3carbonitrile) and its metabolites 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)
sulfonyl]-1H-pyrazole-3-carbonitrile and 5-amino-1-[2,6-dichloro-4-(trifluoromethyl) phenyl]-4[(trifluoromethyl)thio]-1H-pyrazole-3-carbonitrile and its photodegradate 5-amino-1-(2,6-dichloro-4(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)]-1H-pyrazole-3-carbonitrile in or on the following items
at the levels specified:

Commodity

Parts per million

Corn, field, grain

0.02

Corn, field, stover

0.30

Corn, field, forage

0.15

Egg

0.03

Fat of cattle, goat, horse and sheep

0.40

Hog, fat

0.04

Hog, liver

0.02

Hog, meat

0.01

Hog, meat byproducts, except liver

0.01

Liver of cattle, goat, horse and sheep

0.10

Milk, fat (reflecting 0.05 ppm in whole milk)

1.50

Meat Byproducts, except liver of cattle, goat, horse and sheep

0.04

Meat of cattle, goat, horse and sheep

0.04

Potato

0.03

Potato, wet peel

0.10

Poultry, fat

0.05

Poultry, meat

0.02

Poultry, meat byproducts

0.02

Rice, grain

0.04

Rice, straw

0.10

(b) Section 18 emergency exemptions. . Time-limited tolerances are established for combined residues of
the insecticide, fipronil, 5-amino-1-(2,6-dichloro-4-(trifluoromethyl) phenyl)-4-((1,R,S)-trifluoromethyl)
sulfinyl)-1-H-pyrazole-3-carbonitrile and its 2 metabolites MB45950 (5-amino-1-(2,6-dichloro-4(trifluoromethyl)phenyl)-4-[(trifluoromethyl)thio]-1H-pyrazole-3-carbonitrile) and MB46136 (5-amino-1-(2,6dichloro-4-(trifluoromethyl)phenyl)-4-[(trifluoromethyl)sulfonyl]-1H-pyrazole-3-carbonitrile) and its
photodegradate MB46513 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)]-

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1H-pyrazole-3-carbonitrile), in connection with use of the pesticide under Section 18 emergency
exemptions granted by EPA. The tolerances expire and are revoked on the dates specified in the table for
this paragraph.

Commodity

Parts per million

Expiration/revocation date

Rutabaga

1.0

12/31/10

Turnip

1.0

12/31/10

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for combined indirect or inadvertent
residues of the insecticide fipronil and its metabolites and photodegradate in or on food commodities when
present therein as a result of the application of fipronil to growing crops listed in paragraphs (a) and (b) of
this section and other nonfood crops to read as follows:

Commodity

Parts per million

Wheat, forage

0.02

Wheat, grain

0.005

Wheat, hay

0.03

Wheat, straw

0.03

[62 FR 62979, Nov. 26, 1997, as amended at 63 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, 2007]

§ 180.518 Pyrimethanil; tolerances for residues.
top
(a) General . (1) Tolerances are established for the residues of the fungicide pyrimethanil 4,6-dimethyl- N phenyl-2-pyrimidinamine in or on the following raw agricultural commodities:

Commodity
Almond

Parts per million
0.20

Almond, hulls

12

Apple, wet pomace

40

Banana
Citrus, oil

0.10
150

Fruit, citrus, group 10, except lemon, postharvest

10

Fruit, pome, group 11 (pre-harvest and post-harvest)

14

Fruit, stone, group 12

10

Grape

5.0

Grape, raisin

8.0

Lemon, preharvest and postharvest
Onion, bulb
Onion, green
Pistachio

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11
0.10
2.0
0.20

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Strawberry

3.0

Tomato

0.50

Vegetable, tuberous and corm, subgroup 1C

0.05

(2) Tolerances are established for the combined residues of the fungicide pyrimethanil 4,6-dimethyl- N phenyl-2-pyrimidinamine and its metabolite 4-[4,6-dimethyl-2-pyrimidinyl)amino]phenol in or on the
following commodities:

Commodity

Parts per million

Cattle, fat

0.01

Cattle, kidney

2.5

Cattle, meat

0.01

Cattle, meat byproducts, except kidney

0.01

Goat, fat

0.01

Goat, kidney

2.5

Goat, meat

0.01

Goat, meat byproducts, except kidney

0.01

Horse, fat

0.01

Horse, kidney

2.5

Horse, meat

0.01

Horse, meat byproducts, except kidney

0.01

Sheep, fat

0.01

Sheep, kidney

2.5

Sheep, meat

0.01

Sheep, meat byproducts, except kidney

0.01

(3) Tolerances are established for the combined residues of the fungicide pyrimethanil 4,6-dimethyl- N phenyl-2-pyrimidinamine and its metabolite 4,6-dimethyl-2-(phenylamino)-5-pyrimidinol in or on the
following commodity:

Commodity

Parts per million

Milk

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63669, Dec. 2, 1997, as amended at 69 FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, 2008; 74
FR 32448, July 8, 2009]

§ 180.519 Bromide ion and residual bromine; tolerances for residues.
top

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(a) General. The food additives, bromide ion and residual bromine, may be present in water, potable in
accordance with the following conditions:
(1) The food additives are present as a result of treating water aboard ships with a polybrominated ionexchange resin (as a source of bromine) under the supervision of trained personnel.
(2) Residual bromine levels are controlled to not exceed 1.0 part per million (ppm) in the final treated
water. Control is effected using calibrated recirculating or proportioning bromine feeder equipment and
periodic checks of residual bromine using a bromine test kit. To assure safe use of the additives, the label
and labeling of the disinfectant formulation containing the food additives shall conform to the label and
labeling registered by the U.S. Environmental Protection Agency.
(3) No tolerance is established for bromide ion levels.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[41 FR 17893, Apr. 29, 1976. Redesignated at 41 FR 26568, June 28, 1976, and at 53 FR 24667, June
29, 1988. Redesignated and amended at 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. 13, 2006]

§ 180.521 Fumigants for grain-mill machinery; tolerances for residues.
top
(a) General. Fumigants may be safely used in or on grain-mill machinery in accordance with the following
prescribed conditions:
(1) The fumigants consist of methyl bromide.
(2) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling
registered by the U.S. Environmental Protection Agency.
(3) Residues of inorganic bromides (calculated as Br) in milled fractions derived from cereal grain from all
fumigation sources, including fumigation of grain-mill machinery, shall not exceed 125 parts per million.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, as amended at 49 FR 44459,
Nov. 7, 1984. Further redesignated at 53 FR 24667, June 29, 1988, as amended at 54 FR 6130, Feb. 8,
1989. Further redesignated and amended at 63 FR 34319, June 24, 1998]

§ 180.522 Fumigants for processed grains used in production of fermented malt
beverage; tolerances for residues.
top
(a) General . Fumigants for processed grain may be safely used, in accordance with the following
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conditions.
(1) Methyl bromide. Total residues of inorganic bromides (calculated as Br) from the use of this fumigant
shall not exceed 125 parts per milion.
(2) Methyl bromide is used to fumigate corn grits and cracked rice in the production of fermented malt
beverage.
(3) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling
registered by the U.S. Environmental Protection Agency, and the usage employed should conform with
such label or labeling.
(4) The total residue of inorganic bromides in fermented malt beverage, resulting from the use of corn grits
and cracked rice fumigated with the fumigant described in paragraph (a)(2) of this section plus additional
residues of inorganic bromides that may be present from uses in accordance with other regulations in this
chapter promulgated under section 408 and/or 409 of the Act, does not exceed 25 parts per million
bromide (calculated as Br).
(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 74818, Dec. 13, 2006]

§ 180.523 Metaldehyde; tolerances for residues.
top
(a) General . Tolerances are established for residues of the molluscicide metaldehyde in or on food
commodities, as follows:

Commodity

Parts per million

Artichoke, globe

0.07

Berry group 13

0.15

Cactus

0.07

Fruit, citrus, group 10

0.26

Lettuce

1.73

Strawberry

6.25

Tomato

0.24

Vegetable, brassica, leafy, group 5

2.5

Watercress

3.2

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54963, Sept. 24, 2008]
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§ 180.525 Resmethrin; tolerances for residues.
top
(a) General . Tolerances are established for residues of the insecticide resmethrin [5-(phenylmethyl)-3furanyl] methyl 2,2-dimethyl-3-(2-methyl-1-propenyl) cyclopropanecarboxylate in or on food commodities
at 3.0 ppm resulting from use of the insecticide in food handling and storage areas as a space
concentration for spot/or crack and crevice treatment and shall be limited to a maximum of 3.00 percent of
the active ingredient by weight, and as a space treatment shall be limited to a maximum of 0.5 fluid ounce
of 3.0 percent active ingredient by weight per 1000 cubic feet of space provided that the food is removed
or covered prior to such use. To assure safe use of the additive, its label and labeling shall conform to that
registered with the U.S. Environmental Protection Agency, and shall be used in accordance with such
label and labeling.
(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 74819, Dec. 13, 2006]

§ 180.526 Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.
top
(a) General. Synthetic isoparaffinic petroleum hydrocarbons complying with 21 CFR 172.882 (a) and (b)
may be safely used as a component of insecticide formulations for use on animal feed in an amount no
greater than reasonably required to accomplish its intended effect as an adjuvant in the insecticide
formulation and shall not be intended to accomplish any effect in animal feed. It is used or intended for use
as a component of insecticide formulations used in compliance with regulations issued in 40 CFR part 180
and in this part.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[40 FR 14161, Mar. 28, 1975, as amended at 50 FR 2959, Jan. 23, 1985, and amended at 53 FR 24668,
24669, June 29, 1988. Redesignated and amended at 63 FR 34319, June 24, 1998]

§ 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)1, 3, 4-thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 4-fluoro-Nmethylethyl benzenamine tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the herbicide flufenacet, N -(4fluorophenyl)- N -(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide and its
metabolites containing the 4-fluoro- N -methylethyl benzenamine moiety in or on the following
commodities.

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Commodity

Parts per million

Cattle, kidney

0.05

Corn, field, forage

0.4

Corn, field, grain

0.05

Corn, field, stover

0.4

Corn, sweet, forage

0.45

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, stover

0.30

Goat, kidney

0.05

Hog, kidney

0.05

Horse, kidney

0.05

Sheep, kidney

0.05

Soybean, seed

0.1

Wheat, bran

0.80

Wheat, forage

6.0

Wheat, grain

0.60

Wheat, hay

1.2

Wheat, straw

0.35

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations . Tolerances are established for combined residues of flufenacet,
N -(4-fluorophenyl)- N -(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide, and its
metabolites containing the 4-fluoro- N -methylethyl benzenamine moiety, with regional registration.

Commodity

Parts per million

Grass, forage

7.0

Grass, hay

0.4

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the
herbicide flufenacet, N -(4-fluorophenyl)- N -(1-methylethyl)-2-[[5-(trifluoromethyl)-1,3,4-thiadiazol-2-yl]oxy]
acetamide and its metabolites containing the 4-fluoro- N -methylethyl benzenamine moiety in or on the
following raw agricultural commodities when present therein as a result of application of flufenacet to the
growing crops in paragraph (a) of this section.

Commodity

Parts per million

Alfalfa, forage

0.1

Alfalfa, hay

0.1

Alfalfa, seed

0.1

Clover, forage

0.1

Clover, hay

0.1

Grain, cereal, group 15, except rice

0.1

Grain, cereal, forage, fodder, and straw, group 16, except rice

0.1

Grass, forage, fodder, and hay, group 17

0.1

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[63 FR 26473, May 13, 1998, as amended by 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, 1999;
65 FR 64366, Oct. 27, 2000; 68 FR 2247, Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR 37696, June
30, 2005; 71 FR 76200, Dec. 20, 2006; 72 FR 26310, May 9, 2007]

§ 180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol methylcarbamate; tolerances for
residues.
top
(a) General. (1) The insecticide 2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate may be safely used in
spot and/or crack and crevice treatments in animal feed handling establishments, including feed
manufacturing and processing establishments, such as stores, supermarkets, dairies, meat slaughtering
and packing plants, and canneries until the tolerance expiration/revocation date of April 26, 2005.
(2) The insecticide 2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate may be safely used in spot and/or
crack and crevice treatments in food handling establishments, including food service, manufacturing and
processing establishments, such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies,
meat slaughtering and packing plants, and canneries until the tolerance expiration/revocation date of April
26, 2005.
(3) To ensure safe use of the additive, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34828, June 26, 1998, as amended at 69 FR 58083, Sept. 29, 2004]

§ 180.532 Cyprodinil; tolerances for residues.
top
(a) General. Tolerances are established for residues of the fungicide cyprodinil, 4-cyclopropyl-6-methyl- Nphenyl-2-pyrimidinamine in or on the following food commodities:

Commodity
Almond
Almond, hulls
Apple, wet pomace

Parts per million
0.02
8.0
0.15

Avocado

1.2

Bean, dry

0.6

Bean, succulent

0.6

Brassica, head and stem, subgroup 5A

1.0

Brassica, leafy greens, subgroup 5B

10.0

Bushberry subgroup 13B

3.0

Caneberry subgroup 13A

10

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Canistel
Cattle, meat byproducts

1.2
0.02

Citrus, dried pulp

8.0

Citrus, oil

340

Fruit, pome

0.1

Fruit, stone

2.0

Goat, meat byproducts

0.02

Grape

2.0

Grape, raisin

3.0

Herb subgroup 19A, dried, except parsley

15.0

Herb subgroup 19A, fresh, except parsley

3.0

Horse, meat byproducts

0.02

Juneberry

3.0

Kiwifruit

1.8

Leafy greens subgroup 4A, except spinach

30

Lemon

0.60

Lime

0.60

Lingonberry

3.0

Longan

2.0

Lychee

2.0

Mango

1.2

Onion, bulb

0.60

Onion, green

4.0

Papaya

1.2

Parsley, dried leaves

170

Parsley, leaves

35

Pistachio

0.10

Pulasan

2.0

Rambutan

2.0

Salal

3.0

Sapodilla

1.2

Sapote, black

1.2

Sapote, mamey

1.2

Sheep, meat byproducts

0.02

Spanish lime

2.0

Star apple

1.2

Strawberry

5.0

Tomatillo

0.45

Tomato

0.45

Tomato, paste

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Turnip, greens

10.0

Vegetable, cucurbit, group 9

0.70

Vegetable, leaves of root and tuber, group 2

10

Vegetable, root, except sugarbeet, subgroup 1B

0.75

Watercress

20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 17706, Apr. 10, 1998]
Editorial Note: ForFederal Registercitations affecting §180.532, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.533 Esfenvalerate; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide esfenvalerate, (( S )-cyano-(3phenoxyphenyl) methyl ( S )-4-chloro-α-(1-methylethyl) benzeneacetate in or on the following raw
agricultural commodities:

Commodity

Parts per million

Artichoke, globe

1.0

Beet, sugar, dried pulp

2.5

Beet, sugar, roots

0.5

Beet, sugar, tops

5.0

Egg

0.03

Kiwifruit

0.5

Kohlrabi

2.0

Lettuce, head

5.0

Mustard greens

5.0

Poultry, fat

0.3

Poultry, meat
Poultry, meat byproducts, except liver

0.03
0.3

Poultry, liver

0.03

Sorghum, forage

10.0

Sorghum, grain, grain

5.0

Sorghum, grain, stover

10.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
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(d) Indirect or inadvertent residues. [Reserved]
[63 FR 23401, Apr. 29, 1998, as amended at 63 FR 48615, Sept. 11, 1998]

§ 180.535 Fluroxypyr 1-methylheptyl ester; tolerances for residues.
top
(a) General. Tolerances are established for combined residues of fluroxypyr 1-methylheptyl ester [1methylheptyl ((4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy)acetate] and its metabolite fluroxypyr [((4amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy)acetic acid] in or on the following raw agricultural commodities.

Commodity
Barley, grain

Parts per million
0.5

Barley, hay

12.0

Barley, hay

20.0

Barley, straw

12.0

Cattle, fat

0.1

Cattle, kidney

1.5

Cattle, meat

0.1

Cattle, meat byproducts

0.1

Corn, field, forage

1.0

Corn, field, grain

0.02

Corn, field, stover

0.5

Corn, sweet, forage

1.0

Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.02
2.0

Fruit, pome, group 11

0.02

Garlic, bulb

0.03

Goat, fat

0.1

Goat, kidney

1.5

Goat, meat

0.1

Goat, meat byproducts

0.1

Grain, aspirated fractions

0.6

Grass, forage

120

Grass, hay

160

Hog, fat

0.1

Hog, kidney

1.5

Hog, meat

0.1

Hog, meat byproducts

0.1

Horse, fat

0.1

Horse, kidney

1.5

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Horse, meat

0.1

Horse, meat byproducts

0.1

Milk

0.3

Millet, forage

12.0

Millet, grain

0.5

Millet, hay

20.0

Millet, proso, straw

12.0

Oat, forage

12.0

Oat, grain

0.5

Oat, hay

20.0

Oat, straw

12.0

Onion, bulb

0.03

Shallot, bulb

0.03

Sheep, fat

0.1

Sheep, kidney

1.5

Sheep, meat

0.1

Sheep, meat byproducts

0.1

Sorghum, grain, forage

2.0

Sorghum, grain, grain

0.02

Sorghum, grain, stover

4.0

Wheat, forage

12.0

Wheat, grain

0.5

Wheat, hay

20.0

Wheat, straw

12.0

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 52169, Sept. 30, 1998, as amended at 64 FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, 2001;
66 FR 47971, Sept. 17, 2001; 67 FR 46884, July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR 75438,
Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; 70 FR 3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, 2005; 71 FR
76204, Dec. 20, 2006; 72 FR 73635, Dec. 28, 2007]

§ 180.536 Triazamate; tolerances for residues.
top
(a) General. Time-limited tolerances are established for the combined residues of triazamate (RH-7988)
ethyl(3-tert-butyl-1-dimethylcarbamoyl-1 H -1,2,4-triazol-5-ylthio)acetate and its metabolite (RH0422) in or
on the following commoditie(s):

Commodity

Parts per million

Expiration/Revocation Date

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Apple

0.1

12/31/01

(b) Section 18 emergency exemptions.
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 71026, Dec. 23, 1998]

§ 180.537 Isoxaflutole; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of isoxaflutole 5-cyclopropyl-4-(2methylsulfonyl-4-trifluoromethylbenzoyl) isoxazole and its metabolite 1-(2-methylsulfonyl-4trifluoromethylphenyl)-2-cyano-3-cyclopropyl propan-1,3-dione (RPA 202248), calculated as the parent
compound, in or on the following raw agricultural commodities:

Commodity

Parts per million

Corn, field, forage

0.04

Corn, field, grain

0.02

Corn, field, stover

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 50784, Sept. 23, 1998, as amended at 73 FR 75608, Dec. 12, 2008]

§ 180.538 Copper; tolerances for residues.
top
(a) General . A tolerance of 1 part per million is established in water, potable for residues of copper
resulting from the use of the algicides or herbicides basic copper carbonate (malachite), copper sulfate,
copper monoethanolamine, and copper triethanolamine to control aquatic plants in reservoirs, lakes,
ponds, irrigation ditches, and other potential sources of potable water.
(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 74819, Dec. 13, 2006]

§ 180.539 d-Limonene; tolerances for residues.

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(a) General. (1) The insecticide d-limonene may be safely used in insect-repellent tablecloths and in insectrepellent strips used in food- or feed-handling establishments.
(2) To assure safe use of the insect repellent, its label and labeling shall conform to that registered by the
U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33715, May 24, 2000, as amended at 70 FR 55268, Sept. 21, 2005]

§ 180.540 Fenitrothion; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide fenitrothion, O,O -dimethyl O -(4nitro- m -tolyl) phosphorothioate, from the postharvest application of the insecticide to stored wheat in
Australia, in or on the following food commodity:

Commodity

Parts per million

Wheat, gluten1
1There

3.0

are no U.S. registrations on food commodities since 1987.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 54963, Sept. 24, 2008]

§ 180.541 Propetamphos; tolerances for residues.
top
(a) A tolerance of 0.1 part per million is established for residues of the insecticide propetamphos ([(e)-]methylethyl 3-[[(ethylamino) methoxyphosphinothioyl]oxy]-2-butenoate]) in food commodities exposed to
the insecticide during treatment of food- or feed-handling establishments.
(1) Direct application shall be limited solely to spot and/or crack and crevice treatment in food-handling
establishments where food and food products are held, processed, prepared, or served. Spray and dust
concentrations shall be limited to a maximum of 1 percent active ingredient. For crack and crevice
treatment, equipment capable of delivering a dust or a pin-stream of spray directly into cracks and
crevices shall be used. For spot treatment, a coarse, low-pressure spray shall be used to avoid
contamination of food or food-contact surfaces.

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(2) Direct application shall be limited solely to spot and/or crack and crevice treatment in feed-handling
establishments where feed and feed products are held, processed, prepared, or sold. Spray and dust
concentrations shall be limited to a maximum of 1 percent active ingredient. For crack and crevice
treatment, equipment capable of delivering a dust or a pinstream of spray directly into cracks and crevices
shall be used. For spot treatment, a coarse, low-pressure spray shall be used to avoid contamination of
feed or feed-contact surfaces.
(3) To ensure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33716, May 24, 2000]

§ 180.543 Diclosulam; tolerances for residues.
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(a) General. Tolerances are established for residues of the herbicide diclosulam [ N -(2,6-dichlorophenyl)5-ethoxy-7-fluoro[1,2,4] triazolo[1,5- c ]pyrimidine-2-sulfonamide] in or on the following raw agricultural
commodities as follows:

Commodity

Parts per
million

Peanut

0.020

Soybean, seed

0.020

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 12134, Mar. 8, 2000]

§ 180.544 Methoxyfenozide; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of the insecticide methoxyfenozide per se;
benzoic acid, 3-methoxy-2-methyl-, 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide in or on the
following food commodities:

Commodity
Acerola
Almond, hulls
Animal feed, nongrass, group 18, forage
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Parts per million
0.4
25
50.0

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Animal feed, nongrass, group 18, hay

150.0

Apple, wet pomace

7.0

Artichoke, globe

3.0

Avocado

0.6

Bean, dry, seed
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

0.24
7.0
30

Bushberry subgroup 13-07B

3.0

Canistel

0.6

Cattle, fat

0.50

Cattle, meat

0.02

Coriander, leaves

30

Corn, field, forage

15

Corn, field, grain

0.05

Corn, field, refined oil

0.20

Corn, field, stover

125

Corn, pop, grain

0.05

Corn, pop, stover

125

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed

30
0.05

Corn, sweet, stover

60

Cotton, gin byproducts

35

Cotton, undelinted seed

2.0

Cranberry

0.5

Feijoa

0.4

Fruit, pome, group 11

1.5

Fruit, stone, group 12, except plum, prune, fresh

3.0

Goat, fat

0.50

Goat, meat

0.02

Grain, aspirated fractions

2.0

Grape

1.0

Grape, raisin

1.5

Grass, forage, fodder and hay, group 17, forage

18.0

Grass, forage, fodder and hay, group 17, hay

30.0

Guava

0.4

Hog, fat

0.1

Hog, meat

0.02

Horse, fat

0.50

Horse, meat

0.02

Jaboticaba

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Leaf petioles subgroup 4B

25

Leafy greens subgroup 4A

30

Longan

2.0

Lychee

2.0

Mango

0.6

Milk

0.10

Nut, tree, group 14

0.10

Okra

2.0

Onion, green, subgroup 3-07B

5.0

Papaya

0.6

Passionfruit

0.4

Pea and bean, succulent shelled, subgroup 6B

0.2

Pea, blackeyed, seed

4.0

Pea, dry seed

2.5

Pea, southern, seed

4.0

Peanut

0.02

Peanut, hay

55.0

Peanut, oil

0.04

Peppermint, tops

7.0

Pistachio

0.10

Plum, prune, fresh

0.30

Pomegranate

0.6

Poultry, fat

0.02

Poultry, meat

0.02

Pulasan

2.0

Rambutan

2.0

Sapodilla

0.6

Sapote, black

0.6

Sapote, mamey

0.6

Sheep, fat

0.50

Sheep, meat

0.02

Soybean, aspirated grain fractions

160

Soybean, forage

30

Soybean, hay

80

Soybean, hulls

2.0

Soybean, seed

1.0

Spanish lime

2.0

Spearmint, tops

7.0

Star apple

0.6

Starfruit

0.4

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Strawberry

1.5

Turnip, greens

30

Vegetable, cucurbit, group 9

0.3

Vegetable, foliage of legume, except soybean, subgroup 7A

35

Vegetable, fruiting, group 8

2.0

Vegetable, leaves of root and tuber, group 2

30

Vegetable, legume, edible podded, subgroup 6A

1.5

Vegetable, root, subgroup 1A

0.5

Vegetable, tuberous and corm, except potato, subgroup 1D

0.02

Wax jambu

0.4

(2) For combined residues of the insecticide methoxyfenozide; benzoic acid, 3-methoxy-2-methyl-, 2-(3,5dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide and its glucuronide metabolite RH-141,518; β-DGlucopyranuronic acid, 3-[2-(1,1-dimethylethyl)-2-(3,5-dimethylbenzoyl)-hydrazino]carbonyl-2methylphenyl-] in the following commodities:

Commodity

Parts per million

Cattle, liver

0.40

Cattle, meat byproducts, except liver

0.10

Egg

0.02

Goat, liver

0.40

Goat, meat byproducts, except liver

0.10

Hog, liver

0.1

Hog, meat byproducts, except liver

0.02

Horse, liver

0.40

Horse, meat byproducts, except liver

0.10

Poultry, liver

0.10

Poultry, meat byproducts, except liver

0.02

Sheep, liver

0.40

Sheep, meat byproducts, except liver

0.10

(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for residues of the insecticide methoxyfenozide per se (benzoic acid, 3-methoxy-2-methyl-,2(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide), in or on the specified agricultural commodities,
resulting from use of the pesticide pursuant to FFIFRA section 18 emergency exemptions. The tolerances
expire and will be revoked on the date specified in the table.

Commodity

Parts per million

Expiration/revocation date

Sorghum, forage

30.0

12/31/12

Sorghum, grain

0.05

12/31/12

Sorghum, stover

60.0

12/31/12

(c) Tolerances with regional registrations . Tolerances are established for residues of the insecticide
methoxyfenozide, including its metabolites and degradates. Compliance with the tolerance levels specified
in this paragraph is to be determined by measuring only methoxyfenozide, benzoic acid, 3-methoxy-2http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c...&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (432 of 651) [9/8/2009 3:02:25 PM]

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methyl-, 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide.

Commodity

Parts per million

Citrus, Oil

100

Fruit, citrus, group 10

10

(d) Indirect or inadvertent residues. (1) Tolerances are established for the indirect or inadvertent residues
of the insecticide methoxyfenozide per se; benzoic acid, 3-methoxy-2-methyl-, 2-(3,5-dimethylbenzoyl)-2(1,1-dimethylethyl) hydrazide in or on the following raw agricultural commodities, when present therein as
a result of the application of methoxyfenozide to growing crops as listed in paragraph (a) of this section:

Commodity

Parts per million Expiration/revocation date

Vegetable, bulb, group 3-07

0.20

09/30/10

Vegetable, leaves of root and tuber,
group 2

0.20

09/30/10

Vegetable, root and tuber, group 1

0.10

09/30/10

(2) Tolerances are established for the indirect or inadvertent combined residues of methoxyfenozide;
benzoic acid, 3-methoxy-2-methyl-, 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide and its
metabolites RH-117,236 free phenol of methoxyfenozide; 3,5-dimethylbenzoic acid N -tert-butyl- N ′-(3hydroxy-2-methylbenzoyl) hydrazide, RH-151,055 glucose conjugate of RH-117,236; 3,5-dimethyl benzoic
acid N -tert-butyl- N -[3 (β-D-glucopyranosyloxy)-2-methylbenzoyl]-hydrazide and RH-152,072 the
malonylglycosyl conjugate of RH 117,236 in or on the following raw agricultural commodities, when
present therein as a result of the application of methoxyfenozide to growing crops as listed in paragraph
(a) of this section:

Commodity

Parts per million Expiration/revocation date

Animal feed, non-grass, group 18

10.0

09/30/10

Grain, cereal, forage, fodder and
straw, group 16

10.0

09/30/10

Grass, forage, fodder and hay, group
17

10.0

09/30/10

Herb and spice, group 19

10.0

09/30/10

Vegetable, foliage of legume, group 7

10.0

09/30/10

Vegetable, legume, group 6

0.10

09/30/10

[67 FR 59203, Sept. 20, 2002, as amended at 68 FR 32389, May 30, 2003; 68 FR 37765, June 25, 2003;
69 FR 58097, Sept. 29, 2004; 70 FR 7047, Feb. 10, 2005; 70 FR 51604, Aug. 31, 2005; 70 FR 75739,
Dec. 21, 2005; 71 FR 32853, June 7, 2006; 73 FR 11826, Mar. 5, 2008; 74 FR 22468, May 13, 2009; 74
FR 45335, Sept. 2, 2009]

§ 180.545 Prallethrin ( RS
(1 RS
)- cis, trans
residues.

)-2-methyl-4-oxo-3-(2-propynyl)cyclopent-2-enyl
-chrysanthemate; tolerances for

top
(a) General. (1) A tolerance of 1.0 ppm is established for residues of the insecticide prallethrin ( RS )-2methyl-4-oxo-3-(2-propynyl)cyclopent-2-enyl (1 RS )- cis, trans -chrysanthemate as follows:

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(2) In or on food commodities in food handling establishments where food and food products are held,
processed, prepared and/or served.
(3) Application shall be limited to space, general surface, and spot and/or crack and crevice treatment in
food handling establishments where food and food products are held, processed, prepared and/or served.
General surface or space spray applications may be used only when the facility is not in operation
provided exposed food has been covered or removed from the area being treated prior to application. Spot
and/or crack and crevice application may be used while the facility is in operation provided exposed food
is covered or removed from the area being treated prior to application. Spray concentrate shall be limited
to a maximum of 2.0% active ingredient. Contamination of food or food contact surfaces shall be avoided.
Food contact surfaces and equipment should be throughly washed with an effective cleaning compound
and rinsed with potable water after use of the product.
(4) To assure safe use of the additive, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 39313, June 26, 2000, as amended at 71 FR 74819, Dec. 13, 2006]

§ 180.546 Mefenoxam; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of ( R )- and ( S )-2-[(2,6-dimethyl
(phenyl)-methoxyacetylamine]-propionic acid methyl ester, and its metabolites containing the 2,6
dimethylaniline moiety, and N -(2-hydroxy methyl-6-methylphenyl)- N -(methoxyacetyl)-alanine methyl
ester, each expressed as mefenoxam equivalents, in or on the following food commodities:

Commodity

Parts per million

Artichoke, globe

0.05

Atemoya

0.20

Canistel

0.40

Custard apple

0.20

Herbs, dried

55

Herbs, fresh

8.0

Kiwifruit
Lingonberry

0.10
2.0

Mango

0.40

Papaya

0.40

Sapodilla

0.40

Sapote, black

0.40

Sapote, mamey

0.40

Star apple

0.40

Starfruit

0.20

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Sugar apple

0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[65 FR 57556, Sept. 25, 2000, as amended at 66 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, 2002]

§ 180.547 Prohexadione calcium; tolerances for residues.
top
(a) General. Tolerances are established for residues of the plant growth regulator, prohexadione calcium
(calcium 3-oxido-5-oxo-4-propionylcyclohex-3-enecarboxylate) in or on the following raw agricultural
commodities:

Commodity

Parts per
million

Cattle, kidney

0.10

Cattle, meat byproducts, except kidney

0.05

Fruit, pome, group 11

3.0

Goat, kidney

0.10

Goat, meat byproducts, except kidney

0.05

Grass, forage1

0.10

Grass, hay1

0.10

Grass, seed screenings1

3.5

Grass, straw1

1.2

Hog, kidney

0.10

Hog, meat byproducts, except kidney

0.05

Horse, kidney

0.10

Horse, meat byproducts, except kidney

0.05

Peanut

1.0

Peanut, hay

0.60

Sheep, kidney

0.10

Sheep, meat byproducts, except kidney

0.05

1Registration

is limited to grass grown for seed.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[65 FR 25660, May 3, 2000, as amended at 66 FR 29712, June 1, 2001]

§ 180.548 Tralkoxydim; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide, tralkoxydim, 2-Cyclohexen-1-one, 2[1-(ethoxyimino)propyl]-3-hydroxy-5-(2,4,6-trimethylphenyl)-(9Cl) in or on the raw agricultural commodities:

Commodity

Parts per million

Barley, grain

0.02

Barley, hay

0.02

Barley, straw

0.05

Wheat, forage

0.05

Wheat, grain

0.02

Wheat, hay

0.02

Wheat, straw

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 69199, Dec. 16, 1998, as amended at 68 FR 48302, Aug. 13, 2003; 70 FR 70739, Nov. 23, 2005]

§ 180.549 Diflufenzopyr; tolerances for residues.
top
(a) General. Tolerances are established for combined residues of diflufenzopyr, 2-(1-[([3,5difluorophenylamino] carbonyl)hydrazono]ethyl)-3- pyridinecarboxylic acid, and its metabolites convertible
to 8- methylpyrido[2,3-d]pyridazin-5(6H)-one, expressed as diflufenzopyr, in or on the following raw
agricultural commodities:

Commodity

Parts per million

Corn, field, forage

0.05

Corn, field, grain

0.05

Corn, field, stover

0.05

Corn, pop, grain

0.05

Corn, pop, stover

0.05

Corn, sweet, forage

0.05

Corn, sweet, kernel plus cob with husks removed

0.05

Corn, sweet, stover

0.05

Grass, forage

22.0

Grass, hay

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(2) Time-limited tolerances are established for combined residues of diflufenzopyr, 2-(1-[([3,5difluorophenylamino] carbonyl)hydrazono]ethyl)-3- pyridinecarboxylic acid, its metabolites convertible to 8methylpyrido[2,3- d]pyridazin- 5(6H)-one, and free and acid-released 8- hydroxymethylpyrido[2,3-d]
pyridazine-2,5(1H,6H)-dione, expressed as diflufenzopyr, in or on the following raw agricultural
commodities:

Commodity

Parts per million Expiration/Revocation Date

Cattle, fat

0.30

7/31/05

4.0

7/31/05

Cattle, meat

0.60

7/31/05

Cattle, meat byproducts, except
kidney

0.50

7/31/05

Goat, fat

0.30

7/31/05

4.0

7/31/05

Goat, meat

0.60

7/31/05

Goat, meat byproducts, except
kidney

0.50

7/31/05

Hog, fat

0.30

7/31/05

4.0

7/31/05

Hog, meat

0.60

7/31/05

Hog, meat byproducts, except kidney

0.50

7/31/05

Horse, fat

0.30

7/31/05

4.0

7/31/05

Horse, meat

0.60

7/31/05

Horse, meat byproducts, except
kidney

0.50

7/31/05

3.0

7/31/05

0.30

7/31/05

4.0

7/31/05

Sheep, meat

0.60

7/31/05

Sheep, meat byproducts, except
kidney

0.50

7/31/05

Cattle, kidney

Goat, kidney

Hog, kidney

Horse, kidney

Milk
Sheep, fat
Sheep, kidney

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 4308, Jan. 28, 1999, as amended at 67 FR 55338, Aug. 29, 2002]

§ 180.550 Arsanilic acid [(4-aminophenyl) arsonic acid]; tolerances for residues.
top
(a) General. A time-limited tolerance is established for residues of the plant growth regulator arsanilic acid
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[(4-aminophenyl) arsonic acid], in or on the following food commodities in connection with the use of the
pesticide under section 5 experimental use permit. The tolerance will expire on the date specified in the
following table:

Commodity
Grapefruit

Parts per million

Expiration/revocation date

2 (not to exceed 0.7 ppm total arsenic)

2/28/01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 14639, Mar. 26, 1999]

§ 180.551 Fluthiacet-methyl; tolerances for residues.
top
(a) General. (1) A tolerance is established for residues of the herbicide, fluthiacet-methyl, acetic acid [[2chloro-4-fluoro-5-[(tetrahydro-3-oxo-1 H ,3 H -[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]
thio]-methyl ester, in or on the food commodity:

Commodity

Parts per million

Corn, field, forage

0.050

Corn, field, grain

0.010

Corn, field, stover

0.050

Corn, pop, grain

0.010

Corn, pop, stover

0.050

Corn, sweet, forage

0.050

Corn, sweet, kernel plus cob with husks removed

0.010

Corn, sweet, stover

0.050

Soybean, seed

0.01

(2) A tolerance is established for the combined residues of the herbicide fluthiacet-methyland its acid
metabolite: acetic acid, [[2-chloro-4-fluoro-5-[tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1ylidene)amino]phenyl]thio]-methyl ester, and its acid metabolite, acetic acid, [[2-chloro-4-fluoro-5[(tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]- , in or on the
following food commodities:

Commodity

Parts per million

Cotton, gin byproducts

0.20

Cotton, undelinted seed

0.020

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[64 FR 18357, Apr. 14, 1999, as amended at 66 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, 2006]

§ 180.552 Sulfosulfuron; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide sulfosulfuron, 1–(4,6dimethoxypyrimidin-2-yl)-3-[(2-ethanesulfonyl-imidazo[1,2-a]pyridine-3-yl) sulfonyl]urea and its metabolites
converted to 2-(ethylsulfonyl)-imidazo[1,2-a]pyridine and calculated as sulfosulfuron in or on the raw
agricultural commodities.

Commodity

Parts per million

Cattle, fat

0.02

Cattle, meat

0.01

Cattle, meat byproducts

0.3

Goat, fat

0.02

Goat, meat

0.01

Goat, meat byproducts

0.3

Grass, forage, fodder and hay, group 17, forage

14

Grass, forage, fodder and hay, group 17, hay

25

Hog, fat

0.005

Hog, meat

0.005

Hog, meat byproducts

0.05

Horse, fat

0.02

Horse, meat

0.01

Horse, meat byproducts

0.3

Milk

0.02

Sheep, fat

0.02

Sheep, meat

0.01

Sheep, meat byproducts

0.3

Wheat, forage

4.0

Wheat, grain

0.02

Wheat, hay

0.3

Wheat, straw

0.1

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 27192, May 19, 1999, as amended at 70 FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, 2007]

§ 180.553 Fenhexamid; tolerances for residues.
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(a) General. Tolerances are established for the residues of the fungicide fenhexamid (N-2,3-dichloro-4hydroxyphenyl)-1-methyl cyclohexanecarboxamide) in or on the following commodities:

Commodity
Almond, hulls

Parts per million
2.0

Almond

0.02

Asparagus

0.02

Bushberry subgroup 13B

5.0

Caneberry subgroup 13A

20.0

Cilantro, leaves

30.0

Cucumber
Fruit, stone, group 12, except plum, prune, fresh, postharvest

2.0
10.0

Ginseng

0.3

Grape

4.0

Grape, raisin

6.0

Juneberry

5.0

Kiwifruit, postharvest

15.0

Leafy greens subgroup 4A, except spinach

30.0

Lingonberry
Pear

5.0
10

Pepper, nonbell

0.02

Pistachio

0.02

Plum, prune, dried

2.5

Plum, prune, fresh

1.5

Pomegranate

2.0

Salal

5.0

Strawberry

3.0

Vegetable, fruiting, group 8, except nonbell pepper

2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 28924, May 28, 1999, as amended at 65 FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, 2000;
67 FR 19120, Apr. 18, 2002; 68 FR 2247, Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR 15617, Mar.
29, 2006; 71 FR 43664, Aug. 2, 2006; 73 FR 19154, Apr. 9, 2008]

§ 180.554 Kresoxim-methyl; tolerances for residues.
top
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(a) General. (1) Tolerances are established for the combined residues of the fungicide kresoxim-methyl
(methyl ( E )-2-[2-(2-methylphenoxy)-methyl]phenyl-2-(methoxyimido)acetate) and its metabolites as
follows: ( E )-2-[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid; ( E )-2-[2-(2hydroxymethylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid (free and glucose conjugated); and
( E )-2-[2-(4-hydroxy-2-methylphenoxy)-methyl]phenyl-2-(methoxyimido)acetic acid (free and glucose
conjugated) in or on the following commodities:

Commodity

Parts per million

Apple, pomace

1.0

Fruit, pome

0.5

Grape

1.0

Grape, raisin

1.5

Pecan

0.15

Vegetable, cucurbit, group 9

0.40

(2) Tolerances are established in or on the following commodities for the residues of the metabolite ( E )-2[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid resulting from the use of the fungicide
kresoxim-methyl:

Commodity

Parts per million

Cattle, meat byproducts

0.01

Goat, meat byproducts

0.01

Sheep, meat byproducts

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 31136, June 10, 1999, as amended at 71 FR 50359, Aug. 25, 2006]

§ 180.555 Trifloxystrobin; tolerances for residues.
top
(a) General. Tolerances are established for combined residues of trifloxystrobin (Benzeneacetic acid, ( E,
E )-α-(methoxyimino)-2-[[[[1-[3-(trifluoromethyl) phenyl]ethylidene]amino]oxy]methyl]-, methyl ester) and
the free form of its acid metabolite CGA–321113 (( E,E )-methoxyimino-[2-[1-(3-trifluoromethyl-phenyl)ethylideneaminooxymethyl]-phenyl]acetic acid in or on the following commodities.

Commodity
Almond, hulls
Almond
Apple, wet pomace
Asparagus

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Parts per million
3.0
0.04
5.0
0.07

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Banana1

0.10

Barley, grain

0.05

Barley, hay

0.3

Barley, straw

5.0

Beet, sugar, dried pulp

0.4

Beet, sugar, molasses

0.2

Beet, sugar, roots

0.1

Beet, sugar, tops

4.0

Canistel

0.7

Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Citrus, dried pulp
Citrus, oil

1.0
38

Corn, field, forage

0.2

Corn, field, grain

0.05

Corn, field, stover
Corn, field, refined oil
Corn, pop, grain
Corn, pop, stover

7
0.1
0.05
7

Corn, sweet, cannery waste

0.6

Corn, sweet, forage

0.6

Corn, sweet, kernel plus cob with husks removed

0.04

Corn, sweet, stover

0.25

Egg

0.04

Fruit, citrus, group 10

0.6

Fruit, pome

0.5

Fruit, stone, group 12

2

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Grain, aspirated fractions

5.0

Grape

2.0

Grape, raisin

5.0

Grass, forage

12

Grass, hay

17

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.05

Hop, dried cones

11.0

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Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Leaf petioles subgroup 4B

3.5

Mango

0.7

Milk

0.02

Nut, tree, group 14

0.04

Oat, forage

0.3

Oat, grain

0.05

Oat, hay

0.3

Oat, straw

5.0

Papaya

0.7

Peanut, hay

4.0

Peanut

0.05

Pistachio

0.04

Potato

0.04

Poultry, fat

0.04

Poultry, meat

0.04

Poultry, meat byproducts

0.04

Radish, tops

10

Rice, grain

3.5

Rice, hulls

8

Rice, straw

7.5

Sapodilla

0.7

Sapote, black

0.7

Sapote, mamey

0.7

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

Soybean, forage

10.0

Soybean, hay

25.0

Soybean, seed

0.08

Star apple

0.7

Strawberry

1.1

Vegetable, cucurbit, group 9

0.50

Vegetable, fruiting

0.5

Vegetable, root, except sugar beet, subgroup 1B

0.1

Vegetable, root, except sugar beet, subgroup 1B, except radish

0.10

Wheat, bran

0.15

Wheat, forage

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Wheat, grain

0.05

Wheat, hay

0.2

Wheat, straw

5.0

1There

are no U.S. registrations as of September 27, 1999 for use on banana.

(b) Section 18 emergency exemptions. Time-limited tolerances are established for combined residues of
the fungicide trifloxystrobin, (benzeneacetic acid, (E,E)-[alpha]-(methoxyimino)-2- [[[[1-[3-(trifluoromethyl)
phenyl] ethylidene]amino]oxy]methyl]-,methylester) and the free form of its acid metabolite CGA–321113
((E,E)-methoxyimino-[2-[1-(3-trifluoromethylphenyl) ethylideneaminooxymethyl]- phenyl]acetic acid) in
connection with the use of the pesticide under FIFRA section 18 emergency exemptions granted by EPA.
The tolerances will expire and are revoked on the date specified in the table in this unit.

Commodity

Parts per million

Expiration/revocation date

Soybean, forage

4.0

12/31/09

Soybean, hay

6.5

12/31/09

Soybean, seed

0.04

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 51907, Sept. 27, 1999, as amended at 65 FR 44453, July 18, 2000; 67 FR 35924, May 22, 2002;
68 FR 53304, Sept. 10, 2003; 70 FR 36532, June 24, 2005; 71 FR 15604, Mar. 29, 2006; 71 FR 55319,
Sept. 22, 2006; 72 FR 53445, Sept. 19, 2007; 73 FR 57, Jan. 2, 2008]

§ 180.556 Pymetrozine; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide pymetrozine 1,2,4-triazin-3(2H)one,4,5-dihydro-6-methyl-4-[(3-pyridinylmethylene) amino] in or on the following raw agricultural
commodities. The tolerance level for each commodity is expressed in terms of the parent insecticide only,
which serves as an indicator of the use of pymetrozine on these raw agricultural commodities.

Commodity
Asparagus
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

Parts per million
0.04
0.5
0.25

Cotton, gin byproducts

2.0

Cotton, undelinted seed

0.3

Hop, dried cones

6.0

Pecan

0.02

Turnip, greens

0.25

Vegetable, fruiting, group 8

0.2

Vegetable, cucurbit, group 9

0.1

Vegetable, leafy, execpt brassica, group 4

0.6

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Vegetable, tuberous and corm, subgroup 1C

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 48634, Aug. 9, 2000, as amended at 66 FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, 2001; 70
FR 7047, Feb. 10, 2005; 70 FR 43298, July 27, 2005]

§ 180.557 Tetraconazole; tolerances for residues.
top
(a) General . Tolerances are established for residues of the fungicide, tetraconazole, 1-[2-(2,4dichlorophenyl)-3-(1,1,2,2-tetrafluoroethoxy)propyl]-1 H -1,2,4-triazole in or on the following commodities:

Commodity
Aspirated grain fractions

Parts per million
1.0

Beet sugar, dried pulp

0.15

Beet sugar, molasses

0.15

Beet sugar, root

0.05

Cattle, fat

0.02

Cattle, liver

0.20

Cattle, meat

0.01

Cattle, meat byproducts (except liver)

0.01

Eggs

0.02

Goat, fat

0.02

Goat, liver

0.20

Goat, meat

0.01

Goat, meat byproducts (except liver)

0.01

Grape

0.20

Hog, fat

0.01

Hog, liver

0.05

Hog, meat

0.01

Hog, meat byproducts (except liver)

0.01

Horse, fat

0.02

Horse, liver

0.20

Horse, meat

0.01

Horse, meat byproducts (except liver)

0.01

Milk

0.01

Milk, fat

0.25

Peanut

0.03

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Peanut, oil

0.10

Pecan

0.04

Poultry, fat

0.05

Poultry, meat

0.01

Poultry meat byproducts

0.01

Sheep, fat

0.02

Sheep, liver

0.20

Sheep, meat

0.01

Sheep, meat byproducts (except liver)

0.01

Soybean, refined oil

0.80

Soybean, seed

0.15

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[70 FR 20830, Apr. 22, 2005, as amended at 70 FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, 2007; 73
FR 67406, Nov. 14, 2008]

§ 180.558 N,N
tolerances for residues.

-diethyl-2-(4-methylbenzyloxy)ethylamine hydrochloride;

top
(a) General. A tolerance for residues of the plant growth regulator N,N- diethyl-2-(4-methylenzyloxy)
ethylamine hydrochloride in or on raw agricultural commodities is established as follows:

Commodity

Parts per million

Orange, sweet

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 1814, Jan. 12, 2000]

§ 180.559 Clodinafop-propargyl; tolerances for residues.
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(a) General. Tolerances are established for combined residues of clodinafop-propargyl (propanoic acid, 2[4-(5-chloro-3-fluoro-2-pyridinyl)oxy]phenoxy]-,2-propynyl ester, (2R)-) and its acid metabolite (propanoic
acid, 2-[4-[(5-chloro-3-fluoro-2-pyridinyl)oxy]phenoxy]-, (2R)-), in or on wheat, grain at 0.1 ppm ; wheat,
forage at 0.1 ppm; wheat, hay at 0.1 ppm; and wheat, straw at 0.50 ppm.

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Commodity

Parts per million

Wheat, forage

0.1

Wheat, grain

0.1

Wheat, hay

0.1

Wheat, straw

0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 38774, June 22, 2000]

§ 180.560 Cloquintocet-mexyl; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of cloquintocet-mexyl (acetic acid [(5chloro-8-quinolinyl) oxy]-, 1-methylhexyl ester; CAS Reg. No. 99607–70–2) and its acid metabolite (5chloro-8-quinlinoxyacetic acid) when used as an inert ingredient (safener) in pesticide formulations
containing the active ingredients pinoxaden (wheat or barley), clodinafop-propargyl (wheat only), or
pyroxsulum (wheat only) in or on the following food commodities:

Commodity

Parts per million

Barley, grain

0.1

Barley, hay

0.1

Barley, straw

0.1

Wheat, forage

0.2

Wheat, grain

0.1

Wheat, hay

0.5

Wheat, straw

0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 38764, June 22, 2000, as amended at 70 FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, 2008]

§ 180.561 Acibenzolar- S

-methyl; tolerances for residues.

top
(a) General. (1) Tolerances are established for residues of acibenzolar-S-methyl, benzo(1,2,3)thiadiazole7-carbothioic acid-S-methyl ester, in or on the following raw agricultural commodities:

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Commodity

Parts per million

Banana1

0.1

Spinach

1.0

Tomato, paste

3.0

Vegetable, brassica, leafy, group 5

1.0

Vegetable, fruiting, group 8

1.0

Vegetable, leafy, group 4
1There

0.25

are no United States registrations for banana.

(2) Tolerances are established for residues of acibenzolar-S-methyl, benzo(1,2,3)thiadiazole-7-carbothioic
acid-S-methyl ester, including its metabolites and degradates, in or on the commodities in the table below.
Compliance with the tolerance levels specified below is to be determined by measuring only those
acibenzolar-S-methyl residues convertible to benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA-210007),
expressed as the stoichiometric equivalent of acibenzolar-S-methyl, in or on the commodity.

