Attachment B -40 CFR Part 180

eCFR — Code of Federal Regulations

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ELECTRONIC CODE OF FEDERAL REGULATIONS
e-CFR data is current as of December 1, 2015
Title 40 → Chapter I → Subchapter E → Part 180
Title 40: Protection of Environment
PART 180—TOLERANCES AND EXEMPTIONS FOR PESTICIDE CHEMICAL RESIDUES IN FOOD
Contents
Subpart A—Definitions and Interpretative Regulations
§180.1
§180.3
§180.4
§180.5
§180.6

Definitions and interpretations.
Tolerances for related pesticide chemicals.
Exceptions.
Zero tolerances.
Pesticide tolerances regarding milk, eggs, meat, and/or poultry; statement of policy.

Subpart B—Procedural Regulations
§180.7 Petitions proposing tolerances or exemptions for pesticide residues in or on raw agricultural commodities or
processed foods.
§180.8 Withdrawal of petitions without prejudice.
§180.9 Substantive amendments to petitions.
§180.29 Establishment, modification, and revocation of tolerance on initiative of Administrator.
§180.30 Judicial review.
§180.31 Temporary tolerances.
§180.32 Procedure for modifying and revoking tolerances or exemptions from tolerances.
§180.33 Fees.
§180.34 Tests on the amount of residue remaining.
§180.35 Tests for potentiation.
§180.40 Tolerances for crop groups.
§180.41 Crop group tables.
Subpart C—Specific Tolerances
§180.101 Specific tolerances; general provisions.
§180.103 Captan; tolerances for residues.
§180.106 Diuron; tolerances for residues.
§180.108 Acephate; tolerances for residues.
§180.111 Malathion; tolerances for residues.
§180.114 Ferbam; tolerances for residues.
§180.116 Ziram; tolerances for residues.
§180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.
§180.121 Methyl parathion; tolerances for residues.
§180.123 Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.
§180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.
§180.124 Methyl bromide; tolerances for residues.
§180.127 Piperonyl butoxide; tolerances for residues.
§180.128 Pyrethrins; tolerances for residues.
§180.129 o-Phenylphenol and its sodium salt; tolerances for residues.
§180.130 Hydrogen Cyanide; tolerances for residues.
§180.132 Thiram; tolerances for residues.
§180.142 2,4-D; tolerances for residues.
§180.145 Fluorine compounds; tolerances for residues.
§180.151 Ethylene oxide; tolerances for residues.
§180.153 Diazinon; tolerances for residues.
§180.154 Azinphos-methyl; tolerances for residues.
§180.155 1-Naphthaleneacetic acid; tolerances for residues.
§180.163 Dicofol; tolerances for residues.
§180.169 Carbaryl; tolerances for residues.

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§180.172
§180.175
§180.176
§180.178
§180.181
§180.182
§180.183
§180.184
§180.185
§180.189
§180.190
§180.191
§180.198
§180.200
§180.202
§180.204
§180.205
§180.206
§180.207
§180.208
§180.209
§180.210
§180.211
§180.212
§180.213
§180.215
§180.217
§180.220
§180.222
§180.225
§180.226
§180.227
§180.229
§180.231
§180.232
§180.235
§180.236
§180.241
§180.242
§180.243
§180.245
§180.249
§180.252
§180.253
§180.254
§180.257
§180.258
§180.259
§180.261
§180.262
§180.263
§180.269
§180.272
§180.274
§180.275
§180.276
§180.278
§180.284
§180.287
§180.288
§180.289
§180.291
§180.292
§180.293
§180.297
§180.298
§180.299
§180.300

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Dodine; tolerances for residues.
Maleic hydrazide; tolerances for residues.
Mancozeb; tolerances for residues.
Ethoxyquin; tolerances for residues.
Chlorpropham; tolerances for residues.
Endosulfan; tolerances for residues.
Disulfoton; tolerances for residues.
Linuron; tolerances for residues.
DCPA; tolerances for residues.
Coumaphos; tolerances for residues.
Diphenylamine; tolerances for residues.
Folpet; tolerances for residues.
Trichlorfon; tolerances for residues.
Dicloran; tolerances for residues.
p-Chlorophenoxyacetic acid; tolerances for residues.
Dimethoate; tolerances for residues.
Paraquat; tolerances for residues.
Phorate; tolerances for residues.
Trifluralin; tolerances for residues.
Benfluralin; tolerances for residues.
Terbacil; tolerances for residues.
Bromacil; tolerances for residues.
Propachlor; tolerances for residues.
S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.
Simazine; tolerances for residues.
Naled; tolerances for residues.
Metiram; tolerances for residues.
Atrazine; tolerances for residues.
Prometryn; tolerances for residues.
Phosphine; tolerances for residues.
Diquat; tolerances for residues.
Dicamba; tolerances for residues.
Fluometuron; tolerances for residues.
Dichlobenil; tolerances for residues.
Butylate; tolerances for residues.
Dichlorvos; tolerances for residues.
Triphenyltin hydroxide; tolerances for residues.
Bensulide; tolerances for residues.
Thiabendazole; tolerances for residues.
Propazine; tolerances for residues.
Streptomycin; tolerances for residues.
Alachlor; tolerances for residues.
Tetrachlorvinphos; tolerances for residues.
Methomyl; tolerances for residues.
Carbofuran; tolerances for residues.
Chloroneb; tolerances for residues.
Ametryn; tolerances for residues.
Propargite; tolerances for residues.
Phosmet; tolerances for residues.
Ethoprop; tolerances for residues.
Phosalone; tolerances for residues.
Aldicarb; tolerances for residues.
Tribuphos; tolerances for residues.
Propanil; tolerances for residues.
Chlorothalonil; tolerances for residues.
Formetanate hydrochloride; tolerances for residues.
Phenmedipham; tolerances for residues.
Zinc phosphide; tolerances for residues.
Amitraz; tolerances for residues.
2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.
Methanearsonic acid; tolerances for residues.
Pentachloronitrobenzene; tolerance for residues.
Picloram; tolerances for residues.
Endothall; tolerances for residues.
N-1-Naphthyl phthalamic acid; tolerances for residues.
Methidathion; tolerances for residues.
Dicrotophos; tolerances for residues.
Ethephon; tolerances for residues.