Commodity

Parts per million

Onion, bulb, subgroup 3–07A

0.1

Vegetable, cucurbit, group 9

2.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of
acibenzolar- S -methyl, benzo(1,2,3)thiadiazole-7-carbothioic acid- S -methyl ester in connection with use
of the pesticide under section 18 emergency exemptions granted by EPA. The time-limited tolerances will
expire and are revoked on the date specified in the following table:

Commodity

Parts per million

Onion, green

Expiration/revocation date

0.05

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 50446, Aug. 18, 2000, as amended at 70 FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, 2006; 74
FR 24710, May 26, 2009]

§ 180.562 Flucarbazone-sodium; tolerances for residues.
top
(a) General . Tolerances are established for combined residues of the herbicide flucarbazone-sodium, 4,5dihydro-3-methoxy-4-methyl-5-oxo-N-[[2(trifluoromethoxy)phenyl] sulfonyl]-1H-1,2,4-triazole 1carboxamide, sodium salt) and its N-desmethyl metabolite; and its metabolites converted to 2(trifluoromethoxy)benzene sulfonamide and calculated as flucarbazone-sodium in or on the following food
commodities:

Commodity

Parts per million

Cattle, liver

1.50

Cattle, meat

0.01

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Cattle, meat byproducts, except liver

0.01

Goat, liver

1.50

Goat, meat

0.01

Goat, meat byproducts, except liver

0.01

Hog, liver

1.50

Hog, meat

0.01

Hog, meat byproducts, except liver

0.01

Horse, liver

1.50

Horse, meat

0.01

Horse, meat byproducts, except liver

0.01

Milk

0.005

Sheep, liver

1.50

Sheep, meat

0.01

Sheep, meat byproducts, except liver

0.01

Wheat, forage

0.30

Wheat, grain

0.01

Wheat, hay

0.10

Wheat, straw

0.05

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertant residues . [Reserved]
[70 FR 67915, Nov. 9, 2005, as amended at 71 FR 76931, Dec. 22, 2006]

§ 180.563 Ethametsulfuron-methyl; tolerances for residues.
top
(a) General. A tolerance is established for residues of ethametsulfuron methyl (methyl 2- ((((4-ethoxy-6(methylamino)-1,3,5- triazin-2-yl) amino) carbonyl) amino) sulfonyl) benzoate) in or on the following raw
agricultural commodities.

Commodity

Parts per million

Canola, seed

0.02

Crambe, seed

0.02

Rapeseed, seed

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect of inadvertent residues. [Reserved]

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[65 FR 57972, Sept. 27, 2000, as amended at 66 FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, 2002]

§ 180.564 Indoxacarb; tolerances for residues.
top
(a) General. Tolerances are established for residues of indoxacarb, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only indoxacarb, (S)-methyl 7-chloro-2,5-dihydro-2[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2- e ][1,3,4][oxadiazine-4a(3 H )carboxylate, and its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2- e ][1,3,4][oxadiazine-4a(3 H )-carboxylate.

Commodity
Apple, wet pomace

Parts per million
3.0

Alfalfa, forage

10

Alfalfa, hay

50

Beet, garden, roots

0.30

Beet, garden, tops

6.0

Bushberry subgroup 13–07B

1.5

Cattle, fat

1.5

Cattle, meat

0.05

Cattle, meat byproducts

0.03

Corn, sweet, forage
Corn, sweet, kernel plus cob with husk removed

10
0.02

Corn, sweet, stover

15

Cotton, gin byproducts

15

Cotton, undelinted seed

2.0

Cranberry
Fruit, pome, except pear, group 11
Fruit, stone, group 12
Goat, fat

0.90
1.0
0.90
1.5

Goat, meat

0.05

Goat, meat byproducts

0.03

Grain, aspirated fractions

45

Grape

2.0

Grape, raisin

5.0

Hog, fat

1.5

Hog, meat

0.05

Hog, meat byproducts

0.03

Horse, fat

1.5

Horse, meat

0.05

Horse, meat byproducts

0.03

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Milk

0.15

Milk, fat

4.0

Okra

0.50

Pea, southern, seed

0.10

Peanut

0.01

Peanut, hay

40

Pear

0.20

Pear, oriental

0.20

Peppermint, tops

11

Sheep, fat

1.5

Sheep, meat

0.05

Sheep, meat byproducts

0.03

Soybean, hulls

4.0

Soybean, seed

0.80

Spearmint, tops

11

Turnip, greens

12

Vegetable, Brassica

, leafy, group 5

12

Vegetable, cucurbit, group 9

0.60

Vegetable, fruiting, group 8

0.50

Vegetable, leafy, except Brassica

, group 4

Vegetable, tuberous and corm, subgroup 1-C

14
0.01

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 58424, Sept. 29, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 47309, July 18, 2002;
67 FR 58730, Sept. 18, 2002; 68 FR 25830, May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR 28842,
May 19, 2004; 69 FR 29459, May 24, 2004; 69 FR 32282, June 9, 2004; 72 FR 37641, July 11, 2007; 74
FR 33165, July 10, 2009]

§ 180.565 Thiamethoxam; tolerances for residues.
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(a) General . A tolerance is established for the combined residues of the insecticide thiamethoxam [3-[(2chloro-5-thiazolyl)methyl]tetrahydro-5-methyl- N -nitro-4 H -1,3,5-oxadiazin-4-imine] (CAS Reg. No.
153719–23–4) and its metabolite [ N -(2-chloro-thiazol-5-ylmethyl) - N '-methyl- N '-nitro-guanidine],
calculated as parent equivalents, in or on the following raw agricultural commodities:

Commodity
Almond, hulls
Artichoke, globe

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Parts per million
1.2
0.45

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Barley, grain

0.30

Barley, hay

0.40

Barley, straw

0.40

Bean, succulent

0.02

Borage, seed

0.02

Brassica, head and stem, subgroup 5-A

4.5

Brassica, leafy greens, subgroup 5-B

3.0

Bushberry subgroup 13B

0.20

Caneberry subgroup 13-A

0.35

Canola, seed

0.02

Cattle, meat byproducts

0.02

Cattle, meat

0.02

Citrus, dried pulp

0.60 ppm

Coffee, bean, green1

0.05

Corn, field, forage

0.10

Corn, field, grain

0.020

Corn, field, stover

0.05

Corn, pop, forage

0.10

Corn, pop, grain

0.02

Corn, pop, stover

0.05

Corn, sweet, forage

0.10

Corn, sweet, kernel plus cob with husks removed

0.02

Corn, sweet, stover

0.05

Cotton, gin byproducts

1.5

Cotton, undelinted seed

0.10

Crambe, seed

0.02

Cranberry

0.02

Flax, seed

0.02

Fruit, citrus, group 10

0.40

Fruit, pome, group 11

0.2

Fruit, stone, group 12

0.5

Goat, meat byproducts

0.02

Goat, meat

0.02

Grain, aspirated fractions

0.08

Grape

0.20

Grape, raisin

0.30

Hog, meat byproducts

0.02

Hog, meat

0.02

Hop, dried cones

0.10

Horse, meat byproducts

0.02

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Horse, meat

0.02

Juneberry

0.20

Lingonberry

0.20

Milk

0.02

Mustard, seed

0.02

Nut, tree, group 14

0.02

Peppermint, tops

1.5

Pistachio

0.02

Potato

0.25

Radish, tops

0.80

Rapeseed, seed

0.02

Safflower, seed

0.02

Salal

0.20

Sheep, meat byproducts

0.02

Sheep, meat

0.02

Sorghum, forage

0.02

Sorghum, grain

0.02

Sorghum, grain, stover

0.02

Soybean, hulls

2.0

Spearmint, tops

1.5

Strawberry

0.3

Sunflower

0.02

Tomato, paste

0.80

Vegetable, cucurbit, group 9

0.2

Vegetable, fruiting, group 8

0.25

Vegetable, leafy, except brassica, group 4

4.0

Vegetable, legume, group 6

0.02

Vegetable, root, except sugar beet, subgroup 1B

0.02

Vegetable, tuberous and corm, except potato, subgroup 1D

0.02

Wheat, forage

0.50

Wheat, grain

0.02

Wheat, hay

0.02

Wheat, straw

0.02

1There

are no U.S. registrations as of September 17, 2003.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 79762, Dec. 20, 2000, as amended at 65 FR 80353, Dec. 21, 2000; 66 FR 28397, May 23, 2001;
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67 FR 35050, May 17, 2002; 67 FR 66571, Nov. 1, 2002; 68 FR 51479, Aug. 27, 2003; 68 FR 54394,
Sept. 17, 2003; 69 FR 55512, Sept. 15, 2004; 70 FR 719, Jan. 5, 2005; 70 FR 7182, Feb. 11, 2005; 72 FR
34409, June 22, 2007; 73 FR 21048, Apr. 18, 2008; 74 FR 15875, Apr. 8, 2009]

§ 180.566 Fenpyroximate; tolerances for residues.
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(a) General. (1) Tolerances are established for combined residues of the insecticide fenpyroximate, (E)1,1-dimethylethyl 4-[[[[(1,3-dimethyl- 5-phenoxy-1H-pyrazol-4-yl) methylene] amino]oxy]methyl] benzoate
and its Z-isomer, (Z)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5- phenoxy-1H- pyrazol-4-yl)methylene] amino]
oxy] methyl]benzoate in or on the following commodities:

Commodity

Parts per
million

Almond, hulls

3.0

Citrus, dried pulp

2.5

Citrus, oil

10

Cotton, gin byproducts

10

Cotton, undelinted seed

0.10

Cucumber

0.10

Fruit, citrus, group 10

0.60

Fruit, pome, group 11

0.40

Grape

1.0

Hop, dried cones

10

Melon subgroup 9A

0.10

Nut, tree, group 14

0.10

Okra

0.20

Peppermint, tops

7.0

Pistachio

0.10

Spearmint, tops

7.0

Vegetable, fruiting, group 8

0.20

(2) Tolerances are established for combined residues of the insecticide fenpyroximate, (E)-1,1dimethylethyl 4-[[[[(1,3-dimethyl-5 -phenoxy-1H-pyrazol-4-yl) methylene] amino]oxy]methyl] benzoate
and its metabolites, (E)-4- [(1,3-dimethyl-5- phenoxypyrazol-4-yl)-methylene aminooxymethyl]benzoic
acid and (E)-1,1-dimethylethyl-2-hydroxyethyl 4- [[[[(1,3-dimethyl -5-phenoxy-1H-pyrazol-4yl) methylene]amino]oxy]methyl] benzoate, calculated as the parent compound in or on the following
commodities:

Commodity

Parts per million

Cattle, fat

0.03

Cattle, meat

0.03

Cattle, meat byproducts, except kidney and liver

0.03

Goat, fat

0.03

Goat, meat

0.03

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Goat, meat byproducts, except kidney and liver

0.03

Horse, fat

0.03

Horse, meat

0.03

Horse, meat byproducts, except kidney and liver

0.03

Milk

0.015

Sheep, fat

0.03

Sheep, meat

0.03

Sheep, meat byproducts, except kidney and liver

0.03

(3) Tolerances are established for combined residues of the insecticide fenpyroximate, (E)-1,1dimethylethyl 4- [[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl) methylene]amino]oxy]methyl] benzoate and
its metabolite, (E)-4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)-methylene aminooxymethyl]benzoic acid,
calculated as the parent compound in the following commodities:

Commodity

Parts per million

Cattle, kidney

0.25

Cattle, liver

0.25

Goat, kidney

0.25

Goat, liver

0.25

Horse, kidney

0.25

Horse, liver

0.25

Sheep, kidney

0.25

Sheep, liver

0.25

(b) Section 18 emergency exemptions. Time-limited tolerance is established for the combined residues of
fenpyroximate, (E)-1,1-dimethylethyl 4-[[[(E)-[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl) methylene] amino]
oxy] methyl]benzoate in or on honey at 0.10 ppm. This tolerance expires and is revoked on the date
specified in the following table.

Commodity

Parts per million

Honey

Expiration/revocation date

0.10

12/31/10

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 18568, Apr. 10, 2001, as amended at 69 FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, 2006;
72 FR 26321, May 9, 2007; 74 FR 37617, July 29, 2009]

§ 180.567 Zoxamide; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of zoxamide (3,5-dichloro- N -(3-chloro-1-ethyl-1methyl-2-oxopropyl)-4-methylbenzamide) in or on the following commodities:

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Commodity

Parts per million

Grape

3.0

Grape, raisin

15.0

Tomato

2.0

Vegetable, cucurbit, group 9

1.0

(2) Tolerances are established for the combined residues of zoxamide and its metabolites 3,5-dichloro-1,4benzenedicarboxylic acid (RH–1455 and RH–141455) and 3,5-dichloro-4-hydroxymethylbenzoic acid (RH–
1452 and RH–141452) in or on the following commodities:

Commodity

Parts per million

Potato

0.060

Potato, granules/flakes

0.30

Potato, wet peel

0.10

(b) Section 18 emergency exemptions. A time-limited tolerance is established for residues of the fungicide
zoxamide (3,5-dichloro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)-4-methylbenzamide) in connection with
use of the pesticide under a section 18 emergency exemption granted by EPA. The tolerance will expire
and is revoked on the date specified in the following table.

Commodity

Parts per million

Ginseng

Revocation date
0.06

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 18733, Apr. 11, 2001, as amended at 66 FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, 2004;
71 FR 31104, June 1, 2006; 71 FR 76200, Dec. 20, 2006]

§ 180.568 Flumioxazin; tolerances for residues.
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(a) General. Tolerances are established for residues of flumioxazin, 2-[7-fluoro-3,4-dihydro-3-oxo-4-(2propynyl)-2 H -1,4-benzoxazin-6-yl]-4,5,6,7-tetrahydro-1 H -isoindole-1,3(2 H )-dione, in or on the following
raw agricultural commodities:

Commodity

Parts per million

Alfalfa, forage

3.0

Alfalfa, hay

8.0

Almond

0.02

Almond, hulls

0.70

Asparagus

0.02

Bean, dry seed

0.05

Bushberry subgroup 13–07B

0.02

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Corn, field, forage

0.02

Corn, field, grain

0.02

Corn, field, stover

0.02

Cotton, gin byproducts

0.60

Cotton, undelinted seed

0.02

Fruit, pome, group 11

0.02

Fruit, stone, group 12

0.02

Garlic

0.02

Grape

0.02

Melon, subgroup 9A

0.02

Nut, tree, group 14

0.02

Okra

0.02

Onion, bulb

0.02

Peanut

0.02

Peppermint, tops

0.04

Pistachio

0.02

Shallot, bulb

0.02

Soybean, seed

0.02

Spearmint, tops

0.04

Strawberry

0.07

Sugarcane, cane

0.20

Vegetable, fruiting, group 8

0.02

Vegetable, tuberous and corm, subgroup 1C

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 19878, Apr. 18, 2001, as amended at 68 FR 51471, Aug. 27, 2003; 69 FR 16831, Mar. 31, 2004;
69 FR 52198, Aug. 25, 2004; 71 FR 25956, May 3, 2006; 71 FR 61413, Oct. 18, 2006; 73 FR 11831, Mar.
5, 2008; 73 FR 39251, July 9, 2008]

§ 180.569 Forchlorfenuron; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the plant growth regulator forchlorfenuron; N (2-chloro-4-pyridinyl)- N 'phenyl urea in or on the following commodities:

Commodity
Bushberry subgroup 13–07B

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Parts per
million
0.01

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Grape

0.03

Grape, raisin

0.06

Kiwifruit

0.04

(2) Time-limited tolerances are established for residues of the plant growth regulator forchlorfenuron; N- (2chloro-4-pyridinyl)- N′ -phenylurea in or on the food commodities:

Commodity

Parts per million

Expiration/revocation date

Almond

0.01

12/31/11

Almond, hulls

0.15

12/31/11

Cherry, sweet

0.01

12/31/11

Fig

0.01

12/31/11

Pear

0.01

12/31/11

Pistachio

0.01

12/31/11

Plum, prune, fresh

0.01

12/31/11

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional restrictions. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 22936, May 7, 2001, as amended at 69 FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, 2004;
73 FR 47846, Aug. 15, 2008]

§ 180.570 Isoxadifen-ethyl; tolerances for residues.
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(a) General . (1) Tolerances are established for residues of isoxadifen-ethyl (ethyl 5,5-diphenyl-2isoxazoline-3-carboxylate, (CAS No. 163520–33–0), and its metabolite: 4,5-dihydro-5,5-diphenyl-3isoxazolecarboxylic acid, when used as an inert ingredient (safener) in or on the following raw agricultural
commodities:

Commodity

Parts per million

Corn, field, forage

0.20

Corn, field, grain

0.08

Corn, field, stover

0.40

Corn, oil

0.50

Corn, pop, grain

0.04

Corn, pop, stover

0.25

Corn, sweet, forage

0.30

Corn, sweet, kernel plus cob with husk removed

0.04

Corn, sweet, stover

0.45

(2) Tolerances are established for the residues of isoxadifen-ethyl (3-isoxazolecarboxylic acid, 4,5-dihydrohttp://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c...&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (458 of 651) [9/8/2009 3:02:26 PM]

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5,5-diphenyl-, ethyl ester (CAS No. 164520–33–0)), and its metabolites 4,5-dihydro-5,5-diphenyl-3isoxazolecarboxylic acid and β-hydroxy-β-benzenepropanenitrile when used as an inert ingredient
(safener) in or on the following raw agricultural commodities:

Commodity

Parts per million

Rice, grain

0.10

Rice, hulls

0.50

Rice, straw

0.25

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 33187, June 21, 2001, as amended at 66 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, 2002;
69 FR 29890, May 26, 2004; 72 FR 63997, Nov. 14, 2007]

§ 180.571 Mesotrione; tolerances for residues.
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(a) General. Tolerances are established for residues of the herbicide mesotrione, 2-[4-(methylsulfonyl)-2nitrobenzoyl]-1,3-cyclohexanedione, in or on the following commodities:

Commodity

Parts per million

Asparagus

0.01

Berry, group 13

0.01

Corn, field, forage

0.01

Corn, field, grain

0.01

Corn, field, stover

0.01

Corn, pop, grain

0.01

Corn, pop, stover

0.01

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.5
0.01
1.5

Cranberry

0.02

Flax, seed

0.01

Grass, forage

0.01

Grass, hay

0.01

Grass, seed screenings

0.10

Grass, straw

0.10

Lingonberry

0.01

Millet, forage

0.01

Millet, grain

0.01

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Millet, hay

0.02

Millet, straw

0.02

Oat, forage

0.01

Oat, grain

0.01

Oat, hay

0.01

Oat, straw

0.01

Okra

0.01

Rhubarb

0.01

Sorghum, grain, forage

0.01

Sorghum, grain, grain

0.01

Sorghum, grain, stover

0.01

Sorghum, sweet

0.01

Sugarcane, cane

0.01

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the
herbicide mesotrione, 2-[4-(methylsulfonyl)-2-nitrobenzoyl]-1,3-cyclohexanedione, in connection with use
of the herbicide under section 18 emergency exemptions granted by EPA. The tolerances are specified in
the following table. The tolerances will expire on the dates specified in the table.

Commodity

Parts per million Expiration/revocation date

Corn, sweet, kernel plus cob
with husks removed

0.01

06/30/04

Corn, sweet, forage

0.50

06/30/04

Corn, sweet, stover

2.0

06/30/04

0.01

12/31/10

Cranberry

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 33195, June 21, 2001, as amended at 67 FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; 69
FR 58310, Sept. 30, 2004; 70 FR 14551, Mar. 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Jan. 9,
2008; 73 FR 9226, Feb. 20, 2008]

§ 180.572 Bifenazate; tolerance for residues.
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(a) General. (1) Tolerances are established for combined residues of bifenazate (1-methylethyl 2-(4methoxy[1,1′-biphenyl]-3-yl)hydrazinecarboxylate) and diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]3-yl), 1-methylethyl ester (expressed as bifenazate) in or on the following food commodities:

Commodity
Acerola
Almond, hulls
Apple, wet pomace
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Parts per million
0.90
15
1.2

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Black sapote

7.0

Caneberry subgroup 13-07A

5.0

Canistel

7.0

Cattle, fat
Cotton, gin byproducts

0.10
35

Cotton, undelinted seed

0.75

Feijoa

0.90

Fruit, pome, group 11

0.75

Fruit, stone, group 12, except plum

2.5

Goat, fat

0.10

Grape

0.75

Grape, raisin

1.2

Guave

0.90

Hog, fat

0.10

Hop, dried cones

15

Horse, fat

0.10

Jaboticaba

0.90

Longan

5.0

Lychee

5.0

Mango

7.0

Nut, tree, group 14

0.20

Okra

2.0

Papaya

7.0

Passionfruit

0.90

Pea and bean, succulent shelled, subgroup 6B

0.70

Peppermint, tops

25

Pistachio

0.20

Plum

0.20

Pulasan

5.0

Rambutan

5.0

Sapodilla

7.0

Sapote, mamey

7.0

Sheep, fat

0.10

Soybean, succulent shelled

0.70

Spanish lime
Spearmint, tops
Star apple
Starfruit
Strawberry
Vegetable, cucurbit, group 9

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5.0
25
7.0
0.90
1.5
0.75

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Vegetable, fruiting, group 8

2.0

Vegetable, legume, edible-podded, subgroup 6A

6.0

Vegetable, tuberous and corm, subgroup 1C

0.10

Wax jambu

0.90

(2) Tolerances are established for combined residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′biphenyl]-3-yl) hydrazinecarboxylate); diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1methylethyl ester (expressed as bifenazate); 1,1′-biphenyl, 4-ol; and 1,1′-biphenyl, 4-oxysulfonic acid
(expressed as 1,1′-biphenyl, 4-ol) in or on the following food commodities:

Commodity

Parts per million

Cattle, meat

0.02

Cattle, meat byproducts

0.02

Goat, meat

0.02

Goat, meat byproducts

0.02

Hog, meat

0.02

Hog, meat byproducts

0.02

Horse, meat

0.02

Horse, meat byproducts

0.02

Milk

0.02

Sheep, meat

0.02

Sheep, meat byproducts

0.02

(b) Section 18 emergency exemptions. Time-limited tolerances are established for combined residues of
bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)hydrazinecarboxylate) and diazinecarboxylic
acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester (expressed as bifenazate) in connection with
use of the pesticide under section 18 emergency exemptions granted by EPA. The tolerances will expire
and are revoked on the dates specified in the following table.

Commodity

Parts per million

Cherry, tart

Expiration/Revocation Date

5.0

12/31/09

0.05

12/31/06

Soybean, hulls

20

12/31/09

Soybean, meal

3.5

12/31/09

20

12/31/09

1.5

12/31/09

50

12/31/10

150

12/31/10

Potato

Soybean, refined oil
Soybean, seed
Timothy, forage
Timothy, hay
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

[66 FR 34569, June 29, 2001, as amended at 66 FR 42772, Aug. 15, 2001; 67 FR 4922, Feb. 1, 2002; 67
FR 46884, July 17, 2002; 68 FR 55502, Sept. 26, 2003; 69 FR 5297, Feb. 4, 2004; 70 FR 4037, Jan. 28,
2005; 70 FR 74695, Dec. 16, 2005; 71 FR 51505, Aug. 30, 2006; 72 FR 71802, Dec. 19, 2007; 73 FR
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11837, Mar. 5, 2008]

§ 180.573 Tepraloxydim; tolerances for residues.
top
(a) General. (1) Tolerances are established for the residues of tepraloxydim (2-[1-[[[(2E)-3-chloro-2propenyl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)-cyclohexene-1-one) and its metabolites
convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid) and OH-GP (3-hydroxy-3(tetrahydropyran-4-yl)pentane-1,5-dioic acid), calculated as tepraloxydim in or on the following raw
agricultural commodities.

Commodity

Parts per million

Cotton, undelinted seed

0.2

Cotton, gin byproducts

3.0

Flax, seed

0.10

Grain, aspirated fraction

1200.0

Lentil, seed

0.10

Pea, dry, seed

0.10

Soybean, seed

6.0

Soybean, hulls

8.0

(2) Tolerances are established for the combined residues of tepraloxydim and its metabolites convertible
to GP, OH-GP, and GL (3-(2-oxotetrahydropyran-4-yl)-1,5-dioic acid), calculated as tepraloxydim in or on
the following commodities

Commodity

Parts per million

Cattle, fat

0.15

Cattle, kidney

0.50

Cattle, meat

0.20

Cattle, meat byproducts, except kidney

0.20

Egg

0.20

Goat, fat

0.15

Goat, kidney

0.50

Goat, meat

0.20

Goat, meat byproducts, except kidney

0.20

Hog, fat

0.15

Hog, kidney

0.50

Hog, meat

0.20

Hog, meat byproducts, except kidney

0.20

Horse, fat

0.15

Horse, kidney

0.50

Horse, meat

0.20

Horse, meat byproducts, except kidney

0.20

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Milk

0.10

Poultry, fat

0.30

Poultry, liver

1.00

Poultry, meat

0.20

Poultry, meat byproducts, except liver

0.20

Sheep, fat

0.15

Sheep, kidney

0.50

Sheep, meat

0.20

Sheep, meat byproducts, except kidney

0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(n) is
established for the combined residues of tepraloxydim and its metabolites convertible to GP and OH-GP,
calculated as tepraloxydim in or on the following raw agricultural commodity:

Commodity

Parts per million

Canola, seed

0.50

(d) Indirect or inadvertent residues. [Reserved]
[66 FR 40150, Aug. 2, 2001 as amended at 72 FR 54588, Sept. 26, 2007]

§ 180.574 Fluazinam; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of fluazinam, (3-chloro- N -[3-chloro-2,6-dinitro-4(trifluoromethyl) phenyl]-5-(trifluoromethyl)-2-pyridinamine) in or on the following commodities:

Commodity

Parts per million

Aronia berry

7.0

Buffalo currant

7.0

Bushberry subgroup 13B

7.0

Chilean guava

7.0

European barberry

7.0

Ginseng

4.5

Highbush cranberry

7.0

Honeysuckle, edible

7.0

Jostaberry

7.0

Juneberry

7.0

Lingonberry

7.0

Native currant

7.0

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Pea and bean, dried shelled, except soybean, subgroup 6C, except
pea

0.02

Pea and bean, succulent shelled, subgroup 6B, except pea

0.04

Peanut

0.02

Potato

0.02

Salal

7.0

Sea buckthorn

7.0

Turnip, greens

0.01

Vegetable, Brassica leafy, group 5

0.01

Vegetable, legume, edible-podded, subgroup 6A, except pea

0.10

(2) Tolerances are established for residues of fluazinam and its metabolite AMGT 3-[[4-amino-3-[[3-chloro5-(trifloromethyl)-2-pyridinyl]amino]-2-nitro-6-(trifluoromethyl) phenyl] thio]-2-(beta-D-glucopyranosyloxy)
propionic acid) in or on the following commodity:

Commodity

Parts per million
3.0

Grape, wine1
1No

US registration as of March 15, 2002.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 46738, Sept. 7, 2001, as amended at 67 FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, 2007]

§ 180.575 Sulfuryl fluoride; tolerances for residues.
top
(a)(1) General. Tolerances are established for residues of sulfuryl fluoride in or on the following
commodities from the postharvest fumigation with sulfuryl fluoride for the control of insects:

Commodity
All processed food commodities not otherwise listed

Parts per million
2.0

Barley, bran, postharvest

0.05

Barley, flour, postharvest

0.05

Barley, grain, postharvest

0.1

Barley, pearled barley, postharvest
Cacao bean, roasted bean, postharvest
Cattle, meat, dried

0.05
0.2
0.01

Cheese

2.0

Coconut, postharvest

1.0

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Coffee, bean, roasted bean, postharvest

1.0

Corn, field, flour, postharvest

0.01

Corn, field, grain, postharvest

0.05

Corn, field, grits, postharvest

15.0

Corn, field, meal, postharvest

0.01

Corn, pop, grain, postharvest

0.05

Cotton, undelinted seed, postharvest

0.5

Egg, dried

1.0

Fruit, dried, postharvest
Ginger, postharvest
Grain, aspirated fractions, postharvest
Herbs and spices group 19, postharvest
Hog, meat

0.05
0.5
0.05
0.5
0.02

Milk, powdered

2.0

Millet, grain, postharvest

0.1

Nut, pine, postharvest

0.2

Nut, tree, Group 14, postharvest

3.0

Oat, flour, postharvest

0.05

Oat, grain, postharvest

0.1

Oat, groats/rolled oats, postharvest

0.1

Peanut, postharvest

0.5

Pistachio, postharvest

3.0

Rice, bran, postharvest

0.01

Rice, flour, postharvest

0.05

Rice, grain, postharvest

0.04

Rice, hulls, postharvest

0.1

Rice, polished rice, postharvest

0.01

Rice, wild, grain, postharvest

0.05

Sorghum, grain, grain, postharvest

0.1

Triticale, grain, postharvest

0.1

Vegetable, legume, group 6, postharvest

0.5

Wheat, bran, postharvest

0.05

Wheat, flour, postharvest

0.05

Wheat, germ, postharvest

0.02

Wheat, grain, postharvest

0.1

Wheat, milled byproducts, postharvest

0.05

Wheat, shorts, postharvest

0.05

(2) To assure safe use of this pesticide commodities treated with sulfuryl fluoride must be aerated for at
least 24 hours prior to entering commerce.
(b) Section 18 emergency exemptions. [Reserved]
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(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[67 FR 5740, Feb. 7, 2002, as amended at 69 FR 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005]

§ 180.576 Cyhalofop-butyl; tolerances for residues.
top
(a) General. Time-limited tolerances are established for combined residues of cyhalofop (cyhalofop-butyl,
R-(+)-n-butyl-2-(4(4-cyano-2-fluorophenoxy)-phenoxy)propionate, plus cyhalofop acid, R-(+)-2-(4(4-cyano2-fluorophenoxy)-phenoxy)propionic acid) and the di-acid metabolite, (2R)-4-[4-(1-carboxyethoxy)
phenoxy]-3-fluorobenzoic acid, from the application of the herbicide cyhalofop-butyl in or on the following
raw agricultural commodities:

Commodity

Parts per million

Rice, grain

0.03

Rice, wild, grain

0.03

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 43256, June 27, 2002, as amended at 74 FR 15880, Apr. 8, 2009]

§ 180.577 Bispyribac-sodium; tolerances for residues.
top
(a) General. Tolerances are established for residues of bispyribac-sodium, sodium 2,6-bis[(4,6-dimethoxypyrimidin-2-yl)oxy]benzoate, in or on the following raw agricultural commodities:

Commodity

Parts per million

Rice, grain

0.02

Rice, straw

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 48097, Sept. 18, 2001]

§ 180.578 Acetamiprid; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the insecticide acetamiprid N1-[(6-chloro-3pyridyl)methyl]-N2-cyano-N1-methylacetamidine in or on the following commodities:

Commodity

Parts per million

Almond, hulls

5.0

Berry, low growing subgroups 13–07G

0.60

Bushberry subgroup 13–07B

1.6

Caneberry subgroup 13–07A

1.6

Canola, seed

0.010

Citrus, dried pulp

1.20

Cotton, gin byproducts

20.0

Cotton, undelinted seed

0.60

Fruit, citrus, group 10

0.50

Fruit, pome, group 11

1.0

Fruit, stone, group 12, except plum, prune

1.20

Grape

0.20

Mustard, seed

0.010

Nut, tree, group 14

0.10

Onion, bulb, subgroup 3–07A

0.02

Onion, green, subgroup 3–07B

4.5

Pea and bean, succulent shelled, subgroup 6B

0.40

Pistachio

0.10

Plum, prune, dried

0.40

Plum, prune, fresh

0.20

Tomato, paste

0.40

Vegetable, brassica, leafy, group 5

1.20

Vegetable, cucurbit, group 9

0.50

Vegetable, fruiting, group 8

0.20

Vegetable, leafy, except brassica, group 4

3.00

Vegetable, legume, edible podded, subgroup 6A

0.60

Vegetable, tuberous and corm, group 1

0.01

(2) Tolerances are established for the combined residues of the insecticide acetamiprid N1-[(6-chloro-3pyridyl)methyl]-N2-cyano-N1-methylacetamidine and N1-[(6-chloro-3-pyridyl)methyl]-N2-cyanoacetamidine in or on the following commodities:

Commodity

Parts per million

Cattle, fat

0.10

Cattle, meat

0.10

Cattle, meat byproducts

0.20

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Egg

0.010

Goat, fat

0.10

Goat, meat

0.10

Goat, meat byproducts

0.20

Hog, fat

0.10

Hog, meat

0.10

Hog, meat byproducts

0.20

Horse, fat

0.10

Horse, meat

0.10

Horse, meat byproducts

0.20

Milk

0.10

Poultry, fat

0.010

Poultry, liver

0.050

Poultry, meat

0.010

Sheep, fat

0.10

Sheep, meat

0.10

Sheep, meat byproducts

0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 14659, Mar. 27, 2002, as amended at 68 FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, 2005; 72
FR 67262, Nov. 28, 2007; 73 FR 2811, Jan. 16, 2008]

§ 180.579 Fenamidone; tolerances for residues.
top
(a) General. (1) Tolerances are established for residues of fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-, (S)-) from the application of the fungicide fenamidone on
the following raw agricultural commodities:

Commodity
Brassica, head and stem, subgroup 5A

Parts per million
5.0

Brassica, leafy greens, subgroup 5B

55

Cilantro, leaves

60

Cotton, gin byproducts

0.02

Cotton, undelinted seed

0.02

Garlic

0.20

Garlic, great headed

0.20

Leek

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Okra

3.5

Onion, bulb

0.20

Onion, green

1.5

Onion, welsh

1.5

Pepper, nonbell

3.5

Shallot, bulb

0.20

Shallot, fresh leaves

1.5

Sunflower

0.02

Tomato, paste

2.2

Tomato, puree

2.0

Turnip, greens

55

Vegetable, cucurbit, group 9

0.15

Vegetable, fruiting, group 8, except nonbell pepper

1.0

Vegetable, leafy, except Brassica, group 4

60

Vegetable, root, except sugar beet, subgroup 1B, except radish

0.15

Vegetable, tuberous and corm, subgroup 1C

0.02

(2) Tolerances are established for the combined residues of fenamidone (4H-imidazol-4-one, 3,5-dihydro5-methyl-2-(methylthio)-5-phenyl-3-(phenylamino), (S)-) and its metabolite RPA 717879 (2,4imidazolidinedione, 5-methyl-5-phenyl), expressed as parent compound, in or on the following
commodities:

Commodity

Parts per million

Cattle, fat

0.10

Cattle, meat

0.10

Cattle, meat byproducts

0.10

Goat, fat

0.10

Goat, meat

0.10

Goat, meat byproducts

0.10

Milk

0.02

Sheep, fat

0.10

Sheep, meat

0.10

Sheep, meat byproducts

0.10

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration as defined in §180.1(m) is
established for residues of fenamidone, 4 H -Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl3-(phenylamino)-, (S)-, in or on the following commodity:

Commodity

Parts per million
1.0

Grape1
1Applicable

to grapes grown East of the Rocky Mountains.

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(d) Indirect or inadvertent residues . Tolerances are established for residues of the fungicide fenamidone
(4-H-imidazol-4-one, 3,5-dihydro-5-methyl-2-(methlthio)-5-phenyl-3-(phenylamino, (S)-) and its metabolite
RPA 717879 (2,4-imidazolidinedione, 5-methyl-5-phenyl) in or on the following agricultural commodities
when present therein as a result of application of fenamidone to the crops in paragraph (a)(1).

Commodity

Parts per million

Corn, field, forage

0.25

Corn, field, grain

0.02

Corn, field, stover

0.40

Corn, sweet, forage

0.15

Corn, sweet, kernel plus cob with husks removed

0.02

Corn, sweet, stover

0.20

Soybean, forage

0.15

Soybean, hay

0.25

Soybean, seed

0.02

Strawberry

0.15

Wheat, grain

0.10

Wheat, hay

0.50

Wheat, forage

0.15

Wheat, straw

0.35

[67 FR 60976, Sept. 27, 2002, as amended at 69 FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, 2006;
72 FR 60272, Oct. 24, 2007; 74 FR 34257, July 15, 2009]

§ 180.580 Iodosulfuron-Methyl-Sodium; tolerances for residues.
top
(a) General. Tolerances are established for residues of the herbicide Iodosulfuron-Methyl-Sodium (methyl
4-iodo-2-[3-(4-methoxy-6-methyl-1,3,5 triazin-2-yl)ureidosulfonyl]benzoate, sodium salt ) in or on the
following commodities:

Commodity

Parts per million

Corn, field, forage

0.05

Corn, field, grain

0.03

Corn, field, stover

0.05

Wheat, forage

0.10

Wheat, grain

0.02

Wheat, hay

0.05

Wheat, straw

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[67 FR 57532, Sept. 11, 2002, as amended at 74 FR 23644, May 20, 2009]

§ 180.581 Iprovalicarb; tolerances for residues.
top
(a) General. Tolerances are established for residues of iprovalicarb, [2-methyl-1[[[(1S)-(4-methylphenyl)
ethyl] amino]carbonyl] propyl]carbamic acid methylethylester, in or on the following commodities.

Commodity

Parts per million

Grape1

2.0

Tomato1

1.0

1There

is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 54359, Aug. 22, 2002, as amended at 70 FR 55281, Sept. 21, 2005]

§ 180.582 Pyraclostrobin; tolerances for residues.
top
(a) General. (1) Tolerances are established for combined residues of the fungicide pyraclostrobin
(carbamic acid, [2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]methoxy-, methyl ester) and its
desmethoxy metabolite (methyl-N-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenylcarbamate),
expressed as parent compound, in or on the following raw agricultural commodities.

Commodity

Parts per million

Almond, hulls

7.0

Apple, wet pomace

8.0

Avocado

0.6

Banana

0.04

Barley, grain
Barley, hay

1.4
25

Barley, straw

6.0

Bean, succulent shelled

0.5

Beet, sugar, dried pulp

1.0

Beet, sugar, roots

0.2

Beet, sugar, tops

8.0

Berry, group 13

4.0

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Borage, seed
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Canistel

0.45
5.0
16.0
0.6

Castor oil plant, seed

0.45

Chinese tallowtree, seed

0.45

Citrus, dried pulp

12.5

Citrus, oil

9.0

Corn, field, forage

5.0

Corn, field, grain

0.1

Corn, field, refined oil

0.2

Corn, field, stover

17.0

Corn, pop, grain

0.1

Corn, pop, stover

17.0

Corn, sweet, forage

5.0

Corn, sweet, kernel plus cob with husks removed

0.04

Corn, sweet, stover

23.0

Cotton, gin byproducts

30

Cotton, undelinted seed

0.3

Crambe, seed

0.45

Cuphea, seed

0.45

Echium, seed

0.45

Euphorbia, seed

0.45

Evening primrose, seed

0.45

Flax, seed

0.45

Fruit, citrus, group 10

2.0

Fruit, pome, group 11

1.5

Fruit, stone, group 12

0.9

Gold of pleasure, seed

0.45

Grain, aspirated fractions

2.5

Grape

2.0

Grape, raisin

7.0

Grass, forage

10

Grass, hay

4.5

Grass, seed screenings

27

Grass, straw grown for seed

14

Hare's ear mustard, seed

0.45

Hop, dried cones

23.0

Jojoba, seed

0.45

Lesquerella, seed

0.45

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Lunaria, seed
Mango

0.45
0.6

Meadowfoam, seed

0.45

Milkweed, seed

0.45

Mustard, seed

0.45

Niger seed, seed

0.45

Nut, tree, group 14

0.04

Oat, grain

1.2

Oat, hay

18

Oat, straw

15

Oil radish, seed

0.45

Papaya

0.6

Pea, succulent

0.2

Pea and bean, dried shelled, except soybean, subgroup 6C

0.5

Peanut

0.05

Peanut, refined oil

0.1

Peppermint, tops

8.0

Pistachio

0.7

Poppy, seed

0.45

Radish, tops

16

Rapeseed, seed

0.45

Rose hip, seed

0.45

Rye, grain

0.04

Rye, straw

0.5

Safflower, seed

0.45

Sapodilla

0.6

Sapote, black

0.6

Sapote, mamey

0.6

Sesame, seed

0.45

Soybean, forage

5.0

Soybean, hay

7.0

Soybean, hulls

0.06

Soybean, seed

0.04

Spearmint, tops

8.0

Star apple

0.6

Stokes aster, seed
Strawberry

0.45
1.2

Sunflower, seed

0.45

Sweet rocket, seed

0.45

Tallowwood, seed

0.45

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Tea oil plant, seed

0.45

Vegetable, bulb, group 3

0.9

Vegetable, cucurbit, group 9

0.5

Vegetable, foliage of legume, except soybean, subgroup 7A

25.0

Vegetable, fruiting, group 8

1.4

Vegetable, leafy, except brassica, group 4

29.0

Vegetable, leaves of root and tuber, group 2, except sugar beet

16.0

Vegetable, legume, edible podded, subgroup 6A

0.5

Vegetable, root, except sugar beet, subgroup 1B

0.4

Vegetable, tuberous and corm, subgroup 1C

0.04

Vegetables, foliage of legume, group 7

25

Vernonia, seed

0.45

Wheat, grain

0.02

Wheat, hay

6.0

Wheat, straw

8.5

(2) Tolerances are established for combined residues of the fungicide pyraclostrobin carbamic acid, [2-[[[1(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]methoxy-, methyl ester and its metabolites convertible
to 1-(4-chlorophenyl)-1H-pyrazol-3-ol and 1-(4-chloro-2-hydroxyphenyl)-1H-pyrazol-3-ol, expressed as
parent compound, in or on the following raw agricultural commodities.

Commodity

Parts per million

Cattle, fat

0.1

Cattle, liver

1.5

Cattle, meat

0.1

Cattle, meat byproducts, except liver

0.2

Goat, fat

0.1

Goat, liver

1.5

Goat, meat

0.1

Goat, meat byproducts, except liver

0.2

Hog, fat

0.1

Hog, liver

1.5

Hog, meat

0.1

Hog, meat byproducts, except liver

0.2

Horse, fat

0.1

Horse, liver

0.1

Horse, meat

0.1

Horse, meat byproducts, except liver

0.2

Milk

0.1

Sheep, fat

0.1

Sheep, liver

1.5

Sheep, meat

0.1

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Sheep, meat byproducts, except liver

0.2

(b) Section 18 emergency exemptions. A time-limited tolerance is established for combined residues of the
fungicide pyraclostrobin, (carbamic acid, [2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl] phenyl]
methoxy-, methyl ester) and its desmethoxy metabolite (methyl-N-[[[1-(4-chlorophenyl) pyrazol-3-yl]oxy]otolyl]carbamate) in connection with use of the pesticide under section 18 emergency exemptions granted
by EPA. The time-limited tolerance will expire and is revoked on the date specified in the following table.

Commodity

Parts per million

Expiration/Revocation Date

Endive, Belgian

11.0

12/31/09

Sugarcane, cane

0.02

12/31/11

0.4

12/31/11

Sugarcane, molasses
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

[67 FR 60901, Sept. 27, 2002, as amended at 69 FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, 2006; 72
FR 54569, Sept. 26, 2007; 73 FR 15431, Mar. 24, 2008; 73 FR 21842, Apr. 23, 2008; 73 FR 44167, July
30, 2008; 74 FR 11499, Mar. 18, 2009]

§ 180.583 Triticonazole; tolerances for residues.
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(a) General. Tolerances are established for residues of the fungicide triticonazole, (1RS)-(E)-5-[(4chlorophenyl)methylene]-2,2-dimethyl-1-(1 H -1,2,4-triazol-1-ylmethyl)cyclopentanol, from the treatment of
seed prior to planting in or on raw agricultural commodities as follows:

Commodity

Parts per million

Barley, grain

0.05

Barley, hay

0.05

Barley, straw

0.05

Wheat, forage

0.05

Wheat, grain

0.05

Wheat, hay

0.05

Wheat, straw

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 60959, Sept. 27, 2002]

§ 180.584 Tolylfluanid; tolerances for residues.

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(a) General. Tolerances are established for residues of tolylfluanid, 1,1-dichloro-N-[(dimethylamino)sulfonyl]-1-fluoro-N-(4-methylphenyl)methanesulfenamide in or on the following commodities.

Commodity

Parts per million

Apple1

5.0

Grape1

11

Hop, dried cones1

30
2.0

Tomato1
1No

U.S. registration as of August 31, 2002.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 60141, Sept. 25, 2002]

§ 180.585 Pyraflufen-ethyl; tolerances for residues.
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(a) General . Tolerances are established for residues of the herbicide, pyraflufen-ethyl, ethyl 2-chloro-5-(4chloro-5-difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetate, and its acid metabolite, E-1,
2-chloro-5-(4-chloro-5-difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, expressed in
terms of the parent in or on the following food commodities:

Commodity

Parts per million

Expiration/revocation date

Cattle, meat byproducts

0.02

10/15/12

Corn, field, forage

0.01

None

Corn, field, grain

0.01

None

Corn, field, stover

0.01

None

Cotton, gin byproducts

1.5

None

Cotton, undelinted seed

0.04

None

Goat, meat byproducts

0.02

10/15/12

Grass, forage, group 17

1.0

None

Grass, hay, group 17

1.4

None

Horse, meat byproducts

0.02

10/15/12

Milk

0.02

10/15/12

Potato

0.02

None

Sheep, meat byproducts

0.02

10/15/12

Soybean, forage

0.05

None

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Soybean, hay

0.10

None

Soybean, seed

0.01

None

Wheat, forage

0.02

None

Wheat, grain

0.01

None

Wheat, hay

0.01

None

Wheat, straw

0.01

None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 23055, Apr. 30, 2003, as amended at 68 FR 27739, May 21, 2003; 69 FR 26312, May 12, 2004; 73
FR 51743, Sept. 5, 2008]

§ 180.586 Clothianidin; tolerances for residues.
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(a) General. Tolerances are established for residues of the insecticide clothianidin, (E)-1-(2-chloro-1,3thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on the following raw agricultural commodities:

Commodity

Parts per million

Beet, sugar, dried pulp

0.03

Beet, sugar, molasses

0.05

Beet, sugar, roots

0.02

Canola, seed

0.01

Corn, field, forage

0.10

Corn, field, grain

0.01

Corn, field, stover

0.10

Corn, pop, grain

0.01

Corn, pop, stover

0.10

Corn, sweet, forage

0.10

Corn, sweet, kernel plus cob with husk removed

0.01

Corn, sweet, stover

0.10

Cotton, gin byproducts

0.01

Cotton, undelinted seed

0.01

Fruit, pome

1.0

Grape

0.60

Milk

0.01

Potato

0.05

Potato, granules/flakes

0.08

Sorghum, forage, grain, stover

0.01

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(b) Section 18 emergency exemptions . Time-limited tolerances are established for the residues of the
insecticide clothianidin, (E)-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in connection
with use of the pesticide under section 18 emergency exemptions granted by EPA. These tolerances will
expire and are revoked on the dates specified in the following table:

Commodity

Parts per million

Expiration/revocation date

Beet, sugar, roots

0.02

12/31/09

Beet, sugar, tops

0.02

12/31/09

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. Tolerances are established for the indirect or inadvertent residues of
the insecticide clothianidin, (E)-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on the
following raw agricultural commodities when present therein as a result of the application of clothianidin to
crops listed in paragraph (a) of this section:

Commodity

Parts per million

Animal feed, nongrass, group 18

0.02

Grain, cereal, forage, fodder and straw, group 16

0.02

Grass, forage, fodder and hay, group 17

0.02

Soybean, forage

0.02

Soybean, hay

0.02

[68 FR 32399, May 30, 2003, as amended at 70 FR 7894, Feb. 16, 2005; 71 FR 74801, Dec. 13, 2006; 73
FR 6856, Feb. 6, 2008]

§ 180.587 Famoxadone; tolerance for residues.
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(a) General. Tolerances are established for residues of the fungicide famoxadone (3-anilino-5-methyl-5-(4phenoxyphenyl)-1,3-oxazolidine-2,4-dione) in or on the following commodities:

Commodity
Caneberry subgroup 13–07A

Parts per million
10

Cattle, fat

0.02

Cattle, liver

0.05

Cilantro, leaves

25

Goat, fat

0.02

Goat, liver

0.05

Grape, raisin1
Hop, dried cone

4.0
80

Horse, fat

0.02

Horse, liver

0.05

Milk, fat (reflecting negligible residues in whole milk)

0.06

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Onion, bulb, subgroup 3–07A

0.45

Onion, green, subgroup 3–07B

40

Potato

0.02

Sheep, fat

0.02

Sheep, liver

0.05

Spinach

50

Tomato

1.0

Vegetable, cucurbit, group 9

0.30

Vegetable, fruiting, group 8, except tomato

4.0

Vegetable, leafy, except Brassica, group 4, except spinach
1There

25

are no U.S. registrations as of May 15, 2003.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with a regional registrations . Tolerances with a regional registration as defined in Sec.
180.1(n) are established for the residues of the fungicide famoxadone, 3-anilino-5-methyl-5-(4phenoxyphenyl)-1,3-oxazolidine-2,4-dione) in or on the raw agricultural commodities:

Commodity

Parts per million

Grape

2.5

(d) Indirect or inadvertant residues. [Reserved]
[68 FR 39471, July 2, 2003, as amended at 72 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, 2009]

§ 180.588 Quinoxyfen; tolerances for residues.
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(a) General. Tolerances are established for residues of the fungicide quinoxyfen, 5,7-dichloro-4-(4fluorophenoxy)quinoline in or on the following raw agricultural commodities:

Commodity

Parts per million

Artichoke, globe
Fruit, stone, group 12
Hop, dried cones

1.4
0.70
3.0

Gourd, edible

0.20

Grape

0.60

Lettuce, head

7.0

Lettuce, leaf

19

Melon, subgroup 9A

0.08

Pepper, bell

0.35

Pepper, nonbell
Pumpkin
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1.7
0.20

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Squash, winter

0.20

Strawberry

0.90

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55858, Sept. 29, 2003, as amended at 70 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, 2006;
74 FR 14743, Apr. 1, 2009]

§ 180.589 Boscalid; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the fungicide boscalid, 3-pyridinecarboxamide,
2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl) in or on the following raw agricultural commodities:

Commodity

Parts per million

Almond, hulls

17

Apple, wet pomace

10

Avocado
Banana, import1
Brassica, head and stem, subgroup 5A

1.5
0.20
3.0

Brassica, leafy greens, subgroup 5B

18.0

Bushberry, subgroup 13B

13.0

Caneberry, subgroup13A

6.0

Canistel

1.5

Canola, refined oil

5.0

Canola, seed

3.5

Cotton, gin byproducts

55.0

Cotton, undelinted seed

1.0

Cucumber

0.5

Cucumber

0.20

Fruit, pome, group 11

3.0

Fruit, stone, group 12

1.7

Grain, aspirated fractions

3.0

Grape

3.5

Grape, raisin

8.5

Hop, dried cones

35

Leaf petioles subgroup 4B

45

Leafy greens subgroup 4A, except head lettuce and leaf lettuce

60

Lettuce, head
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Lettuce, leaf

11.0

Mango

1.5

Nut, tree, group 14

0.70

Papya

1.5

Pea and bean, dried shelled, except soybean, subgroup 6C, except
cowpea, field pea and grain lupin

2.5

Pea and bean, succulent shelled, subgroup 6B, except cowpea

0.6

Peanut

0.05

Peanut, meal

0.15

Peanut, refined oil

0.15

Peppermint, tops

30.0

Pistachio

0.70

Sapodilla

1.5

Sapote, black

1.5

Sapote, mamey

1.5

Soybean, hulls

0.2

Soybean, seed

0.1

Soybean, vegetable

2.0

Spearmint, tops

30.0

Star apple

1.5

Strawberry

4.5

Sunflower, seed

0.60

Vegetable, bulb, group 3

3.0

Vegetable, cucurbit, group 9, except cucumber

1.6

Vegetable, fruiting, group 8

1.2

Vegetable, legume, edible podded, subgroup 6A

1.6

Vegetable, root, subgroup 1A, except sugar beet, garden beet,
radish, and turnip

1.0

Vegetable, root, subgroup 1A , except sugar beet, garden beet,
radish, and turnip

0.7

Vegetable, tuberous and corm, subgroup 1C
1

0.05

No US registration as of January 31, 2006.