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§180.301 Carboxin; tolerances for residues.
§180.303 Oxamyl; tolerances for residues.
§180.304 Oryzalin; tolerances for residues.
§180.311 Cacodylic acid; tolerances for residues.
§180.314 Triallate; tolerances for residues.
§180.315 Methamidophos; tolerances for residues.
§180.316 Pyrazon; tolerances for residues.
§180.317 Propyzamide; tolerances for residues.
§180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.
§180.319 Interim tolerances.
§180.324 Bromoxynil; tolerances for residues.
§180.328 Napropamide; tolerances for residues.
§180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.
§180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.
§180.332 Metribuzin; tolerances for residues.
§180.337 Oxytetracycline; tolerances for residues.
§180.339 MCPA; tolerances for residues.
§180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.
§180.342 Chlorpyrifos; tolerances for residues.
§180.345 Ethofumesate; tolerances for residues.
§180.349 Fenamiphos; tolerances for residues.
§180.350 Nitrapyrin; tolerances for residues.
§180.352 Terbufos; tolerances for residues.
§180.353 Desmedipham; tolerances for residues.
§180.355 Bentazon; tolerances for residues.
§180.356 Norflurazon; tolerances for residues.
§180.360 Asulam; tolerance for residues.
§180.361 Pendimethalin; tolerances for residues.
§180.362 Fenbutatin-oxide; tolerances for residues.
§180.364 Glyphosate; tolerances for residues.
§180.367 n-Octyl bicycloheptenedicarboximide; tolerances for residues.
§180.368 Metolachlor; tolerances for residues.
§180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.
§180.371 Thiophanate-methyl; tolerances for residues.
§180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.
§180.373 [Reserved]
§180.377 Diflubenzuron; tolerances for residues.
§180.378 Permethrin; tolerances for residues.
§180.380 Vinclozolin; tolerances for residues.
§180.381 Oxyfluorfen; tolerances for residues.
§180.383 Sodium salt of acifluorfen; tolerances for residues.
§180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.
§180.385 Diclofop-methyl; tolerances for residues.
§§180.388-180.389 [Reserved]
§180.390 Tebuthiuron; tolerances for residues.
§180.395 Hydramethylnon; tolerances for residues.
§180.396 Hexazinone; tolerances for residues.
§180.399 Iprodione; tolerances for residues.
§180.401 Thiobencarb; tolerances for residues.
§180.403 Thidiazuron; tolerances for residues.
§180.404 Profenofos; tolerances for residues.
§180.405 Chlorsulfuron; tolerances for residues.
§180.407 Thiodicarb; tolerances for residues.
§180.408 Metalaxyl; tolerances for residues.
§180.409 Pirimiphos-methyl; tolerances for residues.
§180.410 Triadimefon; tolerances for residues.
§180.411 Fluazifop-P-butyl; tolerances for residues.
§180.412 Sethoxydim; tolerances for residues.
§180.413 Imazalil; tolerances for residues.
§180.414 Cyromazine; tolerances for residues.
§180.415 Aluminum tris (O-ethylphosphonate); tolerances for residues.
§180.416 Ethalfluralin; tolerances for residues.
§180.417 Triclopyr; tolerances for residues.
§180.418 Cypermethrin and isomers alpha-cypermethrin and zeta-cypermethrin; tolerances for residues.
§180.419 Chlorpyrifos-methyl; tolerances for residues.
§180.420 Fluridone; tolerances for residues.
§180.421 Fenarimol; tolerances for residues.
§180.422 Tralomethrin; tolerances for residues.

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§180.425 Clomazone; tolerances for residues.
§180.426 2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-quinoline carboxylic acid; tolerance for
residues.
§180.427 Tau-Fluvalinate; tolerances for residues.
§180.428 Metsulfuron methyl; tolerances for residues.
§180.429 Chlorimuron ethyl; tolerances for residues.
§180.430 Fenoxaprop-ethyl; tolerances for residues.
§180.431 Clopyralid; tolerances for residues.
§180.432 Lactofen; tolerances for residues.
§180.433 Fomesafen; tolerances for residues.
§180.434 Propiconazole; tolerances for residues.
§180.435 Deltamethrin; tolerances for residues.
§180.436 Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.
§180.437 Methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-p-toluate and methyl 6-(4-isopropyl-4-methyl-5-oxo-2imidazolin-2-yl)-m-toluate; tolerances for residues.
§180.438 Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for residues.
§180.439 Thifensulfuron methyl; tolerances for residues.
§180.440 Tefluthrin; tolerances for residues.
§180.441 Quizalofop ethyl; tolerances for residues.
§180.442 Bifenthrin; tolerances for residues.
§180.443 Myclobutanil; tolerances for residues.
§180.444 Sulfur dioxide; tolerances for residues.
§180.445 Bensulfuron methyl; tolerances for residues.
§180.446 Clofentezine; tolerances for residues.
§180.447 Imazethapyr; tolerances for residues.
§180.448 Hexythiazox; tolerance for residues.
§180.449 Avermectin B1 and its delta-8,9-isomer; tolerances for residues.
§180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol; tolerances for residues.
§180.451 Tribenuron methyl; tolerances for residues.
§180.452 Primisulfuron-methyl; tolerances for residues.
§180.454 Nicosulfuron; tolerances for residues.
§180.455 Procymidone; tolerances for residues.
§180.457 Bitertanol; tolerances for residues.
§180.458 Clethodim; tolerances for residues.
§180.459 Triasulfuron; tolerances for residues.
§180.460 Benoxacor; tolerances for residues.
§180.461 Cadusafos; tolerances for residues.
§180.462 Pyridate; tolerances for residues.
§180.463 Quinclorac; tolerances for residues.
§180.464 Dimethenamid; tolerances for residues.
§180.465 4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.
§180.466 Fenpropathrin; tolerances for residues.
§180.467 Carbon disulfide; tolerances for residues.
§180.468 Flumetsulam; tolerances for residues.
§180.469 Dichlormid; tolerances for residues.
§180.470 Acetochlor; tolerances for residues.
§180.471 Furilazole; tolerances for residues.
§180.472 Imidacloprid; tolerances for residues.
§180.473 Glufosinate ammonium; tolerances for residues.
§180.474 Tebuconazole; tolerances for residues.
§180.475 Difenoconazole; tolerances for residues.
§180.476 Triflumizole; tolerances for residues.
§180.477 Flumiclorac pentyl; tolerances for residues.
§180.478 Rimsulfuron; tolerances for residues.
§180.479 Halosulfuron-methyl; tolerances for residues.
§180.480 Fenbuconazole; tolerances for residues.
§180.481 Prosulfuron; tolerances for residues.
§180.482 Tebufenozide; tolerances for residues.
§180.484 Flutolanil; tolerances for residues.
§180.485 Cyproconazole; tolerances for residues.
§180.486 Chlorethoxyfos; tolerances for residues.
§180.487 Pyrithiobac sodium; tolerances for residues.
§180.490 Imazapic; tolerances for residues.
§180.491 Propylene oxide; tolerances for residues.
§180.492 Triflusulfuron-methyl; tolerances for residues.
§180.493 Dimethomorph; tolerances for residues.
§180.494 Pyridaben; tolerance for residues.
§180.495 Spinosad; tolerances for residues.

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§180.496 Thiazopyr; tolerances for residues.
§180.497 Clofencet; tolerances for residues.
§180.498 Sulfentrazone; tolerances for residues.
§180.499 Propamocarb; tolerances for residues.
§180.500 Imazapyr; tolerances for residues.
§180.501 Hydroprene; tolerances for residues.
§180.502 Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for residues.
§180.503 Cymoxanil, tolerance for residues.
§180.504 [Reserved]
§180.505 Emamectin; tolerances for residues.
§180.506 Cyclanilide; tolerances for residues.
§180.507 Azoxystrobin; tolerances for residues.
§180.509 Mefenpyr-diethyl; tolerance for residues.
§180.510 Pyriproxyfen; tolerances for residues.
§180.511 Buprofezin; tolerances for residues.
§180.512 [Reserved]
§180.513 Chlorfenapyr; tolerances for residues.
§180.514 Cloransulam-methyl; tolerances for residues.
§180.515 Carfentrazone-ethyl; tolerances for residues.
§180.516 Fludioxonil; tolerances for residues.
§180.517 Fipronil; tolerances for residues.
§180.518 Pyrimethanil; tolerances for residues.
§180.519 Bromide ion and residual bromine; tolerances for residues.
§180.521 Fumigants for grain-mill machinery; tolerances for residues.
§180.522 Fumigants for processed grains used in production of fermented malt beverage; tolerances for residues.
§180.523 Metaldehyde; tolerances for residues.
§180.525 Resmethrin; tolerances for residues.
§180.526 Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.
§180.527 Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide
and its metabolites containing the 4-fluoro-N-methylethyl benzenamine tolerances for residues.
§180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol methylcarbamate; tolerances for residues.
§180.532 Cyprodinil; tolerances for residues.
§180.533 Esfenvalerate; tolerances for residues.
§180.535 Fluroxypyr 1-methylheptyl ester; tolerances for residues.
§180.537 Isoxaflutole; tolerances for residues.
§180.539 d-Limonene; tolerances for residues.
§180.540 Fenitrothion; tolerances for residues.
§180.541 Propetamphos; tolerances for residues.
§180.543 Diclosulam; tolerances for residues.
§180.544 Methoxyfenozide; tolerances for residues.
§180.545 Prallethrin; tolerances for residues.
§180.546 Mefenoxam; tolerances for residues.
§180.547 Prohexadione calcium; tolerances for residues.
§180.548 Tralkoxydim; tolerances for residues.
§180.549 Diflufenzopyr; tolerances for residues.
§180.551 Fluthiacet-methyl; tolerances for residues.
§180.552 Sulfosulfuron; tolerances for residues.
§180.553 Fenhexamid; tolerances for residues.
§180.554 Kresoxim-methyl; tolerances for residues.
§180.555 Trifloxystrobin; tolerances for residues.
§180.556 Pymetrozine; tolerances for residues.
§180.557 Tetraconazole; tolerances for residues.
§180.559 Clodinafop-propargyl; tolerances for residues.
§180.560 Cloquintocet-mexyl; tolerances for residues.
§180.561 Acibenzolar-S-methyl; tolerances for residues.
§180.562 Flucarbazone-sodium; tolerances for residues.
§180.563 Ethametsulfuron-methyl; tolerances for residues.
§180.564 Indoxacarb; tolerances for residues.
§180.565 Thiamethoxam; tolerances for residues.
§180.566 Fenpyroximate; tolerances for residues.
§180.567 Zoxamide; tolerances for residues.
§180.568 Flumioxazin; tolerances for residues.
§180.569 Forchlorfenuron; tolerances for residues.
§180.570 Isoxadifen-ethyl; tolerances for residues.
§180.571 Mesotrione; tolerances for residues.
§180.572 Bifenazate; tolerance for residues.
§180.573 Tepraloxydim; tolerances for residues.
§180.574 Fluazinam; tolerances for residues.

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§180.575
§180.576
§180.577
§180.578
§180.579
§180.580
§180.581
§180.582
§180.583
§180.584
§180.585
§180.586
§180.587
§180.588
§180.589
§180.590
§180.591
§180.592
§180.593
§180.594
§180.595
§180.596
§180.597
§180.598
§180.599
§180.600
§180.601
§180.602
§180.603
§180.604
§180.605
§180.607
§180.608
§180.609
§180.610
§180.611
§180.612
§180.613
§180.614
§180.615
§180.616
§180.617
§180.618
§180.619
§180.620
§180.621
§180.622
§180.623
§180.624
§180.625
§180.626
§180.627
§180.628
§180.629
§180.630
§180.631
§180.632
§180.633
§180.634
§180.635
§180.636
§180.637
§180.638
§180.639
§180.640
§180.641
§180.642
§180.643

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Sulfuryl fluoride; tolerances for residues.
Cyhalofop-butyl; tolerances for residues.
Bispyribac-sodium; tolerances for residues.
Acetamiprid; tolerances for residues.
Fenamidone; tolerances for residues.
Iodosulfuron-Methyl-Sodium; tolerances for residues.
Iprovalicarb; tolerances for residues.
Pyraclostrobin; tolerances for residues.
Triticonazole; tolerances for residues.
Tolylfluanid; tolerances for residues.
Pyraflufen-ethyl; tolerances for residues.
Clothianidin; tolerances for residues.
Famoxadone; tolerance for residues.
Quinoxyfen; tolerances for residues.
Boscalid; tolerances for residues.
2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.
Trifloxysulfuron; tolerances for residues.
Butafenacil; tolerances for residues.
Etoxazole; tolerances for residues.
Thiacloprid; tolerances for residues.
Flufenpyr-ethyl; tolerances for residues.
Fosthiazate; tolerances for residues.
Mesosulfuron-methyl; tolerances for residues.
Novaluron; tolerances for residues.
Acequinocyl; tolerances for residues.
Propoxycarbazone; tolerances for residues.
Cyazofamid; tolerances for residues.
Spiroxamine; tolerances for residues.
Dinotefuran; tolerances for residues.
Mepanipyrim; tolerances for residues.
Penoxsulam; tolerances for residues.
Spiromesifen; tolerances for residues.
Spirodiclofen; tolerances for residues.
Fluoxastrobin; tolerances for residues.
Aminopyralid; tolerances for residues.
Pinoxaden; tolerances for residues.
Topramezone; tolerances for residues.
Flonicamid; tolerances for residues.
Kasugamycin; tolerances for residues.
Amicarbazone; tolerances for residues.
Fenpropimorph; tolerances for residues.
Metconazole; tolerances for residues.
Benthiavalicarb-isopropyl; tolerance for residues.
Epoxiconazole; tolerances for residues.
Etofenprox; tolerances for residues.
Dithianon; tolerances for residues.
Ethaboxam; tolerances for residues.
Flufenoxuron; tolerances for residues.
Metrafenone; tolerances for residues.
Orthosulfamuron; tolerances for residues.
Prothioconazole; tolerances for residues.
Fluopicolide; tolerances for residues.
Chlorantraniliprole; tolerances for residues.
Flutriafol; tolerances for residues.
Flusilazole; tolerances for residues.
Pyrasulfotole; tolerances for residues.
Fenazaquin; Tolerances for residues.
Florasulam; tolerances for residues.
Tembotrione; tolerances for residues.
Spinetoram; tolerances for residues.
1,3-dichloropropene; tolerances for residues.
Mandipropamid; tolerances for residues.
Pyroxsulam; tolerances for residues.
Flubendiamide; tolerances for residues.
Pyridalyl; tolerances for residues.
Spirotetramat; tolerances for residues.
Gentamicin; tolerances for residues.
Uniconazole; tolerances for residues.