(2) Tolerances are established for the combined residues of the fungicide boscalid, 3pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl) and metabolites 2-chloro-N-(4′-chloro-5hydroxy-biphenyl-2-yl)nicotinamide and glucuronic acid conjugate of 2-chloro-N-(4′-chloro-5-hydroxybiphenyl-2-yl)nicotinamide in or on the following food commodities:

Commodity

Parts per million

Cattle, fat

0.30

Cattle, meat

0.10

Cattle, meat byproducts

0.35

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Egg

0.02

Goat, fat

0.30

Goat, meat

0.10

Goat, meat byproducts

0.35

Hog, fat

0.10

Hog, meat

0.05

Hog, meat byproducts

0.10

Horse, fat

0.30

Horse, meat

0.10

Horse, meat byproducts

0.35

Milk

0.10

Poultry, fat

0.05

Poultry, meat

0.05

Poultry, meat byproduct

0.10

Sheep, fat

0.30

Sheep, meat

0.10

Sheep, meat byproducts

0.35

(b) Section 18 emergency exemptions. A time-limited tolerance is established for the residues of the
fungicide boscalid, 2-chloro-N-(4'-chloro [1, 1'-biphenyl]-2-yl)-3-pyridinecarboxamide in connection with
use of the pesticide under a section 18 emergency exemption granted by EPA. This tolerance will expire
and is revoked on the date specified in the following table.

Commodity

Parts per million

Endive, Belgian
Tangerine

Expiration/Revocation Date
16

12/31/09

2.0

12/31/08

(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide boscalid, 3pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl) in or on the following raw agricultural
commodities when present therein as a result of application of boscalid to the growing crops in paragraph
(a)(1) of this section:

Commodity

Parts per million

Animal feed, nongrass, group 18, forage

1.0

Animal feed, nongrass, group 18, hay

2.0

Animal feed, nongrass, group 18, seed

0.05

Beet, garden, roots

0.1

Beet, sugar, roots

0.1

Cotton, gin byproducts

0.30

Cotton, undelinted seed

0.05

Cowpea, seed

0.1

Flax, seed

3.5

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Grain, cereal, forage, fodder and straw, group 16, forage

2.0

Grain, cereal, forage, fodder and straw, group 16, stover

1.5

Grain, cereal, forage, fodder and straw, group 16, straw

3.0

Grain, cereal, group 15

0.20

Grass, forage, fodder, and hay, group 17, forage

2.0

Grass, forage, fodder, and hay, group 17, hay

8.0

Grass, forage, fodder, and hay, group 17, seed screenings

0.20

Grass, forage, fodder, and hay, group 17, straw

0.30

Lupin, grain, grain

0.1

Pea, field, seed

0.1

Radish, roots

0.1

Rice, hulls

0.50

Turnip, roots

0.1

Vegetable, foliage of legume, group 7, forage

1.5

Vegetable, foliage of legume, group 7, hay

2.0

Vegetable, foliage of legume, group 7, vines

0.05

Vegetable, leafy, except brassica, group 4, except celery, lettuce and
spinach

1.0

Vegetable, leaves of root and tuber, group 2

0.1

[68 FR 44651, July 30, 2003, as amended at 69 FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, 2005;
71 FR 6364, Feb. 8, 2006; 71 FR 25961, May 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, Mar.
28, 2008]

§ 180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.
top
(a) General . Time-limited tolerances are established for residues of 2, 6-DIPN in or on the following
commodities resulting from post-harvest applications to potato, when 2, 6-DIPN is used in accordance with
good agricultural practices:

Commodity

Parts per million

Expiration/revocation date

Cattle, fat

0.8

8/1/09

Cattle, liver

0.3

8/1/09

Cattle, meat

0.1

8/1/09

Cattle, meat byproducts

0.1

8/1/09

Goat, fat

0.8

8/1/09

Goat, liver

0.3

8/1/09

Goat, meat

0.1

8/1/09

Goat, meat byproducts

0.1

8/1/09

Hog, fat

0.8

8/1/09

Hog, liver

0.3

8/1/09

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Hog, meat

0.1

8/1/09

Hog, meat byproducts

0.1

8/1/09

Horse, fat

0.8

8/1/09

Horse, liver

0.3

8/1/09

Horse, meat

0.1

8/1/09

Horse, meat byproducts

0.1

8/1/09

Milk

0.1

8/1/09

Potato

2.0

8/1/09

Potato, wet peel

6.0

8/1/09

Sheep, fat

0.8

8/1/09

Sheep, liver

0.3

8/1/09

Sheep, meat

0.1

8/1/09

Sheep, meat byproducts

0.1

8/1/09

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 52011, Sept. 1, 2006]

§ 180.591 Trifloxysulfuron; tolerances for residues.
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(a) General. Tolerances are established for residues of the herbicide trifloxysulfuron, N -[[(4,6-dimethoxy-2pyrimidinyl)amino]carbonyl]-3-(2,2,2-trifluoroethoxy)-2-pyridinesulfonamide in or on the following raw
agricultural commodities.

Commodity

Parts per million

Almond

0.02

Almond, hulls

0.01

Fruit, citrus, Group 10

0.03

Cotton, undelinted seed

0.05

Cotton, gin byproducts

1.0

Sugarcane

0.01

Tomato

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 54386, Sept. 17, 2003]
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§ 180.592 Butafenacil; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo-2(2-propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2 H )-pyrimidinyl]
benzoate) in or on the following raw agricultural commodities:

Commodity

Parts per million

Cotton, gin byproducts

10

Cotton, undelinted seed

0.50

(2) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo-2-(2propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2 H )-pyrimidinyl]
benzoate) and its metabolite CGA-293731 (1-carboxy-1-methylethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6dioxo-4-(trifluoromethyl)-1(2 H )-pyrimidinyl] benzoate), in or on the following livestock commodities:

Commodity

Parts per million

Cattle, kidney

0.05

Cattle, liver

0.50

Goat, kidney

0.05

Goat, liver

0.50

Hog, kidney

0.05

Hog, liver

0.50

Horse, kidney

0.05

Horse, liver

0.50

Sheep, kidney

0.05

Sheep, liver

0.50

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. [Reserved]
[68 FR 54827, Sept. 19, 2003]

§ 180.593 Etoxazole; tolerances for residues.
top
(a) General. Tolerances are established for residues of the insecticide etoxazole, 2-(2,6-difluorophenyl)-4[4-(1,1-dimethylethyl)-2-ethoxyphenyl]-4,5-dihydrooxazole, in or on the following raw agricultural
commodities:

Commodity

Parts per million

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Almond, hulls

2.0

Apple, wet pomace

0.50

Cattle, fat

0.02

Cattle, liver

0.01

Cotton, gin byproducts

1.0

Cotton, undelinted seed

0.05

Cucumber

0.02

Fruit, pome, group 11

0.20

Fruit, stone, group 12, except plum

1.0

Goat, fat

0.02

Goat, liver

0.01

Grape

0.50

Grape, raisin

1.5

Hop, dried cones

7.0

Horse, fat

0.02

Horse, liver

0.01

Milk, fat

0.01

Nut, tree, group 14

0.01

Peppermint, oil

20

Peppermint, tops

10

Pistachio

0.01

Plum

0.15

Plum, prune, dried

0.30

Sheep, fat

0.02

Sheep, liver

0.01

Spearmint, oil

20

Spearmint, tops

10

Strawberry

0.50

Tangerine1

0.10

Tomato

0.20

Vegetable, cucurbit subgroup 9A

0.20

1There

are no U.S. registrations for use of etoxazole on tangerines as of September 26, 2003.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. [Reserved]
[68 FR 55493, Sept. 26, 2003, as amended at 70 FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, 2007;
74 FR 25160, May 27, 2009]

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§ 180.594 Thiacloprid; tolerances for residues.
top
(a) General. Tolerances for combined residues of the insecticide thiacloprid ([3-[(6-chloro-3-pyridinyl)
methyl]-2-thiazolidinylidene] cyanamide) and metabolites retaining the thiazolidine ring intact, measured
and expressed in terms of thiacloprid, per se, in or on the following commodities:

Commodity

Parts per million

Apple, wet pomace

0.60

Cattle, fat

0.020

Cattle, kidney

0.050

Cattle, liver

0.15

Cattle, meat

0.030

Cattle, meat byproducts

0.050

Cotton, gin byproducts

11.0

Cotton, undelinted seed

0.020

Fruit, pome, group 11

0.30

Goat, fat

0.020

Goat, kidney

0.050

Goat, liver

0.15

Goat, meat

0.030

Goat, meat byproducts

0.050

Horse, fat

0.020

Horse, kidney

0.050

Horse, liver

0.15

Horse, meat

0.030

Horse, meat byproducts

0.050

Milk

0.030

Sheep, fat

0.020

Sheep, kidney

0.050

Sheep, liver

0.15

Sheep, meat

0.030

Sheep, meat byproducts

0.050

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55512, Sept. 26, 2003]

§ 180.595 Flufenpyr-ethyl; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the herbicide, flufenpyr-ethyl; acetic acid, [2chloro-4-fluoro-5-[5-methyl-6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], in or on the
following commodities:

Commodity

Parts per million

Corn, field, grain

0.01

Soybean, seed

0.01

Sugarcane, cane

0.01

(2) Tolerances are established for residues of the herbicide flufenpyr-ethyl; acetic acid, [2-chloro-4-fluoro-5[5-methyl-6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], and its metabolite, S-3153
acid-4-OH; [2-chloro-4-hydroxy-5-[5-methyl-6- oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-acetic
acid, free and conjugated, in or on the following commodities:

Commodity

Parts per million

Corn, field, forage

0.05

Corn, field, stover

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 54842, Sept. 19, 2003]

§ 180.596 Fosthiazate; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of Fosthiazate ( O- ethyl S -(1methylpropyl)(2-oxo-3-thiazolidinyl)phosphonothioate and its metabolite O -ethyl S -(1-methylpropyl)[2(methylsulfonyl)ethyl] phosphoramidothioate) (ASC–67131).

Commodity

Parts per million

Tomato
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 18275, Apr. 7, 2004]

§ 180.597 Mesosulfuron-methyl; tolerances for residues.

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(a) General. Tolerances are established for residues of the herbicide mesosulfuron-methyl, (methyl 2[[[[(4,6-dimethoxy-2-pyrimidinyl) amino]carbonyl]amino]sulfonyl] -4-[[(methylsulfonyl)amino] methyl]
benzoate]) in or on the following raw agricultural commodities:

Commodity

Parts per million

Cattle, meat byproducts

0.01

Goat, meat byproducts

0.01

Grain, aspirated fractions

0.60

Horse, meat byproducts

0.01

Sheep, meat byproducts

0.01

Wheat, forage

0.60

Wheat, germ

0.10

Wheat, grain

0.03

Wheat, hay

0.06

Wheat, straw

0.30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 18263, Apr. 7, 2004]

§ 180.598 Novaluron; tolerances for residues.
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(a) General. Tolerances are established for residues of the insecticide novaluron, N -[[[3-chloro-4-[1,1,2trifluoro-2-(trifluoromethoxy)ethoxy]phenyl]amino]carbonyl]-2,6-difluorobenzamide, in or on the following
raw agricultural commodities:

Commodity
Apple, wet pomace
Brassica, head and stem, subgroup 5A
Cattle, fat

Parts per million
8.0
0.50
11

Cattle, kidney

1.0

Cattle, liver

1.0

Cattle, meat

0.60

Cattle, meat byproducts, except kidney and liver

0.60

Cotton, gin byproducts

30

Cotton, undelinted seed

0.60

Egg

0.05

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Fruit, pome, group 11

2.0

Goat, fat

11

Goat, kidney

1.0

Goat, liver

1.0

Goat, meat

0.60

Goat, meat byproducts except kidney and liver

0.60

Hog, fat

0.05

Hog, meat

0.01

Hog, meat byproducts

0.01

Horse, fat

11

Horse, kidney

1.0

Horse, liver

1.0

Horse, meat

0.60

Horse, meat byproducts, except kidney and liver

0.60

Milk

1.0

Milk, fat

20

Poultry, fat

0.40

Poultry, meat

0.03

Poultry, meat byproducts

0.04

Sheep, fat

11

Sheep, kidney

1.0

Sheep, liver

1.0

Sheep, meat

0.60

Sheep, meat byproducts, except kidney and liver

0.60

Sugarcane, cane

0.50

Tomato

1.0

Vegetable, tuberous and corn, subgroup 1C

0.05

(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for residues of the insecticide novaluron, N -[[[3-chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)
ethoxy]phenyl]amino]carbonyl]-2,6-difluorobenzamide in or on the specified agricultural commodities,
resulting from use of the pesticide pursuant to FFIFRA section 18 emergency exemptions. The tolerances
expire and are revoked on the date specified in the following table.

Commodity

Parts per million

Strawberry

Expiration/revocation date

0.50

12/31/11

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[69 FR 31021, June 2, 2004, as amended at 71 FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, 2006; 73
FR 74982, Dec. 10, 2008; 74 FR 637, Jan. 7, 2009; 74 FR 20891, May 6, 2009]

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§ 180.599 Acequinocyl; tolerances for residues.
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(a) General . Tolerances for combined residues of the insecticide acequinocyl, 2-(acetyloxy)-3-dodecyl-1,4naphthalenedione, and its metabolite, 2-dodecyl-3-hydroxy-1,4-naphthoquinone, expressed as
acequinocyl equivalents in or on the following commodities:

Commodity

Parts per million

Almond, hulls

2.0

Apple, wet pomace

1.0

Cattle, fat

0.02

Cattle, liver

0.02

Citrus, oil

30

Fruit, citrus, group 10

0.20

Fruit, pome, group 11

0.40

Goat, fat

0.02

Goat, liver

0.02

Grape

1.6

Horse, fat

0.02

Horse, liver

0.02

Nut, tree, group 14

0.02

Pistachio

0.02

Sheep, fat

0.02

Sheep, liver

0.02

Strawberry

0.40

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[69 FR 43533, July 21, 2004, as amended at 73 FR 17910, Apr. 2, 2008]

§ 180.600 Propoxycarbazone; tolerances for residues
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(a) General . (1) Tolerances are established for combined residues of the herbicide propoxycarbazone
methyl 2-[[[(4,5-dihydro-4-methyl-5-oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate
and its metabolite methyl 2-[[[(4,5-dihydro-3-(2-hydroxypropoxy)-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)
carbonyl]amino]sulfonyl]benzoate in/on the following raw agricultural commodities:

Commodity

Parts per million

Grass, forage
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20

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Grass, hay

25

Wheat, forage

17

Wheat, grain

0.02

Wheat, hay

0.15

Wheat, straw

0.05

(2) Tolerances are established for residues of the herbicide propoxycarbazone methyl 2-[[[(4,5-dihydro-4methyl-5-oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate in/on the following raw
agricultural commodities:

Commodity

Parts per million

Cattle, meat

0.05

Cattle, meat byproducts

0.3

Goat, meat

0.05

Goat, meat byproducts

0.3

Horse, meat

0.05

Horse, meat byproducts

0.3

Milk

0.03

Sheep, meat

0.05

Sheep, meat byproducts

0.3

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[69 FR 40781, July 7, 2004, as amended at 71 FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, 2009]

§ 180.601 Cyazofamid; tolerances for residues.
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(a) General. Tolerances are established for the combined residues of cyazofamid, 4-chloro-2-cyano- N,N dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide, and its metabolite CCIM, 4-chloro-5-(4methylphenyl)-1H-imidazole-2-carbonitrile, expressed as cyazofamid, in or on the following commodities:

Commodity

Parts per million

Carrot, roots

0.09

Okra

0.40

Potato

0.02

Vegetable, cucurbit, group 9

0.10

Vegetable, fruiting, group 8

0.40

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. Tolerances with regional registrations are established for the
combined residues of cyazofamid, 4-chloro-2-cyano- N , N -dimethyl-5-(4-methylphenyl)-1 H -imidazole-1sulfonamide, and its metabolite CCIM, 4-chloro-5-(4-methylphenyl)-1 H -imidazole-2-carbonitrile,
expressed as cyazofamid, in or on the following commodities:

Commodity

Parts per million

Grape

1.5

(d) Indirect or inadvertent residues. [Reserved]
[69 FR 58299, Sept. 30, 2004, as amended at 73 FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, 2009]

§ 180.602 Spiroxamine; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the fungicide spiroxamine (8-(1,1dimethylethyl)-N-ethyl-N-propyl-1,4-dioxaspiro[4,5]decane-2-methanamine) and its metabolites containing
the N-ethyl-N-propyl-1,2-dihydroxy-3-aminopropane moiety, calculated as parent equivalent, in or on the
following raw agricultural commodities:

Commodity

Parts per million

Banana (import)

3.0

Grape (import)

1.0

Hop, dried cones

50

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[69 FR 42570, July 16, 2004]

§ 180.603 Dinotefuran; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of Dinotefuran, [ N -methyl- N 'nitro- N'' -((tetrahydro-3-furanyl)methyl)guanidine] and its metabolites DN [1-methyl-3-(tetrahydro-3furylmethyl)guanidine] and UF [1-methyl-3-(tetrahydro-3-furylmethyl)urea], expressed as dinotefuran.

Commodity

Parts per million

Brassica, head and stem, subgroup 5A

1.4

Cotton, undelinted seed

0.4

Cotton, gin byproducts

8.0

Grape

0.9

Grape, raisin

2.5

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Potato

0.05

Potato, chips

0.1

Potato, granules/flakes

0.15

Tomato, paste

1.0

Vegetable, fruiting, group 8

0.7

Vegetable, cucurbit, group 9

0.5

Vegetable, leafy, except Brassica, group 4

5.0

(2) Tolerances are established for residues of dinotefuran N -methyl- N' -nitro- N'' -tetrahydro-3-furanyl)
methyl)guanidine in/on the following commodities:

Commodity

Parts per million

Cattle, fat

0.05

Cattle, meat

0.05

Cattle, meat byproducts

0.05

Goat, fat

0.05

Goat, meat

0.05

Goat, meat byproducts

0.05

Hog, fat

0.05

Hog, meat

0.05

Hog, meat byproducts

0.05

Horse, fat

0.05

Horse, meat

0.05

Horse, meat byproducts

0.05

Milk

0.05

Sheep, fat

0.05

Sheep, meat

0.05

Sheep, meat byproducts

0.05

(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for combined residues of Dinotefuran, [ N -methyl- N '-nitro- N '' -((tetrahydro-3-furanyl)methyl)
guanidine] and its metabolites DN [1-methyl-3-(tetrahydro-3-furylmethyl)guanidine] and UF [1-methyl-3(tetrahydro-3-furylmethyl)urea], expressed as dinotefuran in or on the specified agricultural commodities,
resulting from use of the pesticide pursuant to FFIFRA section 18 emergency exemptions. The tolerances
expire and are revoked on the date specified in the table.

Commodity

Parts per million

Rice, grain

Expiration/revocation date
2.8

(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[70 FR 14546, Mar. 23, 2005, as amended at 74 FR 12601, Mar. 25, 2009]

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§ 180.604 Mepanipyrim; tolerances for residues.
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(a) General . [Reserved]
(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect of inadvertent residues . [Reserved]
(e) Revoked tolerances subject to the channel of trade provisions . [Reserved]
(f) Import tolerances . Tolerances are established for the combined residues of mepanipyrim, 4-methyl-Nphenyl-6-(1-propynyl)-2-pyrimidinamine, and its metabolite, 4-methyl-N-phenyl-6-(2-hydroxypropylk)-2pyrimidinamine, both free and conjugated in or on the following commodities:

Commodity

Parts per million

Grape

1.5

Grape, raisin

3.0

Strawberry

1.5

Tomato

0.5

[68 FR 60827, Oct. 13, 2004]

§ 180.605 Penoxsulam; tolerances for residues.
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(a) General . Tolerances are established for the herbicide, penoxsulam ( 2-(2,2-difluoroethoxy)-N-(5,8dimethoxy[1,2,4] triazolo[1,5-c]pyrimidin-2-yl)-6-(trifluoromethyl)benzenesulfonamide) in/on the following
raw agricultural commodities:

Commodity

Parts per million

Almond, hulls

0.01

Fish

0.01

Fish, shellfish, crustacean

0.01

Fish, shellfish, mollusc

0.02

Grape

0.01

Nut, tree, group 14

0.01

Pistachio

0.01

Rice, grain

0.02

Rice, straw

0.50

(b) Section 18 emergency exemptions . [Reserved]

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(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 57197, Sept. 24, 2004, as amended at 72 FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, 2009]

§ 180.607 Spiromesifen; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of spiromesifen (2-oxo-3-(2,4,6trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate) and its enol metabolite (4-hydroxy-3(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one), calculated as the parent compound equivalents in
or on the following primary crop commodities:

Commodity

Parts per million

Bean, dry

0.02

Bean, edible podded

0.80

Bean, succulent

0.10

Berry and small fruit, low growing berry, subgroup 13-07G

2.0

Brassica, head and stem, subgroup 5A

2.0

Brassica, leafy greens, subgroup 5B

12

Corn, field, forage

5.0

Corn, field, grain

0.02

Corn, field, stover

8.0

Corn, pop, grain

0.02

Corn, pop, stover

4.0

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed

17
0.02

Corn, sweet, stover

12

Cotton, gin byproducts

15

Cotton, undelinted seed

0.50

Cowpea, forage

30

Cowpea, hay

86

Leafy greens subgroup 4A

12

Tomato, paste

0.80

Vegetable, cucurbit, group 9

0.10

Vegetable, fruiting, group 8

0.45

Vegetable, tuberous and corm, subgroup 1C

0.02

(2) Tolerances are established for the combined residues of spiromesifen (2-oxo-3-(2,4,6-trimethylphenyl)1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate), and its metabolites containing the enol (4-hydroxy-3(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one) and 4-hydroxymethyl (4-hydroxy-3-[4(hydroxymethyl)-2,6-dimethylphenyl]-1-oxaspiro[4.4]non-3-en-2-one) moieties, calculated as the parent
compound equivalents in the following livestock commodities:

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Commodity

Parts per million

Cattle, fat

0.10

Cattle, meat

0.02

Cattle, meat byproducts

0.20

Goat, fat

0.10

Goat, meat

0.02

Goat, meat byproducts

0.20

Horse, fat

0.10

Horse, meat

0.02

Horse, meat byproducts

0.20

Milk

0.01

Milk, fat

0.25

Sheep, fat

0.10

Sheep, meat

0.02

Sheep, meat byproducts

0.20

(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for combined residues of spiromesifen, (2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3en-4-yl 3,3-dimethylbutanoate) and its enol metabolite (4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]
non-3-en-2-one), calculated as the parent compound equivalents in or on the specified agricultural
commodities, resulting from use of the pesticide pursuant to FFIFRA section 18 emergency exemptions.
The tolerances expire and are revoked on the date specified in the table.

Commodity

Parts per million

Expiration/revocation date

Soybean, forage

30

12/31/11

Soybean, hay

86

12/31/11

0.02

12/31/11

Soybean, seed

(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for the inadvertent or indirect combined
residues of spiromesifen (2-oxo-3-(2,4,6-trimethylphenyl)-1- oxaspiro[4.4]non-3-en-4-yl 3,3dimethylbutanoate), its enol metabolite (4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2one), and its metabolites containing the 4-hydroxymethyl moiety (4-hydroxy-3-[4-(hydroxymethyl)-2,6dimethylphenyl]-1-oxaspiro[4.4]non-3-en-2-one), calculated as the parent compound equivalents in the
following rotational crop commodities:

Commodity

Parts per million

Alfalfa, forage

1.5

Alfalfa, hay

3.0

Barley, grain

0.03

Barley, hay

0.25

Barley, straw

0.15

Beet, sugar, roots

0.03

Beet, sugar, tops

0.20

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Oat, forage

0.20

Oat, grain

0.03

Oat, hay

0.25

Oat, straw

0.25

Wheat, forage

0.20

Wheat, grain

0.03

Wheat, hay

0.15

Wheat, straw

0.25

[70 FR 43283, July 27, 2005, as amended at 72 FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, 2008; 73
FR 52606, Sept. 10, 2008; 74 FR 8492, Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009]

§ 180.608 Spirodiclofen; tolerances for residues.
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(a) General . (1) Tolerances are established for residues of spirodiclofen per se (3-(2,4-dichlorophenyl)-2oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2-dimethylbutanoate) in or on the following plant commodities:

Commodity

Parts per million

Almond, hulls

20.0

Apple, wet pomace

2.0

Citrus, juice

0.60

Citrus, oil

20.0

Fruit, citrus, group 10

0.50

Fruit, pome, group 11

0.80

Fruit, stone, group 12

1.0

Grape

2.0

Grape, juice

2.4

Grape, raisin

4.0

Hop, dried cones

30

Nut, tree, group 14

0.10

Pistachio

0.10

(2) Tolerances are established for residues of spirodiclofen (3-(2,4-dichlorophenyl)-2-oxo-1-oxaspiro[4.5]
dec-3-en-4-yl 2,2-dimethylbutanoate) and its free enol metabolite BAJ 2510 (3-(2,4-dichlorophenyl)-4hydroxy-1-oxaspiro[4,5]dec-3-en-2-one) in or on the following livestock commodities:

Commodity

Parts per million

Cattle, fat

0.02

Cattle, meat byproducts

0.10

Cattle, meat

0.02

Goat, fat

0.02

Goat, meat byproducts
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Goat, meat

0.02

Horse, fat

0.02

Horse, meat byproducts

0.1

Horse, meat

0.02

Milk

0.01

Milk, fat

0.03

Sheep, fat

0.02

Sheep. meat byproducts

0.1

Sheep. meat

0.02

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[70 FR 40211, July 13, 2005, as amended at 73 FR 25539, May 7, 2008]

§ 180.609 Fluoxastrobin; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of fluoxastrobin, (1E)-[2-[[6-(2chlorophenoxy)-5-fluoro-4-pyrimydinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone Omethyloxime, and its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimydinyl]oxy]phenyl](5,6dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, in or on the following raw agricultural commodities:

Commodity

Parts per million

Leaf petioles subgroup 4B

4.0

Peanut

0.010

Peanut, hay

20.0

Peanut, refined oil

0.030

Tomato, paste

1.5

Vegetable, fruiting, group 8

1.0

Vegetable, tuberous and corm, subgroup 1C

0.010

(2) Tolerances are established for the combined residues of fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5fluoro-4-pyrimydinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, its Z isomer,
(1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimydinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)
methanone O-methyloxime, and its phenoxy-hydroxypyrimidine metabolite, 6-(2-chlorophenoxy)-5-fluoro-4pyrimidinol, in or on the following raw agricultural commodities:

Commodity

Parts per million

Cattle, fat

0.10

Cattle, meat

0.05

Cattle, meat byproducts

0.10

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Goat, fat

0.10

Goat, meat

0.05

Goat, meat byproducts

0.10

Horse, fat

0.10

Horse, meat

0.05

Horse, meat byproducts

0.10

Milk

0.02

Milk, fat

0.50

Sheep, fat

0.10

Sheep, meat

0.05

Sheep, meat byproducts

0.10

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for the indirect or inadvertent combined
residues of fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimydinyl]oxy]phenyl](5,6-dihydro1,4,2-dioxazin-3-yl)methanone O-methyloxime, and its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4pyrimydinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, in or on the following
raw agricultural commodities when present therein as a result of the application of fluoxastrobin to the
growing crops listed in paragraph (a)(1) of this section:

Commodity

Parts per million

Alfalfa, forage

0.050

Alfalfa, hay

0.10

Cotton, gin byproducts

0.020

Grain, cereal, forage, fodder, and straw, group 16

0.10

Grass, forage

0.10

Grass, hay

0.50

Vegetable, foliage of legume, group 7

0.050

[70 FR 54650, Sept. 16, 2005]

§ 180.610 Aminopyralid; tolerances for residues.
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(a) General . (1) Tolerances are established for free and conjugated residues of the herbicide,
aminopyralid (2-pyridine carboxylic acid, 4-amino-3,6-dichloro-) calculated as aminopyralid in or on:

Commodity

Parts per million

Grain, aspirated fractions

0.2

Grass, forage

25

Grass, hay

50

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Wheat, bran

0.1

Wheat, forage

2.0

Wheat, grain

0.04

Wheat, hay

4.0

Wheat, straw

0.25

(2) Tolerances are established for residues of the herbicide aminopyralid in or on:

Commodity

Parts per million

Cattle, fat

0.02

Cattle, kidney

0.3

Cattle, meat

0.02

Cattle, meat byproducts, except kidney

0.02

Goat, fat

0.02

Goat, kidney

0.3

Goat, meat

0.02

Goat, meat byproducts, except kidney

0.02

Horse, fat

0.02

Horse, kidney

0.3

Horse, meat

0.02

Horse, meat byproducts, except kidney

0.02

Milk

0.03

Sheep, fat

0.02

Sheep, kidney

0.3

Sheep, meat

0.02

Sheep, meat byproducts, except kidney

0.02

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[70 FR 46428, Aug. 10, 2005]

§ 180.611 Pinoxaden; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of pinoxaden (8-(2,6-diethyl-4methylphenyl)-1,2,4,5-tetrahydro-7-oxo-7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9-yl 2,2dimethylpropanoate), and its metabolites 8-(2,6-diethyl-4-methyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5]
oxadiazepine-7,9-dione (M2), and free and conjugated forms of 8-(2,6-diethyl-4-hydroxymethyl-phenyl)tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione (M4), and 4-(7,9-dioxo-hexahydro-pyrazolo[1,2-d]
[1,4,5]oxadiazepin-8-yl)-3,5-diethyl-benzoic acid (M6), calculated as pinoxaden, in/on the following
commodities:
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Commodity

Parts per million

Barley, bran

1.6

Barley, grain

0.9

Barley, hay

1.5

Barley, straw

1.0

Egg

0.06

Poultry, fat

0.06

Poultry, meat

0.06

Poultry, meat byproducts

0.06

Wheat, bran

3.0

Wheat, forage

3.5

Wheat, grain

1.3

Wheat, hay

2.0

Wheat, straw

1.5

(2) For the combined residues of pinoxaden, 8-(2,6-diethyl-4-methylphenyl)-1,2,4,5-tetrahydro-7-oxo-7Hpyrazolo[1,2-d][1,4,5] oxadiazepin-9-yl 2,2-dimethylpropanoate), and its metabolites M2, 8-(2,6-diethyl-4methyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5]oxadiazepine-7,9-dione, and free and conjugated forms of
M4, 8-(2,6-diethyl-4-hydroxymethyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione,
calculated as pinoxaden, in/on the following commodities:

Commodity

Parts per million

Cattle, fat

0.04

Cattle, meat

0.04

Cattle, meat byproducts

0.04

Milk

0.02

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[70 FR 43322, July 27, 2005]

§ 180.612 Topramezone; tolerances for residues.
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(a) General . (1) Tolerances are established for residues of the herbicide topramezone, [3-(4,5-dihydro-3isoxazolyl)-2-methyl-4-(methylsulfonyl)phenyl](5-hydroxy-1-methyl-1H-pyrazol-4-yl)methanone, in or on
the following raw agricultural commodities:

Commodity
Cattle, kidney
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Parts per million
0.05

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Cattle, liver

0.15

Corn, field, forage

0.05

Corn, field, grain

0.01

Corn, field, stover

0.05

Corn, pop, grain

0.01

Corn, pop, stover

0.05

Corn, sweet, forage

0.05

Corn, sweet, kernel plus cob with husks removed

0.01

Corn, sweet, stover

0.05

Goat, kidney

0.05

Goat, liver

0.15

Horse, kidney

0.05

Horse, liver

0.15

Sheep, kidney

0.05

Sheep, liver

0.15

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[70 FR 46419, Aug. 10, 2005]

§ 180.613 Flonicamid; tolerances for residues.
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(a) General . (1) Tolerances are established for the combined residues of flonicamid [ N -(cyanomethyl)-4(trifluoromethyl)-3-pyridinecarboxamide] and its metabolites TFNA [4-trifluoromethylnicotinic acid], TFNAAM [4-trifluoromethylnicotinamide] TFNG [ N -(4-trifluoromethylnicotinoyl)glycine] in or on the following raw
agricultural commodities:

Commodity
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

Parts per million
1.5
16

Cotton, gin byproducts

6.0

Cotton, hulls

2.0

Cotton, meal

1.0

Cotton, undelinted seed

0.50

Fruit, pome, group 11

0.20

Fruit, stone, group 12

0.60

Hop, dried cones
Okra

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7.0
0.40

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Potato, granules/flakes

0.40

Radish, tops

16

Spinach

9.0

Tomato, paste

2.0

Tomato, puree

0.50

Turnip, greens

16

Vegetable, cucurbit, group 9

0.40

Vegetable, fruiting, group 8

0.40

Vegetable, leafy, except brassica, group 4, except spinach

4.0

Vegetable, root, except sugar beet, subgroup 1B

0.60

Vegetable, tuberous and corm, subgroup 1C

0.20

(2) Tolerances are established for combined residues of flonicamid [ N -(cyanomethyl)-4-(trifluoromethyl)-3pyridinecarboxamide], and its metabolites TFNA [4-trifluoromethylnicotinic acid], TFNA-AM [4trifluoromethylnicotinamide] in or on the following raw agricultural commodities:

Commodity

Parts per million

Cattle, fat

0.03

Cattle, meat

0.08

Cattle, meat byproducts

0.08

Egg

0.04

Goat, fat

0.03

Goat, meat

0.08

Goat, meat byproducts

0.08

Horse, fat

0.03

Horse, meat

0.08

Horse, meat byproducts

0.08

Milk

0.03

Poultry, fat

0.03

Poultry, meat

0.03

Poultry, meat byproducts

0.03

Sheep, fat

0.03

Sheep, meat

0.08

Sheep, meat byproducts

0.08

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[70 FR 51614, Aug. 31, 2005, as amended at 71 FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, 2008]

§ 180.614 Kasugamycin; tolerances for residues.
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(a) General . Tolerances are established for residues of kasugamycin, 3-O-[2-amino-4[(carboxyiminomethyl)amino]-2,3,4,6-tetradeoxy-α-D-arabino-hexopyranosyl]-D-chiro-inositol in or on the
following raw agricultural commodity:

Commodity

Parts per million
0.04

Vegetable, fruiting, group 81
1There

is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[70 FR 55752, Sept. 23, 2005]

§ 180.615 Amicarbazone; tolerances for residues.
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(a) General . Tolerances are established for combined residues of the herbicide, amicarbazone [4-amino4, 5-dihydro- N-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and its
metabolites DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole1-carboxamide] and iPr-2-OH DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide], calculated as parent equivalents, in or on the
following commodities:

Commodity

Parts per million

Cattle, fat

0.01

Cattle, liver

1.0

Cattle, meat

0.01

Cattle, meat byproducts, except liver

0.10

Corn, field, forage

0.80

Corn, field, grain

0.05

Corn, field, stover

1.0

Goat, fat

0.01

Goat, liver

1.0

Goat, meat

0.01

Goat, meat byproducts, except liver

0.10

Hog, fat

0.01

Hog, liver

0.10

Hog, meat

0.01

Hog, meat byproducts, except liver

0.01

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Horse, fat

0.01

Horse, liver

1.0

Horse, meat

0.01

Horse, meat byproducts, except liver

0.10

Milk

0.01

Sheep, fat

0.01

Sheep, liver

1.0

Sheep, meat

0.01

Sheep, meat byproducts, except liver

0.10

Poultry, liver

0.10

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for the indirect or inadvertent residues of
amicarbazone [4-amino-4, 5-dihydro-N-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1carboxamide] and its metabolites DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5oxo-1H-1,2,4-triazole-1-carboxamide] and iPr-2-OH DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3(1-hydroxy-1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide], calculated as parent equivalents, in or
on the following commodities when present therein as a result of application of amicarbazone to the
growing crops in paragraph (a) of this section:

Commodity

Parts per million

Alfalfa, forage

0.05

Alfalfa, hay

0.10

Cotton, gin byproducts

0.30

Cotton, undelinted seed

0.07

Soybean, forage

1.50

Soybean, hay

5.0

Soybean, seed

0.80

Wheat, forage

0.50

Wheat, grain

0.10

Wheat, hay

1.0

Wheat, milled byproducts

0.15

Wheat, straw

0.50

[70 FR 55760, Sept. 23, 2005]

§ 180.616 Fenpropimorph; tolerances for residues.
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Tolerances are established for the residues of the fungicide fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1dimethylethyl)phenyl]-2-methylpropyl]-2,6-dimethylmorpholine) in or on the following commodity:

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Commodity

Parts per million

Banana*

2.0

*No U.S. registration as of February 10, 2006.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 15612, Mar. 29, 2006]

§ 180.617 Metconazole; tolerances for residues.
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(a)(1) General . Tolerances are established for the residue of the fungicide metconazole (5-[(4chlorophenyl)methyl]-2,2-dimethyl-1-(1 H -1,2,4-triazol-1-ylmethyl)cyclopentanol) in or on the following
commodity:

Commodity

Parts per million

Almond, hulls

4.0

Banana1

0.1

Barley, grain

2.5

Barley, hay

7.0

Barley, straw

7.0

Beet, sugar, dried pulp

0.70

Beet, sugar, molasses

0.08

Beet, sugar, roots

0.07

Cattle, meat byproducts

0.04

Fruit, stone, group 12

0.20

Goat, meat byproducts

0.04

Grain, aspirated grain fractions

7.0

Horse, meat byproducts

0.04

Nut, tree, group 14

0.04

Oat, grain
Oat, hay
Oat, straw

1.0
17
6.0

Peanut

0.04

Peanut, refined oil

0.05

Pistachio

0.04

Rye, grain

0.25

Rye, straw

14

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Sheep, meat byproducts

0.04

Soybean, forage

3.0

Soybean, hay

6.0

Soybean, hulls

0.08

Soybean, seed

0.05

Wheat, grain

0.15

Wheat, hay

16

Wheat, milled byproducts

0.20

Wheat, straw
1No

18

U.S. registration as of August 30, 2006.

(2) Tolerances are established for the residues of the fungicide metconazole, including its metabolites and
degradates, in or on commodities in the following table. Compliance with the tolerance levels specified in
the table is to be determined by measuring only metconazole, 5-[(4-chlorophenyl)-methyl]-2,2-dimethyl-1(1 H -1,2,4-triazol-1-ylmethyl)cyclopentanol) as the sum of its cis- and trans- isomers in or on the following
commodities:

Commodity

Parts per million

Canola seed

0.04

Corn, field, forage

3.0

Corn, field, grain

0.02

Corn, field, stover

4.5

Corn, pop, grain

0.02

Corn, pop, stover

4.5

Corn, sweet, forage

3.0

Corn, sweet, kernel plus cob with husks removed

0.01

Corn, sweet, stover

4.5

Cotton, gin byproducts

8.0

Cotton, undelinted seed

0.25

Egg

0.04

(b) Section 18 emergency exemptions . Time-limited tolerances are established for the residues of the
fungicide metconazole, including its metabolites and degradates, in or on the commodities listed in the
following table in connection with the use of the pesticide under section 18 emergency exemptions granted
by EPA. The tolerances expire and are revoked on the dates specified in the following table. Compliance
with the tolerance levels specified below is to be determined by measuring only metconazole (5-[(4chlorophenyl)-methyl]-2,2-dimethyl-1-(1 H -1,2,4-triazol-1-ylmethyl)cyclopentanol) as the sum of its cisand trans-isomers in or on the following commodities:

Commodity

Parts per million

Expiration/revocation date

Sugarcane, cane

1.6

12/31/11

Sugarcane, molasses

3.2

12/31/11

(c) Tolerances with regional registrations . [Reserved]

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(d) Indirect or inadvertent residues . [Reserved]
[71 FR 56388, Sept. 27, 2006, as amended at 71 FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, 2008;
74 FR 21266, May 7, 2009]

§ 180.618 Benthiavalicarb-isopropyl; tolerance for residues.
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(a) General . Tolerances are established for the combined residues of benthiavalicarb-isopropyl, isopropyl
[(S)-1-[[[(1R)-1-(6-fluoro-2-benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate and isopropyl
[(S)-1-[[[(1S)-1-(6-fluoro-2-benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate, in or on the
following raw agricultural commodities:

Commodity

Parts per million

Grape, imported

0.25

Grape, raisin

1.0

Tomato

0.45

Note: There are no U.S. registrations as of July 30, 2006.
(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect of inadvertent residues . [Reserved]
[71 FR 52003, Sept. 1, 2006]

§ 180.619 Epoxiconazole; tolerances for residues.
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(a) General . Tolerances are established for the residues of the fungicide epoxiconazole [( rel -1-[[(2R,3S)3-(2-chlorophenyl)-2-(4-fluorophenyl)oxiranyl]methyl]-1 H -1,2,4-triazole]) in or on the following
commodities:

Commodity

Parts per million

Banana*

0.5

Coffee*

0.05

*No

U.S. Registration as of August 4, 2006

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional Registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 53989, Sept. 13, 2006]
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§ 180.620 Etofenprox; tolerances for residues.
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(a) General . A tolerance is established for residues of the insecticide etofenprox [2-(4-ethoxyphenyl)-2methylpropyl 3-phenoxybenzyl ether] in or on the following raw agricultural commodity:

Commodity

Parts per million

Rice, grain

0.01

(b) Section 18 emergency exemptions . Time-limited tolerances are established for residues of etofenprox
(2-[ethoxyphenyl]-2-methylpropyl-3-phenoxy benzyl ether) in connection with use of the pesticide under
section 18 emergency exemptions granted by EPA. The tolerances will expire and are revoked on the
dates specified in the following table.

Commodity

Parts per million

Expiration/revocation date

Rice, grain

0.01

12/31/09

Rice, straw

0.02

12/31/09

(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 54928, Sept. 20, 2006, as amended at 73 FR 75605, Dec. 12, 2008]

§ 180.621 Dithianon; tolerances for residues.
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(a) General . Tolerances are established for residues of the fungicide dithianon, (5,10-dihydro-5,10dioxonaphtho(2,3-b)-1,4-dithiin-2,3-dicarbonitrile) in or on the following commodities:

Commodity

Parts per million

Fruit, pome, group 111
Hop, dried cones1
1No

U.S. registration as of September 5, 2006.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 54922, Sept. 20, 2006]

§ 180.622 Ethaboxam; tolerances for residues.

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100

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(a) General . Tolerances are established for residues of ethaboxam, N -(cyano-2-thienylmethyl)-4-ethyl-2(ethlyamino)-5-thiazolecarboxamide in or on the following commodity:

Commodity

Parts per million
6.0

Grape1
1There

is no U.S. registration as of September 27, 2006

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 56392, Sept. 27, 2006]

§ 180.623 Flufenoxuron; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide, flufenoxuron, 1-[4-(2-chloro-α,α,αtrifluoro-p-tolyloxy)-2-fluorophenyl]-3-(2,6-difluorobenzoyl)urea, in or on the following food commodities.

Commodity

Parts per million

Apple1
Cattle, fat1

0.50
4.5

Cattle, meat1

0.10

Cattle, meat byproducts1

0.50

Goat, fat1

4.5

Goat, meat1

0.10

Goat, meat byproducts1

0.50

Grape1

0.70

Grape, raisin1

2.0

Horse, fat1

4.5

Horse, meat1

0.10

Horse, meat byproducts1

0.50

Milk

0.20

Milk, fat1

4.0

Orange1

0.30

Orange, oil1
Pear1
Sheep, fat1
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60
0.50
4.5

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Sheep, meat1

0.10

Sheep, meat byproducts1

0.50

1There

are no U.S. registrations as of September 30, 2006.

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional restrictions . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 57436, Sept. 29, 2006]

§ 180.624 Metrafenone; tolerances for residues.
top
(a) General . Tolerances are established for residues of metrafenone, (3-bromo-6-methoxy-2methylphenyl)(2,3,4-trimethoxy-6-methylphenyl)methanone, in or on the following commodities.

Commodity

Parts per million

Grape
1There

0.61

is no U.S. registration on grapes as of September 20, 2006.

(b) Section 18 emergency exemption . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[71 FR 54917, Sept. 20, 2006]

§ 180.625 Orthosulfamuron; tolerances for residues.
top
(a) General . Tolerances are established for residues of orthosulfamuron 1-(4,6-dimethoxypyrimidin-2-yl)-3[2-(dimethylcarbamoyl)- phenylsulfamoyl] urea) per se in or on the following commodities:

Commodity

Parts per million

Rice, grain

0.05

Rice, straw

0.05

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect and inadvertant residues . [Reserved]
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[72 FR 8931, Feb. 28, 2007]

§ 180.626 Prothioconazole; tolerances for residues.
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(a) General . (1) Tolerances are established for combined residues of the fungicide prothioconazole, 2-[2(1-chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2-dihydro-3 H -1,2,4-triazole-3-thione, and
prothioconazole-desthio, α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)methyl]-1 H -1,2,4-triazole-1-ethanol,
calculated as parent in or on the following commodities:

Commodity

Parts per million

Barley, grain

0.35

Barley, hay

7.0

Barley, straw

4.0

Beet, sugar, roots

0.25

Grain, aspirated grain fractions

11

Pea and bean, dried shelled, except soybean, subgroup 6C

0.9

Peanut

0.02

Peanut, hay

6.0

Rapeseed, seed

0.15

Soybean, forage

4.5

Soybean, hay

17

Soybean, seed

0.15

Wheat, forage

8

Wheat, grain

0.07

Wheat, hay

4.5

Wheat, straw

5.0

(2) Tolerances are established for combined residues of the fungicide prothioconazole, 2-[2-(1chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2-dihydro-3 H -1,2,4-triazole-3-thione, and
prothioconazole-desthio, α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)methyl]-1 H -1,2,4-triazole-1-ethanol,
and conjugates that can be converted to these two compounds by acid hydrolysis, calculated as parent in
or on the following commodities:

Commodity

Parts per million

Cattle, fat
Cattle, meat

0.1
0.02

Cattle, meat byproducts

0.2

Goat, fat

0.1

Goat, meat

0.02

Goat, meat byproducts

0.2

Hog, meat byproducts

0.05

Horse, fat
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Horse, meat

0.02

Horse, meat byproducts

0.2

Milk

0.02

Poultry liver

0.02

Sheep, fat

0.1

Sheep, meat

0.02

Sheep, meat byproducts

0.2

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 11783, Mar. 14, 2007, as amended at 73 FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, 2009]

§ 180.627 Fluopicolide; tolerances for residues.
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(a) General . Tolerances are established for residues of fluopicolide, 2,6-dichloro- N -[[3-chloro-5(trifluoromethyl)-2-pyridinyl]methyl]benzamide, as an indicator of combined residues of fluopicolide and its
metabolite, 2,6-dichlorobenzamide (BAM).

Commodity

Parts per million

Brassica, head and stem, subgroup 5A

5.0

Grape

2.0

Grape, raisin

6.0

Vegetable, bulb, crop group 3–07

7.0

Vegetable, cucurbit, group 9

0.50

Vegetable, fruiting, group 8

1.60

Vegetable, leafy, except brassica, group 4

25

Vegetable, leaves of root and tuber, group 2

15.0

Vegetable, root, subgroup 1A, except sugar beet and carrot

0.15

Vegetable, tuberous and corm (except potato), subgroup 1D

0.02

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 14447, Mar. 28, 2007, as amended at 73 FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, 2008]

§ 180.628 Chlorantraniliprole; tolerances for residues.

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top
(a) Tolerances are established for residues of the pesticide chlorantraniliprole (3-bromo- N -[4-chloro-2methyl-6-[(methylamino)carbonyl]phenyl]-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxamide) in or on the
following raw agricultural commodities:

Commodity
Almond, hulls
Apple, wet pomace
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

Parts per million
5.0
0.60
4.0
11

Cattle, fat

0.01

Cattle, meat

0.01

Cattle, meat byproducts

0.01

Cotton, gin byproduct

30

Cotton, hulls

0.40

Cotton, undelinted seed

0.30

Fruit, pome, group 11

0.30

Fruit, stone, group 12

1.0

Goat, fat

0.01

Goat, meat

0.01

Goat, meat byproduct

0.01

Grape

1.2

Grape, raisin

2.5

Horse, fat

0.01

Horse, meat

0.01

Horse, meat byproduct

0.01

Milk

0.01

Nut, tree, group 14

0.04

Pistachio

0.04

Potato

0.01

Sheep, fat

0.01

Sheep, meat

0.01

Sheep, meat byproduct

0.01

Vegetable, cucurbit, group 9

0.25

Vegetable, fruiting, group 8

0.70

Vegetable, leafy, except brassica, group 4

13

(b) Section 18 emergency exemptions . A time-limited tolerance is established for the residues of the
insecticide chlorantraniliprole, 3-bromo- N -[4-chloro-2-methyl-6-[(methylamino) carbonyl]phenyl]-1-(3chloro-2-pyridinyl)-1 H-pyrazole-5-carboxamide, in connection with use of the pesticide under a section 18
emergency exemption granted by EPA. This tolerance will expire and is revoked on the date specified in
the following table.

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Commodity

Parts per million Expiration/Revocation Date

Corn, sweet, cannery waste

6.0

12/31/11

Corn, sweet, forage

6.0

12/31/11

0.01

12/31/11

6.0

12/31/11

Milk

0.03

12/31/11

Rice, grain

0.10

12/31/11

Rice, straw

0.25

12/31/11

Corn, sweet, kernel plus cob with
husks removed
Corn, sweet, stover

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues . Time-limited tolerances are established for indirect or inadvertent
residues of the insecticide chlorantraniliprole (3-bromo- N -[4-chloro-2-methyl-6-[(methylamino)carbonyl]
phenyl]-1-(3-chloro-2-pyridinyl)-1 H -pyrazole-5-carboxamide) in or on the following commodities. The
tolerances will expire and are revoked on the dates specified in the following table.

Commodity

Expiration/
Parts per million revocation date

Animal feed, nongrass, group 18

0.20

04/10/10

Cowpea, forage

0.20

04/10/10

Cowpea, hay

0.20

04/10/10

Field pea, hay

0.20

04/10/10

Field pea, vine

0.20

04/10/10

Grain, cereal, forage, fodder and straw, group 16

0.20

04/10/10

Grass, forage, fodder and hay, group 17

0.20

04/10/10

Leek

0.20

04/10/10

Okra

0.70

04/10/10

Onion, green

0.20

04/10/10

Onion, Welsh

0.20

04/10/10

Peanut, hay

0.20

04/10/10

Shallot

0.20

04/10/10

Soybean, forage

0.20

04/10/10

Soybean, hay

0.20

04/10/10

Strawberry

1.20

04/10/10

Sugarcane

0.20

04/10/10

Vegetable, leaves of root and tuber, group 2

0.20

04/10/10

[72 FR 27455, May 16, 2007, as amended at 73 FR 25523, May 7, 2008; 73 FR 51731, Sept. 5, 2008; 74
FR 30474, June 26, 2009]

§ 180.629 Flutriafol; tolerance for residues.
top

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(a) General . [Reserved]
(b) Section 18 emergency exemptions . Time-limited tolerances specifed in the above table are
established for residues of the fungicide flutriafol per se (2,4'-difluoro-α-(1H -1,2,4-triazol-1-yl-methyl)benzhydryl alcohol) in or on the specified agricultural commodities, resulting from use of the pesticide
pursuant to section 18 emergency exemptions. The tolerances expire and are revoked on the date
specified in the following table.