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§180.644
§180.645
§180.646
§180.647
§180.648
§180.649
§180.650
§180.651
§180.652
§180.653
§180.654
§180.655
§180.656
§180.657
§180.658
§180.659
§180.660
§180.661
§180.662
§180.663
§180.664
§180.665
§180.666
§180.667
§180.668
§180.669
§180.671
§180.672
§180.673
§180.674
§180.675
§180.676
§180.677
§180.678
§180.679
§180.680
§180.681
§180.682
§180.684
§180.685
§180.686
§180.687
§180.688

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Cyprosulfamide; tolerances for residues.
Thiencarbazone-methyl; tolerances for residues.
Ipconazole; tolerances for residues.
d-Phenothrin; tolerances for residues.
Meptyldinocap; tolerances for residues.
Saflufenacil; tolerances for residues.
Isoxaben; tolerances for residues.
Imazosulfuron; tolerances for residues.
Ethiprole; tolerances for residues.
Indaziflam; tolerances for residues.
Isopyrazam; tolerances for residues.
Flazasulfuron; tolerances for residues.
Amisulbrom; tolerances for residues.
Metaflumizone; tolerances for residues.
Penthiopyrad; tolerances for residues.
Pyroxasulfone; tolerances for residues.
Pyriofenone; tolerances for residues.
Fluopyram; tolerances for residues.
Trinexapac-ethyl; tolerances for residues.
Ametoctradin; tolerances for residues.
Penflufen; tolerances for residues.
Sedaxane; tolerances for residues.
Fluxapyroxad; tolerances for residues.
Cyflufenamid, tolerance for residues.
Sulfoxaflor; tolerances for residues.
Picoxystrobin; tolerances for residues.
Fenpyrazamine; tolerances for residues.
Cyantraniliprole; tolerances for residues.
Triforine; tolerances for residues.
Proquinazid; tolerances for residues.
Tolfenpyrad; tolerances for residues.
Fenpropidin; tolerances for residues.
Cyflumetofen; tolerances for residues.
Tricyclazole; tolerances for residues.
Flupyradifurone; tolerances for residues.
Fluensulfone; tolerances for residues.
Isofetamid; tolerances for residues.
Bicyclopyrone; tolerances for residues.
Benalaxyl-M; tolerances for residues.
Oxathiapiprolin; tolerances for residues.
Benzovindiflupyr; tolerances for residues.
Teflubenzuron; tolerances for residues.
Diethofencarb; tolerance for residue.

Subpart D—Exemptions From Tolerances
§180.900 Exemptions from the requirement of a tolerance.
§180.905 Pesticide chemicals; exemptions from the requirement of a tolerance.
§180.910 Inert ingredients used pre- and post-harvest; exemptions from the requirement of a tolerance.
§180.920 Inert ingredients used pre-harvest; exemptions from the requirement of a tolerance.
§180.930 Inert ingredients applied to animals; exemptions from the requirement of a tolerance.
§180.940 Tolerance exemptions for active and inert ingredients for use in antimicrobial formulations (Food-contact
surface sanitizing solutions).
§180.950 Tolerance exemptions for minimal risk active and inert ingredients.
§180.960 Polymers; exemptions from the requirement of a tolerance.
§180.1011 Viable spores of the microorganism Bacillus thuringiensis Berliner; exemption from the requirement of a
tolerance.
§180.1016 Ethylene; exemption from the requirement of a tolerance.
§180.1017 Diatomaceous earth; exemption from the requirement of a tolerance.
§180.1019 Sulfuric acid; exemption from the requirement of a tolerance.
§180.1020 Sodium chlorate; exemption from the requirement of a tolerance.
§180.1021 Copper; exemption from the requirement of a tolerance.
§180.1022 Iodine-detergent complex; exemption from the requirement of a tolerance.
§180.1023 Propanoic acid; exemptions from the requirement of a tolerance.
§180.1025 Xylene; exemption from the requirement of a tolerance.
§180.1027 Nuclear polyhedrosis virus of Heliothis zea; exemption from the requirement of a tolerance.
§180.1033 Methoprene; exemption from the requirement of a tolerance.
§180.1037 Polybutenes; exemption from the requirement of a tolerance.