Parts per million
Soybean

Expiration/revocation date
0.10

12/31/10

(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 49665, Aug. 29, 2007]

§ 180.630 Flusilazole; tolerances for residues.
top
(a) General . [Reserved]
(b) Section 18 emergency exemptions . Time-limited tolerances are established for residues of the
fungicide, flusilazole, (1-[[bis(4-fluorophenyl)methylsilyl]methyl]-1H-1,2,4-triazole) in connection with use of
the pesticide under Section 18 emergency exemptions granted by EPA. The tolerances expire and are
revoked on the dates specified in the following table.

Commodity

Parts per million

Soybean, aspirated grain fractions

Expiration/revocation date

2.6

12/31/10

Soybean, seed

0.04

12/31/10

Soybean, oil

0.10

12/31/10

(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertant residues . [Reserved]
[72 FR 49660, Aug. 29, 2007]

§ 180.631 Pyrasulfotole; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide pyrasulfotole and pyrasulfotoledesmethyl, (5-hydroxy-1,3-dimethyl-1 H -pyrazol-4-yl)[2-(methylsulfonyl)-4-(trifluoromethyl)phenyl]
methanone, and its metabolite, 5-hydroxy-3-methyl-1 H -pyrazol-4-yl) [2-methylsulfornyl)-4-(trifluoromethyl)
phenyl]methanone, in or on the following agricultural commodities:

Commodity

Parts per million

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Aspirated grain fractions

0.40

Barley, grain

0.02

Barley, hay

0.30

Barley, straw

0.20

Cattle, fat

0.02

Cattle, liver

0.35

Cattle, meat

0.02

Cattle, meat byproducts, except liver

0.06

Eggs

0.02

Goat, fat

0.02

Goat, liver

0.35

Goat, meat

0.02

Goat, meat byproducts, except liver

0.06

Hog, fat

0.02

Hog, meat

0.02

Hog, meat byproducts

0.02

Horse, fat

0.02

Horse, liver

0.35

Horse, meat

0.02

Horse, meat byproducts, except liver

0.06

Milk

0.01

Oat, forage

0.10

Oat, grain

0.08

Oat, hay

0.50

Oat, straw

0.20

Poultry, fat

0.02

Poultry, meat

0.02

Poultry, meat byproducts

0.02

Rye, forage

0.20

Rye, grain

0.02

Rye, straw

0.20

Sheep, fat

0.02

Sheep, liver

0.35

Sheep, meat

0.02

Sheep, meat byproducts, except liver

0.06

Wheat, forage

0.20

Wheat, grain

0.02

Wheat, hay

0.80

Wheat, straw

0.20

(b) Section 18 emergency exemptions . [Reserved]
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(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 45649, Aug. 15, 2007]

§ 180.632 Fenazaquin; import tolerances for residues.
top
(a) General . Import tolerances are established for residues of the insecticide and miticide, fenazaquin, 4tert-butylphenethyl quinazolin-4-yl ether, in or on raw agricultural commodities as follows:

Commodity

Parts per million

Apple

0.2

Citrus Oil

10

Fruit, Citrus, Group 10, except Grapefruit

0.5

Pear

0.2

(b) Section is emergency exempotions . [Reserved]
(c) Tolerances with regional registration . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 44393, Aug. 8, 2007]

§ 180.633 Florasulam; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide florasulam N-(2,6-difluorophenyl)-8fluoro-5-methoxy(1,2,4)triazolo(1,5-c)pyrimidine-2-sulfonamide in or on the following commodities:

Commodity

Parts per million

Barley, grain

0.01

Barley, hay

0.05

Barley, straw

0.05

Oat, forage

0.05

Oat, grain

0.01

Oat, hay

0.05

Oat, straw

0.05

Rye, forage

0.05

Rye, grain

0.01

Rye, straw

0.05

Wheat, forage

0.05

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Wheat, grain

0.01

Wheat, hay

0.05

Wheat, straw

0.05

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[72 FR 55077, Sept. 28, 2007]

§ 180.634 Tembotrione; tolerances for residues.
top
(a) General . Tolerances are established for residues of the herbicide, tembotrione, 2-[2-chloro-4(methylsulfonyl)-3-[(2,2,2-trifluoroethoxy)methyl]benzoyl]-1,3-cyclohexanedione and its metabolite 2-[2chloro-4-(methylsulfonyl)-3-[(2,2,2-trifluoroethoxy)methyl]benzoyl]-4,6-dihydroxycyclohexane-1,3-dione in
or on the following commodities:

Commodity

Parts per million

Cattle, liver

0.40

Cattle, meat byproducts, except liver

0.07

Corn, field, forage

0.60

Corn, field, grain

0.02

Corn, field, stover

0.45

Corn, pop, grain

0.02

Corn, pop, stover

0.35

Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

1.0
0.04
1.2

Goat, liver

0.40

Goat, meat byproducts, except liver

0.07

Horse, liver

0.40

Horse, meat byproducts, except liver

0.07

Poultry, liver

0.07

Sheep, liver

0.40

Sheep, meat byproducts, except liver

0.07

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]

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[72 FR 55085, Sept. 28, 2007]

§ 180.635 Spinetoram; tolerances for residues.
top
(a) General . Tolerances are established for the combined residues of the insecticide spinetoram,
expressed as a combination of XDE-175-J: 1-H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione, 2-[(6deoxy-3-O-ethyl-2,4-di-O-methyl-a-L-mannopyranosyl) oxy]-13-[[(2R,5S,6R)-5- (dimethylamino)tetrahydro6-methyl-2H-pyran-2-yl] oxy]-9-ethyl-2,3,3a,4,5,5a,5b,6,9, 10,11,12,13,14,16a,16b- hexadecahydro 14methyl-, (2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR); XDE-175-L: 1H-as-indaceno[3,2-d]oxacyclododecin7,15-dione, 2-[(6-deoxy-3-O- ethyl-2,4-di-O-methyl-a-L-mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5(dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9, 10,11,12,13,14,16a,16btetradecahydro-4,14-dimethyl-, (2S,3aR,5aS,5bS,9S, 13S,14R,16aS,16bS); ND-J: (2R,3aR,5aR,5bS,9S,
13S,14R,16aS,16bR)-9-ethyl-14-methyl-13-[[(2S,5S,6R)-6- methyl-5-(methylamino)tetrahydro- 2H-pyran-2yl]oxy]-7,15-dioxo-2,3,3a,4,5,5a,5b,6,7,9, 10,11,12,13,14,15,16a,16b- octadecahydro-1H-as- indaceno[3,2d]oxacyclododecin-2-yl 6-deoxy-3-O-ethyl-2,4-di-O-methyl- alpha-L-mannopyranoside; and NF-J:
(2R,3S,6S)-6-([(2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR)- 2-[(6-deoxy-3-O-ethyl-2,4-di-O- methyl-alphaL-mannopyranosyl) oxy]-9-ethyl-14-methyl-7,15-dioxo-2, 3,3a,4,5,5a,5b,6,7,9, 10,11,12,13,14,15,16a,16boctadecahydro-1H-as- indaceno[3,2-d]oxacyclododecin-13-yl] oxy)-2-methyltetrahydro- 2H-pyran-3-yl
(methyl)formamide, in or on the following raw agricultural commodities:

Commodity
Acerola
Almond, hulls
Amaranth grain, grain

Parts per million
0.30
19
1.0

Apple, wet pomace

0.50

Artichoke, globe

0.30

Asparagus

0.04

Atemoya

0.30

Avocado

0.30

Banana

0.25

Beet, sugar, molasses

0.75

Biriba

0.30

Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

2.0
10

Bushberry, subgroup 13B

0.25

Caneberry, subgroup 13A

0.70

Canistel

0.30

Cattle, fat

5.5

Cattle, liver

0.85

Cattle, meat

0.20

Cattle, meat byproducts (except liver)

0.60

Cherimoya

0.30

Citrus, dried pulp

0.50

Citrus, oil
Corn, sweet, kernel plus cob with husks removed
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3.0
0.04

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Cotton, gin byproducts

1.5

Cotton, undelinted seed

0.04

Cranberry

0.04

Custard apple

0.30

Date

0.10

Egg

0.04

Feijoa

0.30

Fig

0.10

Fruit, citrus, group 10

0.30

Fruit, pome, group 11

0.20

Fruit, stone, group 12

0.20

Goat, fat

5.5

Goat, liver

0.85

Goat, meat

0.20

Goat, meat byproducts (except liver)

0.60

Grain, aspirated fractions
Grain, cereal, group 15, except rice, sorghum, pearl millet and proso
millet
Grain, cereal, group 16, forage

20
0.04
3.5

Grain, cereal, group 16, hay

10

Grain, cereal, group 16, stover

10

Grain, cereal, straw, group 16, except rice

1.0

Grape

0.50

Grape, raisin

0.70

Guava

0.30

Herb, dried, subgroup 19A

22

Herb, fresh, subgroup 19A

3.0

Hog, fat

0.40

Hog, meat

0.04

Hog, meat byproducts

0.04

Hop, dried cones
Horse, fat

22
5.5

Horse, liver

0.85

Horse, meat

0.20

Horse, meat byproducts (except liver)

0.60

Ilama

0.30

Jaboticaba

0.30

Juneberry

0.25

Lingonberry

0.25

Longan

0.30

Lychee

0.30

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Mango

0.30

Milk

0.30

Milk, fat

7.5

Millet, pearl, grain

1.0

Millet, proso, grain

1.0

Nut, tree, group 14

0.10

Okra

0.40

Onion, green

2.0

Papaya

0.30

Passionfruit

0.30

Pea and bean, dried shelled, except soybean, subgroup 6C

0.04

Pea and bean, succulent shelled, subgroup 6B

0.04

Peanut

0.04

Peanut, hay
Peppermint, tops

11
3.5

Pineapple

0.04

Pineapple, processed residue

0.15

Pistachio

0.10

Pomegranate

0.30

Poultry, fat

0.10

Poultry, meat

0.04

Poultry, meat byproducts

0.04

Pulasan

0.30

Rambutan

0.30

Salal

0.25

Sapodilla

0.30

Sapote, black

0.30

Sapote, mamey

0.30

Sapote, white

0.30

Sheep, fat

5.5

Sheep, liver

0.85

Sheep, meat

0.20

Sheep, meat products (except liver)

0.60

Sorghum, grain, grain

1.0

Soursop

0.30

Soybean, seed

0.04

Spanish lime

0.30

Spearmint, tops

3.5

Spice, subgroup 19B, except black pepper

1.7

Star apple

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0.30

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Star fruit

0.30

Strawberry

1.0

Sugar apple

0.30

Ti, leaves

10

Vegetable, bulb, group 3, except green onion

0.10

Vegetable, cucurbit, group 9

0.30

Vegetable, foliage of legume, group 7

8.0

Vegetable, fruiting, group 8

0.40

Vegetable, leafy, except Brassica, group 4

8.0

Vegetable, leaves of root and tuber, group 2

10

Vegetable, legume, edible podded, subgroup 6A

0.30

Vegetable, root and tuber, group 1

0.10

Watercress

8.0

Wax jambu

0.30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect and invertent residues. [Reserved]
[72 FR 57499, Oct. 10, 2007, as amended at 73 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, 2009]

§ 180.636 1,3-dichloropropene; tolerances for residues.
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(a) General . Tolerances are established for the combined residues of the fungicide cis - and trans -1,3dichloropropene and its metabolites cis - and trans -3-chloroacrylic acid, and cis - and trans -3-chloroallyl
alcohol in or on the following commodities.

Commodity

Parts per million

Grape

0.018

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 8218, Feb. 13, 2008]

§ 180.637 Mandipropamid; tolerances for residues.
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(a) General . Tolerances are established for residues of the fungicide mandipropamid, 4-chloro-N-[2-(3http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c...&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (525 of 651) [9/8/2009 3:02:27 PM]

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methoxy-4-(2-propynyloxy)phenyl]ethyl]-alpha-(2-propynyloxy)-benzeneacetamide in or on the following
commodities.

Commodity

Parts per million

Brassica, head and stem, subgroup 5A

3

Brassica, leafy greens, subgroup 5B

25

Grape

1.4

Grape, raisin

3.0

Hop, dried cones

50

Okra

1.0

Onion, dry bulb

0.05

Onion, green

4

Potato, wet peel

0.03

Vegetable, cucurbit, group 9

0.6

Vegetable, fruiting, group 8

1.0

Vegetable, leafy except Brassica, group 4

20

Vegetable, tuberous and corm, subgroup 1C

0.01

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent tolerances . [Reserved]
[73 FR 2816, Jan. 16, 2008, as amended at 74 FR 33169, July 10, 2009]

§ 180.638 Pyroxsulam; tolerances for residues.
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(a) General . Tolerances are established for residues of the herbicide pyroxsulam, N-(5,7-dimethoxy[1,2,4]
triazolo[1,5-a]pyrimidin-2-yl)-2-methoxy-4-(trifluoromethyl)-3-pyridinesulfonamide in or on the raw
agricultural commodities:

Commodity

Parts per million

Wheat, forage

0.06

Wheat, grain

0.01

Wheat, hay

0.01

Wheat, straw

0.03

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 10402, Feb. 27, 2008]
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§ 180.639 Flubendiamide; tolerances for residues.
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(a) General . Tolerances are established for residues of the insecticide flubendiamide per se , N2 -[1,1Dimethyl-2-(methylsulfonyl)ethyl-3-iodo-N1 -[2-methyl-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl]1,2-benzenedicarboxamide, in or on the following food commodities:

Commodity

Parts per million

Almond, hulls

9.0

Apple, wet pomace

2.0

Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

0.60
5.0

Cattle, fat

0.30

Cattle, kidney

0.30

Cattle, liver

0.30

Cattle, muscle

0.05

Corn, field, forage

8.0

Corn, field, grain

0.02

Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed

15
0.02
15
9.0
0.01

Corn, sweet, stover

25

Cotton, gin byproducts

60

Cotton, undelinted seed

0.90

Egg

0.01

Fruit, pome, group 11

0.70

Fruit, stone, group 12

1.6

Goat, fat

0.30

Goat, kidney

0.30

Goat, liver

0.30

Goat, muscle

0.05

Grain, aspirated fractions

5.0

Grape

1.4

Horse, fat

0.30

Horse, kidney

0.30

Horse, liver

0.30

Horse, muscle

0.05

Milk

0.04

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Milk, fat

0.30

Nut, tree, group 14

0.06

Okra

0.30

Poultry, fat

0.02

Poultry, liver

0.01

Poultry, muscle

0.01

Sheep, fat

0.30

Sheep, kidney

0.30

Sheep, liver

0.30

Sheep, muscle

0.05

Vegetable, cucurbit, group 9

0.20

Vegetable, fruiting, group 8

0.60 ppm

Vegetable, leafy, except Brassica, group 4

11

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for the indirect or inadvertent residues of
the insecticide flubendiamide per se , N2 -[1,1-Dimethyl-2-(methylsulfonyl)ethyl-3-iodo-N1 -[2-methyl-4[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl]-1,2-benzenedicarboxamide, in or on the following raw
agricultural commodities when present therein as a result of the application of flubendiamide per se to the
growing crops listed in paragraph (a) of this section:

Commodity

Parts per million

Alfalfa, forage

0.15

Alfalfa, hay

0.04

Barley, hay

0.04

Barley, straw

0.07

Buckwheat

0.07

Clover, forage

0.15

Clover, hay

0.04

Grass, forage

0.15

Grass, hay

0.04

Millet, pearl, forage

0.15

Millet, pearl, hay

0.04

Millet, proso, forage

0.15

Millet, proso, hay

0.04

Millet, proso, straw

0.07

Oats, forage

0.15

Oats, hay

0.04

Oats, straw

0.07

Rye, forage

0.15

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Rye, straw

0.07

Sorghum, grain, forage

0.03

Sorghum, grain, stover

0.06

Soybean, forage

0.02

Soybean, hay

0.04

Teosinte, forage

0.15

Teosinte, hay

0.04

Teosinte, straw

0.07

Triticale, forage

0.15

Triticale, hay

0.04

Triticale, straw

0.07

Wheat, forage

0.15

Wheat, hay

0.03

Wheat, straw

0.03

[73 FR 47062, Aug. 13, 2008]

§ 180.640 Pyridalyl; tolerances for residues.
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(a) General . Tolerances are established for residues of pyridalyl, pyridine,2-[3-[2,6-dichloro-4-[(3,3dichloro-2-propenyl)oxy]phenoxy]propoxy]-5-(trifluoromethyl, in or on the following raw agricultural
commodities:)

Commodity

Brassica

Parts per million

, head and stem, subgroup 5A

3.5

Mustard greens

30

Turnip greens

30

Vegetable, fruiting, group 8
Vegetables, leafy, except Brassica

1.0
, group 4

20

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 25533, May 7, 2008]

§ 180.641 Spirotetramat; tolerances for residues.
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(a) General . (1) Tolerances are established for residues of the insecticide spirotetramat (cis-3-(2,5dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro [4.5] dec-3-en-4-yl-ethyl carbonate) and its metabolites BYI
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08330-enol (cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro 4.5 dec-3-en-2-one), BYI 08330ketohydroxy (cis-3-(2,5-dimethylphenyl)-3-hydroxy-8-methoxy-1-azaspiro 4.5 decane-2,4-dione),
BYI08330-enol-Glc (cis-3-(2,5-dimethylphenyl)-8-methoxy-2-oxo-1-azaspiro 4.5 dec-3-en-4-yl beta-Dglucopyranoside), and BYI 08330-mono-hydroxy (cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1azaspiro 4.5 decan-2-one), calculated as spirotetramat equivalents, in or on the following raw agricultural
commodities:

Commodity

Parts per million

Almond, hulls

9.0

Brassica, head and stem, subgroup 5A

2.5

Brassica, leafy, subgroup 5B

8.0

Citrus, oil

6.0

Fruit, citrus, group 10

0.60

Fruit, pome, group 11

0.70

Fruit, stone, group 12

4.5

Grape, raisin

3.0

Hop, dried cones

10.0

Nut, tree, group 14

0.25

Onion, bulb, subgroup 3A-07

0.3

Potato, flakes

1.6

Small fruit vine climbing subgroup, except fuzzy kiwifruit, subgroup
13-07F

1.3

Strawberry

0.40

Vegetable, cucurbit, group 9

0.30

Vegetable, fruiting, group 8

2.5

Vegetable, leafy, except brassica, group 4

9.0

Vegetable, tuberous and corm, subgroup 1C

0.60

(2) Tolerances are also established for the combined residues of spirotetramat (cis-3-(2,5-dimethlyphenyl)8-methoxy-2-oxo-1-azaspiro [4.5] dec-3-en-4-yl-ethyl carbonate) and its metabolite BYI 08330-enol (cis-3(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro 4.5 dec-3-en-2-one), calculated as spirotetramat
equivalents, in or on the following commodities:

Commodity

Parts per million

Cattle, fat

0.02

Cattle, meat

0.02

Cattle, meat byproducts

0.02

Goat, fat

0.02

Goat, meat

0.02

Goat, meat byproducts

0.02

Horse, fat

0.02

Horse, meat

0.02

Horse, meat byproducts

0.02

Milk

0.01

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Sheep, fat

0.02

Sheep, meat

0.02

Sheep, meat byproducts

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[73 FR 39256, July 9, 2008]

§ 180.642 Gentamicin; tolerances for residues.
top
(a) General . [Reserved]
(b) Section 18 emergency exemptions . Time-limited tolerances specified in the following table are
established for residues of gentamicin in or on the specified agricultural commodities, resulting from use of
the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire and are
revoked on the date specified in the following table.

Commodity

Parts per million

Apple

Expiration/revocation date

0.10

12/31/10

(c) Tolerance with regional restrictions. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[73 FR 44162, July 30, 2008]

§ 180.643 Uniconazole; tolerances for residues.
top
(a) General. Tolerances are established for residues of the fungicide/plant growth regulator uniconazole-P,
(E)-(S)-1-(4-chlorophenyl)-4,4-dimethyl-2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, its R -enantiomer and its Z isomer in or on the following raw agricultural commodities:

Commodity

Parts per million

Vegetable, fruiting, group 8
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[73 FR 51736, Sept. 5, 2008]
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0.01

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§ 180.644 Cyprosulfamide; tolerances for residues.
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(a) General. (1) Tolerances are established for residues of the herbicide safener cyprosulfamide, N -[[4[(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, in or on the following raw agricultural
commodities:

Commodity

Parts per million

Corn, field, forage

0.20

Corn, field, grain

0.01

Corn, field, stover

0.20

Corn, pop, grain

0.01

Corn, pop, stover

0.20

Corn, sweet, forage

0.40

Corn, sweet, kernel plus cob with husks removed

0.01

Corn, sweet, stover

0.35

(2) Tolerances are established for residues of the herbicide safener cyprosulfamide, N -[[4[(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, and its metabolite 4-(aminosulfonyl)N -cyclopropylbenzamide, calculated as cyprosulfamide, in or on the following raw agricultural
commodities:

Commodity

Parts per million

Cattle, meat byproducts

0.02

Goat, meat byproducts

0.02

Horse, meat byproducts

0.02

Sheep, meat byproducts

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[73 FR 60974, Oct. 15, 2008]

§ 180.645 Thiencarbazone-methyl; tolerances for residues.
top
(a) General . (1) Tolerances are established for residues of thiencarbazone-methyl [methyl 4-[[[(4,5dihydro-3-methoxy-4-methyl-5-oxo-1 H -1,2,4-triazol-1-yl)-carbonyl]amino]sulfonyl]-5-methyl-3thiophenecarboxylate], per se , in or on the following food and feed commodities:

Commodity

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Parts per million

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Corn, field, forage

0.04

Corn, field, grain

0.01

Corn, field, stover

0.02

Corn, pop, grain

0.01

Corn, pop, stover

0.01

Corn, sweet, forage

0.05

Corn, sweet, kernel plus cob with husks removed

0.01

Corn, sweet, stover

0.05

Wheat, forage

0.10

Wheat, grain

0.01

Wheat, hay

0.01

Wheat, straw

0.01

(2) Tolerances are established for combined residues of thiencarbazone-methyl and its metabolite BYH
18636-MMT [5-methoxy-4-methyl-2,4-dihydro-3 H -1,2,4-triazol-3-one], calculated as the parent
compound, in or on the following food commodities of animal origin:

Commodity

Parts per million

Cattle, meat

0.02

Cattle, meat byproducts

0.02

Goat, meat

0.02

Goat, meat byproducts

0.02

Horse, meat

0.02

Horse, meat byproducts

0.02

Milk

0.02

Sheep, meat

0.02

Sheep, meat byproducts

0.02

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . Tolerances are established for indirect or inadvertent combined
residues of thiencarbazone-methyl and its metabolite BYH 18636-MMT-glucoside [2-hexopyranosyl-5methoxy-4-methyl-2,4-dihydro-3 H -1,2,4-triazol-3-one], calculated as the parent compound, in or on the
following food commodities:

Commodity

Parts per million

Soybean, forage

0.04

Soybean, hay

0.15

[73 FR 60968, Oct. 15, 2008]

§ 180.646 Ipconazole; tolerances for residues.

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(a) General . Tolerances are established for residues of ipconazole, (2-[(4-chlorophenyl)methyl]-5-(1methylethyl)-1-(1H-1,2,4-triazole-1-ylmethyl) cyclopentanol) from seed treatment in or on the following
commodities:

Commodity

Parts per million

Cotton, gin byproducts

0.01

Cotton, undelinted seed

0.01

Grain, cereal, forage, fodder and straw, group 16, except rice

0.01

Grain, cereal group 15, except rice

0.01

Pea and bean, dried shelled, except soybean, subgroup 6C

0.01

Peanut

0.01

Soybean, forage

0.01

Soybean, seed

0.01

(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[73 FR 69559, Nov. 19, 2008]

§ 180.647 d-Phenothrin; tolerances for residues.
top
(a) General . A tolerance of 0.01 parts per million is established for residues of the insecticide d-phenothrin
in or on all food/feed crops following wide-area mosquito adulticide applications.
(b) Section 18 emergency exemptions . [Reserved]
(c) Tolerances with regional registrations . [Reserved]
(d) Indirect or inadvertent residues . [Reserved]
[74 FR 32443, July 8, 2009]

Subpart D—Exemptions From Tolerances
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§ 180.900 Exemptions from the requirement of a tolerance.
top
An exemption from a tolerance shall be granted when it appears that the total quantity of the pesticide
chemical in or on all raw agricultural commodities for which it is useful under conditions of use currently
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prevailing or proposed will involve no hazard to the public health.
[69 FR 23117, Apr. 28, 2004]

§ 180.905 Pesticide chemicals; exemptions from the requirement of a tolerance.
top
(a) When applied to growing crops, in accordance with good agricultural practice, the following pesticide
chemicals are exempt from the requirement of a tolerance:
(1) [Reserved]
(2) N -Octylbicyclo(2,2,1)-5-heptene-2,3-dicarboximide.
(3) Petroleum oils.
(4) Piperonyl butoxide.
(5) [Reserved]
(6) Pyrethrum and pyrethrins.
(7) Rotenone or derris or cube roots.
(8) Sabadilla.
(b) These pesticides are not exempted from the requirement of a tolerance when applied to a crop at the
time of or after harvest.
[69 FR 23117, Apr. 28, 2004]

§ 180.910 Inert ingredients used pre- and post-harvest; exemptions from the
requirement of a tolerance.
top
Link to an amendment published at 71 FR 45421, August 9, 2006.
The effective date of the above amendment was delayed in part until August 9, 2009, at 73 FR 45312 and
45316, August 4, 2008.
The effective date of the above amendment was further delayed in part until October 9, 2009, at 74 FR
39543 and 39545, August 7, 2009.
Residues of the following materials are exempted from the requirement of a tolerance when used in
accordance with good agricultural practice as inert (or occasionally active) ingredients in pesticide
formulations applied to growing crops or to raw agricultural commodities after harvest:

Inert ingredients

Limits

Acetic acid

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Uses
Catalyst

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Acetic anhydride

Solvent,
cosolvent

Acetone

Do.

Alkanoic and alkenoic acids, mono- and diesters of αhydro-ω-hydroxypoly (oxyethylene) with molecular
weight (in amu) range of 200 to 6,000

Emulsifiers

Alkyl (C8-C24) benzenesulfonic acid and its ammonium,

Surfactants,
related
adjuvants of
surfactants

calcium, magnesium, potassium, sodium, and zinc salts
α-Alkyl(C6–C15)-ω-hydroxypoly(oxyethylene)sulfate,

Not to exceed
30% of
and its ammonium, calcium, magnesium, potassium,
pesticide
sodium, and zinc salts, poly(oxyethylene) content
averages 2–4 moles (CAS Reg. Nos. 3088–31–1, 9004– formulation
82–4, 9004–84–6, 13150–00–0, 25446–78–0, 26183–
44–8, 32612–48–9, 50602–06–7, 62755–21–9, 68424–
50–0, 68511–39–7, 68585–34–2, 68611–55–2, 68891–
38–3, 73665–22–2)

Surfactants,
related
adjuvants of
surfactants

α-alkyl (C12-C15)-ω-hydroxypoly (oxypropylene) poly

Surfactant

(oxyethylene) copolymers (where the poly
(oxypropylene) content is 3–60 moles and the poly
(oxyethylene) content is 5–80 moles)

Not more than
20% of
pesticide
formulations

α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly
(oxyethylene) polymers where the alkyl chain contains
a minimum of six carbons (CAS Reg. Nos. 9002–92–0,
9004–95–9, 9005–00–9, 26183–52–8, 34398–01–1,
52292–17–8, 66455–14–9, 66455–15–0, 68002–97–1,
68131–39–5, 68131–40–8, 68154–96–1, 68213–23–0,
68439–45–2, 68439–46–3, 68526–94–3, 68439–50–9,
68439–49–6, 68551–12–2, 68951–67–7, 71243–46–4,
97043–91–9, 9043–30–5, 60828–78–6, 61827–42–7,
24938–91–8, 68439–54–3, 69011–36–5, 78330–20–8,
78330–21–9, 106232–83–1, 127036–24–2, 160875–
66–1, 9004–98–2, 68920–66–1, 61804–34–0, 61791–
28–4, 71060–57–6, 26468–86–0, 31726–34–8, 52609–
19–5, 61791–20–6, 68155–01–1, 69013–19–0, 69364–
63–2, 70879–83–3, 78330–19–5, 97953–22–5,
157627–86–6, 34398–05–5, 72905–87–4, 84133–50–
6, 61702–78–1, 27306–79–2, 169107–21–5, 61791–
13–7, 39587–22–9, 85422–93–1; 68154–98–3, 61725–
89–1, 68002–96–0, 68154–97–2, 68439–51–0, 68551–
13–3, 68603–25–8, 68937–66–6, 68987–81–5, 69227–
21–0, 70750–27–5, 103818–93–5, 166736–08–9,
120313–48–6, 68213–24–1, 68458–88–8, 68551–14–
4, 69013–18–9, 69227–22–1, 72854–13–8, 73049–34–
0, 78330–23–1, 37311–02–7, 64366–70–7, 37251–67–
5, 9087–53–0, 196823–11–7, 57679–21–7, 111905–
54–5, 61827–84–7, 172588–43–1)

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Surfactants,
related
adjuvants of
surfactants

Electronic Code of Federal Regulations:

Alkyl (C8-C18) sulfate and its ammonium, calcium,

Surfactants.

isopropylamine, magnesium, potassium, sodium, and
zinc salts
Aluminum hydroxide

Diluent, carrier

Aluminum oxide

Diluent

Aluminum stearate

Surfactant

Ammonium bicarbonate

Surfactant,
suspending
agent,
dispersing
agent

Ammonium carbamate

Synergist in
aluminum
phosphide
formulations

Ammonium chloride

Intensifier
when used
with
ammonium
nitrate as a
dessicant or
defoliant. Fire
suppressant in
aluminum
phosphide and
magnesium
phosphide
formulations

Ammonium hydroxide

Solvent,
cosolvent,
neutralizer,
solubilizing
agent

Ammonium stearate

Surfactant

Ammonium sulfate

Solid diluent,
carrier

Ammonium thiosulfate

Intensifier
when used
with
ammonium
nitrate as
desiccant or
defoliant

Amyl acetate

Solvent,
cosolvent,
attractant

Ascorbyl palmitate

Preservative

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Electronic Code of Federal Regulations:

Attapulgite-type clay

Solid diluent,
carrier,
thickener

Bacillus
thuringiensis
fermentation solids and/or solubles

Diluent, carrier

Bentonite

Solid diluent,
carrier

Benzoic acid

Preservative
for formulation

Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–,
homopolymer (Alpha-pinene, homopolymer )(CAS Reg.
No. 25766–18–1)

Surfactants,
related
adjuvants of
surfactants

Bicyclo[3.1.1]heptane, 6,6–dimethyl–2–methylene–,
homopolymer (Beta-pinene, homopolymer) (CAS Reg.
No. 25719–60–2)

Surfactants,
related
adjuvants of
surfactants

Bicyclo[3.1.1]hept–2–ene, 2,6,6–trimethyl–, polymer
with 6,6– dimethyl–2– methylenebicyclo [3.1.1]
heptane (Copolymer of alpha- and beta-pinene) (CAS
Reg. No. 31393–98–3)

Surfactants,
related
adjuvants of
surfactants

2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52–51– 0.04% or less
7)
by weight of
the total
pesticide
formulation

In-can
preservative

Butane

Propellant

n

Solvent,
cosolvent

-Butanol (CAS Reg. No. 71–36–3)

Butylated hydroxyanisole
Butylated hydroxytoluene
Calcareous shale

Antioxidant
Do.
Solid diluent
carrier

Calcite

Do.

Calcium carbonate

Do.

Calcium chloride

Stabilizer

Calcium phosphate

Solid diluent,
carrier

Calcium hydroxide

Do.

Calcium hypochlorite

Sanitizing and
bleaching agent

Calcium lactate pentahydrate (CAS Reg. No. 5743–47–
5)

Nutrient,
stabilizer

Calcium oxide

Solid diluent,
carrier

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Electronic Code of Federal Regulations:

Calcium salt of partially dimerized rosin, conforming to
21 CFR 172.210

Coating agent

Calcium silicate

Solid diluent,
carrier

Calcium stearate

Do.

Carrageenan, conforming to 21 CFR 172.620

Minimum
molecular
weight (in
amu): 100,000

Thickener

Cetyl alcohol (CAS Reg. No. 36653–82–4)

Not more than
5.0% of
pesticide
formulation

Evaporation
retardant

Charcoal, activated

Carrier
Meets
specifications in
the Food
Chemical Codex

Coconut shells

Solid diluent
and carrier

Cod liver oil

Solvent,
cosolvent

Croscarmellose sodium (CAS Reg. No. 74811–65–7)

Disintegrant,
solid diluent,
carrier, and
thickener

Dialkyl (C8-C18) dimethyl ammonium chloride

Not more than
0.2% in silica,
hydrated silica

Flocculating
agent in the
manufacture
of silica,
hydrated silica
for use as a
solid diluent,
carrier

Diatomite (diatomaceous earth)

Solid diluent
carrier

Diethylene glycol abietate

Surfactants,
related
adjuvants of
surfactants

1,1-Difluoroethane (CAS Reg. No. 75–37–6)

For aerosol
pesticide
formulations
used for insect
control in foodand feedhandling
establishments
and animals

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Aerosol
propellant

Electronic Code of Federal Regulations:

1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene

Not more than
0.02% of
pesticide
formulation

Dimethyl ether (methane, oxybis-) (CAS Reg. No. 115–
10–6)
3,6-Dimethyl-4-octyn-3,6-diol

Antioxidant

Propellant
Not more than
2.5% of
pesticide
formulation

Surfactants,
related
adjuvants of
surfactants

Dipropylene glycol

Solvent,
cosolvent

Disodium phosphate

Anticaking
agent,
conditioning
agent

Disodium zinc ethylenediaminetetraacetate dihydride

Sequestrant

Dolomite

Solid diluent,
carrier

Epoxidized linseed oil

Surfactants,
related
adjuvants of
surfactants

Epoxidized soybean oil

Do.

Ethyl acetate

Solvent,
cosolvent

Ethyl alcohol

Do.

Ethyl esters of fatty acids derived from edible fats and
oils
Ethyl maltol (CAS Reg. No.4940–11–8)

Solvent,
cosolvent
Not more than
0.2 % of the
pesticide
formulation

Ethylene oxide adducts of 2,4,7,9-tetramethyl-5decynediol, the ethylene oxide content averages 3.5,
10 or 30 moles (CAS Reg. No. 9014–85–1)

Odor masking
agent

Surfactants,
related
adjuvants of
surfactants

Ethylenediaminetetraacetic acid

3% of pesticide Sequestrant
formulation

Ethylenediaminetetraacetic acid, tetrasodium salt

5% of pesticide Sequestrant
formulation

2-Ethyl-1-hexanol

Not more than
2.5% of
pesticide
formulation

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Solvent,
adjuvant of
surfactants

Electronic Code of Federal Regulations:

Fatty acids, conforming to 21 CFR 172.860

Binder,
defoaming
agent, lubricant

FD&C Blue No. 1

Not more than
0.2% of
pesticide
formulation

Dye

FD&C Red No. 40 (CAS Reg. No. 25956–17–6)
conforming to 21 CFR 74.340

Not to exceed
0.002% by
weight of
pesticide
formulation

Dye, coloring
agent

Ferric Citrate (CAS Reg. No. 2338–05–8)

Stabilizer

Ferric sulfate

Solid diluent,
carrier

Furcelleran

Thickener

D-glucopyranose, oligomeric, C10–16-alkyl glycosides

Surfactant

(CAS Reg. No. 110615–47–9)
Glycerides, edible fats and oils derived from plants and
animals, reaction products with sucrose (CAS Reg.
Nos. 100403–38–1, 100403–41–6, 100403–39–2,
100403–40–5)

Emulsifier,
dispersing
agent

Glycerol mono-, di-, and triacetate

Solvent,
cosolvent

Glyceryl monostearate

Emulsifier

Granite

Do.

Graphite

Solid diluent,
carrier

Gum arabic (acacia)

Surfactant,
suspending
agent,
dispersing
agent

Gypsum

Solid diluent,
carrier

Hexamethylenetetramine

For use in citrus Preservative
washing
solutions only
at not more
than 1%

3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1)

Not more than
0.4% of the
pesticide
formulation

n

-Hexyl alcohol (CAS Reg. No. 111–27–3)

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Odorant,
alerting agent

Solvent,
cosolvent

Electronic Code of Federal Regulations:

Hydrochloric acid

Solvent,
neutralizer

Hydroxyethylidine diphosphonic acid (HEDP) (CAS Reg. For use in
No. 2809–21–4)
antimicrobial
pesticide
formulations at
not more than
1 percent

Stabilizer,
chelator

Iron oxide

Solid diluent,
carrier

Isopropyl myristate (CAS Reg. No. 110–27–0)

Solvent

Kaolinite-type clay

Solid diluent,
carrier

Lactic acid

Solvent

Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283–86–
9)

Solvent

Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No.
186817–80–1)

Solvent

Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651–
69–7)

Solvent

Lauryl alcohol

Surfactant

Lignin (CAS Reg. No. 9005–53–2)

Surfactant,
related
adjuvants of
surfactants

Lignin, alkali (CAS Reg. No. 8068–05–1)

Do.

Lignin, alkali, oxidized, sodium salt (CAS Reg. No.
68201–23–0)

Do.

Lignin alkali reaction products with disodium sulfite
and formaldehyde (CAS Reg. No. 105859–97–0)

Do.

Lignin alkali reaction products with formaldehyde and
sodium bisulfite (CAS Reg. No. 68512–35–6)

Do.

Lignosulfonic acid (CAS Reg. No. 8062–15–5)

Do.

Lignosulfonic acid, ammonium calcium salt (CAS Reg.
No. 12710–04–2)

Do.

Lignosulfonic acid, ammonium magnesium salt (CAS
Reg. No. 123175–37–1)

Do.

Lignosulfonic acid, ammonium salt (CAS Reg. No.
8061–53–8)

Do.

Lignosulfonic acid, ammonium sodium salt (CAS Reg.
No. 166798–73–8)

Do.

Lignosulfonic acid, calcium magnesium salt (CAS Reg.
No. 55598–86–2)

Do.

Lignosulfonic acid, calcium salt (CAS Reg. No. 8061–
52–7)

Do.

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Electronic Code of Federal Regulations:

Lignosulfonic acid, calcium sodium salt (CAS Reg. No.
37325–33–0)

Do.

Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg.
No. 68611–14–3)

Do.

Lignosulfonic acid, magnesium salt (CAS Reg. No.
8061–54–9)

Do.

Lignosulfonic acid, potassium salt (CAS Reg. No.
37314–65–1)

Do.

Lignosulfonic acid, sodium salt (CAS Reg. No. 8061–51–
6)

Do.

Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No.
68855–41–4)

Do.

Lignosulfonic acid, sodium salt, polymer with
formaldehyde and phenol (CAS Reg. No. 37207–89–9)

Do.

Lignosulfonic acid, sodium salt, sulfomethylated (CAS
Reg. No. 68512–34–5)

Do.

Lignosulfonic acid, zinc salt (CAS Reg. No. 57866–49–6)

Do.

d-Limonene (CAS Reg. No. 5989–27–5)

Solvent,
fragrance

Magnesium carbonate

Anticaking
agent,
conditioning
agent

Magnesium chloride

Safener

Magnesium lime

Solid diluent,
carrier

Magnesium oxide

Do.

Magnesium silicate

Do.

Magnesium stearate

Surfactant

Magnesium sulfate

Solid diluent,
carrier, safener

Methyl alcohol

Solvent

Methyl n

Solvent,
cosolvent

-amyl ketone (CAS Reg. No. 110–43–0)

Methylated silicones

Antifoaming
agent

Methyl esters of fatty acids derived from edible fats
and oils

Solvent,
cosolvent

Methyl esters of higher fatty acids conforming to 21
CFR 573.640

Antidusting
agent,
surfactant

Methyl isobutyl ketone

Solvent

Mica

Solid diluent,
carrier

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Electronic Code of Federal Regulations:

Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or
178.3620(a) (CAS Reg. No. 8012–95–1)
Monoammonium phosphate

Diluent,
carrier, and
solvent
No more than
3.75% by
weight in
formulation

Postharvest
fumigation in
formulation
with aluminum
phosphide

Mono- and diglycerides of C8-C18fatty acids

Surfactants,
related
adjuvants of
surfactants

Montmorillonite-type clay

Solid diluent,
carrier

Nonyl, decyl, and undecyl glycoside mixture with a
mixture of nonyl, decyl, and undecyl oligosaccharides
and related reaction products (primarily decanol and
undecanol) produced as an aqueous-based liquid (50
to 65% solids) from the reaction of primary alcohols
(containing 15 to 20% secondary alcohol isomers) in a
ratio of 20% C9, 40% C10, and 40% C11with

Surfactant.

carbohydrates (average glucose to alkyl chain ratio 1.3
to 1.8)
α-( p -Nonylphenyl)-ω-hydroxypoly(oxyethylene)
mixture of dihydrogen phosphate and monohydrogen
phosphate esters and the corresponding ammonium,
calcium, magnesium, monoethanolamine, potassium,
sodium, and zinc salts of the phosphate esters; the
nonyl group is a propylene trimer isomer and the poly
(oxyethylene) content averages 4-14 moles or 30 moles

Surfactants,
related
adjuvants of
surfactants

α-( p -Nonylphenyl)-ω-hydroxypoly(oxyethylene)
produced by the condensation of 1 mole of
nonylphenol (nonyl group is a propylene trimer isomer)
with an average of 4-14 or 30-90 moles of ethylene
oxide; if a blend of products is used, the average
number of moles of ethylene oxide reacted to produce
any product that is a component of the blend shall be
in the range of 4-14 or 30-90

Do.

α-( p -Nonylphenyl)-ω-hydroxypoly(oxyethylene)
sulfate, ammonium, calcium, magnesium, potassium,
sodium, and zinc salts; the nonyl group is a propylene
trimer isomer and the poly(oxyethylene) content
averages 4 moles

Do.

1-Octanal (CAS Reg. No. 124–13–0)

Not more than
0.2% of the
pesticide
formulation

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Odor masking
agent

Electronic Code of Federal Regulations:

Surfactants,
related
adjuvants of
surfactants

Octyl and decyl glucosides mixture with a mixture of
octyl and decyloligosaccharides and related reaction
products (primarily ndecanol) produced as an
aqueous-based liquid (68-72% solids) from the
reaction of straight chain alcohols (C8(45%), C10
(55%)) with anhydrous glucose
Oleic acid

Diluent

Oleic acid diester of α-hydro-ω-hydroxypoly
(oxyethylene); the poly(oxyethylene) having average
molecular weight (in amu) 400

Surfactants,
related
adjuvants of
surfactants

α-Oleoyl-ω-hydroxypoly(oxyethylene), average
molecular weight (in amu) of 600

Emulsifier

Oleyl alcohol (CAS Reg. No. 143–28–2

15%

Cosolvent

Oxalic acid

No more oxalic Calcium
acid should be chelating hard
water inhibitor
used than is
necessary to
chelate calcium
and in no case
should more
than 2 lb oxalic
acid per acre
be used

Palmitic acid

Diluent

Pentaerythritol ester of maleic anhydride modified
wood rosin

Plasticizer

Petrolatum, conforming to 21 CFR 172.880

Coating agent

Petroleum hydrocarbons, light odorless conforming to
21 CFR 172.884

Solvent,
diluent.

Petroleum hydrocarbons, synthetic isoparaffinic,
conforming to 21 CFR 172.882

Do.

Petroleum naphtha, conforming to 21 CFR 172.250(d)

Component of
coating agent

Petroleum wax, conforming to 21 CFR 172.886(d)

Coating agent

Phosphoric acid

Buffer

Polyethylene, conforming to 21 CFR 177.1520(c)

Binder, carrier,
and coating
agent

Polyethylene glycol[α-hydro-ω-hydroxypoly
(oxyethylene)]; mean molecular weight (in amu) 194
to 9,500 conforms to 21 CFR 178.3750

Surfactants,
related
adjuvants of
surfactants

Polyglycerol esters of fatty acids conforming to 21 CFR
172.854

Surfactants,
related
adjuvants of
surfactants

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Electronic Code of Federal Regulations:

Polyglyceryl phthalate ester of coconut oil fatty acids
(CAS Reg. Nos. 67746–6070–9

Surfactants,
related
adjuvants of
surfactants

Poly(oxy-1,2-ethanediyl), α-(carboxymethyl)-ω(nonylphenoxy) produced by the condensation of 1
mole of nonylphenol (nonyl group is a propylene trimer
isomer) with an average of 4-14 or 30-90 moles of
ethylene oxide. The molecular weight (in amu) ranges
are 454-894 and 1598-4238

Surfactant

Polyoxyethylene (20) sorbitan monostearate

Surfactants,
related
adjuvants of
surfactants

[Poly[oxy(methyl-1,2-ethanediyl)], α-[2-bis(2hydroxyethyl)amino]propyl]-ω-hydroxy,-ether with αhydro-ω-hydroxypoly(oxy-1,2-ethanediyl) (1:2), monoC12–16alkyl ethers, (CAS Reg. No. 176022–82–5)

Not to exceed
15% in the
formulated
product; only
for use with
glyphosate

Surfactant

Polysorbate 65, conforming to 21 CFR 172.838

Emulsifier

Potassium aluminum silicate

Solid diluent,
carrier

Potassium hydroxide

Neutralizer

Potassium phosphate

Buffer

Potassium sulfate

Solid diluent

Propane

Propellant

n-Propanol

Solvent,
cosolvent

2-Propenoic acid, 2-methyl-, polymer with ethyl 2propenoate and methyl 2-methyl-2-propenoate,
ammonium salt (CAS Registration No. 55989–05–4),
minimum number average molecular weight (in amu),
18,900.

Encapsulating
agent,
dispensers,
resins, fibers
and beads

Propylene glycol

Solvent,
cosolvent.

Propylene glycol alginate (as defined in 21 CFR
172.858)

Defoaming
agent

Propyl gallate

Antioxidant

Propyl p

Preservative
for formulations

-hydroxybenzoate

Pyrophyllite

Rhizobium
Sinorhizobium,
Bradyrhizobium
& Rhizobium

Solid diluent,
carrier
inoculants (e.g.
)

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All leguminous
food
commodities

Electronic Code of Federal Regulations:

Rosin, partially dimerized (as defined in 21 CFR
172.615)

Surfactants,
related
adjuvants of
surfactants

Rosin, partially hydrogenated (as defined in 21 CFR
172.615)

Do.

Rosin, wood

Do.

Salts of fatty acids, conforming to 21 CFR 172.863

Binder,
emulsifier,
anticaking
agent

Sand

Solid diluent,
carrier

Shellac, bleached; refined, food grade, arsenic and
rosin-free

Coating agent

Soapstone

Solid diluent

Sodium acid pyrophosphate

Surfactant,
suspending
agent,
dispersing
agent, buffer

Sodium alkyl naphthalenesulfonates (CAS Reg. Nos.
68909–83–1, 68909–84–2, 68909–82–0, 27213–90–7,
26264–58–4, 27178–87–6, 111163–74–7, 908356–16–
1, 25417–20–3, 25638–17–9, 145578–88–7, 1322–93–
6, 1323–19–9, 7403–47–6, 68442–09–1, 127646–44–
0, 908356–18–3)

Limited to no
more than 30%
by weight in
pesticide enduse products

Surfactants,
related
adjuvants of
surfactants

Sodium aluminum silicate

Solid diluent,
carrier

Sodium dioctylsulfosuccinate

Surfactants,
related
adjuvants of
surfactants

Sodium hexametaphosphate

Surfactant,
emulsifier,
wetting agent,
suspending
agent,
dispersing
agent, buffer

Sodium hydroxide

Neutralizer

Sodium metasilicate

Surfactants,
emulsifiers,
wetting
agents,
dispersing
agents, buffer

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Electronic Code of Federal Regulations:

Sodium monoalkyl and dialkyl (C6-C16) phenoxy
benzenedisulfonates and related acids (CAS Reg. Nos.
147732–59–0, 147732–60–3, 169662–22–0, 70191–
75–2, 36445–71–3, 39354–74–0, 70146–13–3,
119345–03–8, 149119–20–0, 149119–19–7, 119345–
04–9, 28519–02–0, 25167–32–2, 30260–73–2, 65143–
89–7, 70191–76–3)

Not to exceed
20% in
pesticide
formulations

Surfactants,
related
adjuvants of
surfactants

Sodium α-olefinsulfonate (sodium C14-C16) (Olefin
sulfonate)

Surfactants,
related
adjuvants of
surfactants

Sodium N -oleoyl- N
137–20–2)

Surfactants,
related
adjuvants of
surfactants

-methyl taurine (CAS Reg. No.

Sodium salt of sulfated oleic acid

Surfactants,
related
adjuvants of
surfactants

Sodium silicate

Surfactant,
emulsifier,
wetting agent,
stabilizer,
inhibitor

Sodium starch glycolate (CAS Reg. No. 9063–38–1)

Granular and
tableted
products only;
not to exceed
8% of the
formulated
product

Disintegrant

Sodium sulfate

Solid diluent,
carrier

Sodium tripolyphosphate

Buffer,
surfactant,
suspending
agent,
dispersing
agent,
anticaking
agent,
conditioning
agent

Sorbic acid (CAS Reg. No. 110–44–1)

Preservative
for formulations

Sorbitan fatty acid esters (fatty acids limited to C12,
C14, C16, and C18containing minor amounts of

Surfactants,
related
adjuvants or
surfactants.

associated fatty acids) and their derivatives; the poly
(oxyethylene) content averages 5-20 moles
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Electronic Code of Federal Regulations:

Soybean flour

Expires May 24, Surfactant
2005.