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§180.1040 Ethylene glycol; exemption from the requirement of a tolerance.
§180.1041 Nosema locustae; exemption from the requirement of a tolerance.
§180.1043 Gossyplure; exemption from the requirement of a tolerance.
§180.1049 Carbon dioxide; exemption from the requirement of a tolerance.
§180.1050 Nitrogen; exemption from the requirements of a tolerance.
§180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine; exemption from the requirement of a tolerance.
§180.1054 Calcium hypochlorite; exemptions from the requirement of a tolerance.
§180.1056 Boiled linseed oil; exemption from requirement of tolerance.
§180.1057 Phytophthora palmivora; exemption from requirement of tolerance.
§180.1058 Sodium diacetate; exemption from the requirement of a tolerance.
§180.1064 Tomato pinworm insect pheromone; exemption from the requirement of a tolerance.
§180.1065 2-Amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one; exemption from the requirement
of a tolerance.
§180.1067 Methyl eugenol and malathion combination; exemption from the requirement of a tolerance.
§180.1068 C12-C18 fatty acid potassium salts; exemption from the requirement of a tolerance.
§180.1069 (Z)-11-Hexadecenal; exemption from the requirement of a tolerance.
§180.1070 Sodium chlorite; exemption from the requirement of a tolerance.
§180.1071 Peanuts, Tree Nuts, Milk, Soybeans, Eggs, Fish, Crustacea, and Wheat; exemption from the requirement of a
tolerance.
§180.1072 Poly-D-glucosamine (chitosan); exemption from the requirement of a tolerance.
§180.1073 Isomate-M; exemption from the requirement of a tolerance.
§180.1074 F.D.&C. Blue No. 1; exemption from the requirement of a tolerance.
§180.1075 Colletotrichum gloeosporioides f. sp. aeschynomene; exemption from the requirement of a tolerance.
§180.1076 Viable spores of the microorganism Bacillus popilliae; exemption from the requirement of a tolerance.
§180.1080 Plant volatiles and pheromone; exemptions from the requirement of a tolerance.
§180.1083 Dimethyl sulfoxide; exemption from the requirement of a tolerance.
§180.1084 Monocarbamide dihydrogen sulfate; exemption from the requirement of a tolerance.
§180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11-trimethyl-2,6,10-dodecatriene-3-ol; exemption from the
requirement of a tolerance.
§180.1087 Sesame stalks; exemption from the requirement of a tolerance.
§180.1089 Poly-N-acetyl-D-glucosamine; exemption from the requirement of tolerance.
§180.1090 Lactic acid; exemption from the requirement of a tolerance.
§180.1091 Aluminum isopropoxide and aluminum secondary butoxide; exemption from the requirement of a tolerance.
§180.1092 Menthol; exemption from the requirement of a tolerance.
§180.1095 Chlorine gas; exemptions from the requirement of a tolerance.
§180.1097 GBM-ROPE; exemption from the requirement of a tolerance.
§180.1098 Gibberellins [Gibberellic Acids (GA3 and GA4 + GA7), and Sodium or Potassium Gibberellate]; exemption
from the requirement of a tolerance.
§180.1100 Gliocladium virens isolate GL-21; exemption from the requirement of a tolerance.
§180.1101 Parasitic (parasitoid) and predatory insects; exemption from the requirement of a tolerance.
§180.1102 Trichoderma harzianum KRL-AG2 (ATCC #20847) strain T-22; exemption from requirement of a tolerance.
§180.1103 Isomate-C; exemption from the requirement of a tolerance.
§180.1107 Delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed Pseudomonas fluorescens;
exemption from the requirement of a tolerance.
§180.1108 Delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed Pseudomonas
fluorescens; exemption from the requirement of a tolerance.
§180.1110 3-Carbamyl-2,4,5-trichlorobenzoic acid; exemption from the requirement of a tolerance.
§180.1111 Bacillus subtilis GB03; exemption from the requirement of a tolerance.
§180.1113 Lagenidium giganteum; exemption from the requirement of a tolerance.
§180.1114 Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and Pseudomonas syringae 742RS;
exemptions from the requirement of a tolerance.
§180.1118 Spodoptera exigua nuclear polyhedrosis virus; exemption from the requirement of a tolerance.
§180.1119 Azadirachtin; exemption from the requirement of a tolerance.
§180.1120 Streptomyces sp. strain K61; exemption from the requirement of a tolerance.
§180.1121 Boric acid and its salts, borax (sodium borate decahydrate), disodium octaborate tetrahydrate, boric oxide
(boric anhydride), sodium borate and sodium metaborate; exemptions from the requirement of a tolerance.
§180.1122 Inert ingredients of semiochemical dispensers; exemptions from the requirement of a tolerance.
§180.1124 Arthropod pheromones; exemption from the requirement of a tolerance.
§180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; exemption from the requirement of a tolerance.
§180.1127 Biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde, cinnamyl alcohol,
4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole, and 1,2,4-trimethoxybenzene;
exemptions from the requirement of a tolerance.
§180.1128 Bacillus subtilis MBI 600; exemption from the requirement of a tolerance.
§180.1130 N-(n-octyl)-2-pyrrolidone and N-(n-dodecyl)-2-pyrrolidone; exemptions from the requirement of a tolerance.
§180.1131 Ampelomyces quisqualis isolate M10; exemption from the requirement of a tolerance.
§180.1135 Pasteuria penetrans; exemption from the requirement of a tolerance.
§180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of a tolerance.
§180.1140 Sodium o-nitrophenolate; exemption from the requirement of a tolerance.

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§180.1141 Sodium p-nitrophenolate; exemption from the requirement of a tolerance.
§180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of a tolerance.
§180.1143 Methyl anthranilate; exemption from the requirement of a tolerance.
§180.1144 Candida oleophila isolate I-182; exemption from the requirement of a tolerance.
§180.1145 Pseudomonas syringae; exemption from the requirement of a tolerance.
§180.1146 Beauveria bassiana Strain GHA; exemption from the requirement of a tolerance.
§180.1148 Occlusion Bodies of the Granulosis Virus of Cydia pomenella; tolerance exemption.
§180.1149 Inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha falcifera; exemption from the
requirement of a tolerance.
§180.1150 6-Benzyladenine; exemption from the requirement of a tolerance.
§180.1153 Lepidopteran pheromones; exemption from the requirement of a tolerance.
§180.1154 CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki encapsulated in killed
Pseudomonas fluorescens, and the expression plasmid and cloning vector genetic constructs.
§180.1156 Cinnamaldehyde; exemption from the requirement of a tolerance.
§180.1157 Cytokinins; exemption from the requirement of a tolerance.
§180.1158 Auxins; exemption from the requirement of a tolerance.
§180.1159 Pelargonic acid; exemption from the requirement of tolerances.
§180.1160 Jojoba oil; exemption from the requirement of a tolerance.
§180.1161 Clarified hydrophobic extract of neem oil; exemption from the requirement of a tolerance.
§180.1162 Acrylate polymers and copolymers; exemption from the requirement of a tolerance.
§180.1163 Killed Myrothecium verrucaria; exemption from the requirement of a tolerance.
§180.1165 Capsaicin; exemption from the requirement of a tolerance.
§180.1167 Allyl isothiocyanate as a component of food grade oil of mustard; exemption from the requirement of a
tolerance.
§180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance.
§180.1177 Potassium bicarbonate; exemption from the requirement of a tolerance.
§180.1178 Formic acid; exemption from the requirement of a tolerance.
§180.1179 Plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and Rhizophoria mangle;
exemption from the requirement of a tolerance.
§180.1180 Kaolin; exemption from the requirement of a tolerance.
§180.1181 Bacillus cereus strain BPO1; exemption from the requirement of a tolerance.
§180.1187 L-glutamic acid; exemption from the requirement of a tolerance.
§180.1188 Gamma aminobutyric acid; exemption from the requirement of a tolerance.
§180.1189 Methyl salicylate; exemption from the requirement of a tolerance.
§180.1191 Ferric phosphate; exemption from the requirement of a tolerance.
§180.1193 Potassium dihydrogen phosphate; exemption from the requirement of a tolerance.
§180.1195 Titanium dioxide.
§180.1196 Peroxyacetic acid; exemption from the requirement of a tolerance.
§180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance.
§180.1198 Gliocladium catenulatum strain J1446; exemption from the requirement of a tolerance.
§180.1199 Lysophosphatidylethanolamine (LPE); exemption from the requirement of a tolerance.
§180.1200 Pseudomonas fluorescens strain PRA-25; temporary exemption from the requirement of a tolerance.
§180.1201 Trichoderma harzianum strain T-39; exemption from the requirement of a tolerance.
§180.1202 Bacillus sphaericus; exemption from the requirement of a tolerance.
§180.1204 Harpin protein; exemption from the requirement of a tolerance.
§180.1205 Beauveria bassiana ATCC #74040; exemption from the requirements of a tolerance.
§180.1206 Aspergillus flavus AF36; exemption from the requirement of a tolerance.
§180.1207 N-acyl sarcosines and sodium N-acyl sarcosinates; exemption from the requirement of a tolerance.
§180.1209 Bacillus subtilis strain QST 713 and strain QST 713 variant soil; exemption from the requirement of a
tolerance.
§180.1210 Phosphorous acid; exemption from the requirement of a tolerance.
§180.1212 Pseudomonas chlororaphis Strain 63-28; exemption from the requirement of a tolerance.
§180.1213 Coniothyrium minitans strain CON/M/91-08; exemption from the requirement of a tolerance.
§180.1218 Indian Meal Moth Granulosis Virus; exemption from the requirement of a tolerance.
§180.1219 Foramsulfuron; exemption from the requirement of a tolerance.
§180.1220 1-Methylcyclopropene; exemption from the requirement of a tolerance.
§180.1221 Pseudozyma flocculosa strain PF-A22 UL; exemption from the requirement of a tolerance.
§180.1222 Sucrose octanoate esters; exemption from the requirement of a tolerance.
§180.1223 Imazamox; exemption from the requirement of a tolerance.
§180.1224 Bacillus pumilus GB34; exemption from the requirement of a tolerance.
§180.1225 Decanoic acid; exemption from the requirement of a tolerance.
§180.1226 Bacillus pumilus strain QST2808; temporary exemption from the requirement of a tolerance.
§180.1228 Diallyl sulfides; exemption from the requirement of a tolerance.
§180.1230 Ferrous sulfate; exemption from the requirement of a tolerance.
§180.1231 Lime; exemption from the requirement of a tolerance.
§180.1232 Lime-sulfur; exemption from the requirement of a tolerance.
§180.1233 Potassium sorbate; exemption from the requirement of a tolerance.
§180.1234 Sodium carbonate; exemption from the requirement of a tolerance.

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§180.1235 Sodium hypochlorite; exemption from the requirement of a tolerance.
§180.1236 Sulfur; exemption from the requirement of a tolerance.
§180.1237 Sodium metasilicate; exemption from the requirement of a tolerance.
§180.1240 Thymol; exemption from the requirement of a tolerance.
§180.1241 Eucalyptus oil; exemption from the requirement of a tolerance.
§180.1243 Bacillus subtilis var. amyloliquefaciens strain FZB24; exemption from the requirement of a tolerance.
§180.1244 Ammonium bicarbonate; exemption from the requirement of a tolerance.
§180.1245 Rhamnolipid biosurfactant; exemption from the requirement of a tolerance.
§180.1246 Yeast Extract Hydrolysate from Saccharomyces cerevisiae: exemption from the requirement of a tolerance.
§180.1248 Exemption of citronellol from the requirement of a tolerance.
§180.1250 C8, C10, and C12 fatty acid monoesters of glycerol and propylene glycol; exemption from the requirement of
a tolerance.
§180.1251 Geraniol; exemption from the requirement of a tolerance.
§180.1253 Streptomyces lydicus WYEC 108; exemption from the requirement of a tolerance.
§180.1254 Aspergillus flavus NRRL 21882; exemption from the requirement of a tolerance.
§180.1255 Bacillus pumilus strain QST 2808; exemption from the requirement of a tolerance.
§180.1256 Alternaria destruens strain 059; exemption from the requirement of a tolerance.
§180.1257 Paecilomyces lilacinus strain 251; exemption from the requirement of a tolerance.
§180.1258 Acetic acid; exemption from the requirement of a tolerance.
§180.1259 Reynoutria sachalinensis extract; exemption from the requirement of a tolerance.
§180.1260 Muscodor albus QST 20799 and the volatiles produced on rehydration; exemption from the requirement of a
tolerance.
§180.1261 Xanthomonas campestris pv. vesicatoria and Pseudomonas syringae pv. tomato specific Bacteriophages.
§180.1262 Sorbitol octanoate; exemption from the requirement of a tolerance.
§180.1263 Tetrahydrofurfuryl alcohol; exemption from the requirement of a tolerance.
§180.1267 Pantoea agglomerans strain C9-1; exemption from the requirement of a tolerance.
§180.1268 Potassium silicate; exemption from the requirement of a tolerance.
§180.1269 Bacillus mycoides isolate J; exemption from the requirement of a tolerance.
§180.1270 Isophorone; exemption from the requirement of a tolerance.
§180.1271 Eucalyptus oil; exemption from the requirement of a tolerance.
§180.1272 Pantoea agglomerans strain E325; exemption from the requirement of a tolerance.
§180.1273 Beauveria bassiana HF23; exemption from the requirement of a tolerance.
§180.1274 Tris (2-ethylhexyl) phosphate; exemption from the requirement of a tolerance.
§180.1275 Pythium; exception from the requirement of a tolerance.
§180.1276 Tobacco mild green mosaic tobamovirus strain U2; exemption from the requirement of a tolerance.
§180.1277 Dibasic esters; exemption from the requirement of a tolerance.
§180.1278 Quillaja saponaria extract (saponins); exemption from the requirement of a tolerance.
§180.1279 Zucchini yellow mosaic virus—weak strain; exemption from the requirement of a tolerance.
§180.1280 Poly(hexamethylenebiguanide) hydrochloride (PHMB); exemption from the requirement of a tolerance.
§180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy-2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)-3-methyl-penta-(2Z,4E)-dienoic
Acid; exemption from the requirement of a tolerance.
§180.1282 Bacillus firmus I-1582; exemption from the requirement of a tolerance.
§180.1283 (Z)-7,8-epoxy-2-methyloctadecane (Disparlure); exemption from the requirement of a tolerance.
§180.1284 Ammonium salts of higher fatty acids (C8-C18 saturated; C8-C12 unsaturated); exemption from the requirement
of a tolerance.
§180.1285 Polyoxin D zinc salt; exemption from the requirement of a tolerance.
§180.1287 Extract of Chenopodium ambrosioides near ambrosioides; exemption from the requirement of a tolerance.
§180.1288 Tristyrylphenol ethoxylates; exemption from the requirement of a tolerance.
§180.1289 Candida oleophila Strain O; exemption from the requirement of a tolerance.
§180.1290 Pasteuria usgae; exemption from the requirement of a tolerance.
§180.1291 Cold pressed neem oil; exemption from the requirement of a tolerance.
§180.1292 Ulocladium oudemansii (U3 Strain); exemption from the requirement of a tolerance.
§180.1293 Trichoderma gamsii strain ICC 080; exemption from the requirement of a tolerance.
§180.1294 Trichoderma asperellum strain ICC 012; exemption from the requirement of a tolerance.
§180.1295 Laminarin; exemption from the requirement of a tolerance.
§180.1296 Terpene Constituents α-terpinene, d-limonene and p-cymene, of the Extract of Chenopodium ambrosioides
near ambrosioides as Synthetically Manufactured; exemption from the requirement of a tolerance.
§180.1297 Homobrassinolide; exemption from the requirement of a tolerance.
§180.1298 Trichoderma hamatum isolate 382; exemption from the requirement of a tolerance.
§180.1299 Prohydrojasmon; exemption from the requirement of a tolerance.
§180.1300 Potassium hypochlorite; exemption from the requirement of a tolerance.
§180.1301 Escherichia coli O157:H7 specific bacteriophages; temporary exemption from the requirement of a tolerance.
§180.1302 Sodium Ferric Ethylenediaminetetraacetate (EDTA); exemption from the requirement of a tolerance.
§180.1303 Metarhizium anisopliae strain F52; exemption from the requirement of a tolerance.
§180.1304 Pseudomonas fluorescens strain CL145A; exemption from the requirement of a tolerance.
§180.1305 Chromobacterium subtsugae strain PRAA4-1; exemption from the requirement of a tolerance.
§180.1306 Isaria fumosorosea (formerly Paecilomyces fumosoroseus) Apopka strain 97; exemption from the requirement
of a tolerance.