Soybean oil-derived fatty acids

Solvent,
cosolvent

Sperm oil conforming to 21 CFR 172.210

Coating agent

Stearic acid

Diluent

α-Stearoyl-ω-hydroxypoly(oxyethylene), average
molecular weight (in amu) of 600

Emulsifier

α-Stearoyl-ω-hydroxypoly(oxyethylene); the poly
(oxyethylene) content averages either 8, 9, or 40
moles; if a blend of products is used, the average
number of moles ethylene oxide reacted to produce
any product that is a component of the blend shall be
either 8, 9, or 40

Surfactants,
related
adjuvants of
surfactants

Sucrose octaacetate

Adhesive

Sulfite liquors and cooking liquors, spent, oxidized
(CAS Reg. No. 68514–09–0)

Surfactant,
related
adjuvants of
surfactants

Sulfuric acid (CAS Reg. No.7664–93–9)

Not to exceed
10% of the
pesticide
formulation;
non-aerosol
formulations
only

pH Control
agent

Synthetic paraffin and its succinic derivatives
conforming to 21 CFR 172.275

Carrier, binder,
and carrying
agent

Synthetic petroleum wax, conforming to 21 CFR
172.888

Binder, carrier,
and coating
agent

Talc

Solid diluent,
carriers

Tall oil; fatty acids not less than 58%, rosin acids not
more than 44%, unsaponifiables not more than 8%

Surfactants,
related
adjuvants of
surfactants

Tartrazine

Dye

Terpenes and terpenoids, turpentine oil, alpha-pinene
fraction, polymd. (CAS Reg. No. 70750–57–1)

Surfactants,
related
adjuvants of
surfactants

1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811–97–2)

Aerosol
propellant

Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No 97–
99–4)

Expires
February 9,
2008

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Solvent/
cosolvent

Electronic Code of Federal Regulations:

α-[ p -(1,1,3,3-Tetramethylbutyl)phenyl]-ωhydroxypoly(oxyethylene) produced by the
condensation of 1 mole of p -(1,1,3,3tetramethylbutyl)phenol with a range of 1-14 or 30-70
moles of ethylene oxide: if a blend of products is used,
the average range number of moles of ethylene oxide
reacted to produce any product that is a component of
the blend shall be in the range of 1-14 or 30-70
2,4,7,9-Tetramethyl-5-decyn-4, 7-diol

Surfactants,
related
adjuvants of
surfactants

Not more than
2.5% of
pesticide
formulation

Surfactants,
related
adjuvants of
surfactants

Tetrasodium pyrophosphate

Anticaking
agent,
conditioning
agent

Thiosulfuric acid, disodium salt, anhydrous. (CAS Reg.
No 7772–98–7)

Dechlorinator,
reducing agent

Thiosulfuric acid, disodium salt, pentahydrate. (CAS
Reg. No. 10102–17–7)

Do.

d-Alpha tocopherol (CAS Reg. No. 9–02–9

None

Safener

d-Alpha tocopheryl acetate (CAS Reg. No. 58–95–7)

None

Do.

dl-Alpha tocopherol (CAS Reg. No.10191–41–0)

None

Do.

dl-Alpha tocopheryl acetate (CAS Reg. No. 7695–91–2) None

Do.

Tricalcium phosphate

Surfactant,
suspending
agent,
dispersing
agent,
anticaking
agent,
conditioning
agent

Trisodium phosphate

Surfactant,
emulsifier,
wetting agent

Vermiculite

Solid diluent,
carrier.

Vitamin E (CAS Reg. No. 1406–18–4)

None

Walnut shells

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Safener
Leaching
inhibitor,
binder for
waterdispersible
aggregates,
sticker and
suspension
stabilizer

Electronic Code of Federal Regulations:

Wintergreen oil

Attractant

Wood flour

Derived from
wood free of
chemical
preservatives

Solid diluent
and carrier

Xanthan gum-modified, produced by the reaction of
xanthan gum and glyoxal (maximum 0.3% by weight)

Not more than
0.5% of
pesticide
formulation

Surfactant

Xylene meeting the specifications listed in 21 CFR
172.884(b)(4)

In pesticide
Solvent,
formulations for cosolvent
grain storage
only

Zeolite (hydrated alkali aluminum silicate)

Solid diluent,
carrier

Zinc oxide

Coating agent

Zinc sulfate (basic and monohydrate)

Do.

Zinc sulfate (basic and monohydrate)

Solid diluent,
carrier

[69 FR 23117, Apr. 28, 2004, as amended at 69 FR 33578, June 16, 2004; 69 FR 34949, June 23, 2004;
69 FR 40786, July 7, 2004; 69 FR 47025, Aug. 4, 2004; 69 FR 58304, 58314, Sept. 30, 2004; 70 FR
28443, 28451, May 18, 2005; 70 FR 31364, June 1, 2005; 70 FR 37692, June 30, 2005; 70 FR 38786,
July 6, 2005; 70 FR 43311, July 27, 2005; 70 FR 44496, Aug. 3, 2005; 70 FR 51628, Aug. 31, 2005; 70
FR 54286, Sept. 14, 2005; 70 FR 55296, Sept. 21, 2005; 70 FR 55733, Sept. 23, 2005; 70 FR 67910,
Nov. 9, 2005; 71 FR 14414, Mar. 22, 2006; 71 FR 30810, May 31, 2006; 71 FR 43660, Aug. 2, 2006; 71
FR 45414, 45421, Aug. 9, 2006; 73 FR 9217, Feb. 20, 2008; 73 FR 17913, Apr. 2, 2008; 74 FR 22460,
May 13, 2009; 74 FR 32460, July 8, 2009; 74 FR 37577, 37597, 37604, 37612, July 29, 2009; 74 FR
38943, 38969, Aug. 5, 2009]

§ 180.920 Inert ingredients used pre-harvest; exemptions from the requirement of a
tolerance.
top
The following materials are exempted from the requirement of a tolerance when used in accordance with
good agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to
growing crops only:

Inert ingredients

Limits

Acetophenone
Adenosine (CAS Reg. No. 58–61–7)

Uses
Attractant

Maximum of
0.5% of
formulation

Alder bark

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Synergist

Seed
germination
stimulator

Electronic Code of Federal Regulations:

α-Alkyl (minimum C6linear, branched, saturated and/ Not to exceed
30% of pesticide
or unsaturated)-ω-hydroxypolyoxyethylene polymer
with or without polyoxypropylene, mixture of di- and formulation.
monohydrogen phosphate esters and the
corresponding ammonium, calcium, magnesium,
monoethanolamine, potassium, sodium, and zinc
salts of the phosphate esters; minimum oxyethylene
content is 2 moles; minimum oxypropylene content is
0 moles (CAS Reg. Nos. 9046–01–9, 37280–82–3,
39464–66–9, 42612–52–2, 50643–20–4, 52019–36–
0, 58318–92–6, 60267–55–2, 61837–79–4, 67711–
84–6, 68070–99–5, 68071–35–2, 68071–17–0,
68130–47–2, 68186–37–8, 68186–36–7, 68311–02–
4, 68425–73–0, 68458–48–0, 68511–37–5, 68610–
65–1, 68585–36–4, 68649–29–6, 68815–11–2,
68908–64–5, 68891–13–4, 73038–25–2, 78330–24–
2, 108818–88–8, 154518–39–5, 317833–96–8,
873662–29–4, 936100–29–7, 936100–30–0)

Surfactants,
related
adjuvants of
surfactants

N-alkyl (C8-C18) primary amines and their acetate

Concentration in
formulated endsalts where the alkyl group is linear and may be
saturated and/or unsaturated (CAS Reg. Nos. 61790– use products not
to exceed 10%
57–6, 61790–58–7, 61790–59–8, 61790–60–1,
by weight in
61788–46–3, 61790–33–8, 68155–38–4)
herbicide
products, 4% by
weight in
insecticide
products, and
4% by weight in
fungicide
products.

Surfactants,
related
adjuvants of
surfactants

N,N
-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2ethanediyl) C8-C18saturated and unsaturated

Not to exceed
25% in herbicide
alkylamines; the poly(oxy-1,2-ethanediyl) content is formulations and
2–60 moles (CAS Reg. Nos. 10213–78–2, 25307–17– 10% in
9, 26635–92–7, 26635–93–8, 288259–52–9, 58253– insecticide and
fungicide
49–9, 61790–82–7, 61791–14–8, 61791–24–0,
61791–26–2, 61791–31–9, 61791–44–4, 68155–33– formulations
9, 68155–39–5, 68155–40–8,70955–14–5, 73246–
96–5)

Surfactants,
related
adjuvants of
surfactants

N,N
–Bis-α-ethyl-ω-hydroxypoly(oxy-1,2ethanediyl/oxy(methyl-1,2-ethanediyl) C8-

Surfactants,
related
adjuvants of
surfactants

C18saturated and unsaturated alkylamines; the poly
(oxy-1,2-ethanediyl/oxy(methyl-1,2-ethanediyl)
content is 2–60 moles (CAS Reg. Nos. 68213–26–3,
68153–97–9, 75601–76–2)

Not to exceed
25% in herbicide
formulations and
10% in
insecticide and
fungicide
formulations

Aluminum sulfate

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Safener
adjuvant

Electronic Code of Federal Regulations:

Ammonium nitrate (CAS Reg. No. 6484–52–2)

Adjuvant/
intensifier for
herbicides

Ammonium polyphosphate (CAS Reg. No. 68333–79–
9)

Sequestrant,
buffer, or
surfactant

Barium sulfate

Carrier

1,2-Benzisothiazolin-3-one

Not more than
0.1% of
formulation. Not
more than 0.02
lb to be applied
per acre

Boric acid
Buffalo gourd root powder
( Cucurbita
root
foetidissima
powder); or, Zucchini juice
( Cucurbita
pepo
juice) or Hawkesbury melon
Citrullus
.
lanatus

Preservative/
stabilizer

Sequestrant
No more than
Gustatory
2.5 lbs/acre/
stimulant
season (3.4 gm/
acre/season of
Cucurbitacin)

Butyl stearate

Defoamer

γ-Butyrolactone

Solvent

C.I. Pigment Blue #15 (CAS Reg. No. 147–14–8;
containing no more than 50 ppm polychlorinated
biphenyls (PCBs))

For seed
treament use
only

Dye, coloring
agent

C.I. Pigment Green #7 (CAS Reg. No. 1328–53–6;
containing no more than 50 ppm polychlorinated
biphenyls (PCBs))

For seed
treatment use
only

Dye, coloring
agent

C.I. Pigment Violet #23 (CAS Reg. No. 6358–30–1;
containing no more than 20 ppb of polychlorinated
dibenzo- p -dioxins and/or polychlorinated
dibenzofurans)

For seed
treatment use
only

Dye, coloring
agent

Camphor (CAS Reg. No. 76–22–2)

Not more than
5% weight to
weight (w/w) of
pesticide
formulations

Deodorant,
melting point
adjustment

Carbon Black (CAS Reg. No. 1333–86–4)

For seed
treatment use
only

Colorant

Carbonic acid, dipotassium salt (CAS Reg. No. 584–
08–7)

Buffering agent

Carbonic acid, dipotassium salt, trihydrate (CAS Reg.
No. 18662–52–7)

Buffering agent

Carous chloride

10 ppm in
formulation

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Tagging agent

Electronic Code of Federal Regulations:

Carrageenan, conforming to 21 CFR 172.260

Not more than
0.15% of
pesticide
formulation

Thickener and
stabilizer for
pesticide
formulations
applied to
seeds before
planting

Chlorobenzene

Contains not
more than 1%
impurities. Not
for use after
edible parts of
plant begin to
form. Do not
graze livestock
in treated areas
within 48 hours
after application

Solvent,
cosolvent

5-Chloro-2-methyl-4-isothiazolin-3-one (in
combination with 2-methyl-4-isothiazolin-3-one)

Preservative
Not more than
0.0022% (22.5
ppm) in the
formulation;
0.00022% (or
2.25 ppm) in the
final solution
applied to
growing crops

Cis-isomer of 1-(3-chloroallyl)-3,5,7-triaza-1Maximum of
azoniaadamantane chloride (CAS Reg. No. 51229–78– 0.14% by
8)
weight of
formulation

Preservative

Copper naphthenate

Mercaptan
scavenger in
technical
pesticide

Not more than
2.5% of
formulation;
application
limited to before
edible portions
of plants begin
to form

Cyclohexane

Solvent,
cosolvent

Cyclohexanone
Cysteine (CAS Reg. No. 52–90–4)

Do.
Maximum of
0.5% of
formulation

Synergist

D&C Green No. 6

Dye

D&C Red No. 17, technical grade

Dye

D&C Red No. 33 (CAS Reg. No. 3567–66–6); meeting
the specifications listed in 21 CFR 74.1333

Dye

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Electronic Code of Federal Regulations:

D&C Violet No. 2, technical grade

Not more than
0.005% of
pesticide
formulation

Dye

Decanamide, N,N-dimethyl (CAS Reg. No. 14433–76–
2)

Emulsifier,
solvent,
cosolvent

n

Dye

-Decyl alcohol

Diammonium phosphate (CAS Reg. No. 7783–28–0)

Buffer,
surfactant

Diethanolamine

Stabilizer,
inhibitor for
formulations
used before
crop emerges
from soil

Diethanolamine salts of alkyl (C8-C24)
benzenesulfonic acid (CAS Reg. Nos. 26545–53–9
and 68953–97–9)

Not to exceed
7% of pesticide
formulation

Surfactants,
related
adjuvants of
surfactants

Diethylene glycol

Deactivator,
adjuvant for
formulations
used before
crop emerges
from soil

Diethylene glycol and diethylene glycol monobutyl,
monoethyl, and monomethyl ethers

Deactivator for
formulations
used before
crop emerges
from soil,
stabilizer

Dimethylaminopropylamine, isopropylamine,
ethanolamine, and triethanolamine salts of alkyl (C8-

Surfactants,
related
adjuvants of
surfactants

C24) benzenesulfonic acid (CAS Reg. Nos. 26264–05–
1, 27323–41–7, 55470–69–4, 68411–31–4, 68584–
24–7, 68584–25–8, 68648–81–7, 68648–96–4,
68649–00–3, 68910–32–7, 68953–93–5, 90194–42–
6, 90194–53–9, 90218–35–2, 157966–96–6, 319926–
68–6, 877677–48–0, 1093628–27–3)
3,6-Dimethyl-4-octyn-3,6-diol

In pesticide
formulations, for
soil prior to
planting or to
plants before
edible parts form

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Surfactants,
related
adjuvants of
surfactants

Electronic Code of Federal Regulations:

Dimethyl sulfoxide

Solvent or
cosolvent for
formulations
used before
crop emerges
from soil or
prior to
formation of
edible parts of
food plants

Dipotassium hydrogen phosphate

Buffering agent

Dipropylene glycol monomethyl ether

Stabilizer

Douglas-fir bark, ground

Solid diluent,
carrier

Dysprosium chloride

10 ppm in
formulation

Tagging agent

1,2-ethanediamine, N , N , N ', N 'tetramethyl-, polymer with 1,1'-oxybis[2chloroethane] (CAS Reg. No. 31075–24–8)

For use in
Adjuvant or
pesticide
water
formulations
conditioner
applied to cotton
or wheat only

(S,S)–Ethylenediaminedisuccinic acid (CAS Reg. No.
20846–91–7)

Sequestrant or
chelating agent

Ethylene glycol

Antifreeze,
deactivator for
all pesticides
used before
crop emerges
from soil and in
herbicides
before or after
crop emerges

Ethylene glycol monobutyl ether
2-Ethylhexanol

Europic chloride

Cosolvent,
defoamer,
solvent for all
pesticides used
before crop
emerges from
soil and in
herbicides
before or after
crop emerges
10 ppm in
formulation

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Tagging agent

Electronic Code of Federal Regulations:

FD&C Blue No. 1, methyl-polyethylene glycol
derivative (CAS Reg. No. 9079–34–9)

For seed
Dye, coloring
treatment use
agent
only; Number
average
molecular weight
(in amu) is
greater than
1,000; Not to
exceed 5% of
the formulated
pesticide product

Dye, coloring
FD&C Blue No. 1, polyethylene glycol derivative (CAS For seed
agent
Reg. No. 9079–33–8)
treatment use
only; Number
average
molecular weight
(in amu) is
greater than
1,000; Not to
exceed 5% of
the formulated
pesticide product
FD&C Red No. 40 (CAS Reg. No. 25956–17–6)

For seed
treatment use
only. Not to
exceed 2% by
weight of the
pesticide
formulation

Dye, coloring
agent

Ferric chloride

Not greater
than 2% of
suspending,
dispersing
agent, pesticide
formulation

Fluoroapatite

Solid diluent,
carrier

Folic acid (CAS Reg. No. 59–30–3)

Maximum of
0.5% of
formulation

Synergist

Gluconic acid (and sodium salt)

Sequestrant

l

Plant nutrient

-Glutamic acid (C5H9NO4;CAS Reg. No. 56–86–0) Seet treatment
use only

[alpha]-D-glucopyranoside, 2-ethylhexyl 6-O-[alpha]D glucopyranosyl- (CAS Reg. No. 330980–61–5)

Surfactant

[alpha]-D-glucopyranoside, 2-ethylhexyl (CAS Reg.
No. 125590–73–0)

Surfactant

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Electronic Code of Federal Regulations:

Glutamine (CAS Reg. No. 56–85–9)

Maximum of
0.5% of
formulation

Synergist

Glycerol—propylene oxide polymer (CAS Reg. No.
25791-96-2)

Component in
water-soluble
film

Glyceryl triacetate

Stabilizer

Glyceryl tris-12-hydroxystearate

Flow control
agent

Graphite

Treatment aid
for seeds

Hexamethylenetetramine

Stabilizer for
carriers in solid
pesticide
formulations

2-Hydroxy-4- n
No. 1843–05–6)

-octoxybenzophenone (CAS Reg.

Not more than
0.2 pt of
pesticide
formulation

Light stabilizer

Hydroxypropyl guar gum

Thickener

Isobornyl acetate

Solvent

Isobutyl alcohol

Do.

Isobutylene-butene copolymers

For soil
application only

Binder

Isooctadecanol

Not more than
2% of pesticide
formulation

Defoaming
agent

Lanthanum chloride

10 ppm in
formulation

Tagging agent.

Magnesium nitrate (in combination with 2-methyl-4isothiazolin-3-one and 5-chloro-2-methyl-4isothiazolin-3-one)

None

Preservation

Maleic acid and maleic anhydride

Stabilizer
For pesticide
formulations
applied to apples
with a minimum
preharvest
interval of 21
days

Manganese carbonate
Mesityl oxide

Plant nutrient
Not for use after Solvent,
edible parts of
cosolvent
plant begin to
form. Do not
graze livestock
in treated areas
within 48 hours
after application

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Electronic Code of Federal Regulations:

Methionine (CAS Reg. No. 59–51–8)

Maximum of
0.5% of
formulation

Methyl alcohol

Synergist

Do.

Methyl ethyl ketone

Surfactant

Methyl p-

Preservative for
formulations

hydroxybenzoate

Methyl isobutyl ketone

Solvent,
cosolvent

2-Methyl-4-isothiazolin-3-one (in combination with 5- Not more than
Preservative
chloro-2-methyl-4-isothiazolin-3-one)
0.0022% (22.5
ppm) in the
formulation;
0.00022% (or
2.25 ppm) in the
final solution
applied to
growing crops
Mono-, di-, and trimethylnapthalenesulfonic acids
and napthalenesulfonic acids formaldehyde
condensates, ammonium and sodium salts (CAS Reg.
Nos. 9008–63–3, 9069–80–1, 9084–06–4, 36290–04–
7, 91078–68–1, 141959–43–5, 68425–94–5)

Surfactants,
related
adjuvants of
surfactants

Methyl oleate

Surfactant

2-Methyl-2,4-pentanediol

Solvent for
formulations
used before
crop emerges
from soil

Methyl poly(oxyethylene)C8–C18alkylammonium

Concentration in
formulated end
chlorides where the poly(oxyethylene) content is
n=2–15 and where C8–C18alkyl is linear and may be use products not
to exceed 10%
saturated or unsaturated (CAS Reg. Nos. 3010–24–0, by weight in
18448–65–2, 70750–47–9, 22340–01–8, 67784–77– herbicide
4, 64755–05–1, 61791–10–4, 28724–32–5, 28880–
products and
55–9, 68187–69–9, 68607–27–2, 60687–90–3
5% by weight in
all other
pesticide
products

Surfactants,
related
adjuvants of
surfactants

N

Solvent,
cosolvent

-Methylpyrrolidone (CAS Reg. No. 872-504)

Mixed phytosterols (consisting of campesterol,
sitosterol and stigmasterol, with minor amounts of
associated plant sterols) derived from edible
vegetable oils

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Surfactant

Electronic Code of Federal Regulations:

Mono- and bis-(1 H , 1 H , 2 H , 2 H perfluoroalkyl) phosphates where the alkyl group is
even numbered and in the C6-C12range

Not more than
0.5% of
pesticide
formulation.
Expires February
9, 2008

Mono- and dialkyl (C8-C18) methylated ammonium

Surfactant,
related
adjvants of
surfactants

Surfactants,
related
adjuvants of
surfactants

chloride compounds, where the alkyl group(s) (C8C18) are derived from coconut, cottonseed, soya,
tallow, or hogfat fatty acids
Morpholine 4-C6-12Acyl Derivatives (CAS Reg. No.
887947–29–7)
Nicotinamide (CAS Reg. No. 98–92–0)

As a solvent
Maximum of
0.5% of
formulation

Synergist

α-( p -Nonylphenyl)-ω-hydroxypoly(oxyethylene);
produced by the condensation of 1 mole of
nonylphenol (nonyl group is a propylene trimer
isomer) with an average of 4-14 or 30-100 moles of
ethylene oxide; if a blend of products is used, the
average number of moles of ethylene oxide reacted
to produce any product that is a component of the
blend shall be in the range 4-14 or 30-100

Surfactant

Octanamide, N,N-dimethyl (CAS Reg. No. 1118–92–9)

Emulsifier,
solvent,
cosolvent

n-

Solvent,
cosolvent

Octyl alcohol

α-Oleoyl-ω-(oleoyloxy) poly(oxyethylene) derived
from α-hydro-ω-hydroxypoly(oxyethylene) (molecular
weight 600 amu)

Component of
defoamers

Oxo-decyl acetate (CAS reg. No. 108419–33–6)

Solvent

Oxo-heptyl acetate (CAS Reg. No. 90438–79–2)

Solvent

Oxo-hexyl acetate (CAS Reg. No. 88230–35–7)

Solvent

Oxo-nonyl acetate (CAS Reg. No. 108419–34–7)

Solvent

Oxo-octyl acetate (CAS Reg. No. 108419–32–5)

Solvent

Oxo-tridecyl acetate (CAS Reg. No. 108419–35–8)

Solvent

Phenol

Solvent,
cosolvent

Phenolsulfonic acid—formaldehyde—urea condensate Applied to
and its sodium salt
growing plants
only

Dispersant
surfactant

(Phthalocyaninato (2)) copper; (C.I. pigment blue
No. 15)

Coloring agent,
pigment

When used as a
colorant in lowdensity plastic
films

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Pigment red 48

For seed
treatment use
only

Dye

α-Pinene

Not more than
2% of
formulation by
weight

Stabilizer

Poly(oxyethylene) adducts of mixed phytosterols
(such sterols to consist of campesterol, stigmasterol
and sitosterol with minor amounts of associated plant
sterols) derived from edible vegetable oils;
polyoxyethylene content averaging 5-26 moles
Polyoxyethylene polyoxypropylene mono(di-secbutylphenyl) ether (CAS Reg. No. 69029–39–6)

Surfactant,
related
adjuvants

Limited to
herbicide
formulations
only, and to no
more than 30%
by weight in
herbicide
formulations
intended for
application to turf

Surfactants,
related
adjuvants of
surfactants

Poly(oxyethylene) (5) sorbitan monooleate

Surfactants,
related
adjuvants of
surfactants

Polysorbate 60, conforming to 21 CFR 172.836

Surfactant

Potassium dihydrogen phosphate

Buffering agent

2-Propanamine, compound with α-phosphono-ωbutoxypoly (oxy-1,2-ethanediyl) (2:1) (CAS Reg. No.
431040–31–2)

Not more than
15% in the
formulated
product

Surfactant

2-Propanamine, compounds with polyethylene glycol
dihydrogen phosphate C8– 10- alkyl ether (2:1) (CAS

Not more than
15% in the
formulated
product

Surfactant

Reg. No. 431062–72–5)
Propylene glycol monomethyl ether
Pyridoxine (CAS Reg. No. 65–23–6)

Solvent
Maximum of
0.5% of
formulation

Rosin, dark wood (as defined in 21 CFR 178.3870(a)
(1)(v))

Synergist

Surfactants,
related
adjuvants of
surfactants

Rosin, gum

Do.

Rosin, tall oil

Do.

Scandium chloride

10 ppm in
formulation

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Tagging agent

Electronic Code of Federal Regulations:

Sodium bisulfate (CAS Reg. No. 7681–38–1)

Acidifying/
buffering agent

Sodium 1,4-dicyclohexyl sulfosuccinate

Surfactants,
related
adjuvants of
surfactants

Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No.
3006–15–3)

Surfactants,
related
adjuvants of
surfactants

Sodium dihydrogen phosphate (CAS Reg. No. 7558–
80–7) conforming to 21 CFR 182.6778

Buffering agent

Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No.
127–39–9)

Surfactants,
related
adjuvants of
surfactants

Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No.
922–80–5)

Surfactants,
related
adjuvants of
surfactants

Sodium metaborate

Sequestrant

Sodium molybdate

Plant nutrient

Sodium nitrate

Solid diluent

Sodium nitrite

Not more than
3% of pesticide
formulation

Stabilizer,
inhibitor.

Sodium o

Not more than
0.1% of
pesticide
formulation

Preservative for
formulation

-phenylphenate

Sodium salt of the insoluble fraction of rosin

Surfactants,
related
adjuvants of
surfactants

Sodium salts of N-alkyl (C8-C18)-betaiminodipropionic acid where the C8-C18 is linear and
may be saturated and/or unsaturated (CAS Reg. Nos.
3655-00-3, 61791-56-8, 14960-06-6, 26256-79-1,
90170-43-7, 91696-17-2, 97862-48-1)

Concentration in
formulated enduse products not
to exceed 30%
by weight in
pesticide
formulations

Surfactants,
related
adjuvants of
surfactants

Sodium tetraborate

Not more than
2% of pesticide
formulation

Buffering
agent;
corrosion
inhibitor

Tannin

Dispersing
agent

Tertiary butylhydroquinone

Antioxidant

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Electronic Code of Federal Regulations:

1-Tetradecanamine, N,N
-dimethyl-, N
oxide (CAS Reg. No. 3332–27–2)

-

Component in
water-soluble
film

N,N,N
′,N″-Tetrakis-(2-hydroxypropyl)
ethylenediamine (CAS Reg. No. 102–60–3)

Concentration in Stabilizer for
formulated end- formulations
use products not
to exceed 20%
by weight in
pesticide
formulations

2,4,7,9-Tetramethyl-5-decyne 4,7-diol

In pesticide
formulations, for
application to
soil prior to
planting or to
plants before
edible parts form

Surfactants,
related
adjuvants of
surfactants

Tetrapotassium pyrophosphate (CAS Reg. No. 7320–
345)

Not to exceed
10% of
formulation

Sequestrant,
anticaking
agent,
conditioning
agent

Titanium dioxide (CAS Reg. No. 13463–67–7)

Pigment/
coloring agent
in plastic bags
used to wrap
growing
banana
(preharvest),
colorant on
seeds for
planting

Toluenesulfonic acid and its ammonium, calcium,
magnesium, potassium, sodium, and zinc salts

Solvent,
cosolvent

Triethanolamine

Stabilizer,
inhibitor for
formulations
used before
crop emerges
from soil

Triethanolamine (CAS Reg. No. 102–71–6)

Stabilizer,
inhibitor

Triethylene glycol

Deactivator

Triethyl phosphate

Stabilizer for
formulations
used before
crop emerges
from soil

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Electronic Code of Federal Regulations:

Trimethylolpropane (CAS Reg. No. 77–99–6)

Not to exceed
15% by weight
of the film

α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly Not more than
(oxyethylene), the poly(oxyethylene) content
15% of the
averages 4-150 moles)
formulation

Component in
water-soluble
film
Surfactant.

α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly Not more than
(oxyethylene); mixture of monohydrogen and
15% of the
dihydrogen phosphate esters and the corresponding formulation
ammonium, calcium, magnesium, potassium,
sodium, and zinc salts, the poly(oxyethylene) content
averages 4-150 moles)

Do.

α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly
(oxyethylene) sulfate, and the corresponding
ammonium, calcium, magnesium, potassium,
sodium, and zinc salts, the poly(oxyethylene) content
averages 4-150 moles

Not more than
15% of the
pesticide
formulation

Do.

Tryptophan (CAS Reg. No. 73–22–3)

Maximum of
0.5% of
formulation

Synergist

Valeric acid, normal

Not more than
2% in pesticide
formulations

Stenching
agent or
odorant

Xylene

Solvent,
cosolvent

Xylenesulfonic acid its ammonium calcium,
magnesium, potassium, sodium, and zinc salts

Surfactants,
related
adjuvants of
surfactants

Yucca extract from Yucca schidigera

Wetting agent

Ytterbium chloride

10 ppm in
formulation

Tagging agent

Yttrium chloride

10 ppm in
formulation

Tagging agent

Zinc orthophosphate

Plant nutrient
and safener

Zinc stearate, conforming to 21 CFR 182.5994 and
582.5994

Flow control
agent

[69 FR 23124, Apr. 28, 2004, as amended at 70 FR 7900, Feb. 16, 2005; 70 FR 31369, June 1, 2005; 70
FR 41619, July 20, 2005; 70 FR 54280, Sept. 14, 2005; 70 FR 55296, Sept. 21, 2005; 70 FR 55733, Sept.
23, 2005; 71 FR 14415, Mar. 22, 2006; 71 FR 18642, Apr. 12, 2006; 71 FR 30811, May 31, 2006; 71 FR
43667, Aug. 2, 2006; 71 FR 45408, 45411, 45421, Aug. 9, 2006; 72 FR 45656, Aug. 15, 2007; 73 FR
67400, Nov. 14, 2008; 74 FR 12620, Mar. 25, 2009; 74 FR 20887, May 6, 2009; 74 FR 28623, June 17,
2009; 74 FR 32437, July 8, 2009; 74 FR 37570, 37577, 37584, 37590, July 29, 2009; 74 FR 38935,
38952, 38955, 38962, Aug. 5, 2009; 74 FR 40513, Aug. 12, 2009; 74 FR 41798, Aug. 19, 2009]

§ 180.930 Inert ingredients applied to animals; exemptions from the requirement of
a tolerance.

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Electronic Code of Federal Regulations:

top
Link to an amendment published at 71 FR 45422, August 9, 2006.
The effective date of the above amendment was delayed in part until August 9, 2009, at 73 FR 45312 and
45316, August 4, 2008.
The effective date of the above amendment was further delayed in part until October 9, 2009, at 74 FR
39543 and 39545, August 7, 2009.
The following materials are exempted from the requirement of a tolerance when used in accordance with
good agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to
animals:

Inert ingredients
Acetic acid (CAS Reg. No. 64–19–7)

Limits
Not more than 0.5%
of pesticide
formulation

Uses
Catalyst

Acetic anhydride

Solvent, cosolvent,
stabilizer

Alkanoic and alkenoic acids, mono- and
diesters of α-hydro-ω-hydroxypoly
(oxyethylene) with molecular weight (in
amu) range of 200 to 6,000

Emulsifiers

Alkyl (C8-C24) benzenesulfonic acid and its

Surfactants,
emulsifier, related
adjuvants of
surfactants

ammonium, calcium, magnesium,
potassium, sodium, and zinc salts
α-Alkyl(C6-C15)-ω-hydroxypoly
(oxyethylene)sulfate, and its ammonium,
calcium, magnesium, potassium, sodium,
and zinc salts, poly(oxyethylene) content
averages 2–4 moles (CAS Reg. Nos. 3088–
31–1, 9004–82–4, 9004–84–6, 13150–00–
0, 25446–78–0, 26183–44–8, 32612–48–9,
50602–06–7, 62755–21–9, 68424–50–0,
68511–39–7, 68585–34–2, 68611–55–2,
68891–38–3, 73665–22–2)
α-alkyl (C12-C15)-ωhydroxypoly (oxypropylene)
poly (oxyethylene)copolymers (where the
poly(oxypropylene) content is 3-60 moles
and the poly(oxyethylene) content is 5-80
moles), the resulting ethoxylated
propoxylated (C12-C15) alcohols having a

Not to exceed 30% of Surfactants, related
pesticide formulation adjuvants of
surfactants

Not to exceed 20% of Surfactant
pesticide formulations

minimum molecular weight (in amu) of
1,500, CAS Reg. No. 68551–13–3

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Electronic Code of Federal Regulations:

α-alkyl-ω-hydroxypoly (oxypropylene) and/
or poly (oxyethylene) polymers where the
alkyl chain contains a minimum of six
carbons (CAS Reg. Nos. 9002–92–0, 9004–
95–9, 9005–00–9, 26183–52–8, 34398–01–
1, 52292–17–8, 66455–14–9, 66455–15–0,
68002–97–1, 68131–39–5, 68131–40–8,
68154–96–1, 68213–23–0, 68439–45–2,
68439–46–3, 68526–94–3, 68439–50–9,
68439–49–6, 68551–12–2, 68951–67–7,
71243–46–4, 97043–91–9, 9043–30–5,
60828–78–6, 61827–42–7, 24938–91–8,
68439–54–3, 69011–36–5, 78330–20–8,
78330–21–9, 106232–83–1, 127036–24–2,
160875–66–1, 9004–98–2, 68920–66–1,
61804–34–0, 61791–28–4, 71060–57–6,
26468–86–0, 31726–34–8, 52609–19–5,
61791–20–6, 68155–01–1, 69013–19–0,
69364–63–2, 70879–83–3, 78330–19–5,
97953–22–5, 157627–86–6, 34398–05–5,
72905–87–4, 84133–50–6, 61702–78–1,
27306–79–2, 169107–21–5, 61791–13–7,
39587–22–9, 85422–93–1; 68154–98–3,
61725–89–1, 68002–96–0, 68154–97–2,
68439–51–0, 68551–13–3, 68603–25–8,
68937–66–6, 68987–81–5, 69227–21–0,
70750–27–5, 103818–93–5, 166736–08–9,
120313–48–6, 68213–24–1, 68458–88–8,
68551–14–4, 69013–18–9, 69227–22–1,
72854–13–8, 73049–34–0, 78330–23–1,
37311–02–7, 64366–70–7, 37251–67–5,
9087–53–0, 196823–11–7, 57679–21–7,
111905–54–5, 61827–84–7, 172588–43–1)

Surfactants, related
adjuvants of
surfactants

Alkyl (C8-C18) sulfate and its ammonium,

Surfactant

calcium, magnesium, potassium, sodium,
and zinc salts

N,N
-Bis-α-ethyl-ω-hydroxypoly
(oxy-1,2-ethanediyl) C8-C18saturated and

Not to exceed 25% in Surfactants, related
herbicide formulations adjuvants of
surfactants
unsaturated alkylamines; the poly(oxy-1,2- and 10% in
insecticide
and
ethanediyl) content is 2–60 moles (CAS
fungicide formulations
Reg. Nos. 10213–78–2, 25307–17–9,
26635–92–7, 26635–93–8, 288259–52–9,
58253–49–9, 61790–82–7, 61791–14–8,
61791–24–0, 61791–26–2, 61791–31–9,
61791–44–4, 68155–33–9, 68155–39–5,
68155–40–8,70955–14–5, 73246–96–5)

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Electronic Code of Federal Regulations:

N,N
-Bis-α-ethyl-ω-hydroxypoly
(oxy-1,2-ethanediyl/oxy(methyl-1,2ethanediyl) C8-C18saturated and

Not to exceed 25% in Surfactants, related
herbicide formulations adjuvants of
and 10% in
surfactants
insecticide
and
unsaturated alkylamines; the poly(oxy-1,2fungicide formulations
ethanediyl/oxy(methyl-1,2-ethanediyl)
content is 2–60 moles (CAS Reg. Nos.
68213–26–3, 68153–97–9, 75601–76–2)

Ascorbyl palmitate

Preservative

Attapulgite-type clay

Solid diluent, carrier

Barium sulfate (CAS Reg. No. 7727–43–7)

Carrier, density
control agent

Benzoic acid

Preservative for
formulations

2-Bromo-2-nitro-1,3-propanediol (CAS
Reg. No. 52–51–7)

0.04% or less by
weight of the total
pesticide formulation

In-can preservative

Butane

Propellant

n

Solvent for blended
emulsifiers

-Butanol (CAS Reg. No. 71–36–3)

Butylated hydroxyanisole

Antioxidant

Butylated hydroxytoluene

Do.

Calcium carbonate

Solid diluent, carrier

Calcium chloride

Stabilizer

Calcium silicate, hydrated calcium silicate

Anticaking agent,
solid diluent, carrier

Calcium stearate (CAS Reg. No. 1592–23–
0)

Stabilizer,
component of plastic
animal tag

Calcium sulfate

Solid diluent, carrier

Carbon black (CAS Reg. No. 1333–86–4)

Colorant/pigment in
animal tag

Carrageenan, conforming to 21 CFR
172.620

Minimum molecular
weight (in amu):
100,000

Thickener

Cyclohexanone

Solvent, cosolvent

D&C Green No. 6

Dye, coloring agent

D&C Red No. 17

Do.

D&C Violet No. 2

Do.

Dialkyl (C8-C18) dimethylammonium
chloride

Not more than 0.2%
Flocculating agent in
in silica hydrated silica the manufacture of
silica hydrated silica
for use as a solid
diluent, carrier

Diatomite (diatomaceous earth)

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Solid diluent, carrier

Electronic Code of Federal Regulations:

Diethanolamine salts of alkyl (C8-C24)
benzenesulfonic acid (CAS Reg. Nos.
26545–53–9 and 68953–97–9)

Not to exceed 7% of
pesticide formulation

Diethylphthalate

Surfactants, related
adjuvants of
surfactants
Solvent, cosolvent

1,1-Difluoroethane (CAS Reg. No. 75–37–6) For aerosol pesticide
Aerosol propellant
formulations used for
insect control in foodand feed-handling
establishments and
animals
Dimethyl ether (CAS Reg. No. 115–10–6)

Propellant

Dimethylaminopropylamine,
isopropylamine, ethanolamine, and
triethanolamine salts of alkyl (C8-C24)

Surfactants, related
adjuvants of
surfactants

benzenesulfonic acid (CAS Reg. Nos.
26264–05–1, 27323–41–7, 55470–69–4,
68411–31–4, 68584–24–7, 68584–25–8,
68648–81–7, 68648–96–4, 68649–00–3,
68910–32–7, 68953–93–5, 90194–42–6,
90194–53–9, 90218–35–2, 157966–96–6,
319926–68–6, 877677–48–0, 1093628–27–
3)
3,6-Dimethyl-4-octyne-3,6-diol

Not more than 2.5%
of pesticide
formulation

Surfactants, related
adjuvants of
surfactants

Dimethylpolysiloxane (CAS Reg. No. 9016–
00–6)

Defoaming agent

Dipropylene glycol monomethyl ether

Surfactants, related
adjuvants of
surfactants

Epoxidized soybean oil (CAS Reg. No.
8013–07–8)

Stabilizer, plasticizer,
component animal
tag

Ethyl alcohol

Solvent, cosolvent

Ethyl maltol (CAS Reg. No.4940–11–8)

Not more than 0.2 %
of the pesticide
formulation

Ethylene oxide adducts of 2,4,7,9tetramethyl-5-decynediol, the ethylene
oxide content averages 3.5, 10 or 30
moles (CAS Reg. No. 9014–85–1)
2-Ethyl-1-hexanol

Odor masking agent

Surfactants, related
adjuvants of
surfactants
Not more than 2.5%
of pesticide
formulation

FD&C Blue No. 1

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Solvent, adjuvant of
surfactants
Dye, coloring agent

Electronic Code of Federal Regulations:

FD&C Yellow No. 6 Aluminum Lake (CAS
Reg. No. 15790–07–5)

Not more than 2% by Pigment in animal
weight of pesticide
tag and similar slowformulation
release devices

D-glucopyranose, oligomeric, C10–16-alkyl

Surfactant

glycosides (CAS Reg. No. 110615–47–9)
Glycerol monooleate

Surfactants, related
adjuvants of
surfactants

Glyceryl monostearate

Emulsifier

Glyceryl tris-12-hydroxystearate

Flow control agent

Graphite

Solid diluent, carrier

n
3)

Solvent, cosolvent

-Hexyl alcohol (CAS Reg. No. 111–27–

2-(2'-Hydroxy-5'-methylphenyl)
benzotriazole (CAS Reg. No. 2440–22–4)

Not more than 0.5%
Ultraviolet light
by weight of pesticide absorber/stabilizer in
formulation
animal tag and
similar slow-release
devices

Iron oxide (CAS Reg. No. 1309–37–1)

Colorant in pesticide
formulations for
animal tags

Isopropyl myristate, CAS Reg. No. 110–27–
0

Solvent

Kaolinite-type clay

Solid diluent, carrier

Kerosene, U.S.P. reagent

Solvent, cosolvent

Lactic acid

Solvent

Lactic acid, 2-ethylhexyl ester (CAS Reg.
No. 6283–86–9)

Solvent

Lactic acid, 2-ethylhexyl ester, (2S)- (CAS
Reg. No. 186817–80–1)

Solvent

Lactic acid, n-propyl ester, (S); (CAS Reg.
No. 53651–69–7)

Solvent

Lignin (CAS Reg. No. 9005–53–2)

Surfactant, related
adjuvants of
surfactants

Lignin, alkali (CAS Reg. No. 8068–05–1)

Do.

Lignin, alkali, oxidized, sodium salt (CAS
Reg. No. 68201–23–0)

Do.

Lignin alkali reaction products with
disodium sulfite and formaldehyde (CAS
Reg. No. 105859–97–0)

Do.

Lignin alkali reaction products with
formaldehyde and sodium bisulfite (CAS
Reg. No. 68512–35–6)

Do.

Lignosulfonic acid (CAS Reg. No. 8062–15–
5)

Do.

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Electronic Code of Federal Regulations:

Lignosulfonic acid, ammonium calcium salt
(CAS Reg. No. 12710–04–2)

Do.

Lignosulfonic acid, ammonium magnesium
salt (CAS Reg. No. 123175–37–1)

Do.

Lignosulfonic acid, ammonium salt (CAS
Reg. No. 8061–53–8)

Do.

Lignosulfonic acid, ammonium sodium salt
(CAS Reg. No. 166798–73–8)

Do.

Lignosulfonic acid, calcium magnesium salt
(CAS Reg. No. 55598–86–2)

Do.

Lignosulfonic acid, calcium salt (CAS Reg.
No. 8061–52–7)

Do.

Lignosulfonic acid, calcium sodium salt
(CAS Reg. No. 37325–33–0)

Do.

Lignosulfonic acid, ethoxylated, sodium
salt (CAS Reg. No. 68611–14–3)

Do.

Lignosulfonic acid, magnesium salt (CAS
Reg. No. 8061–54–9)

Do.

Lignosulfonic acid, potassium salt (CAS
Reg. No. 37314–65–1)

Do.

Lignosulfonic acid, sodium salt (CAS Reg.
No. 8061–51–6)

Do.

Lignosulfonic acid, sodium salt, oxidized
(CAS Reg. No. 68855–41–4)

Do.

Lignosulfonic acid, sodium salt, polymer
with formaldehyde and phenol (CAS Reg.
No. 37207–89–9)

Do.

Lignosulfonic acid, sodium salt,
sulfomethylated (CAS Reg. No. 68512–34–
5)

Do.

Lignosulfonic acid, zinc salt (CAS Reg. No.
57866–49–6)

Do.

d-Limonene (CAS Reg. No. 5989–27–5)

Solvent, fragrance

Magnesium carbonate

Solid diluent, carrier

Magnesium silicate, hydrated magnesium
silicate

Do.

Methyl alcohol

Solvent, cosolvent

Methyl n -amyl ketone (CAS Reg. No.
110–43–0)

Solvent, cosolvent

Methyl esters of higher fatty acids
conforming to 21 CFR 573.640

Antidusting agent

Methyl- p
paraben)

-hydroxybenzoate (Methyl

Meets specifications
of Food Chemicals
Codex; not to exceed
0.1% in formulations

Methyl isobutyl ketone
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Preservative

Solvent, cosolvent

Electronic Code of Federal Regulations:

Mineral oil, U.S.P., or conforming to 21
CFR 172.878 or 178.3620(a), (b)

Solvent, diluent

Montmorillonite-type clay

Solid diluent, carrier

Nonyl, decyl, and undecyl glycoside
mixture with a mixture of nonyl, decyl, and
undecyl oligosaccharides and related
reaction products (primarily decanol and
undecanol) produced as an aqueous-based
liquid (50 to 65% solids) from the reaction
of primary alcohols (containing 15 to 20%
secondary alcohol isomers) in a ratio of
20% C9, 40% C10, and 40% C11with

Surfactant

carbohydrates (average glucose to alkyl
chain ratio 1.3 to 1.8)
α-( p -Nonylphenyl)-ω-hydroxypoly
(oxyethylene) mixture of dihydrogen
phosphate and monohydrogen phosphate
esters and the corresponding ammonium,
calcium, magnesium, monoethanolamine,
potassium, sodium, and zinc salts of the
phosphate esters; the nonyl group is a
propylene trimer isomer and the poly
(oxyethylene) content averages 4-14 moles

Surfactants, related
adjuvants of
surfactants

α-( p -Nonylphenyl)-ω-hydroxypoly
(oxyethylene) produced by the
condensation of 1 mole of nonylphenol
(nonyl group is a propylene trimer isomer)
with an average of 4-15 or 30-90 moles of
ethylene oxide; if a blend of products is
used, the average number of moles of
ethylene oxide reacted to produce any
product that is a component of the blend
shall be in the range of 4-15 or 30-90
moles

Surfactants,
emulsifier, related
adjuvants of
surfactants.

α-( p -Nonylphenyl)-ω-hydroxypoly
(oxyethylene) sulfate, and its ammonium,
calcium, magnesium, potassium, sodium,
and zinc salts; the nonyl group is a
propylene trimer isomer and the poly
(oxyethylene) content averages 4 moles

Surfactants, related
adjuvants of
surfactants

α-( p -Nonylphenyl)-ω-hydroxypoly
(oxyethylene) sulfate, and its ammonium,
calcium, magnesium, monoethanolamine,
potassium, sodium, and zinc salts; the
nonyl group is a propylene trimer isomer
and the poly(oxyethylene) content
averages 4-14 or 30-90 moles of ethyiene
oxide

Surfactants, related
adjuvants of
surfactants

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Electronic Code of Federal Regulations:

Octadecyl 3,5-di- tert
-butyl-4- Not more than 0.5%
Thermal stabilizer/
hydroxyhydro cinnamate (CAS Reg. No.
by weight of pesticide antioxidant in animal
2082–79–3)
formulation
tag and similar slowrelease devices
1-Octanal (CAS Reg. No. 124–13–0)

Not more than 0.2%
of the pesticide
formulation

Odor masking agent

Thermal stabilizer/
antioxidant in animal
tag and similar slowrelease devices

Octyl and decyl glucosides mixture with a
mixture of octyl and decyl oligosaccharides
and related reaction products (primarily
n -decanol) produced as an aqueousbased liquid (68-72% solids) from the
reaction of straight chain alcohols (C8
(45%), C10) with anhydrous glucose
Octyl epoxytallate (CAS Reg. No. 61788–
72–5)

Plasticizer,
component animal
tag

Oleic acid, conforming to 21 CFR 172.862
(CAS Reg. No. 112–80–1)

Defoaming agent

α-Oleoyl-ω-hydroxypoly(oxyethylene),
average molecular weight (in amu) of 600

Emulsifier

α-Oleoyl-ω-(oleyloxy)poly(oxyethylene)
derived from α-hydro-ω-hydroxypoly
(oxyethylene), molecular weight (in amu)
600

Emulsifier,
defoaming agent

Petroleum hydrocarbons, light, odorless,
conforming to 21 CFR 172.884 or 178.3650

Solvent, diluent

Petroleum hydrocarbons, synthetic
isoparaffinic, conforming to 21 CFR
172.882 or 178.3530

Do.

Phenol
α-Pinene

Solvent, cosolvent
Not more than 2% of Stabilizer
formulation by weight

Polyethylene (CAS Reg. No. 9002–88–4)
conforming to 21 CFR 172.615

Component of
plastic slow release
tag

Polyethylene glycol [α-hydro-ω-hydroxypoly
(oxyethylene)]; mean molecular weight (in
amu) 194 to 9,500 conforms to 21 CFR
178.3750

Surfactants, related
adjuvants of
surfactants

Potassium hydroxide

Meeting Food
Chemicals, Codex
specifications

Neutralizer

Propane

Propellant

n

Solvent, for blended
emulsifiers

-Propanol

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2-Propenoic acid, 2-methyl-, polymer with
ethyl 2-propenoate and methyl 2-methyl-2propenoate, ammonium salt (CAS
Registration No. 55989–05–4), minimum
number average molecular weight (in
amu), 18,900.

Encapsulating agent,
dispensers, resins,
fibers and beads

Propylene glycol

Solvent, cosolvent

Propylene glycol monomethyl ether

Deactivator,
emmolient

Propyl gallate

Antioxidant

Propyl p -hydroxybenzoate (Propyl
paraben)

Meets specifications
of Food Chemicals
Codex; not to exceed
0.1% in formulations

Preservative

Pyrophylite

Solid diluent, carrier

Silica, hydrated silica

Anticaking agent,
solid diluent, carrier

Silica aerogel (finely powdered
microcellular silica foam having a minimum
silica content of 89.5%)

Component of
antifoaming agent

Soapstone

Solid diluent

Sodium alkyl naphthalenesulfonates (CAS
Reg. Nos. 68909–83–1, 68909–84–2,
68909–82–0, 27213–90–7, 26264–58–4,
27178–87–6, 111163–74–7, 908356–16–1,
25417–20–3, 25638–17–9, 145578–88–7,
1322–93–6, 1323–19–9, 7403–47–6,
68442–09–1, 127646–44–0, 908356–18–3)

Limited to no more
than 30% by weight
in pesticide end-use
products

Surfactants, related
adjuvants of
surfactants

Sodium dioctylsulfosuccinate

Surfactants, related
adjuvants of
surfactants

Sodium hydroxide

Neutralizer

Sodium monoalkyl and dialkyl (C6-C16)
Not to exceed 20% in Surfactants, related
phenoxy benzenedisulfonates and related pesticide formulations adjuvants of
acids (CAS Reg. Nos. 147732–59–0,
surfactants
147732–60–3, 169662–22–0, 70191–75–2,
36445–71–3, 39354–74–0, 70146–13–3,
119345–03–8, 149119–20–0, 149119–19–
7, 119345–04–9, 28519–02–0, 25167–32–
2, 30260–73–2, 65143–89–7, 70191–76–3)
Sodium N -oleoyl- N -methyl taurine
(CAS Reg. No. 137–20–2)
Sodium starch glycolate (CAS Reg. No.
9063–38–1)

Surfactants, related
adjuvants of
surfactants
Granular and tableted Disintegrant
products only; not to
exceed 8% of the
formulated product

Sodium sulfate
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Solid diluent, carrier

Electronic Code of Federal Regulations:

Buffering agent;
corrosion inhibition

Sorbitan fatty acid esters (fatty acids
limited to C12, C14, C16, and C18containing
minor amounts of associated fatty acids)
and poly(oxyethylene) derivatives of
sorbitan fatty acid esters; the poly
(oxyethylene) content averages 16-20
moles
Sorbitol

Antidusting agent.

Stearic acid (CAS Reg. No. 57–11–4)

Lubricant,
component animal
tag

α-Stearoyl-ω-hydroxypoly(oxyethylene),
average molecular weight (in amu) of 600

Emulsifier

α-Stearoyl-ω-hydroxypoly(oxyethylene);
the poly(oxyethylene) content averages 8,
9, or 40 moles; if a blend of products is
used, the average number of moles of
ethylene oxide reacted to produce any
product that is a component of the blend
shall be 8, 9, or 40

Surfactants; related
adjuvants of
surfactants

Sulfite liquors and cooking liquors, spent,
oxidized (CAS Reg. No. 68514–09–0)

Surfactant, related
adjuvants of
surfactants

Sulfur (CAS Reg. No. 7704–34–9)

Stabilizer

Talc

Do.

Tall oil; fatty acids not less than 58%,
rosin acids not more than 44%,
unsaponifiables not more than 8%

Surfactants, related
adjuvants of
surfactants

Tartrazine

Dye, coloring agent

2,4,7,9-Tetramethyl-5-decyne-4.7-diol

Not more than 2.5%
of pesticide
formulation

Titanium dioxide (CAS Reg. No. 13463–67–
7)

Toluenesulfonic acid and its ammonium,
calcium, magnesium, potassium, sodium,
and zinc salts

Surfactants, related
adjuvants of
surfactants
Pigment/colorant in
pesticide
formulations for
animal tag
Do.

Triacetin (glyceryl triacetate)

Solvent, cosolvent

Trisodium phosphate

Precipitant, buffer,
filler

Xylene

Solvent, cosolvent

Xylenesulfonic acid and its ammonium,
calcium, magnesium, potassium, sodium,
and zinc salts

Surfactants, related
adjuvants of
surfactants

Zinc oxide

Solid diluent, carrier

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Zinc stearate, conforming to 21 CFR
182.5994 and 582.5994

Water repellant,
dessicant, and
coating agent.

Zinc stearate (CAS Reg. No. 557–05–1)

Water repellant,
desiccant, and
coating agent;
stabilizer,
component of plastic
animal tag

Zinc sulfate (basic and monohydrate)

Water repellant,
dessicant, and
coating agent

[69 FR 23130, Apr. 28, 2004, as amended at 69 FR 29894, May 26, 2004; 69 FR 34949, June 23, 2004;
69 FR 58070, Sept. 29, 2004; 69 FR 58304, Sept. 30, 2004; 70 FR 37692, June 30, 2005; 70 FR 43312,
July 27, 2005; 70 FR 44496, Aug. 3, 2005; 70 FR 51628, Aug. 31, 2005; 70 FR 54286, Sept. 14, 2005; 70
FR 55296, Sept. 21, 2005; 70 FR 67910, Nov. 9, 2005; 70 FR 55733, Sept. 23, 2005; 71 FR 14415, Mar.
22, 2006; 71 FR 30811, May 31, 2006; 71 FR 45422, Aug. 9, 2006; 74 FR 28623, June 17, 2009; 74 FR
37578, 37597, 37605, 37612, July 29, 2009; 74 FR 38935, 38943, 38970, Aug. 5, 2009]

§ 180.940 Tolerance exemptions for active and inert ingredients for use in
antimicrobial formulations (Food-contact surface sanitizing solutions).
top
Residues of the following chemical substances are exempted from the requirement of a tolerance when
used in accordance with good manufacturing practice as ingredients in an antimicrobial pesticide
formulation, provided that the substance is applied on a semi-permanent or permanent food-contact
surface (other than being applied on food packaging) with adequate draining before contact with food.
(a) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation
may be applied to: Food-contact surfaces in public eating places, dairy-processing equipment, and foodprocessing equipment and utensils.

Pesticide Chemical

CAS Reg. No.

Limits

Acetic acid

64–19–7

When ready for use, the enduse concentration is not to
exceed 290 ppm

α-alkyl-ω-hydroxypoly (oxypropylene)
and/or poly (oxyethylene) polymers
where the alkyl chain contains a
minimum of six carbons

9002–92–0,
9004–95–9,
9005–00–9,
26183–52–8,
34398–01–1,
52292–17–8,
66455–14–9,
66455–15–0,
68002–97–1,
68131–39–5,
68131–40–8,
68154–96–1,
68213–23–0,
68439–45–2,

None

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Electronic Code of Federal Regulations:

68439–46–3,
68526–94–3,
68439–50–9,
68439–49–6,
68551–12–2,
68951–67–7,
71243–46–4,
97043–91–9,
9043–30–5,
60828–78–6,
61827–42–7,
24938–91–8,
68439–54–3,
69011–36–5,
78330–20–8,
78330–21–9,
106232–83–1,
127036–24–2,
160875–66–1,
9004–98–2,
68920–66–1,
61804–34–0,
61791–28–4,
71060–57–6,
26468–86–0,
31726–34–8,
52609–19–5,
61791–20–6,
68155–01–1,
69013–19–0,
69364–63–2,
70879–83–3,
78330–19–5,
97953–22–5,
157627–86–6,
34398–05–5,
72905–87–4,
84133–50–6,
61702–78–1,
27306–79–2,
169107–21–5,
61791–13–7,
39587–22–9,
85422–93–1;
68154–98–3,
61725–89–1,
68002–96–0,
68154–97–2,
68439–51–0,
68551–13–3,
68603–25–8,
68937–66–6,
68987–81–5,
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Electronic Code of Federal Regulations:

69227–21–0,
70750–27–5,
103818–93–5,
166736–08–9,
120313–48–6,
68213–24–1,
68458–88–8,
68551–14–4,
69013–18–9,
69227–22–1,
72854–13–8,
73049–34–0,
78330–23–1,
37311–02–7,
64366–70–7,
37251–67–5,
9087–53–0,
196823–11–7,
57679–21–7,
111905–54–5,
61827–84–7,
172588–43–1)
Ammonium chloride

12125–02–9

When ready for use, the enduse concentration is not to
exceed 48 ppm

Amylopectin, acid-hydrolyzed, 1oxtenylbutanedioate

113894–85–2

None

Amylopectin, hydrogen 1octadecenylbutanedioate

125109–81–1

None

Ethanol

64–17–5

None

Ethylenediaminetetraacetic acid (EDTA), 64–02–8
tetrasodium salt

None

Hydrogen peroxide

7722–84–1

When ready for use, the enduse concentration is not to
exceed 91 ppm

Hypochlorous acid, sodium salt

7681–52–9

When ready for use, the enduse concentration of all
hypochlorous acid chemicals
in the solution is not to
exceed 200 ppm determined
as total available chlorine

Iodine

7553–56–2

When ready for use, the
total end-use concentra tion
of all iodide-producing
chemicals in the solution is
not to exceed 25 ppm of
titratable iodine

Magnesium oxide

1309–48–4

None

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Electronic Code of Federal Regulations:

Methylene blue

61–73–4

When ready for use, the enduse concentration is not to
exceed 0.4 ppm

α-(p-Nonylphenyl)-ω-hydroxypoly
(oxyethylene) average poly
(oxyethylene) content 11 moles)

None

None

Octadecanoic acid, calcium salt

1592–23–0

None

1-Octanesulfonic acid, sodium salt

5324–84–5

When ready for use, the enduse concentration is not to
exceed 46 ppm

Octanoic acid

124–07–2

When ready for use, the enduse concentration is not to
exceed 52 ppm

Oxirane, methyl-, polymer with oxirane,
minimum molecular weight (in amu),
1900

9003–11–6

None

Peroxyacetic acid

79–21–0

When ready for use, the enduse concentration is not to
exceed 58 ppm

Peroxyoctanoic acid

33734–57–5

When ready for use, the enduse concentration is not to
exceed 52 ppm

Phosphonic acid, (1-hydroxyethylidene)
bis-

2809–21–4

When ready for use, the enduse concentration is not to
exceed 14 ppm

Phosphoric acid, trisodium salt

7601–54–9

When ready for use, the enduse concentration is not to
exceed 5916 ppm

Potassium bromide

7758–02–3

When ready for use, the enduse concentration is not to
exceed 46 ppm total
available halogen

Potassium iodide

7681–11–0

When ready for use, the
total end-use concentration
of all iodide-producing
chemicals in the solution is
not to exceed 25 ppm of
titratable iodine

Quaternary ammonium compounds,
8001–54–5
alkyl (C12-C18) benzyldimethyl, chlorides

When ready for use, the enduse concentration of all
quaternary chemicals in the
solution is not to exceed 200
ppm of active quaternary
compound

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Quaternary ammonium compounds: nalkyl (C12-18) dimethyl benzyl

68424–85–1

When ready for use, the enduse concentration of all
quaternary chemicals in
solution is not to exceed 400
ppm of active quaternary
compound

None

When ready for use, the enduse concentration of all
quaternary chemicals in the
solution is not to exceed 200
ppm of active quaternary
compound

None

When ready for use, the enduse concentration of all
quaternary chemicals in the
solution is not to exceed 200
ppm of active quaternary
compound

Quaternary ammonium compounds, Di-n- None
Alkyl (C8-10) dimethyl ammonium

When ready for use, the enduse concentration of these
specific in quaternary
ammonium compounds is
not to exceed 240 ppm of
active quaternary ammonium
compound; the end-use
concentration of all
quaternary chemicals in the
solution is not to exceed 400
ppm of active quaternary
compound

ammonium chloride

Quaternary ammonium compounds, nalkyl (C12-C14) dimethyl ethylbenzyl
ammonium chloride, average molecular
weight (in amu), 377 to 384
Quaternary ammonium compounds nalkyl (C12-C18) dimethyl ethylbenzyl
ammonium chloride average molecular
weight (in amu) 384

chloride, average molecular weight (in
amu) 332 to 361

Quaternary ammonium compounds,
148788–55–
When ready for use, the enddidecyl dimethyl ammonium carbonate/ 0/148812–654–1 use concentration of these
didecyl dimethyl ammonium bicarbonate
specific ammonium
compounds is not to exceed
240 ppm of active
quaternary ammonium
compound
Silver ions resulting from the use of
electrolytically-generated silver ions
stabilized in citric acid as silver
dihydrogen citrate (does not include
metallic silver)

14701–21–4

Sulfuric acid monododecyl ester, sodium 151–21–3
salt (sodium lauryl sulfate)

When ready for use, the enduse concentration of silver
ions is not to exceed 50 ppm
of active silver
When ready for use, the enduse concentration is not to
exceed 350 ppm

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Electronic Code of Federal Regulations:

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione,
1,3-dichloro-, sodium salt

2893–78–9

When ready for use, the enduse concentration of all dior trichloroisocyanuric acid
chemicals in the solution is
not to exceed 100 ppm
determined as total available
chlorine

(b) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation
may be applied to: Dairy processing equipment, and food-processing equipment and utensils.

Pesticide Chemical

CAS Reg. No.

Limits

Acetic acid

64–19–7

When ready for use, the
end-use concentration is
not to exceed 686 ppm

Acetic acid, chloro-, sodium salt, reaction
products with 4,5-dihydro-2-undecyl-1Himidazole-1-ethanol and sodium hydroxide

68608–66–2

When ready for use, the
end-use concentration is
not to exceed 42 ppm
chloroacetic acid

Benzenesulfonic acid, dodecyl-

27176–87–0

When ready for use, the
end-use concentration is
not to exceed 5.5 ppm

Butanedioic acid, octenyl-

28805–58–5

When ready for use, the
end-use concentration is
not to exceed 156 ppm

Butoxy monoether of mixed (ethylenepropylene) polyalkylene glycol, minimum
average molecular weight (in amu), 2400

None

None

Calcium chloride

10043–52–4

When ready for use, the
end-use concentration is
not to exceed 17 ppm

n-Carboxylic acids (C6-C12), consisting of a

None

When ready for use, the
end-use concentration is
not to exceed 39 ppm

Decanoic acid

334–48–5

When ready for use, the
end-use concentration is
not to exceed 90 ppm

Ethanesulfonic acid, 2-[cyclohexyl (1oxohexadecyl) amino]-, sodium salt

132–43–4

When ready for use, the
end-use concentration is
not to exceed 237 ppm

Ethylenediaminetetraacetic acid (EDTA),
disodium salt

139–33–3

When ready for use, the
end-use concentration is
not to exceed 1400 ppm

mixture of not less than 56% octanoic acid
and not less than 40% decanoic acid

FD&C Yellow No. 5 (Tartrazine) (conforming to 1934–21–0
21 CFR 74.705)

None

D-Gluconic acid, monosodium salt

When ready for use, the
end-use concentration is
not to exceed 760 ppm

527–07–1

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Electronic Code of Federal Regulations:

Hydriodic acid

10034–85–2

When ready for use, the
total end-use
concentration of all
iodide-producing
chemicals is not to
exceed 25 ppm of
titratable iodine

Hydrogen peroxide

7722–84–1

When ready for use, the
end-use concentration is
not to exceed 465 ppm

Hypochlorous acid

7790–92–3

When ready for use, the
end-use concentration of
all hypochlorous acid
chemicals in the solution
is not to exceed 200
ppm determined as total
available chlorine

Iodine

7553–56–2

When ready for use, the
total end-use
concentration of all
iodide-producing
chemicals in the solution
is not to exceed 25 ppm
of titratable iodine

Lactic acid

50–21–5

When ready for use, the
end-use concentration is
not to exceed 138 ppm

Nonanoic acid

112–05–0

When ready for use, the
end-use concentration is
not to exceed 90 ppm

1-Octanamine, N,N-dimethyl-

7378–99–6

When ready for use, the
end-use concentration is
not to exceed 113 ppm

1,2-Octanedisulfonic acid

113669–58–2

When ready for use, the
end-use concentration is
not to exceed 102 ppm

1-Octanesulfonic acid

3944–72–7

When ready for use, the
end-use concentration is
not to exceed 172 ppm

1-Octanesulfonic acid, sodium salt

5324–84–5

When ready for use, the
end-use concentration is
not to exceed 297 ppm

1-Octanesulfonic acid, 2-sulfino-

113652–56–5

When ready for use, the
end-use concentration is
not to exceed 102 ppm

Octanoic acid

124–07–2

When ready for use, the
end-use concentration is
not to exceed 176 ppm

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Oxychloro species (including chlorine dioxide)
generated by acidification of an aqueous
solution of sodium chlorite

None

When ready for use, the
end-use concentration is
not to exceed 200 ppm
of chlorine dioxide as
determined by the
method titled,
Iodometric Method for
the Determination of
Available Chlorine
Dioxide (50-250 ppm
available chlorine
dioxide)

Peroxyacetic acid

79–21–0

When ready for use, the
end-use concentration is
not to exceed 315 ppm

Peroxyoctanoic acid

33734–57–5

When ready for use, the
end-use concentration is
not to exceed 122 ppm

Phosphonic acid, (1-hydroxyethylidene)bis-

2809–21–4

When ready for use, the
end-use concentration is
not to exceed 34 ppm

Phosphoric acid

7664–38–2

None

Phosphoric acid, monosodium salt

7558–80–7

When ready for use, the
end-use concentration is
not to exceed 350 ppm

Potassium iodide

7681–11–0

When ready for use, the
total end-use
concentration of all
iodide-producing
chemicals in the solution
is not to exceed 25 ppm
of titratable iodine

Propanoic acid

79–09–4

When ready for use, the
end-use concentration is
not to exceed 297 ppm

2,6-Pyridinedicarboxylic acid

499–83–2

When ready for use, the
end-use concentration is
not to exceed 1.2 ppm

Sulfuric acid

7664–93–9

When ready for use, the
end-use concentration is
not to exceed 288 ppm

Sulfuric acid monododecyl ester, sodium salt
(sodium lauryl sulfate)

151–21–3

When ready for use, the
end-use concentration is
not to exceed 350 ppm

(c) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation
may be applied to: Food-processing equipment and utensils.

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Pesticide Chemical
Acetic acid

CAS Reg.
No.
64–19–7

Limits
When ready for use, the enduse concentration is not to
exceed 686 ppm

Acetic acid, chloro-, sodium salt, reaction 68608–66–2
products with 4,5-dihydro-2-undecyl-1Himidazole-1-ethanol and sodium hydroxide

When ready for use, the enduse concentration is not to
exceed 42 ppm chloroacetic
acid

Ammonium chloride

12125–02–9

When ready for use, the enduse concentration is not to
exceed 48 ppm

Benzenesulfonic acid, dodecyl-

27176–87–0

When ready for use, the enduse concentration is not to
exceed 400 ppm

Benzenesulfonic acid, dodecyl-, sodium
salt

25155–30–0

When ready for use, the enduse concentration is not to
exceed 430 ppm

[1,1′-Biphenyl]-2-ol

90–43–7

When ready for use, the enduse concentration is not to
exceed 400 ppm

Boric acid, sodium salt

7775–19–1

None

Butanedioic acid, octenyl-

28805–58–5

When ready for use, the enduse concentration is not to
exceed 156 ppm

Butanedioic acid, sulfo-, 1,4-dioctyl ester,
sodium salt

1639–66–3

None

Butoxy monoether of mixed (ethyleneNone
propylene) polyalkylene glycol, cloudpoint
of 90 - 100oC in 0.5 aqueous solution,
average molecular weight (in amu), 3300

None

Butoxy monoether of mixed (ethylenepropylene) polyalkylene glycol, minimum
average molecular weight (in amu), 2400

None

None

Calcium chloride

10043–52–4

When ready for use, the enduse concentration is not to
exceed 17 ppm

n-Carboxylic acids (C6-C12), consisting of

None

a mixture of not less than 56% octanoic
acid and not less than 40% decanoic acid

When ready for use, the enduse concentration is not to
exceed 39 ppm

3-Cyclohexene-1-methanol,α,α,4-trimethyl- 98–55–5

None

1-Decanaminium, N-decyl-N, N-dimethyl-, 7173–51–5
chloride

When ready for use, the enduse concentration is not to
exceed 200 ppm of active
quaternary compound

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Decanoic acid

3347–48–5

When ready for use, the enduse concentration is not to
exceed 234 ppm

Ethanesulfonic acid, 2-[cyclohexyl (1oxohexadecyl) amino]-, sodium salt

132–43–4

When ready for use, the enduse concentration is not to
exceed 237 ppm

Ethanol

64–17–5

None

Ethanol, 2 butoxy-

111–76–2

None

Ethanol, 2-(2-ethoxyethoxy)-

111–90–0

None

Ethylenediaminetetraacetic acid (EDTA),
disodium salt

139–33–3

When ready for use, the enduse concentration is not to
exceed 1400 ppm

Ethylenediaminetetraacetic acid (EDTA),
tetrasodium salt

64–02–8

None

Fatty acids, coco, potassium salts

61789–30–8

None

Fatty acids, tall-oil, sulfonated, sodium
salts

68309–27–3

When ready for use, the enduse concentration is not to
exceed 66 ppm

FD&C Yellow No. 5 (Tartrazine)
(conforming to 21 CFR 74.705)

1934–21–0

None

D-Gluconic acid, monosodium salt

527–07–1

When ready for use, the enduse concentration is not to
exceed 760 ppm

Hydriodic acid

10034–85–2

When ready for use, the total
end-use concentration of all
iodide-producing chemicals in
the solution is not to exceed
25 ppm of titratable iodine

Hydrogen peroxide

7722–84–1

When ready for use, the enduse concentration is not to
exceed 1100 ppm

Hypochlorous acid

7790–92–3

When ready for use, the enduse concentration of all
hypochlorous acid chemicals
in the solution is not to
exceed 200 ppm determined
as total available chlorine

Hypochlorous acid, calcium salt

7778–54–3

When ready for use, the enduse concentration of all
hypochlorous acid chemicals
in the solution is not to
exceed 200 ppm determined
as total available chlorine

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Hypochlorous acid, lithium salt

13840–33–0

When ready for use, the enduse concentration of all
hypochlorous acid chemicals
in the solution is not to
exceed 200 ppm determined
as total available chlorine and
30 ppm lithium

Hypochlorous acid, potassium salt

7778–66–7

When ready for use, the enduse concentration of all
hypochlorous acid chemicals
in the solution is not to
exceed 200 ppm determined
as total available chlorine

Hypochlorous acid, sodium salt

7681–52–9

When ready for use, the enduse concentration of all
hypochlorous acid chemicals
in the solution is not to
exceed 200 ppm determined
as total available chlorine

Iodine

7553–56–2

When ready for use, the total
end-use concentration of all
iodide-producing chemicals in
the solution is not to exceed
25 ppm of titratable iodine

Lactic acid

50–21–5

None

Magnesium oxide

1309–48–4

None

Methylene blue

61–73–4

When ready for use, the enduse concentration is not to
exceed 0.4 ppm

Neodecanoic acid

26896–20–8

When ready for use, the enduse concentration is not to
exceed 174 ppm

Nonanoic acid

112–05–0

When ready for use, the enduse concentration is not to
exceed 90 ppm

α-(p-Nonylphenyl)-ω-hydroxypoly
(oxyethylene) maximum average
molecular weight (in amu), 748

None

None

α-(p-Nonylphenol)-ω-hydroxypoly
(oxyethylene) average poly(oxyethylene)
content 11 moles

None

None

α-(p-Nonylphenyl)-ω-hydroxypoly
(oxyethylene) produced by the
condensation of 1 mole p-nonylphenol
with 9 to 12 moles ethylene oxide

None

None

α-(p-Nonylphenyl)-ω-hydroxypoly
(oxyethylene), 9 to 13 moles ethylene
oxide

None

None

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Octadecanoic acid, calcium salt

1592–23–0

None

9-Octadecenoic acid (9Z)-, sulfonated

68988–76–1

When ready for use, the enduse concentration is not to
exceed 312 ppm

9-Octadecenoic acid (9Z)-sulfonated,
sodium salts

68443–05–0

When ready for use, the enduse concentration is not to
exceed 200 ppm

1-Octanamine, N,N-dimethyl-

7378–99–6

When ready for use, the enduse concentration is not to
exceed 113 ppm

1,2-Octanedisulfonic acid

113669–58–2 When ready for use, the enduse concentration is not to
exceed 102 ppm

1-Octanesulfonic acid

3944–72–7

When ready for use, the enduse concentration is not to
exceed 172 ppm

1-Octanesulfonic acid, sodium salt

5324–84–5

When ready for use, the enduse concentration is not to
exceed 312 ppm

1-Octanesulfonic acid, 2-sulfino-

113652–56–5 When ready for use, the enduse concentration is not to
exceed 102 ppm

Octanoic acid

124–07–2

Oxirane, methyl-, polymer with oxirane,
9003–11–6
minimum molecular weight (in amu), 1900

When ready for use, the enduse concentration is not to
exceed 234 ppm
None

Oxirane, methyl-, polymer with oxirane,
106392–12–5 None
block, average molecular weight (in amu),
1900
Oxirane, methyl-, polymer with oxirane,
None
block, minimum average molecular weight
(in amu), 2000

None

Oxirane, methyl-, polymer with oxirane,
block, 27 to 31 moles of
polyoxypropylene, average molecular
weight (in amu) 2000

None

None

Oxychloro species (predominantly
chlorite, chlorate and chlorine dioxide in
an equilibrium mixture) generated either
(i) by directly metering a concentrated
chlorine dioxide solution prepared just
prior to use, into potable water, or (ii) by
acidification of an aqueous alkaline
solution of oxychloro species
(predominately chlorite and chlorate)
followed by dilution with potable water

None

When ready for use, the enduse concentration is not to
exceed 200 ppm of chlorine
dioxide as determined by the
method titled, “Iodometric
Method for the Determination
of Available Chlorine Dioxide
(50-250 ppm available
chlorine dioxide)”

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Oxychloro species (including chlorine
dioxide) generated by acidification of an
aqueous solution of sodium chlorite

None

When ready for use, the enduse concentration is not to
exceed 200 ppm of chlorine
dioxide as determined by the
method titled, “Iodometric
Method for the Determination
of Available Chlorine Dioxide
(50-250 ppm available
chlorine dioxide)”

2,4-Pentanediol, 2-methyl-

107–41–5

None

Peroxyacetic acid

79–21–0

When ready for use, the enduse concentration is not to
exceed 315 ppm

Peroxyoctanoic acid

33734–57–5

When ready for use, the enduse concentration is not to
exceed 122 ppm

Phenol, 4-chloro-2-(phenylmethyl)-

120–32–1

When ready for use, the enduse concentration is not to
exceed 320 ppm

Phenol, 4-(1,1-dimethylpropyl)-

80–46–6

When ready for use, the enduse concentration is not to
exceed 80 ppm

Phosphonic acid, (1-hydroxyethylidene)bis- 2809–21–4

When ready for use, the enduse concentration is not to
exceed 34 ppm

Phosphoric acid

7664–38–2

None

Phosphoric acid, monosodium salt

7558–80–7

When ready for use, the enduse concentration is not to
exceed 350 ppm

Phosphoric acid, trisodium salt

7601–54–9

When ready for use, the enduse concentration is not to
exceed 5916 ppm

Poly(oxy-1,2-ethanediyl), α-[(1,1,3,3tetramethylbutyl) phenyl]-ω-hydroxy-,
produced with one mole of the phenol
and 4 to 14 moles ethylene oxide

None

None

Potassium bromide

7758–02–3

When ready for use, the enduse concentration of all
bromide-producing chemicals
in the solution is not to
exceed 200 ppm total
available halogen

Potassium iodide

7681–11–0

When ready for use, the total
end-use concentration of all
iodide-producing chemicals in
the solution is not to exceed
25 ppm of titratable iodine

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Propanoic acid

79–09–4

When ready for use, the enduse concentration is not to
exceed 297 ppm

2,6-Pyridinedicarboxylic acid

499–83–2

When ready for use, the enduse concentration is not to
exceed 1.2 ppm

Quaternary ammonium compounds, alkyl
(C12-C18) benzyldimethyl, chlorides

8001–54–5

When ready for use, the enduse concentration of this
specific quaternary compound
is not to exceed 200 ppm
within the end-use total
concentration that is not to
exceed 400 ppm active
quaternary compound

Quaternary ammonium compounds, nalkyl (C12-C14) dimethyl ethylbenzyl

None

When ready for use, the enduse concentration of this
specific quaternary compound
is not to exceed 200 ppm
within the end-use total
concentration that is not to
exceed 400 ppm active
quaternary compound

None

When ready for use, the enduse concentration of this
specific quaternary compound
is not to exceed 200 ppm
within the end-use total
concentration that is not to
exceed 400 ppm active
quaternary compound

None

When ready for use, the enduse concentration of this
specific quaternary compound
is not to exceed 240 ppm
within the end-use total
concentration that is not to
exceed 400 ppm active
quaternary compound

None

None

7647–15–6

When ready for use, the enduse concentration of all
bromide-producing chemicals
in the solution is not to
exceed 200 ppm total
available halogen

ammonium chloride, average molecular
weight (in amu), 377 to 384

Quaternary ammonium compounds, nalkyl (C12-C18) dimethyl ethylbenzyl
ammonium chloride average molecular
weight (in amu) 384

Quaternary ammonium compounds, di-nAlkyl (C8-C10) dimethyl ammonium
chloride, average molecular weight (in
amu), 332 to 361

Sodium-α-alkyl(C12-C15)-ω-hydroxypoly
(oxyethylene) sulfate with the poly
(oxyethylene) content averaging one mole
Sodium bromide

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Sodium iodide

7681–82–5

When ready for use, the total
end-use concentration of all
iodide-producing chemicals in
the solution is not to exceed
25 ppm of titratable iodine

Sulfuric acid

7664–93–9

When ready for use, the enduse concentration is not to
exceed 228 ppm

Sulfuric acid monododecyl ester, sodium
salt (sodium lauryl sulfate)

151–21–3

None

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2782–57–2
dichloro-

When ready for use, the enduse concentration of all di- or
trichloroisocyanuric acid
chemicals in the solution is
not to exceed 100 ppm
determined as total available
chlorine

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2244–21–5
dichloro-, potassium salt

When ready for use, the enduse concentration of all di- or
trichloroisocyanuric acid
chemicals in the solution is
not to exceed 100 ppm
determined as total available
chlorine

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3- 2893–78–9
dichloro-, sodium salt

When ready for use, the enduse concentration of all di- or
trichloroisocyanuric acid
chemicals in the solution is
not to exceed 100 ppm
determined as total available
chlorine

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione,
1,3,5-trichloro-

87–90–1

When ready for use, the enduse concentration of all di- or
trichloroisocyanuric acid
chemicals in the solution is
not to exceed 100 ppm
determined as total available
chlorine

1,3,5-Triazine, N,N′,N″-trichloro-2,4,6triamino-

7673–09–8

When ready for use, the enduse concentration of all di- or
trichloroisocyanuric acid
chemicals in the solution is
not to exceed 200 ppm
determined as total available
chlorine

Xylenesulfonic acid, sodium salt

1300–72–7

When ready for use, the enduse concentration is not to
exceed 62 ppm

[69 FR 23136, Apr. 28, 2004, as amended at 71 FR 30811, May 31, 2006; 71 FR 45423, Aug. 9, 2006; 71
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FR 46125, Aug. 11, 2006; 72 FR 51186, Sept. 6, 2007; 73 FR 37858, July 2, 2008; 73 FR 49107, Aug. 20,
2008; 73 FR 53725, Sept. 17, 2008; 74 FR 27454, June 10, 2009; 74 FR 38944, Aug. 5, 2009; 74 FR
40509, Aug. 12, 2009]

§ 180.950 Tolerance exemptions for minimal risk active and inert ingredients.
top
Unless specifically excluded, residues resulting from the use of the following substances as either an inert
or an active ingredient in a pesticide chemical formulation, including antimicrobial pesticide chemicals, are
exempted from the requirement of a tolerance under FFDCA section 408, if such use is in accordance with
good agricultural or manufacturing practices.
(a) Commonly consumed food commodities. Commonly consumed food commodities means foods that
are commonly consumed for their nutrient properties. The term commonly consumed food commodities
shall only apply to food commodities (whether a raw agricultural commodity or a processed commodity) in
the form the commodity is sold or distributed to the public for consumption.
(1) Included within the term commonly consumed food commodities are:
(i) Sugars such as sucrose, lactose, dextrose and fructose, and invert sugar and syrup.
(ii) Spices such as cinnamon, cloves, and red pepper.
(iii) Herbs such as basil, anise, or fenugreek.
(2) Excluded from the term commonly consumed food commodities are:
(i) Any food commodity that is adulterated under 21 U.S.C. 342.
(ii) Both the raw and processed forms of peanuts, tree nuts, milk, soybeans, eggs, fish, crustacea, and
wheat.
(iii) Alcoholic beverages.
(iv) Dietary supplements.
(b) Animal feed items. Animal feed items means meat meal and all items derived from field crops that are
fed to livestock excluding both the raw and processed forms of peanuts, tree nuts, milk, soybeans, eggs,
fish, crustacea, and wheat. Meat meal is an animal feed composed of dried animal fat and protein that has
been sterilized. Other than meat meal, the term animal feed item does not extend to any item designed to
be fed to animals that contains, to any extent, components of animals. Included within the term animal
feed items are:
(1) The hulls and shells of the commodities specified in paragraph (a)(2)(ii) of this section, and cocoa bean.
(2) Bird feed such as canary seed.
(3) Any feed component of a medicated feed meeting the definition of an animal feed item.
(c) Edible fats and oils. Edible fats and oils means all edible (food or feed) fats and oils, derived from either
plants or animals, whether or not commonly consumed, including products derived from hydrogenating
(food or feed) oils, or liquefying (food or feed) fats.
(1) Included within the term edible fats and oils are oils (such as soybean oil) that are derived from the
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commodities specified in paragraph (a)(2)(ii) of this section when such oils are highly refined via a solvent
extraction procedure.
(2) Excluded from the term edible fats and oils are plant oils used in the pesticide chemical formulation
specifically to impart their characteristic fragrance and/or flavoring.
(d) [Reserved]
(e) Specific chemical substances. Residues resulting from the use of the following substances as either an
inert or an active ingredient in a pesticide chemical formulation, including antimicrobial pesticide
chemicals, are exempted from the requirement of a tolerance under FFDCA section 408, if such use is in
accordance with good agricultural or manufacturing practices.

Chemical
Acetic acid, sodium salt
Alpha-cyclodextrin

CAS No.
127–09–3
10016–20–3

Amylopectin, acid-hydrolyzed, 1-octenylbutanedioate

113894–85–2

Amylopectin, hydrogen 1-octadecenylbutanedioate

125109–81–1

Animal glue
Ascorbic acid (vitamin C)
Beeswax
Benzoic acid, sodium salt
Beta-cyclodextrin

None
50–81–7
8012–89–3
532–32–1
7585–39–9

Carbonic acid, monopotassium salt

298–14–6

Carbonic acid, monosodium salt (sodium bicarbonate)

144–55–8

Carnauba wax

8015–86–9

Carob gum (locust bean gum)

9000–40–2

Castor oil

8001–79–4

Castor oil, hydrogenated

8001–78–3

Cellulose

9004–34–6

Cellulose acetate

9004–35–7

Cellulose, carboxy methyl ether, sodium salt

9004–32–4

Cellulose, 2-hydroxyethyl ether

9004–62–0

Cellulose, 2-hydroxypropyl ether

9004–64–2

Cellulose, 2-hydroxypropyl methyl ether

9004–65–3

Cellulose, methyl ether

9004–67–5

Cellulose, mixture with cellulose carboxymethyl ether, sodium salt

51395–75–6

Cellulose, pulp

65996–61–4

Cellulose, regenerated

68442–85–3

Citric acid

77–92–9

Citric acid, 2-(acetyloxy)-, tributyl ester

77–90–7

Citric acid, calcium salt

7693–13–2

Citric acid, calcium salt (2:3)

813–94–5

Citric acid, dipotassium salt

3609–96–9

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Citric acid, disodium salt

144–33–2

Citric acid, monohydrate

5949–29–1

Citric acid, monopotassium salt
Citric acid, monosodium salt
Citric acid, potassium salt
Citric acid, triethyl ester
Citric acid, tripotassium salt
Citric acid, tripotassium salt, monohydrate
Citric acid, sodium salt
Citric acid, trisodium salt

866–83–1
18996–35–5
7778–49–6
77–93–0
866–84–2
6100–05–6
994–36–5
68–04–2

Citric acid, trisodium salt, dihydrate

6132–04–3

Citric acid, trisodium salt, pentahydrate

6858–44–2

Coffee grounds
Dextrins

68916–18–7
9004–53–9

1,3-Dioxolan-2-one, 4-methyl-(propylene carbonate)

108–32–7

Fumaric acid

110–17–8

Gamma-cyclodextrin

17465–86–0

Gellan gum

71010–52–1

D-Glucitol (sorbitol)

50–70–4

Glycerol (glycerin) (1,2,3-propanetriol)

56–81–5

Guar gum

9000–30–0

Humic acid

1413–93–6

Humic acid, potassium salt

68514–28–3

Humic acid, sodium salt

68131–04–4

Lactic acid, n-butyl ester
Lactic acid, n-butyl ester, (S)
Lactic acid, ethyl ester
Lactic acid, ethyl ester,(S)

138–22–7
34451–19–9
97–64–3
687–47–8

Lanolin

8006–54–0

Lecithins

8002–43–5

Lecithins, soya

8030–76–0

Licorice Extract

68916–91–6

Maltodextrin
Paper
Potassium chloride
2-Propanol (isopropyl alcohol)
Red cabbage color, expressed from edible red cabbage heads via a
pressing process using only acidified water
Silica, amorphous, fumed (crystalline free)
Silica, amorphous, precipitated and gel
Silica gel
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9050–36–6
None
7447–40–7
67–63–0
None
112945–52–5
7699–41–4
63231–67–4

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Silica gel, precipitated, crystalline-free

112926–00–8

Silica, hydrate

10279–57–9

Silica, vitreous

60676–86–0

Soap (The water soluble sodium or potassium salts of fatty acids produced
by either the saponification of fats and oils, or the neutralization of fatty
acid)

None

Sorbic acid, potassium salt

24634–61–5

Soapbark (Quillaja saponin)

1393–03–9

Sodium alginate

9005–38–3

Sodium chloride

7647–14–5

Syrups, hydrolyzed starch, hydrogenated

68425–17–2

Ultramarine blue (C.I. Pigment Blue 29)

57455–37–5

Urea

57–13–6

Vanillin

121–33–5

Xanthan gum

11138–66–2

[67 FR 36537, May 24, 2002]
Editorial Note: ForFederal Registercitations affecting §180.950, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.960 Polymers; exemptions from the requirement of a tolerance.
top
Residues resulting from the use of the following substances, that meet the definition of a polymer and the
criteria specified for defining a low-risk polymer in 40 CFR 723.250, as an inert ingredient in a pesticide
chemical formulation, including antimicrobial pesticide chemical formulations, are exempted from the
requirement of a tolerance under FFDCA section 408, if such use is in accordance with good agricultural
or manufacturing practices.

Polymer

CAS No.

Acetic acid ethenyl ester, polymer with ethenol and (α)-2-propenyl- 137091–12–4
(ω)-hydroxypoly (oxy-1,2-ethanediyl) minimum number average
molecular weight (in amu), 15,000
Acetic acid ethenyl ester, polymer with 1-ethenyl-2-pyrrolidinone

25086–89–9

Acetic acid ethenyl ester, polymer with sodium 2-methyl-2-[(1-oxo- 924892–37–5
2-propen-1-yl)amino]-1-propanesulfonate (1:1), hydrolyzed,
minimum number average molecular weight (in amu), 61,000
Acrylic acid, polymerized, and its ethyl and methyl esters

None

Acrylic acid-sodium acrylate-sodium-2-methylpropanesulfonate
copolymer, minimum average molecular weight (in amu), 4,500

97953–25–8

Acrylic acid-stearyl methacrylate copolymer, minimum number
average molecular weight (in amu), 2,500

27756–15–6

Acrylic acid, styrene, α-methyl styrene copolymer, ammonium salt,
minimum number average molecular weight (in amu), 1,250

89678–90–0

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Acrylic acid terpolymer, partial sodium salt, minimum number
average molecular weight (in amu), 2,400

151006–66–5

Acrylic polymers composed of one or more of the following
monomers: Acrylic acid, methyl acrylate, ethyl acrylate, butyl
acrylate, hydroxyethyl acrylate, hydroxypropyl acrylate,
hydroxybutyl acrylate, carboxyethyl acrylate, methacrylic acid,
methyl methacrylate, ethyl methacrylate, butyl methacrylate,
isobutyl methacrylate, hydroxyethyl methacrylate, hydroxypropyl
methacrylate, hydroxybutyl methacrylate, lauryl methacrylate, and
stearyl methacrylate; with none and/or one or more of the
following monomers: Acrylamide, N-methyl acrylamide, N,Ndimethyl acrylamide, N-octylacrylamide, maleic anhydride, maleic
acid, monoethyl maleate, diethyl maleate, monooctyl maleate,
dioctyl maleate; and their corresponding sodium, potassium,
ammonium, isopropylamine, triethylamine, monoethanolamine,
and/or triethanolamine salts; the resulting polymer having a
minimum number average molecular weight (in amu), 1,200

None

Acrylonitrile-butadiene copolymer conforming to 21 CFR 180.22,
minimum average molecular weight (in amu), 1,000

9003–18–3

Acrylonitrile-styrene-hydroxypropyl methacrylate copolymer,
minimum number average molecular weight (in amu), 447,000

None

α-alkyl (C12–C15) - ω- hydroxypoly(oxypropylene)poly(oxyethylene) 68551–13–3
copolymers (where the poly(oxypropylene) content is 3–60 moles
and the poly(oxyethylene) content is 5–80 moles), the resulting
ethoxylated propoxylated (C12–C15) alcohols having a minimum
molecular weight (in amu), 1,500
α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly (oxyethylene)
9002–92–0, 9004–
polymers where the alkyl chain contains a minimum of six carbons, 95–9, 9005–00–9,
minimum number average molecular weight (in amu) 1,100
26183–52–8, 34398–
01–1, 52292–17–8,
66455–14–9, 66455–
15–0, 68002–97–1,
68131–39–5, 68131–
40–8, 68154–96–1,
68213–23–0, 68439–
45–2, 68439–46–3,
68526–94–3, 68439–
50–9, 68439–49–6,
68551–12–2, 68951–
67–7, 71243–46–4,
97043–91–9, 9043–
30–5, 60828–78–6,
61827–42–7, 24938–
91–8, 68439–54–3,
69011–36–5, 78330–
20–8, 78330–21–9,
106232–83–1,
127036–24–2,
160875–66–1, 9004–
98–2, 68920–66–1,
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61804–34–0, 61791–
28–4, 71060–57–6,
26468–86–0, 31726–
34–8, 52609–19–5,
61791–20–6, 68155–
01–1, 69013–19–0,
69364–63–2, 70879–
83–3, 78330–19–5,
97953–22–5,
157627–86–6,
34398–05–5, 72905–
87–4, 84133–50–6,
61702–78–1, 27306–
79–2, 169107–21–
5, 61791–13–7,
39587–22–9, 85422–
93–1; 68154–98–3,
61725–89–1, 68002–
96–0, 68154–97–2,
68439–51–0, 68551–
13–3, 68603–25–8,
68937–66–6, 68987–
81–5, 69227–21–0,
70750–27–5,
103818–93–5,
166736–08–9,
120313–48–6,
68213–24–1, 68458–
88–8, 68551–14–4,
69013–18–9, 69227–
22–1, 72854–13–8,
73049–34–0, 78330–
23–1, 37311–02–7,
64366–70–7, 37251–
67–5, 9087–53–0,
196823–11–7,
57679–21–7,
111905–54–5,
61827–84–7,
172588–43–1
Alkyl (C12–C20) methacrylate-methacrylic acid copolymer, minimum None
molecular weight (in amu), 11,900
2H-Azepin-2-one, 1-ethenylhexahydro-, homopolymer

25189–83–7

1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-dimethyl ester, sodium
salt, polymer with 1,3-benzene dicarboxylic acid, 1,4-benzene
dicarboxylic acid, dimethyl 1,4-benzene dicarboxylate and 1,2ethanediol, minimum number average molecular weight (in amu),
2,580

212842–88–1

87823–33–4
3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine-2,4,6-(3H,5H)trione, polymer with diethylenetriamine, minimum number average
molecular weight (in amu), 1,000,000
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Butadiene-styrene copolymer

None

1,4-Butanediol-methylenebis(4-phenylisocyanate)-poly
(tetramethylene glycol) copolymer, minimum molecular weight (in
amu) 158,000

9018– 04–6

Butene, homopolymer

9003–29–6

2-butenedioic acid (2Z)-, monobutyl ester, polymer with
methoxyethene, sodium salt, minimum number average molecular
weight (in amu), 18,200

205193–99–3

2-Butenedioic acid (Z)-, polymer with ethenol and ethenyl acetate,
sodium salt, minimum number average molecular weight (in amu),
75,000

139871–83–3

Butyl acrylate-vinyl acetate-acrylic acid copolymer, minimum
number average molecular weight (in amu), 18,000

65405–40–5

Castor oil, ethoxylated, oleate, minimum number average
molecular weight (in amu) 2,000

220037–02–5

Castor oil, polyoxyethylated; the poly(oxyethylene) content
averages 5–54 moles

None

Chlorinated polyethylene

64754–90–1

Cross-linked nylon-type polymer formed by the reaction of a
mixture of sebacoyl chloride and polymethylene
polyphenylisocycanate with a mixture of ethylenediamine and
diethylenetriamine

None

Cross-linked polyurea-type encapsulating polymer

None

Dimethylpolysiloxane minimum number average molecular weight
(in amu), 6,800

63148–62–9

Dimethyl silicone polymer with silica, minimum number average
molecular weight (in amu), 1,100,000

67762–90–7

α-(o,p-Dinonylphenyl)-ω-hydroxypoly(oxyethylene) produced by
condensation of 1 mole of dinonylphenol (nonyl group is a
propylene trimer isomer) with an average of 140-160 moles of
ethylene oxide

9014–93–1

Docosyl methacrylate-acrylic acid copolymer, or docosyl
methacrylate-octadecyl methacrylate-acrylic acid copolymer,
minimum number average molecular weight (in amu), 3,000

None

1,12-Dodecanediol dimethacrylate polymer, minimum molecular
weight (in amu), 100,000

None

α-(p-Dodecylphenyl)-ω-hydroxypoly(oxyethylene) produced by the
condensation of 1 mole of dodecylphenol (dodecyl group is a
propylene tetramer isomer) with an average of 30-70 moles of
ethylene oxide

9014–92–0
26401–47–8

1, 2-Ethanediamine, polymer with methyl oxirane and oxirane,
minimum number average molecular weight (in amu), 1,100

26316–40–5

Ethylene glycol dimethyacrylate-lauryl methacrylate copolymer,
minimum molecular weight (in amu), 100,000

None

Ethylene glycol dimethacrylate polymer, minimum molecular weight None
(in amu), 100,000

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Formaldehyde, polymer with α-[bis(1-phenylethyl)phenyl]-ωhydroxypoly(oxy-1,2-ethanediyl), number average molecular
weight (in amu), 1,803

157291–93–5

Formaldehyde, polymer with 2-methyloxirane and 4-nonylphenol,
minimum number average molecular weight (in amu), 4,000

37523–33–4

Fumaric acid-isophthalic acid-styrene-ethylene/propylene glycol
copolymer, minimum average molecular weight (in amu), 1×1018

None

Hexadecyl acrylate-acrylic acid copolymer, hexadecyl acrylate-butyl None
acrylate-acrylic acid copolymer, or hexadecyl acrylate-dodecyl
acrylate-acrylic acid copolymer, minimum number average
molecular weight (in amu), 3,000
Hexamethyl disilizane, reaction product with silica, minimum
number average molecular weight (in amu), 645,000

68909–20–6

1,6-Hexanediol dimethyacrylate polymer, minimum molecular
weight (in amu), 100,000

None

α-Hydro-ω-hydroxy-poly(oxyethylene) C8 alkyl ether citrates, poly
(oxyethylene) content is 4–12 moles, minimum number average
molecular weight (in amu) 1,300

330977–00–9

α-Hydro-ω-hydroxy-poly(oxyethylene) C10–C16-alkyl ether citrates, 330985–58–5
poly(oxyethylene) content is 4–12 moles, minimum number
average molecular weight (in amu) 1,100
α-Hydro-ω-hydroxy-poly(oxyethylene) C16–C18-alkyl ether citrates, 330985–61–0
poly(oxyethylene) content is 4–12 moles, minimum number
average molecular weight (in amu) 1,300
α-Hydro-ω-hydroxypoly(oxyethylene), minimum molecular weight
(in amu), 100,000

None

None
α-Hydro-ω-hydroxypoly(oxyethylene)poly (oxypropylene) poly
(oxyethylene) block copolymer; the minimum poly(oxypropylene)
content is 27 moles and the minimum molecular weight (in amu) is
1,900
α-Hydro-ω-hydroxypoly(oxypropylene); minimum molecular weight None
(in amu) 2,000
12-Hydroxystearic acid-polyethylene glycol copolymer, minimum
number average molecular weight (in amu), 3,690

70142–34–6

Isodecyl alcohol ethoxylated (2–8 moles) polymer with
chloromethyl oxirane, minimum number average molecular weight
(in amu) 2,500

None

Lauryl methacrylate-1,6-hexanediol dimethacrylate copolymer,
minimum molecular weight (in amu), 100,000

None

Maleic acid-butadiene copolymer

None

Maleic acid monobutyl ester-vinyl methyl ether copolymer,
minimum average molecular weight (in amu), 52,000

25119–68–0

Maleic acid monoethyl ester-vinyl methyl ether copolymer,
minimum average molecular weight (in amu), 46,000

25087–06–3

Maleic acid monoisopropyl ester-vinyl methyl ether copolymer,
minimum average molecular weight (in amu), 49,000

31307–95–6

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Maleic anhydride-diisobutylene copolymer, sodium salt, minimum
number average molecular weight (in amu) 5,0007–18,000

37199–81–8

Maleic anhydride-methylstyrene copolymer sodium salt, minimum
number average molecular weight (in amu), 15,000

60092–15–1

Maleic anhydride-methyl vinyl ether, copolymer, average molecular None
weight (in amu), 250,000
Methacrylic acid-methyl methacrylate-polyethylene glycol methyl
ether methacrylate copolymer, minimum number averge molecular
weight (in amu), 3,700

100934–04–1

Methacrylic copolymer, minimum number average molecular
weight (in amu), 15,000

63150–03–8

Methyl methacrylate-methacrylic acid-monomethoxypolyethylene
glycol methacrylate copolymer,) minimum number average
molecular weight (in amu), 2,730

119724–54–8

Methyl methacrylate-2-sulfoethyl methacrylatedimethylaminoethylmethacrylate-glycidyl methacrylate-styrene-2ethylhexyl acrylate graft copolymer, minimum average molecular
weight (in amu), 9,600

None

Methyl vinyl ether-maleic acid copolymer), minimum number
average molecular weight (in amu), 75,000

25153–40–6

Methyl vinyl ether-maleic acid copolymer, calcium sodium salt,
minimum number average molecular weight (in amu), 900,000

62386–95–2

Monophosphate ester of the block copolymer α-hydro-ωhydroxypoly(oxyethylene) poly(oxypropylene) poly(oxyethylene);
the poly(oxypropylene) content averages 37–41 moles, average
molecular weight (in amu), 8,000

None

α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) mixture of
None
dihydrogen phosphate and monohydrogen phosphate esters and
the corresponding ammonium, calcium, magnesium,
monoethanolamine, potassium, sodium, and zinc salts of the
phosphate esters; the nonyl group is a propylene trimer isomer and
the poly(oxyethylene) content averages 30 moles
α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) sulfate, and its
None
ammonium, calcium, magnesium, monoethanolamine, potassium,
sodium, and zinc salts; the nonyl group is a propylene trimer
isomer and the poly(oxyethylene) content averages 30-90 moles of
ethylene oxide
α-( p -Nonylphenyl-ω-hydroxypoly(oxypropylene) block polymer
with poly(oxyethylene); polyoxypropylene content of 10–60 moles;
polyoxyethylene content of 10–80 moles; molecular weight (in
amu), 1,200–7,100.