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§180.1307 Bacteriophage of Clavibacter michiganensis subspecies michiganensis; exemption from the requirement of a
tolerance.
§180.1308 Bacillus amyloliquefaciens strain D747; exemption from the requirement of a tolerance.
§180.1309 Bacillus subtilis strain CX-9060; exemption from the requirement of a tolerance.
§180.1310 Trichoderma virens strain G-41; exemption from the requirement of a tolerance.
§180.1311 Pasteuria nishizawae—Pn1; exemption from the requirement of a tolerance.
§180.1312 Aureobasidium pullulans strains DSM 14940 and DSM 14941; exemption from the requirement of a tolerance.
§180.1313 Bacillus pumilus strain GHA 180; exemption from the requirement of a tolerance.
§180.1314 Killed, nonviable Streptomyces acidiscabies strain RL-110; exemption from the requirement of a tolerance.
§180.1315 Natamycin; exemption from the requirement of a tolerance.
§180.1316 Pasteuria spp. (Rotylenchulus reniformis nematode)—Pr3; exemption from the requirement of a tolerance.
§180.1317 Pesticide chemicals; exemption from the requirements of a tolerance.
§180.1318 3-decen-2-one; exemption from the requirement of a tolerance.
§180.1319 Banda de Lupinus albus doce (BLAD); exemption from the requirement of a tolerance.
§180.1320 Methyl jasmonate; exemption from the requirement of a tolerance.
§180.1321 Complex Polymeric Polyhydroxy Acids; exemption from the requirement of a tolerance.
§180.1322 Bacillus pumilus strain BU F-33; exemption from the requirement of a tolerance.
§180.1323 Ethyl-2E,4Z-decadienoate (Pear Ester); exemption from the requirement of a tolerance.
§180.1324 GS-omega/kappa-Hxtx-Hv1a; exemption from the requirement of a tolerance.
§180.1325 Heat-killed Burkholderia spp. strain A396 cells and spent fermentation media exemption from the requirement
of a tolerance.
§180.1326 Pseudomonas fluorescens strain D7; exemption from the requirement of a tolerance.
§180.1327 Tetraacetylethylenediamine (TAED) and its metabolite Diacetylethylenediamine (DAED); exemption from the
requirement of a tolerance.
§180.1328 Beauveria bassiana strain ANT-03; exemption from the requirement of a tolerance.
§180.1329 Bacillus subtilis strain IAB/BS03, exemption from the requirement of a tolerance.
§180.1330 1-Octanol; exemption from the requirement of a tolerance.
§180.1331 Trichoderma asperelloides strain JM41R; exemption from the requirement of a tolerance.
§180.1332 Lavandulyl senecioate; exemption from the requirement of a tolerance.
§180.1333 Potassium Salts of Hops Beta acids; exemption from the requirement of a tolerance.
Subpart E—Pesticide Chemicals Not Requiring a Tolerance or an Exemption From a Tolerance
§180.2000
§180.2003
§180.2010
§180.2020

Scope.
Definitions.
Threshold of regulation determinations.
Non-food determinations.

AUTHORITY: 21 U.S.C. 321(q), 346a and 371.
SOURCE: 36 FR 22540, Nov. 25, 1971, unless otherwise noted.
EDITORIAL NOTE: Nomenclature changes to part 180 appear at 62 FR 66023, Dec. 17, 1997.

GLOSSARY
NOTE: The items in this glossary were compiled as an aid to the users of the Code of Federal Regulations. Inclusion or
exclusion from this glossary has no legal significance.
APPLI = APPLICATION
C-I MET = CHOLINESTERASE-INHIBITING METABOLITES
CARB = CARBAMATES
EPWRR = EDIBLE PORTION WITH RIND REMOVED
EXC = EXCEPT
I (IN PPM COLUMN) = INTERIM TOLERANCE
INC = INCLUDING
K = CWHR = KERNEL PLUS COB WITH HUSK REMOVED
MBYP = MEAT BYPRODUCTS
MIN = MINIMUM
N (IN PPM COLUMN) = NEGLIGIBLE RESIDUES
NMT = NOT MORE THAN
NON-PER BAG/PKGD RAC = NON-PERISHABLE PACKAGED OR BAGGED RAW AGRICULTURAL COMMODITY

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PPM = PART(S) PER MILLION
POST-H = POSTHARVEST APPLICATION
PRE-H = PREHARVEST APPLICATION
PRE-S = PRESLAUGHTER APPLICATION
PRODS = PRODUCTS rollert
T (IN PPM COLUMN) = TEMPORARY TOLERANCE
[41 FR 4537, Jan. 30, 1976]