None

α-( p -Nonylphenyl)poly(oxypropylene) block polymer with poly
None
(oxyethylene); poly oxyethylene content 30 to 90 moles; molecular
weight (in amu) averages 3,000
Octadecanoic acid, 12-hydroxy-, homopolymer, octadecanoate
minimum number average molecular weight (in amu), 1,370

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58128–22–6),

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α-cis-9-Octadecenyl-ω-hydroxypoly(oxyethylene); the octadecenyl
group is derived from oleyl alcohol and the poly(oxyethylene)
content averages 20 moles

None

Octadecyl acrylate-acrylic acid copolymer, octadecyl acrylatedodecyl acrylate-acrylic acid copolymer, octadecyl methacrylatebutyl acrylate-acrylic acid copolymer, octadecyl methacrylate-hexyl
acrylate-acrylic acid copolymer, octadecyl methacrylate-dodecyl
acrylate-acrylic acid copolymer, or octadecyl methacrylate-dodecyl
methacrylate-acrylic acid copolymer, minimum number average
molecular weight (in amu) 3,000

None

Oleic acid diester of α-hydro-ω-hydroxypoly(oxyethylene); the poly
(oxyethylene), average molecular weight (in amu), 2,300

None

2-oxepanone, homopolymer, minimum number average molecular
weight (in amu) 52,000

24980–41–4

Oxirane, decyl-, reaction products with polyethylene-polypropylene
glycol ether with trimethylolpropane (3:1)

903890–89–1

Oxirane, hexadecyl-, reaction products with polyethylenepolypropylene glycol ether with trimethylolpropane (3:1)

893427–80–0

Oxirane, methyl-, polymer with oxirane, ether with 2-ethyl-2(hydroxymethyl) – 1,3 - propanediol (3:1), reaction products with
tetradecyloxirane

903890–90–4

Oxirane, methyl-, polymer with oxirane, mono[2-(2-butoxyethoxy) 85637–75–8
ethyl] ether, minimum number average molecular weight (in amu),
2,500
Oxirane, methyl-, polymer with Oxirane, Monobutyl Ether

9038–95–3

Oxirane, 2-methyl-, polymer with oxirane, minimum number
average molecular weight (in amu), 1,100

9003–11–6

Oxirane, 2-methyl-, polymer with oxirane, mono [2-[2-(2butoxymethylethoxy)methylethoxy]methylethyl] ether, minimum
number average molecular weight (in amu), 3,000

926031–36–9

Polyamide polymer derived from sebacic acid, vegetable oil acids
with or without dimerization, terephthalic acid and/or
ethylenediamine

None

Polyethylene glycol-polyisobutenyl anhydride-tall oil fatty acid
copolymer, minimum number average molecular weight (in amu),
2,960

68650–28–2

Polyethylene, oxidized, minimum number average molecular weight None
(in amu), 1,200
Polymethylene polyphenylisocyanate, polymer with ethylene
diamine, diethylene triamine and sebacoyl chloride, cross-linked;
minimum number average molecular weight (in amu), 100,000

None

Polyoxyethylated primary amine (C14–C18); the fatty amine is
derived from an animal source and contains 3% water; the poly
(oxyethylene) content averages 20 moles

None

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Polyoxyethylated sorbitol fatty acid esters; the polyoxyethylated
sorbitol solution containing 15% water is reacted with fatty acids
limited to C12, C14, C16, and C18, containing minor amounts of

None

associated fatty acids; the poly(oxyethylene) content averages 30
moles.
Polyoxyethylated sorbitol fatty acid esters; the sorbitol solution
containing up to 15% water is reacted with 20–50 moles of
ethylene oxide and aliphatic alkanoic and/or alkenoic fatty acids
C8through C22with minor amounts of associated fatty acids; the

None

resulting polyoxyethylene sorbitol ester having a minimum
molecular weight (in amu), 1,300
Poly(oxyethylene/oxypropylene) monoalkyl (C6–C10) ether sodium

102900–02–7

fumarate adduct, minimum number average molecular weight (in
amu), 1,900
Polyoxymethylene copolymer, minimum number average molecular None
weight (in amu), 15,000
Poly(oxypropylene) block polymer with poly(oxyethylene),
molecular weight (in amu), 1,800–16,000

None

Poly(phenylhexylurea), cross-linked, minimum average molecular
weight (in amu), 36,000

None

Polypropylene

9003–07–0

Polystyrene, minimum number average molecular weight (in amu), 9003–53–6
50,000
Polytetrafluoroethylene

9002–84–0

Polyvinyl acetate, copolymer with maleic anhydride, partially
hydrolyzed, sodium salt, minimum number average molecular
weight (in amu), 53,000

None

Polyvinylpyrrolidone butylated polymer, minimum number average
molecular weight (in amu), 9,500

26160–96–3

Polyvinyl acetate, minimum molecular weight (in amu), 2,000

None

Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number
average molecular weight (in amu), 50,000

25213–24–5

Polyvinyl alcohol

9002–89–5

Polyvinyl chloride

None

Polyvinyl chloride, minimum number average molecular weight (in
amu), 29,000

9002–86–2

Poly(vinylpyrrolidone), minimum number average molecular weight 9003–39–8
(in amu), 4,000
Poly(vinylpyrrolidone-1-eicosene), minimum average molecular
weight (in amu), 3,000

28211–18–9

Poly(vinylpyrrolidone-1-hexadecene), minimum average molecular
weight (in amu), 4,700

63231–81–2

1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propenyl)amino]-,
monosodium salt, polymer with ethenol and ethenyl acetate,
minimum number average molecular weight (in amu) 50,000

107568–12–7

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2-Propene-1-sulfonic acid sodium salt, polymer with ethenol and
None
ethenyl acetate, number average molecular weight (in amu) 6,000–
12,000
2-Propenoic acid, butyl ester, polymer with ethyl 2-propenoate and 33438–19–6
N-(hydroxymethyl)-2-propenamide, minimum number average
molecular weight (in amu), 30,000
2-Propenoic acid, 2-hydroxyethyl ester, polymer with α-[4(ethenyloxy)butyl]-ω-hydroxypoly (oxy-1,2-ethanediyl), minimum
number average molecular weight (in amu), 17,000

1007234–89–0

2-Propenoic acid, methyl ester, polymer with ethenyl acetate,
hydrolyzed, sodium salts.

886993–11–9

2-Propenoic acid, 2-Methyl-, Polymer with Butyl 2-Propenoate,
153163–36–1
Methyl 2-Methyl-2-Propenoate, Methyl 2-Propenoate and 2Propenoic Acid, graft, Compound with 2-Amino-2-Methyl-1-Propanol
2-Propenoic Acid, 2-Methyl-, Polymer with Ethenylbenzene, 2Ethylhexyl 2-Propenoate, 2-Hydroxyethyl 2-Propenoate, N(Hydroxymethyl) -2-Methyl-2-Propenamide and Methyl 2-Methyl-2Propenoate, Ammonium Salt

146753–99–3

2-Propenoic acid, 2-methyl-, polymers with Bu acrylate, Et acrylate, 890051–63–5
Me methacrylate and polyethylene glycol methacrylate C16-18-alkyl
ethers, minimum number average molecular weight (in amu),
13,000
2-Propenoic acid, monoester with 1,2-propanediol, polymer with α- 955015–23–3
[4-(ethenyloxy) butyl]-ω-hydroxypoly (oxy-1,2-ethanediyl) and 2,5furandione, minimum number average molecular weight (in amu),
25,000
2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1,2-ethanediyl) and 2,5-furandione, sodium salt,
minimum number average molecular weight (in amu), 25,000

251479–97–7

2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1,2-ethanediyl) and 1,2-propanediol mono-2propenoate, potassium sodium salt, minimum number average
molecular weight (in amu), 16,000

518026–64–7

2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1, 2-ethanediyl), sodium salt, minimum number
average molecular weight (in amu), 24,000

250591–84–5

2-Propenoic acid, polymer with 2-propenamide, sodium salt,
minimum number average molecular weight (in amu), 18,000

25085–02–3

2-Propenoic acid, sodium salt, polymer with 2-propenamide,
minimum number average molecular weight (in amu), 18,000

25987–30–8

2-Propenoic, 2-methyl-, polymers with ethyl acrylate and
polyethylene glycol methylacrylate C18-22alkyl ethers

888969–14–0

Silane, dichloromethyl- reaction product with silica minimum
number average molecular weight (in amu), 3,340,000

68611–44–9

Silane, trimethoxy[3-(oxiranylmethoxy)propyl]-, hydrolysis products 68584–82–7
with silica, minimum number average molecular weight (in amu),
640,000
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Sodium polyflavinoidsulfonate, consisting chiefly of the copolymer
of catechin and leucocyanidin

None

Soybean oil, ethoxylated; the poly(oxyethylene) content averages
10 moles or greater

61791–23–9

Starch, oxidized, polymers with Bu acrylate, tert-Bu acrylate and
styrene, minimum number average molecular weight (in amu),
10,000

204142–80–3

Stearyl methacrylate-1,6-hexanediol dimethacrylate copolymer,
minimum molecular weight (in amu), 100,000

None

Styrene, copolymers with acrylic acid and/or methacrylic acid, with
none and/or one or more of the following monomers:
Acrylamidopropyl methyl sulfonic acid, methallyl sulfonic acid, 3sulfopropyl acrylate, 3-sulfopropyl methacrylate, hydroxypropyl
methacrylate, hydroxypropyl acrylate, hydroxyethyl methacrylate,
and/or hydroxyethyl acrylate; and its sodium, potassium,
ammonium, monoethanolamine, and triethanolamine salts; the
resulting polymer having a minimum number average molecular
weight (in amu), 1,200

None

Styrene, 2-ethylhexyl acrylate, butyl acrylate copolymer, minimum
number average molecular weight (in amu), 4,200

30795–23–4

Styrene-2-ethylhexyl acrylate-glycidyl methacrylate-2-acrylamido-2- None
methylpropanesulfonic acid graft copolymer, minimum number
average molecular weight (in amu), 12,500
Styrene-maleic anhydride copolymer

None

Styrene-maleic anhydride copolymer, ester derivative

None

Tetradecyl acrylate-acrylic acid copolymer, minimum number
average molecular weight (in amu), 3,000

None

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum
number average molecular weight (in amu), 6,500

104133–09–7

α-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-ω-hydroxypoly
(oxyethylene) produced by the condensation of 1 mole of p(1,1,3,3-tetramethylbutyl)phenol with a range of 30-70 moles of
ethylene oxide

9036–19–5
9002–93–1

α-[ p -(1,1,3,3-Tetramethylbutyl)phenyl] poly(oxypropylene)
block polymer with poly(oxyethylene); the poly(oxypropylene)
content averages 25 moles, the poly(oxyethylene) content
averages 40 moles, the molecular weight (in amu) averages 3,400

None

α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene)
poly(oxypropylene) copolymer, the poly(oxypropylene) content
averages 2–8 moles, the poly(oxyethylene) content averages 16–
30moles, average molecular weight (in amu), 1,500

None

Urea-formaldehyde copolymer, minimum average molecular weight 9011–05–6
(in amu), 30,000
Vinyl acetate-allyl acetate-monomethyl maleate copolymer,
minimum average molecular weight (in amu), 20,000

None

Vinyl acetate-ethylene copolymer, minimum number average
molecular weight (in amu), 69,000

24937–78–8

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Vinyl acetate polymer with none and/or one or more of the
None
following monomers: Ethylene, propylene, N-methyl acrylamide,
acrylamide, monoethyl maleate, diethyl maleate, monooctyl
maleate, dioctyl maleate, maleic anhydride, maleic acid, octyl
acrylate, butyl acrylate, ethyl acrylate, methyl acrylate, acrylic acid,
octyl methacrylate, butyl methacrylate, ethyl methacrylate, methyl
methacrylate, methacrylic acid, carboxyethyl acrylate, and diallyl
phthalate; and their corresponding sodium, potassium, ammonium,
isopropylamine, triethylamine, monoethanolamine and/or
triethanolamine salts; the resulting polymer having a minimum
number average molecular weight (in amu), 1,200
Vinyl acetate-vinyl alcohol-alkyl lactone copolymer, minimum
number average molecular weight (in amu), 40,000; minimum
viscosity of 18 centipoise

None

Vinyl alcohol-disodium itaconate copolymer, minimum average
molecular weight (in amu), 50,290

None

Vinyl alcohol-vinyl acetate copolymer, benzaldehyde-o-sodium
sulfonate condensate, minimum number average molecular weight
(in amu), 20,000

None

Vinyl alcohol-vinyl acetate-monomethyl maleate, sodium saltmaleic acid, disodium salt-γ-butyrolactone acetic acid, sodium salt
copolymer, minimum number average molecular weight (in amu),
20,000

None

Vinyl chloride-vinyl acetate copolymers

None

Vinyl pyrrolidone-acrylic acid copolymer, minimum number average 28062–44–4
molecular weight (in amu), 6,000
Vinyl pyrrolidone-dimethylaminoethylmethacrylate copolymer,
minimum number average molecular weight (in amu), 20,000

30581–59–0

Vinyl pyrrolidone-styrene copolymer

25086–29–7

[67 FR 36528, May 24, 2002]
Editorial Note: ForFederal Registercitations affecting §180.960, see the List of CFR Sections Affected,
which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 180.1011 Viable spores of the microorganism Bacillus
thuringiensis
Berliner; exemption from the
requirement of a tolerance.
top
(a) For the purposes of this section the microbial insecticide for which exemption from the requirement of a
tolerance is being established shall have the following specifications:
(1) The microorganism shall be an authentic strain of Bacillus thuringiensis Berliner conforming to the
morphological and biochemical characteristics of Bacillus thuringiensis as described in Bergey's Manual of
Determinative Bacteriology, Eighth Edition.
(2) Spore preparations of Bacillus thuringiensis Berliner shall be produced by pure culture fermentation
procedures with adequate control measures during production to detect any changes from the

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characteristics of the parent strain or contamination by other microorganisms.
(3) Each lot of spore preparation, prior to the addition of other materials, shall be tested by subcutaneous
injection of at least 1 million spores into each of five laboratory test mice weighing 17 grams to 23 grams.
Such test shall show no evidence of infection or injury in the test animals when observed for 7 days
following injection.
(4) Spore preparations shall be free of the Bacillus thuringiensis β-exotoxin when tested with the fly larvae
toxicity test (“Microbial Control of Insects and Mites,” R.P.M. Bond et al., p. 280 ff., 1971). This
specification can be satisfied either by determining that each master seed lot brought into production is a
Bacillus thuringiensis strain which does not produce β-exotoxin under standard manufacturing conditions
or by periodically determining that β-exotoxin synthesized during spore production is eliminated by the
subsequent spore-harvesting procedure.
(b) Exemption from the requirement of a tolerance is established for residues of the microbial insecticide
Bacillus thuringiensis Berliner, as specified in paragraph (a) of this section, in or on honey and honeycomb
and all other raw agricultural commodities when it is applied either to growing crops, or when it is applied
after harvest in accordance with good agricultural practices.
[36 FR 22540, Nov. 25, 1971, as amended at 38 FR 19045, July 17, 1973; 42 FR 28540, June 3, 1977; 45
FR 43721, June 30, 1980; 45 FR 56347, Aug. 25, 1980; 74 FR 26533, June 3, 2009]

§ 180.1016 Ethylene; exemption from the requirement of a tolerance.
top
Ethylene is exempted from the requirement of a tolerance for residues when:
(a) For all food commodities, it is used as a plant regulator on plants, seeds, or cuttings and on all food
commodities after harvest and when applied in accordance with good agricultural practices.
(b) Injected into the soil to cause premature germination of witchweed in bean (lima and string), cabbage,
cantaloupe, collard, corn, cotton, cucumber, eggplant, okra, onion, pasture grass, pea (field and sweet),
peanut, pepper, potato, sweet potato, sorghum, soybean, squash, tomato, turnip, and watermelon fields
as part of the U.S. Department of Agriculture witchweed control program.
[39 FR 33315, Sept. 17, 1974, as amended at 40 FR 19477, May 5, 1975; 64 FR 31505, June 11, 1999]

§ 180.1017 Diatomaceous earth; exemption from the requirement of a tolerance.
top
(a) Diatomaceous earth is exempted from the requirement of a tolerance for residues when used in
accordance with good agricultural practice in pesticide formulations applied to growing crops, to food
commodities after harvest, and to animals.
(b) Diatomaceous earth may be safely used in accordance with the following conditions. Application shall
be limited solely to spot and/or crack and crevice treatments in food or feed processing and food or feed
storage areas in accordane with the precribed conditions:
(1) It is used or intended for use for control of insects in food or feed processing and food or feed storage
areas: Provided, That the food or feed is removed or covered prior to such use.
(2) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

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[65 FR 33716, May 24, 2000]

§ 180.1019 Sulfuric acid; exemption from the requirement of a tolerance.
top
(a) Residues of sulfuric acid are exempted from the requirement of a tolerance when used in accordance
with good agricultural practice when used as a herbicide in the production of garlic and onions, and as a
potato vine dessicant in the production of potatoes.
(b) Residues of sulfuric acid are exempted from the requirement of a tolerance in cattle, meat; goat, meat;
hog, meat; horse, meat; sheep, meat; poultry, fat; poultry, meat; poultry, meat, byproducts; egg; milk; fish,
shellfish, and irrigated crops when it results from the use of sulfuric acid as an inert ingredient in a
pesticide product used in irrigation conveyance systems and lakes, ponds, reservoirs, or bodies of water in
which fish or shellfish are cultivated. The sulfuric acid is not to exceed 10% of the pesticide formulation
(non-aerosol formulations only).
[69 FR 40787, July 7, 2004, as amended by 74 FR 26533, June 3, 2009]

§ 180.1020 Sodium chlorate; exemption from the requirement of a tolerance.
top
(a) Sodium chlorate is exempted from the requirement of a tolerance for residues in or on the following
raw agricultural commodities when used as a defoliant, desiccant, or fungicide in accordance with good
agricultural practice.

Commodity
Bean, dry, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Cotton, undelinted seed
Cowpea, forage
Cowpea, hay
Cowpea, seed
Flax, seed
Flax, straw
Grain, aspirated fractions
Guar, seed
Pepper, chili
Potato
Rice, grain
Rice, straw
Safflower, seed
Sorghum, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Sunflower, seed
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(b) A time-limited exemption from the requirement of a tolerance is established for residues of the defoliant/
desiccant in connection with use of the pesticide under section 18 emergency exemptions granted by
EPA. The exemption will expire and is revoked on the date specified in the following table:

Commodity

Parts per million

Expiration/revocation date

Wheat, forage

NA

12/31/06

Wheat, grain

NA

12/31/06

Wheat, hay

NA

12/31/06

Wheat, straw

NA

12/31/06

[54 FR 9800, Mar. 8, 1989, as amended at 60 FR 4862, Jan. 25, 1995; 62 FR 63863, Dec. 3, 1997; 63 FR
35846, July 1, 1998; 64 FR 42849, Aug. 6, 1999; 65 FR 48639, Aug. 9, 2000; 68 FR 2247, Jan. 16, 2003;
69 FR 71717, Dec. 10, 2004; 74 FR 26533, June 3, 2009]

§ 180.1021 Copper; exemption from the requirement of a tolerance.
top
(a) Copper is exempted from the requirement of a tolerance in cattle, meat; goat, meat; hog, meat; horse,
meat; sheep, meat; milk, poultry, fat; poultry, meat; poultry, meat byproducts; egg, fish, shellfish, and
irrigated crops when it results from the use of:
(1) Copper sulfate as an algicide or herbicide in irrigation conveyance systems and lakes, ponds,
reservoirs, or bodies of water in which fish or shellfish are cultivated.
(2) Basic copper carbonate (malachite) as an algicide or herbicide in impounded and stagnant bodies of
water
(3) Copper triethanolamine and copper monoethanolamine as an algicide or herbicide in fish hatcheries,
lakes, ponds, and reservoirs
(4) Cuprous oxide bearing antifouling coatings for control of algae or other coatings for control of algae or
other organisms on submerged concrete or other (irrigation) structures.
(b) The following copper compounds are exempt from the requirement of a tolerance when applied
(primarily) as a fungicide to growing crops using good agricultural practices: Bordeaux mixture, basic
copper carbonate (malachite) (CAS Reg. No. 1184–64–1), copper ethylenediamine complex, copper
hydroxide (CAS Reg. No. 20427–59–2), copper lime mixtures, copper linoleate (CAS Reg. No. 7721–15–
5), copper octanoate (CAS Reg. No. 20543–04–8), copper oleate (CAS Reg. No. 10402–16–1), copper
oxychloride (CAS Reg. No. 1332–40–7), copper sulfate basic (CAS Reg. No. 1344–73–6), cupric oxide
(CAS Reg. No. 1317–38–0), and cuprous oxide (CAS Reg. No. 1317–19–1).
(c) Copper sulfate pentahydrate (CAS Reg. No. 7758–99–8) is exempt from the requirement of a tolerance
when applied as a fungicide to growing crops or to raw agricultural commodities after harvest, and as a
bactericide/fungicide in or on meat, fat and meat by-products of cattle, sheep, hogs, goats, horses and
poultry, milk and eggs when applied as a bactericide/fungicide to animal premises and bedding.
(d) Copper (II) hydroxide (CAS Reg. No. 20427–59–2) is exempt from the requirement of a tolerance when
applied to growing crops or to raw agricultural commodities as an inert ingredient (for pH control) in
pesticide products.
[65 FR 68912, Nov. 15, 2000, as amended at 69 FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, 2006; 74
FR 26534, June 3, 2009]
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§ 180.1022 Iodine-detergent complex; exemption from the requirement of a
tolerance.
top
The aqueous solution of hydriodic acid and elemental iodine, including one or both of the surfactants (a)
polyoxypropylene-polyoxyethylene glycol nomionic block polymers (minimum average molecular weight
1,900) and (b) α-(p- nonylphenyl)- omega - hydroxypoly (oxyethylene) having a maximum average
molecular weight of 748 and in which the nonyl group is a propylene trimer isomer, is exempted from the
requirement of a tolerance for residues in egg, and poultry, fat; poultry, meat; poultry, meat byproducts
when used as a sanitizer in poultry drinking water.
[74 FR 26534, June 3, 2009]

§ 180.1023 Propanoic acid; exemptions from the requirement of a tolerance.
top
(a) Postharvest application of propanoic acid or a mixture of methylene bispropionate and oxy
(bismethylene) bisproprionate when used as a fungicide is exempted from the requirement of a tolerance
for residues in or on the following raw agricultural commodities: Alfalfa, forage; alfalfa, hay; alfalfa, seed;
barley, grain; Bermudagrass, forage; Bermudagrass, hay; bluegrass, forage; bluegrass, hay; bromegrass,
forage; bromegrass, hay; clover, forage; clover, hay; corn, field, grain; corn, pop, grain; cowpea, hay;
fescue, forage; fescue, hay; lespedeza, forage; lespedeza, hay; lupin; oat, grain; orchardgrass, forage;
orchardgrass, hay; peanut, hay; pea, field, hay; ryegrass, Italian, hay; sorghum, grain, grain; soybean,
hay; sudangrass, forage; sudangrass, hay; timothy, forage; timothy, hay; vetch, forage; vetch, hay; and
wheat, grain.
(b) Propanoic acid is exempt from the requirement of a tolerance for residues in or on cattle, meat; cattle,
meat byproducts; goat, meat; goat, meat byproducts; hog, meat; hog meat byproducts; horse, meat;
horse, meat byproducts; sheep, meat; sheep meat byproducts; and, poultry, fat; poultry meat; poultry meat
byproducts; milk, and egg when applied as a bactericide/fungicide to livestock drinking water, poultry litter,
and storage areas for silage and grain.
(c) Preharvest and postharvest application of propanoic acid (CAS Reg. No. 79–09–4), propanioc acid,
calcium salt (CAS Reg. No. 4075–81–4), and propanioc sodium salt (CAS Reg. No. 137–40–6) are
exempted from the requirement of a tolerance on all crops when used as either an active or inert
ingredient in accordance with good agricultural practice in pesticide formulations applied to growing crops,
to raw agricultural commodities before and after harvest and to animals.
[69 FR 47025, Aug. 4, 2004, as amended at 74 FR 26534, June 3, 2009]

§ 180.1025 Xylene; exemption from the requirement of a tolerance.
top
Xylene is exempted from the requirement of a tolerance when used as an aquatic herbicide applied to
irrigation conveyance systems in accordance with the following conditions:
(a) It is to be used only in programs of the Bureau of Reclamation, U.S. Department of Interior, and
cooperating water user organizations.
(b) It is to be applied as an emulsion at an initial concentration not to exceed 750 parts per million.

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(c) It is not to be applied when there is any likelihood that the irrigation water will be used as a source of
raw water for a potable water system or where return flows of such treated irrigation water into receiving
rivers and streams would contain residues of xylene in excess of 10 parts per million.
(d) Xylene to be used as an aquatic herbicide shall meet the requirement limiting the presence of a
polynuclear aromatic hydrocarbons as listed in 21 CFR 172.250.
[38 FR 16352, June 22, 1973, as amended at 50 FR 2980, Jan. 3, 1985]

§ 180.1027 Nuclear polyhedrosis virus of Heliothis zea; exemption from the
requirement of a tolerance.
top
(a) For the purposes of this section, the viral insecticide must be produced with an unaltered and
unadulterated inoculum of the single-embedded Heliothis zea nuclear polyhedrosis virus (HzSNPV). The
identity of the seed virus must be assured by periodic checks.
(b) Each lot of active ingredient of the viral insecticide shall have the following specifications:
(1) The level of extraneous bacterial contamination of the final unformulated viral insecticide should not
exceed 107 colonies per gram as determined by an aerobic plate on trypticase soy agar.
(2) Human pathogens, e.g., Salmonella, Shigella, or Vibrio, must be absent.
(3) Safety to mice as determined by an intraperitoneal injection study must be demonstrated.
(4) Identity of the viral product, as determined by the most sensitive and standardized analytical technique,
e.g., restriction endonuclease and/or SDS-PAGE analysis, must be demonstrated.
(c) Exemptions from the requirement of a tolerance are established for the residues of the microbial
insecticide Heliothis zea NPV, as specified in paragraphs (a) and (b) of this section, in or on all agricultural
commodities.
[60 FR 42460, Aug. 16, 1995, as amended at 74 FR 26534, June 3, 2009]

§ 180.1033 Methoprene; exemption from the requirement of a tolerance.
top
Methoprene is exempt from the requirement of a tolerance in or on all food commodities when used to
control insect larvae.
[68 FR 34829, June 11, 2003]

§ 180.1035 Pine oil; exemption from the requirement of a tolerance.
top
Pine oil is exempted from the requirement of a tolerance for residues in the raw agricultural commodities
honey and honeycomb, when present therein as a result of its use as a deodorant at no more than 12
percent in formulation with the bee repellent butanoic anhydride applied in an absorbent pad over the hive.

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Pine oil is exempted from the requirement of a tolerance for residues in the raw agricultural commodities
honey and honeycomb, when present therein as a result of its use as a deodorant at no more than 12
percent in formulation with the bee repellent butanoic anhydride applied in an absorbent pad over the hive.
[74 FR 26534, June 3, 2009]

§ 180.1037 Polybutenes; exemption from the requirement of a tolerance.
top
(a) Polybutenes are exempt from the requirement of a tolerance for residues in or on the raw agricultural
commodity cotton, undelinted seed when used as a sticker agent for formulations of the attractant
gossyplure (1:1 mixture of ( Z,Z )- and ( Z,E )-7,11-hexadecadien-1-ol acetate) to disrupt the mating of the
pink bollworm.
(b) Polybutenes are exempt from the requirement of a tolerance for residues in or on the raw agricultural
commodity artichoke when used as a sticker agent in multi-layered laminted controlled-release dispensers
of (Z)-11-hexaadecenal to disrupt the mating of the artichoke plume moth.
[74 FR 26534, June 3, 2009]

§ 180.1040 Ethylene glycol; exemption from the requirement of a tolerance.
top
Ethylene glycol as a component of pesticide formulations is exempt from the requirement of a tolerance
when used in foliar applications to peanut plants.
[43 FR 41393, Sept. 18, 1978]

§ 180.1041 Nosema locustae; exemption from the requirement of a tolerance.
top
The insecticide Nosema locustae is exempted from the requirement of a tolerance for residues in or on all
raw agricultural commodities.
[47 FR 21537, May 19, 1982]

§ 180.1043 Gossyplure; exemption from the requirement of a tolerance.
top
The pheromone gossyplure, a 1:1 mixture of ( Z,Z )- and ( Z,E )-7,11-hexadecadien-1-ol acetate) is
exempt from the requirement of a tolerance in or on the raw agricultural commodity cotton, undelinted
seed when applied to cotton from capillary fibers.
[74 FR 26534, June 3, 2009]

§ 180.1049 Carbon dioxide; exemption from the requirement of a tolerance.
top

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The insecticide carbon dioxide is exempted from the requirement of a tolerance when used after harvest in
modified atmospheres for stored insect control on food commodities.
[65 FR 33716, May 24, 2000]

§ 180.1050 Nitrogen; exemption from the requirements of a tolerance.
top
The insecticide nitrogen is exempted from the requirements of a tolerance when used after harvest in
modified atmospheres for stored product insect control on all food commodities.
[65 FR 33716, May 24, 2000]

§ 180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine; exemption from the
requirement of a tolerance.
top
2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine is exempted from the requirement of a tolerance when
used as an inert ingredient in formulations of the herbicides S -ethyl dipropylthiocarbamate, S -propyl
dipropylthiocarbamate, and S -ethyl diisobutylthiocarbamate applied to corn fields before the corn plants
emerge from the soil with a maximum of 0.5 pound of the inert ingredient per acre.
[45 FR 51201, Aug. 1, 1980]

§ 180.1054 Calcium hypochlorite; exemptions from the requirement of a tolerance.
top
(a) Calcium hypochlorite is exempted from the requirement of a tolerance when used preharvest or
postharvest in solution on all raw agricultural commodities.
(b) Calcium hypochlorite is exempted from the requirement of a tolerance in or on grape when used as a
fumigant postharvest by means of a chlorine generator pad.
[59 FR 59165, Nov. 16, 1994, as amended at 74 FR 26534, June 3, 2009]

§ 180.1056 Boiled linseed oil; exemption from requirement of tolerance.
top
Boiled linseed oil (containing no more than 0.33 percent manganese naphthenate and no more than 0.33
percent cobalt naphthenate) is exempt from the requirement of a tolerance when used as a coating agent
for S -ethyl hexahydro-1 H -azepine-1-carbothioate. No more than 15 percent of the pesticide formulation
may consist of “boiled linseed oil.” This exemption is limited to use on rice before edible parts form.
[46 FR 33270, June 29, 1981]

§ 180.1057 Phytophthora palmivora; exemption from requirement of tolerance.
top

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Phytophthora palmivora is exempted from the requirement of a tolerance in or on the raw agricultural
commodity fruit, citrus.
[74 FR 26534, June 3, 2009]

§ 180.1058 Sodium diacetate; exemption from the requirement of a tolerance.
top
Sodium diacetate, when used postharvest as a fungicide, is exempt from the requirement of a tolerance
for residues in or on alfalfa, hay; Bermudagrass, hay; bluegrass, hay; bromegrass, hay; clover,hay; corm,
field, grain; corn, pop, grain; oat, grain; orchardgrass, hay; sorghum, grain, grain; sudangrass, hay;
ryegrass, Italian, hay; timothy, hay.
[74 FR 26534, June 3, 2009]

§ 180.1064 Tomato pinworm insect pheromone; exemption from the requirement of
a tolerance.
top
An exemption from the requirement of a tolerance is established for combined residues of both
components of the tomato pinworm insect pheromone ( E )-4-tridecen-1-yl acetate and ( Z )-4-tridecen-1-yl
acetate in or on all raw agricultural commodities (preharvest) in accordance with the following prescribed
conditions:
(a) Application shall be limited solely to point source dispensers or point source chopped fibers containing
the tomato pinworm insect pheromone.
(b) Cumulative yearly application cannot exceed 200 grams of tomato pinworm pheromone per acre.
[58 FR 34376, June 25, 1993]

§ 180.1065 2-Amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5one; exemption from the requirement of a tolerance.
top
The inert ingredient, 2-amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one is
exempted from the requirement of a tolerance when used as an emetic at not more than 0.3 percent in
formulations of paraquat dichloride. Further restrictions on this exemption are that this ingredient may not
be advertised as an emetic and the paraquat product may not be promoted in any way because of the
inclusion of this inert ingredient.
[70 FR 46431, Aug. 10, 2005]

§ 180.1067 Methyl eugenol and malathion combination; exemption from the
requirement of a tolerance.
top
The insect attractant methyl eugenol and the insecticide malathion are exempt from the requirement of
tolerances on all raw agricultural commodities when used in combination in Oriental fruit fly eradication
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programs under the authority of the U.S. Department of Agriculture, in accordance with the following
directions and specifications:
(a) The combination shall be at the ratio of three parts methyl eugenol to one part technical malathion (3:1).
(b) This combination is to be impregnated on a carrier (cigarette filter tips (cellulose acetate); cotton
strings; fiberboard squares) or mixed with a jel cleared under 40 CFR 180.920 or 180.950.
(c) The maximum actual dosage per application per acre shall be 28.35 grams (one ounce avoirdupois)
methyl eugenol and 9.45 grams (one-third (0.33) ounce avoirdupois) technical malathion.
[47 FR 9002, Mar. 3, 1982, as amended at 69 FR 23142, Apr. 28, 2004]

§ 180.1068 C12-C18 fatty acid potassium salts; exemption from the requirement of a
tolerance.
top
C12-C18fatty acids (saturated and unsaturated) potassium salts are exempted from the requirement of a
tolerance for residues in or on all raw agricultural commodities when used in accordance with good
agricultural practice.
[60 FR 34871, July 5, 1995]

§ 180.1069 ( Z
tolerance.

)-11-Hexadecenal; exemption from the requirement of a

top
An exemption from the requirement of a tolerance is established for residues of the biological insecticide
(pheromone) ( Z )-11-hexadecenal when used as a sex attractant on artichoke plants to control the
artichoke plume moth.
[47 FR 14906, Apr. 7, 1982]

§ 180.1070 Sodium chlorite; exemption from the requirement of a tolerance.
top
Sodium chlorite is exempted from the requirement of a tolerance for residues when used in accordance
with good agricultural practice as a seed-soak treatment in the growing of the raw agricultural commodities
vegetable, brassica, leafy, group 5 and radish, roots and radish, tops.
[74 FR 26534, June 3, 2009]

§ 180.1071 Peanuts, Tree Nuts, Milk, Soybeans, Eggs, Fish, Crustacea, and Wheat;
exemption from the requirement of a tolerance.
top
(a) General . Residues resulting from the following uses of the food commodity forms of peanuts, tree
nuts, milk, soybeans, eggs (including putrescent eggs), fish, crustacea, and wheat are exempted from the

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requirement of a tolerance in or on all food commodities under FFDCA section 408 (when used as either
an inert or an active ingredient in a pesticide formulation), if such use is in accordance with good
agricultural practices:
(1) Use in pesticide products intended to treat seeds.
(2) Use in nursery and greenhouse operations, as defined in 40 CFR 170.3, which includes seeding,
potting and transplanting activities.
(3) Pre-plant and at-transplant applications.
(4) Incorporation into seedling and planting beds.
(5) Applications to cuttings and bare roots.
(6) Applications to the field that occur after the harvested crop has been removed.
(7) Soil-directed applications around and adjacent to all plants.
(8) Applications to rangelands, which is land, mostly grasslands, whose plants can provide food ( i.e. ,
forage) for grazing or browsing animals.
(9) Use in chemigation and irrigation systems (via flood, drip, or furrow application with no overhead spray
applications).
(10) Application as part of a dry fertilizer on which an active ingredient is impregnated.
(11) Aerial and ground applications that occur when no above-ground harvestable food commodities are
present (usually pre-bloom).
(12) Application as part of an animal feed-through product.
(13) Applications as gel and solid (non-liquid/non-spray) crack and crevice treatments that place the gel or
bait directly into or on top of the cracks and crevices via a mechanism such as a syringe.
(14) Applications to the same crop from which the food commodity is derived, whether the plant fraction(s)
intended for harvest are present or not, e.g., applications of peanut meal when applied to peanut plants.
(b) Specific chemical substances . Residues resulting from the use of the following substances as either
an inert or an active ingredient in a pesticide formulation are exempted from the requirement of a tolerance
under FFDCA section 408, if such use is in accordance with good agricultural practices and such use is
included in paragraph (a):

Chemical Substance

CAS No.

Caseins

9000–71–9

Caseins, ammonium complexes

9005–42–9

Caseins, hydrolyzates

65072–00–6

Caseins, potassium complexes

68131–54–4

Caseins, sodium complexes
[70 FR 1360, Jan. 7, 2005]

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9005–46–3

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§ 180.1072 Poly- D
a tolerance.

-glucosamine (chitosan); exemption from the requirement of

top
(a) An exemption from the requirement of a tolerance is established for residues of the biological plant
growth regulator poly- D -glucosamine when used as a seed treatment in or on barley, beans, oats, peas,
rice, and wheat.
(b) An exemption from the requirement of a tolerance is established for residues of the biological plant
growth regulator poly-D-glucosamine when used as a pesticide in the production any raw agricultural
commodity.
[60 FR 19524, Apr. 19, 1995]

§ 180.1073 Isomate-M; exemption from the requirement of a tolerance.
top
The oriental fruit moth pheromone (Isomate-M) (Z-8-dodecen-l-yl acetate, E-8-dodecen-l-yl acetate, Z-8dodecen-l-ol) is exempt from the requirement of a tolerance in or on all the raw agricultural commodities
(food and feed) including, peach; quince; nectarine; and nut, macadamia when used in orchards with
encapsulated polyethylene tubing to control oriental fruit moth.
[74 FR 26534, June 3, 2009]

§ 180.1074 F.D.&C. Blue No. 1; exemption from the requirement of a tolerance.
top
F.D.&C. Blue No. 1 is exempted from the requirement of a tolerance when used as an aquatic plant
control agent.
[47 FR 25963, June 16, 1982]

§ 180.1075 Colletotrichum
gloeosporioides
aeschynomene;
tolerance.

f. sp.
exemption from the requirement of a

top
An exemption from the requirement of a tolerance is established for residues of the mycoherbicide
Colletotrichum gloeosporioides f. sp. aeschynomene in or on the following raw agricultural commodities:

Commodity
Aspirated grain fractions
Rice, grain
Soybean, forage

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Soybean, hay
Soybean, seed
[47 FR 25742, June 15, 1982, as amended at 74 FR 26534, June 3, 2009]

§ 180.1076 Viable spores of the microorganism Bacillus
popilliae;
exemption from the requirement of a tolerance.
top
(a) For the purposes of this section the microbial insecticide for which exemption from the requirement of a
tolerance is being established shall have the following specifications:
(1) The microorganism shall be an authentic strain of Bacillus popilliae conforming to the morphological
and biochemical characteristics of Bacillus popilliae as described in Bergey's Manual of Determinative
Bacteriology, Eighth Edition.
(2) Spore preparations of Bacillus popilliae shall be produced by an extraction process from diseased
Japanese beetles, and may contain a small percentage of the naturally occurring milky disease bacterium
Bacillus lentimorbus.
(3) Each lot of spore preparation, prior to the addition of other materials, shall be tested by subcutaneous
injection of at least 1 million spores into each of five laboratory test mice weighing 17 grams to 23 grams.
Such test shall show no evidence of infection of injury in the test animals when observed for 7 days
following injection.
(b) Exemption from the requirement of a tolerance is established for residues of the microbial insecticide
Bacillus popilliae , as specified in paragraph (a) of this section in or on grass, pasture, forage and grass,
rangeland, forage when it is applied to growing crops in accordance with good agricultural practices.
[47 FR 38535, Sept. 1, 1982, as amended at 74 FR 26535, June 3, 2009]

§ 180.1080 Plant volatiles and pheromone; exemptions from the requirement of a
tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the plant volatiles cyclic
decadiene, cyclic decene, cyclic pentadecatriene, and decatriene and the pheromone Z-2-isopropenyl-1methylcyclobutaneethanol; Z-3,3-dimethyl-Δ1,β-cyclohexaneethanol; Z-3,3-dimethyl-Δ1,αcyclohexaneethanal; E-3,3-dimethyl-Δ1,α-cyclohexaneethanal combination when applied to cotton in
hollow synthetic fibers.
[48 FR 28442, June 22, 1983]

§ 180.1083 Dimethyl sulfoxide; exemption from the requirement of a tolerance.
top
Dimethyl sulfoxide (DMSO) [CAS Registry Number 67–68–5] is exempted from the requirement of a
tolerance when used as an inert solvent or cosolvent in formulations with the following pesticides when
used in accordance with good agricultural practices in or on the following raw agricultural commodities:

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(a) Carbaryl (1-naphthyl methyl-carbamate)

Pea, dry, seed
Pea, succulent
(b) O - O -Diethyl O -(2-isopropyl-6-methyl-4-pyrimidinyl) phosphorothioate

Pea, dry, seed
Pea, succulent
[48 FR 54819, Dec. 7, 1983, as amended at 74 FR 26535, June 3, 2009]

§ 180.1084 Monocarbamide dihydrogen sulfate; exemption from the requirement of a
tolerance.
top
Monocarbamide dihydrogen sulfate is exempted from the requirement of a tolerance when used as a
herbicide or desiccant in or on all raw agricultural commodities.
[53 FR 12152, Apr. 13, 1988]

§ 180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11-trimethyl-2,6,10dodecatriene-3-ol; exemption from the requirement of a tolerance.
top
The insect pheromone containing the active ingredients 3,7,11-trimethyl-1,6,10-dodecatriene-1-ol and
3,7,11-trimethyl-2,6,10-dodecatriene-3-ol is exempted from the requirement of a tolerance in or on all raw
agricultural commodities.
[52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. 5, 1987]

§ 180.1087 Sesame stalks; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the biorational nematicide
sesame stalk in or on the following raw agricultural commodities: Almond; almond, hulls; cotton, undelinted
seed; cotton, gin byproducts; soybean, seed; soybean, forage; soybean, hay; aspirated grain fractions;
potato; beet, sugar, roots; beet, sugar, tops; tomato; pepper, bell; squash; strawberry; eggplant;
cucumber; carrot, roots; radish, roots; radish, top; turnip, roots; turnip, tops; onion; pea, dry; pea,
succulent; melon; grape; walnut; orange; grapefruit; mulberry; peach; apple; apricot; blackberry;
loganberry; pecan; cherry; plum, and cranberry.
[74 FR 26535, June 3, 2009]

§ 180.1089 Poly- N
-acetyl- D
requirement of tolerance.

-glucosamine; exemption from the

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An exemption from the requirement of a tolerance is established for residues of the biochemical
nematicide poly- N -acetyl- D -glucosamine on a variety of agricultural crops.
[53 FR 10249, Mar. 30, 1988]

§ 180.1090 Lactic acid; exemption from the requirement of a tolerance.
top
Lactic acid (2-hydroxypropanoic acid) is exempted from the requirement of a tolerance when used as a
plant growth regulator in or on all raw agricultural commodities.
[53 FR 15286, May 4, 1988]

§ 180.1091 Aluminum isopropoxide and aluminum secondary butoxide; exemption
from the requirement of a tolerance.
top
Aluminum isopropoxide (CAS Reg. No. 555–31–7) and aluminum secondary butoxide (CAS Reg. No.
2269–22–9) are exempted from the requirement of a tolerance when used in accordance with good
agricultural practices as stabilizers in formulations of the insecticide amitraz [ N ′-(2,4-dimethylphenyl)- N [[(2,4-dimethylphenyl)imino]- N -methylmethanimidamide] applied to growing crops or animals.
[53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. 21, 1988]

§ 180.1092 Menthol; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the pesticidal chemical
menthol in or on honey and honeycomb when used in accordance with good agricultural practice in overwintering bee hives.
[74 FR 26535, June 3, 2009]

§ 180.1095 Chlorine gas; exemptions from the requirement of a tolerance.
top
Chlorine gas is exempted from the requirement of a tolerance when used preharvest or postharvest in
solution on all raw agricultural commodities.
[56 FR 21309, May 8, 1991]

§ 180.1097 GBM-ROPE; exemption from the requirement of a tolerance.
top
The grape berry moth pheromone (GBM-ROPE) containing the active ingredients (Z)-9-dedecenyl acetate
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and (Z)-11-tetradecenyl acetate is exempt from the requirement of a tolerance in or on the raw agricultural
commodity grape when used in orchards with encapsulated polyethylene tubing to control grape berry
moth.
[74 FR 26535, June 3, 2009]

§ 180.1098 Gibberellins [Gibberellic Acids (GA3 and GA4 + GA7), and Sodium or
Potassium Gibberellate]; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of gibberellins [gibberellic
acids (GA3 and GA4 + GA7), and sodium or potassium gibberellate] in or on all food commodities when
used as plant regulators on plants, seeds, or cuttings and on all food commodities after harvest in
accordance with good agricultural practices.
[64 FR 31505, June 11, 1999]

§ 180.1100 Gliocladium virens
21; exemption from the requirement of a tolerance.

isolate GL-

top
An exemption from the requirement of a tolerance is established for residues of the biofungicide
Gliocladium virens GL-21 in or on all raw agricultural commodities when used either as a fungicide for
inoculation of plant growth media in greenhouses or on terrestrial food crops grown outdoors in
accordance with good agricultural practices.
[60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. 5, 1995]

§ 180.1101 Parasitic (parasitoid) and predatory insects; exemption from the
requirement of a tolerance.
top
Parasitic (parasitoid) and predatory insects are exempted from the requirement of a tolerance for residues
when they are used in accordance with good agricultural and pest control practices to control insect pests
of stored raw whole grains such as corn, small grains, rice, soybeans, peanuts, and other legumes either
bulk or warehoused in bags. For the purposes of this rule, the parasites (parasitoids) and predators are
considered to be species of Hymenoptera in the genera Trichogramma, Trichogrammatidae; Bracon,
Braconidae; Venturia, Mesostenus, Ichneumonidae; Anisopteromalus, Choetospila, Lariophagus,
Dibrachys, Habrocytus, Pteromalus, Pteromalidae; Cephalonomia, Holepyris, Laelius, Bethylidae; and of
Hemiptera in the genera Xylocoris, Lyctocoris, and Dufouriellus, Anthocoridae. Whole insects, fragments,
parts, and other residues of these parasites and predators remain subject to 21 U.S.C. 342(a)(3).
[57 FR 14646, Apr. 22, 1992]

§ 180.1102 Trichoderma harzianum
KRL-AG2 (ATCC #20847) strain T–22; exemption from requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the biofungicide
Trichoderma harzianum KRL-AG2 (ATCC #20847); also known as strain T-22 when applied in/or on all
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food commodities.
[64 FR 16860, Apr. 7, 1999]

§ 180.1103 Isomate-C; exemption from the requirement of a tolerance.
top
The codling moth pheromone (Isomate-C) E,E-8,10-dodecenyl alcohol, dodecanol, tetradecanol is exempt
from the requirements of a tolerance in or on all raw agricultural commodities when formulated in
polyethylene pheromone dispensers for use in orchards with encapsulated polyethylene tubing to control
codling moth.
[74 FR 26535, June 3, 2009]

§ 180.1107 Delta endotoxin of Bacillus
thuringiensis
encapsulated into killed Pseudomonas
fluorescens;
tolerance.

variety kurstaki
exemption from the requirement of a

top
The delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed Pseudomonas
fluorescens is exempt from the requirements of a tolerance in or on all raw agricultural commodities.
[56 FR 28328, June 20, 1991]

§ 180.1108 Delta endotoxin of Bacillus
thuringiensis
encapsulated into killed Pseudomonas
fluorescens;
tolerance.

variety San Diego
exemption from the requirement of a

top
The delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed Pseudomonas
fluorescens is exempt from the requirements of a tolerance in or on all raw agricultural commodities.
[56 FR 28326, June 20, 1991]

§ 180.1110 3-Carbamyl-2,4,5-trichlorobenzoic acid; exemption from the requirement
of a tolerance.
top
An exemption from the requirement of a tolerance is established for the residues of 3-carbamyl-2,4,5trichlorobenzoic acid in or on all raw agricultural commodities which occur from the direct application of
chlorothalonil to crops in §180.275 (a) and (b) and/or as an inadvertent residue resulting from the soil
metabolism of chlorothalonil when applied to crops in §180.275 (a) and (b), and subsequent uptake by
rotated crops when used according to approved agricultural practices.
[57 FR 24552, June 10, 1992]

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§ 180.1111 Bacillus subtilis GB03; exemption from the requirement of a tolerance.
top
The biofungicide Bacillus subtilis GB03 is exempted from the requirement of a tolerance in or on all raw
agricultural commodities when used in accordance with good agricultural practices.
[73 FR 50556, Aug. 27, 2008]

§ 180.1113 Lagenidium giganteum
exemption from the requirement of a tolerance.

;

top
Lagenidium giganteum (a fungal organism) is exempt from the requirement of a tolerance in or on the raw
agricultural commodities aspirated grain fractions; grass, forage; grass, hay; rice, grain; rice, straw;
soybean, seed; soybean, forage; soybean, hay; rice, wild, grain.
[74 FR 26535, June 3, 2009]

§ 180.1114 Pseudomonas
fluorescens
A506, Pseudomonas
fluorescens
1629RS, and
Pseudomonas syringae
exemptions from the requirement of a tolerance.

742RS;

top
The biological pesticides Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and
Pseudomonas syringae 742RS are exempted from the requirement of a tolerance in or on all raw
agricultural commodities when applied as a frost protection agent or biological control agent to growing
agricultural crops in accordance with good agricultural practices.
[57 FR 42700, Sept. 16, 1992]

§ 180.1118 Spodoptera exigua
polyhedrosis virus; exemption from the requirement of a tolerance.

nuclear

top
An exemption from the requirement of a tolerance is established for the microbial pest control agent
Spodoptera exigua nuclear polyhedrosis virus when used as a pesticide control agent on all raw
agricultural commodities.
[58 FR 25784, Apr. 28, 1993]

§ 180.1119 Azadirachtin; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for the biochemical azadirachtin, which is
isolated from the berries of the Neem tree ( Azadirachta indica ), when used as a pesticide at 20 grams or
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less per acre on all raw agricultural commodities.
[58 FR 8696, Feb. 17, 1993]

§ 180.1120 Streptomyces
from the requirement of a tolerance.

sp. strain K61; exemption

top
The biological pesticide Streptomyces sp. strain K61 is exempted from the requirement of a tolerance in or
on all raw agricultural commodities when used as a fungicide for the treatment of seeds, cuttings,
transplants, and plants of agricultural crops in accordance with good agricultural practices.
[58 FR 21403, Apr. 21, 1993]

§ 180.1121 Boric acid and its salts, borax (sodium borate decahydrate), disodium
octaborate tetrahydrate, boric oxide (boric anhydride), sodium borate and sodium
metaborate; exemptions from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the pesticidal chemical
boric acid and its salts, borax (sodium borate decahydrate), disodium octaborate tetrahydrate, boric oxide
(boric anhydride), sodium borate and sodium metaborate, in or on raw agricultural commodities when
used as an active ingredient in insecticides, herbicides, or fungicides preharvest or postharvest in
accordance with good agricultural practices.
[58 FR 44283, Aug. 20, 1993]

§ 180.1122 Inert ingredients of semiochemical dispensers; exemptions from the
requirement of a tolerance.
top
(a) All inert ingredients of semiochemical dispenser products formulated with, and/or contained in,
dispensers made of polymeric matrix materials (including the monomers, plasticizers, dispersing agents,
antioxidants, UV protectants, stabilizers, and other inert ingredients) are exempted from the requirement of
a tolerance when used as carriers in pesticide formulations for application to growing crops only. These
dispensers shall conform to the following specifications:
(1) Exposure must be limited to inadvertent physical contact only. The design of the dispenser must be
such as to preclude any contamination by its components of the raw agricultural commodity (RAC) or
processed foods/feeds derived from the commodity by virtue of its proximity to the RAC or as a result of its
physical size.
(2) The dispensers must be applied discretely. This exemption does not apply to components of
semiochemical formulations applied in a broadcast manner either to a crop field plot or to individual plants.
(b) A semiochemical dispenser is a single enclosed or semi-enclosed unit that releases semiochemical(s)
into the surrounding atmosphere via volatilization and is applied in a manner to provide discrete
application of the semiochemical(s) into the environment.
(c) Semiochemicals are chemicals that are emitted by plants or animals and modify the behavior of
receiving organisms. These chemicals must be naturally occurring or substantially identical to naturally
occurring semiochemicals.
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[58 FR 64494, Dec. 8, 1993]

§ 180.1124 Arthropod pheromones; exemption from the requirement of a tolerance.
top
Arthropod pheromones, as described in §152.25(b) of this chapter, when used in retrievably sized
polymeric matrix dispensers are exempt from the requirement of a tolerance in or on all raw agricultural
commodities when applied to growing crops only at a rate not to exceed 150 grams active ingredient/acre/
year in accordance with good agricultural practices.
[59 FR 14759, Mar. 30, 1994]

§ 180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; exemption from the requirement of
a tolerance.
top
An exemption from the requirement of a tolerance is established for the insect pheromone codlure, (E,E)8,10-dodecadien-1-ol, on all raw agricultural commodities in accordance with the following prescribed
conditions:
(a) Application shall be limited solely to codlure dispensers that conform to the following specifications:
(1) Commodity exposure must be limited to inadvertent physical contact. The design of the dispenser must
be such as to preclude any exposure of its components to the raw agricultural commodity (RAC) or
processed foods/feeds derived from the commodity due to its proximity to the RAC or as a result of its
physical size. Dispensers must be of such size and construction that they are readily recognized postapplication.
(2) The dispensers must be applied discretely, i.e. , placed in the field in easily perceived distinct locations
in a manner that does not prevent later retrieval. This exemption does not apply to codlure applied in a
broadcast manner either to a crop field plot or to individual plants.
(b) A codlure dispenser is a single enclosed or semi-enclosed unit that releases codlure into the
surrounding atmosphere via volatilization and is applied in a manner to provide discrete application ( i.e. ,
in easily perceived distinct locations in a manner that does not prevent later retrieval) of the codlure into
the environment.
[59 FR 9931, Mar. 2, 1994]

§ 180.1127 Biochemical pesticide plant floral volatile attractant compounds:
cinnamaldehyde, cinnamyl alcohol, 4-methoxy cinnamaldehyde, 3-phenyl propanol, 4methoxy phenethyl alcohol, indole, and 1,2,4-trimethoxybenzene; exemptions from
the requirement of a tolerance.
top
Residues of the biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde,
cinnamyl alcohol, 4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole,
and 1,2,4-trimethoxybenzene are exempt from the requirement of a tolerance in or on the following raw
agricultural commodities: the following field crops—alfalfa, clover, cotton, dandelion, peanuts (including
hay), rice, sorghum (milo), soybeans, sunflower, sweet potatoes, and wheat; the following vegetable crops
—asparagus, beans (including forage hay), beets, carrots, celery, cole crops (cabbage, broccoli, brussels
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sprouts, cauliflower), collards (kale, mustard greens, turnip greens, kohlrabi), corn, fresh (field, sweet, pop,
seed), corn fodder and forage, chinese cabbage, cowpeas, cucurbitis (cucumbers, squash, pumpkin), egg
plant, endive (escarole), horseradish (radish, rutabagas, turnip roots), leafy greens (spinach, swiss chard),
lettuce (head leaf), okra, parsley, parsnip, peas, peas with pods, peppers, potatoes, sugar beets,
tomatoes; the following tree fruit, berry and nut crops—almonds, apples, apricots, berries (blackberry,
boysenberry, dewberry, loganberry, raspberry), blueberry, cherry, citrus (grapefruit, kumquat, lemon, lime,
orange, tangelo, and tangerine) cranberry, grapes, melons, (watermelon, honeydew, crenshaw,
cantaloupe, casaba, persian), nectarines, pears, pecans, peaches, and strawberry as dispersed from the
end-use product Corn Rootworm Bait®, a pesticidal bait, in accordance with the prescribed conditions in
paragraph (a) of this section.
(a) Cumulative yearly application cannot exceed 20 grams of each floral attractant/acre/application.
(b) [Reserved]
[59 FR 15857, Apr. 5, 1994]

§ 180.1128 Bacillus subtilis
exemption from the requirement of a tolerance.

MBI 600;

top
An exemption from the requirement of a tolerance is established for residues of the biofungicide Bacillus
subtilis MBI 600 in or on all food commodities, including residues resulting from post-harvest uses, when
applied or used in accordance with good agricultural practices.
[74 FR 15869, Apr. 8, 2009]

§ 180.1130 N
-( n
-octyl)-2-pyrrolidone and N
-( n
pyrrolidone; exemptions from the requirement of a tolerance.

-dodecyl)-2-

top
N -( n -octyl)-2-pyrrolidone and N -( n -dodecyl)-2-pyrrolidone are exempt from the requirement of a
tolerance when used as solvents in cotton defoliant formulations containing thidiazuron and diuron as
active ingredients.
[59 FR 32084, June 22, 1994]

§ 180.1131
quisqualis
tolerance.

Ampelomyces

isolate M10; exemption from the requirement of a

top
The biological fungicide Ampelomyces quisqualis isolate M10 is exempted from the requirement of a
tolerance in or on all raw agricultural commodities when used as a fungicide on agricultural crops in
accordance with good agricultural practices.
[59 FR 33437, June 29, 1994]

§ 180.1135 Pasteuria penetrans;
exemption from the requirement of a tolerance.

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The biological nematicide Pasteuria penetrans is exempted from the requirement of a tolerance in or on all
raw agricultural commodities, except roots and tubers, when used as a nematicide in the production of
fruits and vegetables in greenhouses.
[59 FR 66741, Dec. 28, 1994]

§ 180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of a
tolerance.
top
The biochemical sodium 5-nitroguiacolate is exempted from the requirement of a tolerance when used as
a plant growth regulator in end-use products at a concentration of 0.1% by weight and applied at an
application rate of 20 g of a.i. per acre or less per application, in or on all food commodities.
[65 FR 66181, Nov. 3, 2000]

§ 180.1140 Sodium o
tolerance.

-nitrophenolate; exemption from the requirement of a

top
The biochemical sodium o -nitrophenolate is exempted from the requirement of a tolerance when used as
a plant growth regulator in end-use products at a concentration of 0.2% by weight and applied at an
application rate of 20 g of a.i. per acre or less per application, in or on all food commodities.
[65 FR 66181, Nov. 3, 2000]

§ 180.1141 Sodium p
tolerance.

-nitrophenolate; exemption from the requirement of a

top
The biochemical sodium p -nitrophenolate is exempted from the requirement of a tolerance when used as
a plant growth regulator in end-use product at a concentration of 0.3% by weight and applied at an
application rate of 20 g of a.i. per acre or less per application, in or on all food commodities.
[65 FR 66181, Nov. 3, 2000]

§ 180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of a
tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the plant growth regulator
1,4-dimethylnaphthalene when applied post harvest to potatoes in accordance with good agricultural
practices.
[60 FR 7457, Feb. 8, 1995]

§ 180.1143 Methyl anthranilate; exemption from the requirement of a tolerance.
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Residues of methyl anthranilate, a biochemical pesticide, are exempt from the requirement of a tolerance
in or on all food commodities, when used in accordance with good agricultural practices.
[67 FR 51088, Aug. 7, 2002]

§ 180.1144 Candida oleophila
182; exemption from the requirement of a tolerance.

isolate I-

top
Candida oleophila isolate I-182, when used as a post-harvest biological fungicide, is exempted from the
requirement of a tolerance in or on all raw agricultural commodities.
[60 FR 11033, Mar. 1, 1995]

§ 180.1145 Pseudomonas syringae;
exemption from the requirement of a tolerance.
top
Pseudomonas syringae is exempted from the requirement of a tolerance on all raw agricultural
commodities when applied postharvest according to good agricultural practices.
[60 FR 12703, Mar. 8, 1995]

§ 180.1146 Beauveria bassiana
GHA; exemption from the requirement of a tolerance.

Strain

top
Beauveria bassiana Strain GHA is exempted from the requirement of a tolerance in or on all raw
agricultural commodities when applied to growing crops according to good agricultural practices.
[60 FR 18547, Apr. 12, 1995]

§ 180.1148 Occlusion Bodies of the Granulosis Virus of Cydia
pomenella;
tolerance exemption.
top
An exemption from the requirement of a tolerance is established for residues of the microbial pest control
agent Occlusion Bodies of the Granulosis Virus of Cydia pomonella (codling moth) in or on all raw
agricultural commodities.
[60 FR 42450, Aug. 16, 1995]

§ 180.1149 Inclusion bodies of the multi-nuclear polyhedrosis virus of
Anagrapha falcifera;
exemption from
the requirement of a tolerance.
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The microbial pest control agent inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha
falcifera is exempted from the requirement of a tolerance in or on all raw agricultural commodities when
used to control certain lepidopteran pest species.
[60 FR 37020, July 19, 1995]

§ 180.1150 6-Benzyladenine; exemption from the requirement of a tolerance.
top
The biochemical plant regulator 6-benzyladenine (6–BA) is exempt from the requirement of a tolerance in
or on apple and pear when applied at a rate of ≤182 grams of active ingredient per acre per season, and
in or on pistachio when applied at a rate of ≤60 grams of active ingredient per acre per season.
[72 FR 13179, Mar. 21, 2007]

§ 180.1153 Lepidopteran pheromones; exemption from the requirement of a
tolerance.
top
Lepidopteran pheromones that are naturally occurring compounds, or identical or substantially similar
synthetic compounds, designated by an unbranched aliphatic chain (between 9 and 18 carbons) ending in
an alcohol, aldehyde or acetate functional group and containing up to 3 double bonds in the aliphatic
backbone, are exempt from the requirement of a tolerance in or on all raw agricultural commodities. This
exemption only pertains to those situations when the pheromone is: Applied to growing crops at a rate not
to exceed 150 grams active ingredient/acre/year in accordance with good agricultural practices; and
applied as a post-harvest treatment to stored food commodities at a rate not to exceed 3.5 grams active
ingredient/1,000 ft2 /year (equivalent to 150 grams active ingredient/acre/year) in accordance with good
agricultural practices.
[71 FR 45399, Aug. 9, 2006]

§ 180.1154 CryIA(c) and CryIC derived delta-endotoxins of
Bacillus thuringiensis
kurstaki
encapsulated in killed
Pseudomonas fluorescens,
the expression plasmid and cloning vector genetic constructs.

var.
and

top
CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki encapsulated in killed
Pseudomonas fluorescens and the expression plasmid and cloning vector genetic constructs are exempt
from the requirement of a tolerance when used in or on all raw agricultural commodities.
[60 FR 47489, Sept. 13, 1995]

§ 180.1156 Cinnamaldehyde; exemption from the requirement of a tolerance.
top

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Cinnamaldehyde (3-phenyl-2-propenal) is exempted from the requirement of a tolerance in or on all food
commodities, when used as a fungicide, insecticide, and algaecide in accordance with good agricultual
practices.
[64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, 1999]

§ 180.1157 Cytokinins; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of cytokinins (specifically:
aqueous extract of seaweed meal and kinetin) in or on all food commodities when used as plant regulators
on plants, seeds, or cuttings and on all food commodities after harvest in accordance with good
agricultural practices.
[64 FR 31505, June 11, 1999]

§ 180.1158 Auxins; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of auxins (specifically: indole3-acetic acid and indole-3-butyric acid) in or on all food commodities when used as plant regulators on
plants, seeds, or cuttings and on all food commodities after harvest in accordance with good agricultural
practices.
[64 FR 31505, June 11, 1999]

§ 180.1159 Pelargonic acid; exemption from the requirement of tolerances.
top
(a) An exemption from the requirement of a tolerance is established for residues of pelargonic acid in or on
all food commodities when used as a plant regulator on plants, seeds, or cuttings and on all food
commodities after harvest in accordance with good agricultural practices.
(b) Pelargonic acid when used as an herbicide is exempt from the requirement of a tolerance on all plant
food commodities provided that:
(1) Applications are not made directly to the food commodity except when used as a harvest aid or
desiccant to: any root and tuber vegetable, bulb vegetable or cotton.
(2) When pelargonic acid is used as a harvest aid or desiccant, applications must be made no later than
24 hours prior to harvest.
(c) An exemption from the requirement of a tolerance is established for residues of pelargonic acid in or on
all raw agricultural commodities and in processed commodities, when such residues result from the use of
pelargonic acid as an antimicrobial treatment in solutions containing a diluted end-use concentration of
pelargonic acid up to 170 ppm per application on food contact surfaces such as equipment, pipelines,
tanks, vats, fillers, evaporators, pasteurizers and aseptic equipment in restaurants, food service
operations, dairies, breweries, wineries, beverage and food processing plants.
[62 FR 28364, May 23, 1997, as amended at 64 FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, 2003]

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§ 180.1160 Jojoba oil; exemption from the requirement of a tolerance.
top
The insecticide and spray tank adjuvant jojoba oil is exempted from the requirement of a tolerance in or on
all raw agricultural commodities when applied at the rate of 1.0% or less of the final spray in accordance
with good agricultural practices, provided the jojoba oil does not contain simmondsin, simmondsin-2ferulate, and related conjugated organonitriles including demethyl simmondsin and didemethylsimmondsin.
[61 FR 2121, Jan. 25, 1996]

§ 180.1161 Clarified hydrophobic extract of neem oil; exemption from the
requirement of a tolerance.
top
Clarified hydrophobic extract of neem oil is exempt from the requirement of a tolerance on all food
commodities when used as a botanical fungicide/insecticide/miticide.
[67 FR 43552, June 28, 2002]

§ 180.1162 Acrylate polymers and copolymers; exemption from the requirement of a
tolerance.
top
(a) Acrylate polymers and copolymers are exempt from the requirement of a tolerance when used as inert
ingredients in pesticidal formulations applied to growing, raw agricultural commodities. This tolerance
exemption covers the acrylate polymers/copolymers that are intrinsically safe and already listed in TSCA
inventory or will meet the polymer tolerance exemption from requirements of premanufacturing notification
under 40 CFR 723.250. Polymers exempted can be used as dispensers, resins, fibers, and beads, as long
as the fibers, beads and resins particle sizes are greater than 10 microns and insoluble in water. This
exemption pertains to the acrylate polymers/copolymers used as inert ingredients for sprayable and
dispenser pesticide formulations that are applied on food crops. Any acrylate polymers/copolymers used
for encapsulating material must be cleared as an inert ingredient when used in pesticide formulation
applied on food crops.
(b) For the purposes of this exemption, acrylate polymers/copolymers used as inert ingredients in an enduse formulation must meet the definition for a polymer as given in 40 CFR 723.250(b), are not
automatically excluded by 40 723.250(d), and meet the tolerance exemption criteria in 40 CFR 723.250(e)
(1), 40 CFR 723.250 (e)(2) or 40 CFR 723.250(e)(3). Therefore, acrylate polymers and copolymers that
are already listed in the TSCA inventory or will meet the polymer tolerance exemption under 40 CFR
723.250 as amended on March 29, 1995 are covered by this exemption.
[61 FR 6551, Feb. 21, 1996]

§ 180.1163 Killed Myrothecium
verrucaria;
tolerance.

exemption from the requirement of a

top
Killed Myrothecium verrucaria is exempted from the requirement of a tolerance in or on all raw agricultural
commodities when applied as a pre-seed or pre- or post-planting soil treatment alone or mixed with water

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and the mixed suspension be applied through drip or border irrigation systems and the indicator mycotoxin
levels do not exceed 15 ppm.
[61 FR 11315, Mar. 20, 1996, as amended at 61 FR 58332, Nov. 14, 1996]

§ 180.1165 Capsaicin; exemption from the requirement of a tolerance.
top
Capsaicin is exempt from the requirement of a tolerance in or on all food commodities when used in
accordance with approved label rates and good agricultural practice.
[63 FR 39521, July 23, 1998]

§ 180.1167 Allyl isothiocyanate as a component of food grade oil of mustard;
exemption from the requirement of a tolerance.
top
The insecticide and repellent Allyl isothiocyanate is exempt from the requirement of a tolerance for
residues when used as a component of food grade oil of mustard, in or on all raw agricultural
commodities, when applied according to approved labeling.
[61 FR 24894, May 17, 1996]

§ 180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance.
top
The biochemical pesticide sodium bicarbonate is exempted from the requirement of a tolerance in or on all
raw agricultural commodities when applied as a fungicide or post-harvest fungicide in accordance with
good agricultural practices.
[61 FR 67473, Dec. 23, 1996]

§ 180.1177 Potassium bicarbonate; exemption from the requirement of a tolerance.
top
The biochemical pesticide potassium bicarbonate is exempted from the requirement of a tolerance in or on
all raw agricultural commodities when applied as a fungicide or post-harvest fungicide in accordance with
good agricultural practices.
[61 FR 67473, Dec. 23, 1996]

§ 180.1178 Formic acid; exemption from the requirement of a tolerance.
top
The pesticide formic acid is exempted from the requirement of a tolerance in or on honey and honeycomb
when used to control tracheal mites and suppress varroa mites in bee colonies, and applied in accordance
with label use directions.

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[74 FR 26535, June 3, 2009]

§ 180.1179 Plant extract derived from Opuntia
lindheimeri, Quercus
falcata, Rhus aromatica,
and Rhizophoria mangle;
the requirement of a tolerance.

exemption from

top
The biochemical pesticide plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus
aromatica, and Rhizophoria mangle is exempted from the requirement of a tolerance in or on all raw
agricultural commodities when applied as a nematicide/plant regulator in accordance with good
agricultural practices.
[62 FR 24842, May 7, 1997]

§ 180.1180 Kaolin; exemption from the requirement of a tolerance.
top
(a) The biochemical pesticide kaolin is temporarily exempted from the requirement of a tolerance for
residues of the insecticide Kaolin, when used on crops (apples, apricots, bananas, beans, cane berries,
citrus fruits, corn, cotton, cranberries, cucurbits, grapes, melons, nuts, ornamentals, peaches, peanuts,
pears, peppers, plums, potatoes, seed crops, small grains, soybeans, strawberries, sugar beets, and
tomatoes) to control certain insect, fungus, and bacterial damage to plants. This temporary exemption
from the requirement of a tolerance will permit the marketing of the food commodities in this paragraph
when treated in accordance with the provisions of experimental use permit 70060–EUP–1, which is being
issued under the Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA), as amended (7 U.S.C.
136). This temporary exemption from the requirement of a tolerance expires and is revoked December 31,
1999. This temporary exemption from the requirement of a tolerance may be revoked at any time if the
experimental use permit is revoked or if any experience with or scientific data on this pesticide indicate
that the tolerance is not safe.
(b) Kaolin is exempted from the requirement of a tolerance for residues when used on or in food
commodities to aid in the control of insects, fungi, and bacteria (food/feed use).
[62 FR 19685, Apr. 23, 1997, as amended at 63 FR 9430, Feb. 25, 1998]

§ 180.1181 Bacillus cereus
exemption from the requirement of a tolerance.

strain BPO1;

top
An exemption from the requirement of a tolerance for residues of the Bacillus cereus strain BPO1 in or on
all raw agricultural commodities when applied/used in accordance with label directions.
[67 FR 70017, Nov. 20, 2002]

§ 180.1187 L-glutamic acid; exemption from the requirement of a tolerance.
top

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L-glutamic acid is exempt from the requirement of a tolerance on all food commodities when used in
accordance with good agricultural practices.
[66 FR 33198, June 21, 2001]

§ 180.1188 Gamma aminobutyric acid; exemption from the requirement of a
tolerance.
top
Gamma aminobutyric acid is exempt from the requirement of a tolerance on all food commodities when
used in accordance with good agricultural practices.
[66 FR 33198, June 21, 2001]

§ 180.1189 Methyl salicylate; exemption from the requirement of a tolerance.
top
The biochemical pesticide methyl salicylate is exempt from the requirement of a tolerance for residues in
or on food or feed when used as an insect repellant in food packaging and animal feed packaging at an
application rate that does not exceed 0.2 mg of methyl salicylate per square inch of packaging materials.
[62 FR 61639, Nov. 19, 1997]

§ 180.1191 Ferric phosphate; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide,
ferric phosphate (FePO4, CAS No. 11045–86–0) in or on all food commodities.
[62 FR 56105, Oct. 29, 1997]

§ 180.1193 Potassium dihydrogen phosphate; exemption from the requirement of a
tolerance.
top
Potassium dihydrogen phosphate is exempted from the requirement of a tolerance in or on all food
commodities when applied as a fungicide in accordance with good agricultural practices.
[63 FR 43085, Aug. 12, 1998]

§ 180.1195 Titanium dioxide.
top
Titanium dioxide is exempted from the requirement of a tolerance for residues in or on growing crops,
when used as an inert ingredient (UV protectant) in microencapsulated formulations of the insecticide
lambdacyhalothrin at no more than 3.0% by weight of the formulation.

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[63 FR 14363, Mar. 25, 1998]

§ 180.1196 Peroxyacetic acid; exemption from the requirement of a tolerance.
top
(a) An exemption from the requirement of a tolerance is established for residues of peroxyacetic acid in or
on all food commodities, when such residues result from the use of peroxyacetic acid as an antimicrobial
treatment in solutions containing a diluted end use concentration of peroxyacetic acid up to 100 ppm per
application on fruits, vegetables, tree nuts, cereal grains, herbs, and spices.
(b) An exemption from the requirement of a tolerance is established for residues of peroxyacetic acid, in or
on all food commodities when used in sanitizing solutions containing a diluted end-use concentration of
peroxyacetic acid up to 500 ppm, and applied to tableware, utensils, dishes, pipelines, tanks, vats, fillers,
evaporators, pasteurizers, aseptic equipment, milking equipment, and other food processing equipment in
food handling establishments including, but not limited to dairies, dairy barns, restaurants, food service
operations, breweries, wineries, and beverage and food processing plants.
[74 FR 26535, June 3, 2009]

§ 180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of hydrogen peroxide in or
on all food commodities at the rate of ≤ 1% hydrogen peroxide per application on growing and postharvest
crops.
[67 FR 41844, June 20, 2002]

§ 180.1198 Gliocladium
catenulatum
requirement of a tolerance.

strain J1446; exemption from the

top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide,
Gliocladium catenulatum strain J1446 when used in or on all food commodities.
[63 FR 37288, July 10, 1998]

§ 180.1199 Lysophosphatidylethanolamine (LPE); exemption from the requirement
of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide
lysophosphatidylethanolamine in or on all food commodities.
[67 FR 17636, Apr. 11, 2002]

§ 180.1200
fluorescens

Pseudomonas

strain PRA–25; temporary exemption from the

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requirement of a tolerance.
top
A temporary exemption from the requirement of a tolerance is established for residues of the microbial
pesticide, pseudomonas fluorescens strain PRA–25 when used on peas, snap beans and sweet corn and
will expire July 31, 2001.
[63 FR 38498, July 17, 1998]

§ 180.1201 Trichoderma harzianum
strain T-39; exemption from the requirement of a tolerance.
top
Trichoderma harzianum strain T-39 is exempt from the requirement of a tolerance on all food commodities.
[65 FR 38757, June 22, 2000]

§ 180.1202 Bacillus sphaericus;
exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticides,
Bacillus sphaericus when used in or on all food crops.
[63 FR 48597, Sept. 11, 1998]

§ 180.1204 Harpin protein; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of individual harpin proteins
that meet specified physiochemical and toxicological criteria when used as biochemical pesticides on all
food commodities to enhance plant growth, quality and yield, to improve overall plant health, and to aid in
pest management. The physiochemical and toxicological criteria identifying harpin proteins are as follows:
(a) Consists of a protein less than 100 kD in size, that is acidic (pI<7.0), glycine rich (>10%), and contains
no more than one cystine residue.
(b) The source(s) of genetic material encoding the protein are bacterial plant pathogens not known to be
mammalian pathogens.
(c) Elicits the hypersensitive response (HR) which is characterized as rapid, localized cell death in plant
tissue after infiltration of harpin into the intercellular spaces of plant leaves.
(d) Possesses a common secondary structure consisting of α and β units that form an HR domain.
(e) Is heat stable (retains HR activity when heated to 65 °C for 20 minutes).
(f) Is readily degraded by a proteinase representative of environmental conditions (no protein fragments
>3.5 kD after 15 minutes degradation with Subtilisin A).
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(g) Exhibits a rat acute oral toxicity (LD50) of greater than 5,000 mg product/kg body weight.
[69 FR 24996, May 5, 2004]

§ 180.1205 Beauveria bassiana
#74040; exemption from the requirements of a tolerance.

ATCC

top
An exemption from the requirement of a tolerance is established for residues of the insecticide Beauveria
bassiana (ATCC #74040) in or on all food commodities when applied or used as ground and aerial foliar
sprays for use only on terrestrial crops.
[64 FR 22796, Apr. 28, 1999]

§ 180.1206 Aspergillus flavus
exemption from the requirement of a tolerance.

AF36;

top
(a) An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Aspergillus flavus AF36 in or on cotton, gin byproducts; cotton, hulls; cotton, meal; cotton, refined oil;
cotton, undelinted seed.
(b) Aspergillus flavus AF36 is temporarily exempt from the requirement of a tolerance on pistachio when
used in accordance with the Experimental Use Permit, EPA File Symbol 71693–EUP–1. This temporary
exemption from tolerance expires on December 31, 2011.
(c) Aspergillus flavis AF 36 is temporarily exempt from the requirement of a tolerance on corn, field,
forage; corn, field, grain; corn, field, stover; corn, pop, grain; corn, pop, stover; corn, sweet, forage; corn,
sweet, kernel plus cob with husks removed; corn, sweet, stover when used in accordance with the
Experimental Use Permit 71693–EUP–2. This temporary exemption from the tolerance will expire
December 31, 2011.
[68 FR 41541, July 14, 2003, as amended at 72 FR 28871, May 23, 2007; 72 FR 72965, Dec. 26, 2007;
74 FR 26535, 26546, June 3, 2009]

§ 180.1207 N-acyl sarcosines and sodium N-acyl sarcosinates; exemption from the
requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the following substances
when used as inert ingredients (surfactants) at levels not to exceed 10% in pesticide formulations
containing glyphosate:

Name

CAS Reg. No.

N-acyl sarcosines
N-cocoyl sarcosine mixture
N-lauroyl sarcosine
N-myristoyl sarcosine
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68411-97-2
97-78-9
52558-73-3

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N-oleoyl sarcosine

110-25-8

N-stearoyl sarcosine

142-48-3

Sodium N-acyl sarcosinates
N-cocoyl sarcosine sodium salt mixture

61791-59-1

N-methyl-N-(1-oxo-9-octodecenyl) glycine

3624-77-9

N-methyl-N-(1-oxododecyl) glycine

137-16-6

N-methyl-N-(1-oxooctadecyl) glycine

5136-55-0

N-methyl-N-(1-oxotetradecyl glycine

30364-51-3

[64 FR 68046, Dec. 6, 1999]

§ 180.1209 Bacillus subtilis
713; exemption from the requirement of a tolerance.

strain QST

top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Bacillus subtilis strain QST 713 when used in or on all food commodities.
[65 FR 41369, July 5, 2000]

§ 180.1210 Phosphorous acid; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of phosphorous acid and its
ammonium, sodium, and potassium salts in or on all food commodities when used as an agricultural
fungicide and in or on potatoes when applied as a post-harvest treatment at 35,600 ppm or less
phosphorous acid.
[71 FR 49373, Aug. 23, 2006]

§ 180.1212 Pseudomonas
chlororaphis
requirement of a tolerance.

Strain 63–28; exemption from the

top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Pseudomonas chlororaphis Strain 63–28 in or on all food commodities.
[66 FR 53346, Oct. 22, 2001]

§ 180.1213 Coniothyrium minitans
strain CON/M/91–08; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Coniothyrium minitans strain CON/M/91–08 when used in or on all food commodities.
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[66 FR 16874, Mar. 28, 2001]

§ 180.1218 Indian Meal Moth Granulosis Virus; exemption from the requirement of a
tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Indian Meal Moth Granulosis Virus when used in or on all food commodities.
[68 FR 55875, Sept. 29, 2003]

§ 180.1219 Foramsulfuron; exemption from the requirement of a tolerance.
top
The pesticide foramsulfuron is exempted from the requirement of a tolerance in corn, field, grain/corn,
field, forage/ corn, field, stover/corn, pop, grain/corn, pop, forage/corn, pop, stover; corn, sweet, forage;
corn, sweet, kernel plus cob with husks removed; corn, sweet, stover when applied as a herbicide in
accordance with good agricultural practices.
[74 FR 26535, June 3, 2009]

§ 180.1220 1-Methylcyclopropene; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the 1-Methylcyclopropene
in or on fruits and vegetables when:
(a) Used as a post harvest plant growth regulator, i.e. , for the purpose of inhibiting the effects of ethylene.
(b) Applied or used outdoors for pre-harvest treatments.
[73 FR 19150, Apr. 9, 2008]

§ 180.1221 Pseudozyma flocculosa
strain PF-A22 UL; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of Pseudozyma flocculosa
strain PF-A22 UL in or on all food commodities.
[67 FR 60966, Sept. 27, 2002]

§ 180.1222 Sucrose octanoate esters; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of sucrose octanoate esters
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[(α-D-glucopyranosyl-β-D-fructofuranosyl-octanoate), mono-, di-, and triesters of sucrose octanoate] in or
on all food commodities when used in accordance with good agricultural practices.
[67 FR 60152, Sept. 25, 2002]

§ 180.1223 Imazamox; exemption from the requirement of a tolerance.
top
The herbicide imazamox, (±) 2, -[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5(methoxymethyl)-3-pyridinecarboxylic acid, is exempt from the requirement of a tolerance on all food
commodities when applied as a herbicide in accordance with good agricultural practices.
[68 FR 7433, Feb. 14, 2003]

§ 180.1224 Bacillus pumilus
exemption from the requirement of a tolerance.

GB34;

top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Bacillus pumilus GB34 when used as a seed treatment in or on all food commodities. An exemption is also
granted for such residues on treated but unplanted soybean seeds.
[69 FR 76625, Dec. 22, 2004]

§ 180.1225 Decanoic acid; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of decanoic acid in or on all
raw agricultural commodities and in processed commodities, when such residues result from the use of
decanoic acid as an antimicrobial treatment in solutions containing a diluted end-use concentration of
decanoic acid (up to 170 ppm per application) on food contact surfaces such as equipment, pipelines,
tanks, vats, fillers, evaporators, pasteurizers and aseptic equipment in restaurants, food service
operations, dairies, breweries, wineries, beverage and food processing plants.
[68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, 2003]

§ 180.1226 Bacillus pumilus
temporary exemption from the requirement of a tolerance.

strain QST2808;

top
A temporary exemption from the requirement of a tolerance is established for residues of the microbial
pesticide Bacillus pumilus strain QST2808 when used in or on all agricultural commodities when applied/
used in accordance with label directions.
[68 FR 36480, June 18, 2003]

§ 180.1228 Diallyl sulfides; exemption from the requirement of a tolerance.
top
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An exemption from the requirement of a tolerance is established for residues of diallyl sulfides when used
in/on garlic, leeks, onions, and shallots.
[68 FR 40808, July 9, 2003]

§ 180.1230 Ferrous sulfate; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of ferrous sulfate.
[70 FR 33363, June 8, 2005]

§ 180.1231 Lime; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of lime.
[70 FR 33363, June 8, 2005]

§ 180.1232 Lime-sulfur; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of lime-sulfur.
[70 FR 33363, June 8, 2005]

§ 180.1233 Potassium sorbate; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of potassium sorbate.
[70 FR 33363, June 8, 2005]

§ 180.1234 Sodium carbonate; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of sodium carbonate.
[70 FR 33363, June 8, 2005]

§ 180.1235 Sodium hypochlorite; exemption from the requirement of a tolerance.
top

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An exemption from the requirement of a tolerance is established for residues of sodium hypochlorite.
[70 FR 33363, June 8, 2005]

§ 180.1236 Sulfur; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of sulfur.
[70 FR 33363, June 8, 2005]

§ 180.1237 Sodium metasilicate; exemption from the requirement of a tolerance.
top
(a) An exemption from the requirement of a tolerance is established for residues of sodium metasilicate in
or on all food commodities when used in accordance with approved label rates and good agricultural
practices as a plant desiccant, so long as the sodium metasilicate does not exceed 4% by weight in
aqueous solution.
(b) An exemption from the requirement of a tolerance is established for residues of sodium metasilicate in
or on all food commodities when used in accordance with approved label rates and good agricultural
practices as an insecticide and fungicide, so long as the sodium metasilicate does not exceed 2.41% by
weight in aqueous solution.
[71 FR 19441, Apr. 14, 2006]

§ 180.1240 Thymol; exemption from the requirement of a tolerance.
top
(a) Time-limited exemptions from the requirement of a tolerance are established for residues of thymol on
honey and honeycomb in connection with use of the pesticide under section 18 emergency exemptions
granted by the EPA. These time-limited exemptions from the requirement of a tolerance for residues of
thymol will expire and are revoked on June 30, 2007.
(b) An exemption from the requirement of a tolerance for residues of the thymol (as present in thyme oil) in
or on food commodities when applied/used in/on public eating places, dairy processing equipment, and/or
food processing equipment and utensils.
[70 FR 37696, June 30, 2005, as amended at 71 FR 2895, Jan. 18, 2006; 74 FR 12617, Mar. 25, 2009]

§ 180.1241 Eucalyptus oil; exemption from the requirement of a tolerance.
top
Time-limited exemptions from the requirement of a tolerance are established for residues of eucalyptus oil
on honey and honeycomb in connection with use of the pesticide under section 18 emergency exemptions
granted by the EPA. These time-limited exemptions from the requirement of a tolerance for residues of
eucalyptus oil will expire and are revoked on June 30, 2007.
[70 FR 37696, June 30, 2005]

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§ 180.1243 Bacillus subtilis
amyloliquefaciens
from the requirement of a tolerance.

var.
strain FZB24; exemption

top
An exemption from the requirement of a tolerance for residues of the Bacillus subtilis var.
amyloliquefaciens strain FZB24 in or on all agricultural commodities when applied/used in accordance with
label directions.
[68 FR 44640, July 30, 2003]

§ 180.1244 Ammonium bicarbonate; exemption from the requirement of a tolerance.
top
An exemption from the requirement of tolerance is established for residues of ammonium bicarbonate
used in or on all food commodities when used in accordance with good agricultural practices.
[69 FR 13745, Mar. 24, 2004]

§ 180.1245 Rhamnolipid biosurfactant; exemption from the requirement of a
tolerance.
top
An exemption from the requirement of a tolerance is established for residues of rhamnolipid biosurfactant
when used in accordance with good agricultural practices as a fungicide in or on all food commodities.
[69 FR 16800, Mar. 31, 2004]

§ 180.1246 Yeast Extract Hydrolysate fromSaccharomyces cerevisiae:exemption
from the requirement of a tolerance.
top
This regulation establishes an exemption from the requirement of a tolerance for residues of the
biochemical pesticide Yeast Extract Hydrolysate from Saccharomyces cerevisiae on all food commodities
when applied/used for the management of plant diseases.
[69 FR 9958, Mar. 3, 2004]

§ 180.1248 Exemption of citronellol from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide
citronellol in or on all food commodities.
[69 FR 23146, Apr. 28, 2004]

§ 180.1250 C8, C10, and C12 fatty acid monoesters of glycerol and propylene glycol;
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exemption from the requirement of a tolerance.
top
The C8, C10, and C12 straight-chain fatty acid monoesters of glycerol (glycerol monocaprylate, glycerol
monocaprate, and glycerol monolaurate) and propylene glycol (propylene glycol monocaprylate, propylene
glycol monocaprate, and propylene glycol monolaurate) are exempt from the requirement of a tolerance in
or on all food commodities when used in accordance with approved label rates and good agricultural
practice.
[69 FR 34944, June 23, 2004]

§ 180.1251 Geraniol; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide
geraniol in or on all food commodities.
[69 FR 23151, Apr. 28, 2004]

§ 180.1253 Streptomyces lydicus
WYEC 108; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Streptomyces lydicus WYEC 108 when used in or on all agricultural commodities when applied/used in
accordance with label directions.
[69 FR 31301, June 3, 2004]

§ 180.1254 Aspergillus flavus NRRL 21882 on peanut; exemption from requirement
of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus NRRL
21882 in or on peanut; peanut hay; peanut, meal; peanut, refined oil.
[74 FR 26535, June 3, 2009]

§ 180.1255 Bacillus pumilus
exemption from the requirement of a tolerance.

strain QST 2808;

top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Bacillus pumilus strain QST 2808 when used in or on all agricultural commodities when applied/used in
accordance with label directions.
[69 FR 63954, Nov. 3, 2004]

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§ 180.1256 Alternaria destruens
strain 059; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Alternaria destruens Strain 059 when used in or on all raw agricultural commodities when applied/used in
accordance with label directions.
[70 FR 28459, May 18, 2005]

§ 180.1257
lilacinus
tolerance.

Paecilomyces

strain 251; exemption from the requirement of a

top
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Paecilomyces lilacinus strain 251 when used in or on all agricultural commodities when applied/used in
accordance with label directions.
[70 FR 19283, Apr. 13, 2005]

§ 180.1258 Acetic acid; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide
acetic acid when used as a preservative on post-harvest agricultural commodities intended for animal
feed, including Alfalfa, seed; alfalfa, hay; barley, grain; bermudagrass, hay; bluegrass, hay; bromegrass,
hay; clover, hay; corn, field, grain; corn, pop, grain; cowpea, hay; fescue, hay; lespedeza, hay; lupin; oat,
grain; orchardgrass, hay; peanut, hay; timothy, hay; vetch, hay; and wheat, grain, or commodities
described as grain or hay.
[74 FR 26536, June 3, 2009]

§ 180.1259 Reynoutria
sachalinensis
requirement of a tolerance.

extract; exemption from the

top
Residues of the biochemical pesticide Reynoutria sachalinensis extract, when derived from the whole
plant extract, are exempt from the requirement of a tolerance in or on all food commodities.
[70 FR 55277, Sept. 21, 2005]

§ 180.1260 Muscodor albus
QST 20799 and the
volatiles produced on rehydration; exemption from the requirement of a tolerance.
top

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An exemption from the requirement of a tolerance is established on all food/feed commodities, for
residues of Muscodor albus QST 20799, and the volatiles produced on its rehydration, when the pesticide
is used for all agricultural applications, including seed, propagule and post harvest treatments.
[70 FR 56576, Sept. 28, 2005]

§ 180.1261 Xanthomonas
campestris pv.
vesicatoria
syringae pv. tomato
Bacteriophages.

and Pseudomonas

specific

top
An exemption from the requirement of a tolerance is established for residues of Xanthomonas campestris
pv. vesicatoria and Pseudomonas syringae pv. tomato specific bacteriophages in or on pepper and tomato.
[74 FR 26536, June 3, 2009]

§ 180.1262 Sorbitol octanoate; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of sorbitol octanoate in or on
all food commodities when used in accordance with label directions.
[71 FR 4518, Jan. 27, 2006]

§ 180.1263 Tetrahydrofurfuryl alcohol; exemption from the requirement of a
tolerance.
top
Tetrahydrofurfuryl alcohol (THFA, CAS Reg. No. 97–99–4) is exempt from the requirement of a tolerance
in or on all raw agricultural commodities when used in accordance with good agricultural practices as an
inert ingredient applied only:
(a) For use as a seed treatment.
(b) For applications prior to planting and at the time of planting.
(c) For use on cotton.
(d) For use in herbicides with one application to wheat and barley prior to the pre-boot stage, and two
applications to canola and soybeans pre-bloom.
(e) For use in herbicides with two applications to field corn up to 24 inches tall (V 5 stage).
[71 FR 45415, Aug. 9, 2006]

§ 180.1267 Pantoea agglomerans
C9–1; exemption from the requirement of a tolerance.

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strain

Electronic Code of Federal Regulations:

top
An exemption from the requirement of a tolerance is established for residues of Pantoea agglomerans
strain C9–1 when used on apples and pears.
[71 FR 24596, Apr. 26, 2006]

§ 180.1268 Potassium silicate; exemption from the requirement of a tolerance.
top
Potassium silicate is exempt from the requirement of a tolerance in or on all food commodities so long as
the potassium silicate is not applied at rates exceeding 1% by weight in aqueous solution and when used
in accordance with good agricultural practices.
[71 FR 34272, June 14, 2006]

§ 180.1269 Bacillus mycoides
exemption from the requirement of a tolerance.

Isolate J:

top
Bacillus mycoides isolate J is temporarily exempt from the requirement of a tolerance when used as a
fungicide on pecans, potatoes, sugar beets, tomatoes, and peppers in accordance with the Experimental
Use Permit 82761–EUP–2. This temporary exemption from the requirement of a tolerance expires and is
revoked on March 31, 2011.
[74 FR 10498, Mar. 11, 2009]

§ 180.1270 Isophorone; exemption from the requirement of a tolerance.
top
Isophorone (CAS Reg. No. 78–59–1) is exempt from the requirement of a tolerance when used as an inert
ingredient in pesticide formulations applied to beets, ginseng, rice, spinach, sugar beets, and Swiss chard.
[71 FR 45408, Aug. 9, 2006]

§ 180.1271 Eucalyptus oil; exemption from the requirement of a tolerance.
top
An exemption from the requirement of tolerance is established for residues of eucalyptus oil in or on
honey, honeycomb, and honeycomb with honey when used at 2g or less eucalyptus oil per hive, where
the eucalyptus oil contains 80% or more eucalyptol.
[71 FR 53979, Sept. 13, 2006]

§ 180.1272 Pantoea agglomerans
E325; exemption from the requirement of a tolerance.
top

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strain

Electronic Code of Federal Regulations:

An exemption from the requirement of a tolerance is established for residues of Pantoea agglomerans
strain E325 when used on apples and pears.
[71 FR 54933, Sept. 20, 2006]

§ 180.1273 Beauveria bassiana
exemption from the requirement of a tolerance.

HF23;

top
An exemption from the requirement of a tolerance is established on all food/feed commodities, for
residues of Beauveria bassiana HF23 when the pesticide is used for chicken manure treatment.
[72 FR 1183, Jan. 10, 2007]

§ 180.1274 Tris (2-ethylhexyl) phosphate; exemption from the requirement of a
tolerance.
top
Tris (2-ethylhexyl) phosphate (TEHP, CAS Reg. No. 78–42–2) is exempt from the requirement of a
tolerance for residues in grain, aspirated fractions; barley, grain, barley, hay, barley, straw; wheat, grain;
wheat, forage; wheat, hay; wheat, straw when used under the following conditions:
(a) The use is in accordance with good agricultural practices;
(b) Tris (2-ethylhexyl) phosphate is used as an inert ingredient in pesticide formulations with the active
ingredients pinoxaden, clodinafop-propargyl, and tralkoxydium;
(c) Tris (2-ethylhexyl) phosphate is applied no more than twice per season; and
(d) The applications occur no later than the pre-boot stage (prior to formation of edible grain).
[72 FR 5624, Feb. 7, 2007, as amended at 74 FR 26536, June 3, 2009]

§ 180.1275 Pythium; exception from the requirement of a tolerance.
top
An exemption from the requirement of tolerance is established on all food/feed commodities, for residues
of pythium oligandrum DV 74 when the pesticide is used on food crops.
[72 FR 27452, May 16, 2007]

§ 180.1276 Tobacco mild green mosaic tobamovirus (TMGMV); temporary exemption
from the requirement of a tolerance.
top
A temporary exemption from the requirement of a tolerance is established for residues of tobacco mild
green mosaic tobamovirus in or on all grass, forage and grass, hay.

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[74 FR 26536, June 3, 2009]

§ 180.1277 Dibasic esters; exemption from the requirement of a tolerance.
top
Dibasic esters (CAS Reg. No. 95481–62–2) is exempted from the requirement of a tolerance for residues
when used as an inert ingredient (solvent and/or anti-freeze) at 10% W/W or less in microencapsulated
pesticide formulations with the active ingredient cyfluthrin.
[73 FR 10398, Feb. 27, 2008]

§ 180.1278 Quillaja saponaria
(saponins); exemption from the requirement of a tolerance.

extract

top
Residues of the biochemical pesticide Quillaja saponaria extract (saponins) are exempt from the
requirement of a tolerance in or on all food commodities.
[72 FR 41935, Aug. 1, 2007]

§ 180.1279 Zucchini yellow mosaic virus—weak strain; exemption from the
requirement of a tolerance.
top
An exemption from the requirement of a tolerance for residues of the ZYMV–WK strain in or on all raw
cucurbit when applied/used in accordance with label directions.
[74 FR 26536, June 3, 2009]

§ 180.1280 Poly(hexamethylenebiguanide) hydrochloride (PHMB); exemption from
the requirement of a tolerance.
top
Poly(hexamethylenebiguanide) hydrochloride (PHMB)(CAS Reg. No. 32289–58–0) is exempt from the
requirement of a tolerance for residues of the antimicrobial in or on all food commodities when the
residues are the result of the lawful application of a food contact surface sanitizer containing PHMB at 550
parts per million (ppm).
[73 FR 1517, Jan. 9, 2008]

§ 180.1281 S-Abscisic Acid; temporary exemption from the requirement of a
tolerance.
top
(a) S -Abscisic Acid, ( S )-5-(1-hydroxy-2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)-3-methyl-penta-(2 Z ,4 E )dienoic Acid is temporarily exempt from the requirement of a tolerance when used as a plant regulator in
or on grape in accordance with the Experimental Use Permit 73049–EUP–4. This temporary exemption

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from tolerance will expire October 1, 2010.
(b) A temporary exemption from the requirement of a tolerance is established for the residues of S Abscisic Acid, ( S )-5-(1-hydroxy-2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)-3-methyl-penta-(2 Z ,4 E )dienoic Acid when used as a plant regulator in or on grape, herbs and spices, leafy vegetables, pineapple,
pome fruit, and stone fruit in accordance with the Experimental Use Permit 73049–EUP–7. This temporary
exemption from tolerance will expire August 7, 2012.
[74 FR 37621, July 29, 2009]

§ 180.1282 Bacillus firmus I-1582; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established in/on all food/feed commodities, for
residues of Bacillus firmus I-1582 when used as a soil application or seed treatment.
[73 FR 25528, May 7, 2008]

§ 180.1283 (Z)-7,8-epoxy-2-methyloctadecane (Disparlure); exemption from the
requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for residues of (Z)-7,8-epoxy-2methyloctadecane on all food and feed crops that occur when it is used to treat trees, shrubs, and
pastures and such use results in unintentional spray and drift to non-target vegetation including non-food,
food, and feed crops. This active ingredient is also known as Disparlure.
[73 FR 33714, June 13, 2008]

§ 180.1284 Ammonium salts of higher fatty acids (C8–C18saturated; C8–
C12unsaturated); exemption from the requirement of a tolerance.
top
This regulation establishes an exemption from the requirement of a tolerance for residues of the
ammonium salts of higher fatty acids C8–C18saturated; C8–C12unsaturated on in or on all food
commodities when applied for the suppression and control of a wide variety of grasses and weeds.
[73 FR 39268, July 9, 2008]

§ 180.1285 Polyoxin D zinc salt; exemption from the requirement of a tolerance.
top
An exemption from the requirement of a tolerance is established for the residues of the biochemical
pesticide polyoxin D zinc when used as a fungicide on almonds, cucurbit vegetables, fruiting vegetables,
ginseng, grapes, pistachios, pome fruits, potatoes and strawberries.
[73 FR 69564, Nov. 19, 2008]

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§ 180.1287 Extract of Chenopodium
ambrosioides
ambrosioides
tolerance.

near
; exemption from the requirement of a

top
An exemption from the requirement of a tolerance is established for the residues of Extract of
Chenopodium ambrosioides near ambrosioides when used as an insecticide/acaricide on all food
commodities.
[74 FR 634, Jan. 7, 2009]

§ 180.1288 Tristyrylphenol ethoxylates; exemption from the requirement of a
tolerance.
top
An exemption from the requirement of a tolerance is established for residues of poly(oxy-1,2-ethanediyl), α[2,4,6-tris(1-phenylethyl)phenyl]-ω-hydroxy-, (CAS Reg. No. 70559–25–0) and poly(oxy-1,2-ethanediyl), α[tris(1-phenylethyl)phenyl]-ω-hydroxy-, (CAS Reg. No. 99734–09–5) on citrus crops, group 10, when used
as inert ingredients under the following conditions:
(a) They are applied post-harvest;
(b) They are used as inert ingredients in pesticide formulations with azoxystrobin and fludioxonil; and
(c) They constitute no more than 10.0% of the formulated pesticide product.
[74 FR 12625, Mar. 25, 2009]

§ 180.1289 Candida oleophila
exemption from the requirement of a tolerance.

Strain O;

top
An exemption from the requirement of a tolerance is established for the residues of the microbial pesticide,
Candida oleophila Strain O, on apples and pears when applied/used as a post-harvest biofungicide.
[74 FR 22464, May 13, 2009]

§ 180.1290 Pasteuria usgae
exemption from the requirement of a tolerance.

; temporary

top
Pasteuria usgae is temporarily exempt from the requirement of a tolerance when applied/used as a
nematicide on strawberries in accordance with the terms of EUP 85004-EUP-1. This temporary exemption
from the requirement of a tolerance expires and is revoked on December 31, 2010.
[74 FR 38974, Aug. 5, 2009]

Subpart E—Pesticide Chemicals Not Requiring a Tolerance or an Exemption From a
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Tolerance
top

Source: 66 FR 66772, Dec. 27, 2001, unless otherwise noted.
§ 180.2000 Scope.
top
This subpart sets forth the pesticide chemicals for use in agricultural or other food-related settings for
which neither a tolerance nor an exemption is deemed to be needed by EPA.

§ 180.2003 Definitions.
top
(a) Food uses are the uses of a pesticide chemical that are likely to yield residues in food or feed crops,
meat, milk, poultry or egg.
(b) Non-food uses are those uses that are not likely to yield residues in food or feed crops, meat, milk,
poultry or egg.
[66 FR 66772, Dec. 27, 2001, as amended at 73 FR 60158, Oct. 10, 2008]

§ 180.2010 Threshold of regulation determinations.
top
The following pesticide chemical uses on food or feed, or food or feed crops, do not need a tolerance or
exemption from the requirement of a tolerance, and may be registered under the Federal Insecticide,
Fungicide, and Rodenticide Act, 7 U.S.C. 136 et seq ., without obtaining such tolerance or exemption,
based on EPA's determination that the uses are below the threshold of regulation.

Pesticide
Chemical

CAS
Reg.
No.

Use/
Limits

Thiabendazole 148– As a seed
79–8 treatment
for dry
pea
(including
field pea,
pigeon
pea,
chickpea
or lentil),
using a
maximum
application
rate of

Analytical Method
High Performance Liquid Chromatography/Florescence
Detector method1; Modification of IonPairing Liquid
Chromatographic
Determination
of
Benzimidazole
Fungicides in
Foods
, Gilvydis and Walters, JAOAC, vol.
73, no. 5, 1990.

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0.075
pounds of
active
ingredient
per 100
pounds of
seed.
Vines or
hay grown
from
treated
seed may
not be fed
to
livestock.
1Available

from: Chief, Analytical Chemistry Branch, Environmental Science Center, 701 Mapes Rd., Ft.
Meade, MD 20755–5350; telephone number: (410) 305–2905; e-mail address: [email protected]
[73 FR 1978, Jan. 11, 2008]

§ 180.2020 Non-food determinations.
top
The following pesticide chemical uses do not need a tolerance or exemption from the requirement of a
tolerance based on EPA's determination that they are not likely to result in residues in or on food.

Pesticide Chemical
Methyl bromide

CAS Reg. No.
74–83–9

Limits
When applied as a preplant soil fumigant

Uses
All pre-plant soil uses

Potassium triiodide (KI3) 12298–68–9

When applied to
Bananas, grapes, and
growing crops in foreign melons
countries

Rhodamine B

Not to exceed 2% by
weight of the
formulated product and
60 ppm on the treated
seed

81–88–9

Dye for seed
treatment

[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]
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Electronic Code of Federal Regulations:

http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c...&rgn=div5&view=text&node=40:23.0.1.1.28&idno=40 (651 of 651) [9/8/2009 3:02:30 PM]


File Typeapplication/pdf
File TitleElectronic Code of Federal Regulations:
File Modified2009-09-08
File Created2009-09-08

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