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Subpart A—Definitions and Interpretative Regulations
Back to Top
§180.1 Definitions and interpretations.
(a) Administrator, without qualification, means the Administrator of the Environmental Protection Agency.
(b) Agency, without qualification, means the Environmental Protection Agency.
(c) FFDCA means the Federal Food, Drug, and Cosmetic Act, as amended, 21 U.S.C. 301-392.
(d) Raw agricultural commodities include, among other things, fresh fruits, whether or not they have been washed and
colored or otherwise treated in their unpeeled natural form; vegetables in their raw or natural state, whether or not they
have been stripped of their outer leaves, waxed, prepared into fresh green salads, etc.; grains, nuts, eggs, raw milk,
meats, and similar agricultural produce. It does not include foods that have been processed, fabricated, or manufactured
by cooking, freezing, dehydrating, or milling.
(e) Where a raw agricultural commodity bearing a pesticide chemical residue that has been exempted from the
requirement of a tolerance, or which is within a tolerance permitted under FFDCA section 408, is used in preparing a
processed food, the processed food will not be considered unsafe within the meaning of FFDCA sections 402 and 408(a),
despite the lack of a tolerance or exemption for the pesticide chemical residue in the processed food, if:
(1) The pesticide chemical has been used in or on the raw agricultural commodity in conformity with a tolerance under
this section;
(2) The pesticide chemical residue has been removed to the extent possible in good manufacturing practice; and
(3) The concentration of the pesticide chemical residue in the processed food is not greater than the tolerance
prescribed for the pesticide chemical residue on the raw agricultural commodity.
(f) For the purpose of computing fees as required by §180.33, each group of related crops listed in §180.34(e) and
each crop group or subgroup listed in §180.41 is counted as a single raw agricultural commodity in a petition or request for
tolerances or exemption from the requirement of a tolerance.
(g) Tolerances and exemptions established for pesticide chemicals in or on the general category of raw agricultural
commodities listed in column A apply to the corresponding specific raw agricultural commodities listed in column B.
However, a tolerance or exemption for a specific commodity in column B does not apply to the general category in column
A.
A
Alfalfa
Banana
Bean

Bean, dry
Bean,
succulent
Blackberry

Broccoli
Cabbage
Caneberry

B
Medicago sativa L. Subsp. sativa, (alfalfa, lucerne); Onobrychis viciifolia Scop. (sainfoin, holy clover, esparcet); and Lotus corniculatus L.
(trefoil); and varieties and/or hybrids of these.
Banana, plantain.
Cicer arietinum (chickpea, garbanzo bean); Lupinus spp. (including sweet lupine, white sweet lupine, white lupine, and grain lupine).
Phaseolus spp. (including kidney bean, lima bean, mung bean, navy bean, pinto bean, snap bean, and waxbean; Vicia faba (broad bean, fava
bean); Vigna spp. (including asparagus bean, blackeyed pea and cowpea).
All beans above in dry form only.
All beans above in succulent form only.
Rubus eubatus (including bingleberry, black satin berry, boysenberry Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry,
darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry,
marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangerberry, ravenberry, rossberry, Shawnee blackberry,
and varieties and/or hybrids of these).
Broccoli, chinese broccoli (gia lon, white flowering broccoli).
Cabbage, Chinese cabbage (tight-heading varieties only).
Rubus spp. (including blackberry);
Rubus caesius (youngberry);

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Rubus loganbaccus (loganberry);
Rubus idaeus (red and black raspberry); cultivars, varieties, and/or hybrids of these.
Celery
Celery, Florence fennel (sweet anise, sweet fennel, finochio) (fresh leaves and stalks only).
Cherry
Cherry, sweet, and cherry, tart.
Endive
Endive, escarole.
Fruit, citrus
Grapefruit, lemon, lime, orange, tangelo, tangerine, citrus citron, kumquat, and hybrids of these.
Garlic
Garlic, great headed; garlic, and serpent garlic.
Lettuce
Lettuce, head; and lettuce, leaf
Lettuce, head Lettuce, head; crisphead varieties only
Lettuce, leaf Lettuce, leaf; cos (romaine), butterhead varieties
Marjoram
Origanum spp. (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram).
Melon
Muskmelon, including hybrids and/or varieties of Cucumis melo (including true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw
melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon); and
watermelon, including hybrids and/or varieties of (Citrullus spp.).
Muskmelon
Cucumis melo (includes true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Persian
melon, golden pershaw melon, mango melon, pineapple melon, snake melon, and other varieties and/or hybrids of these.)
Onion
Bulb onion; green onion; and garlic.
Onion, bulb
Bulb onion; garlic; great headed garlic; serpent garlic; Chinese onion; pearl onion; potato onion; and shallot, bulb.
Onion, green Green onion; lady's leek; leek; wild leek; Beltsville bunching onion; fresh onion; tree onion, tops; Welsh onion; and shallot, fresh leaves.
Peach
Peach, nectarine
Pea
Cajanus cajan (includes pigeon pea); Cicer spp. (includes chickpea and garbanzo bean); Lens culinaris (lentil); Pisum spp. (includes dwarf
pea, garden pea, green pea, English pea, field pea, and edible pod pea). [Note: A variety of pesticide tolerances have been previously
established for pea and/or bean. Chickpea/garbanzo bean is now classified in both the bean and the pea categories. For garbanzo
bean/chickpea only, the highest established pea or bean tolerance will apply to pesticide residues found in this commodity.]
Pea, dry
All peas in dry form only.
Pea, succulent All peas in succulent form only.
Pepper
All varieties of pepper including pimento and bell, hot, and sweet pepper.
Radish,
Raphanus sativus var. longipinnatus (roots and tops), including Chinese or Japanese radish (both white and red), winter radish, daikon, lobok,
oriental, roots lo pak, and other cultivars and/or hybrids of these.
Radish,
Raphanus sativus var. longipinnatus (roots and tops), including Chinese or Japanese radish (both white and red), winter radish, daikon, lobok,
oriental, tops) lo pak, and other cultivars and/or hybrids of these.
Rapeseed
Brassica napus, B. campestris, and Crambe abyssinica (oilseed-producing varieties only which include canola and crambe.)
Raspberry
Rubus spp. (including bababerry; black raspberry; blackcap; caneberry; framboise; frambueso; himbeere; keriberry; mayberry; red raspberry;
thimbleberry; tulameen; yellow raspberry; and cultivars, varieties, and/or hybrids of these).
Sorghum,
Sorghum spp. [sorghum, grain, sudangrass (seed crop), and hybrids of these grown for its seed].
grain, grain
Sorghum,
Sorghum spp. [sorghum, forage; sorghum, stover; sudangrass, and hybrids of these grown for forage and/or stover.
forage, stover
Squash
Pumpkin, summer squash, and winter squash.
Sugar apple Annona squamosa L. (sugar apple, sweetsop, anon), and its hybrid A. squamosa L. x A. cherimoya M. (atemoya). Also A. reticulata L. (true
custard apple).
Squash,
Fruits of the gourd (Cucurbitaceae) family that are consumed when immature, 100% of the fruit is edible either cooked or raw, once picked it
summer
cannot be stored, has a soft rind which is easily penetrated, and if seeds were harvested they would not germinate; e.g., Cucurbita pepo (i.e.,
crookneck squash, straightneck squash, scallop squash, and vegetable marrow); Lagenaria spp. (i.e., spaghetti squash, hyotan, cucuzza);
Luffa spp. (i.e., hechima, Chinese okra); Momordica spp. (i.e., bitter melon, balsam pear, balsam apple, Chinese cucumber); Sechium edule
(chayote); and other cultivars and/or hybrids of these.
Sweet potato Sweet potato, yam.
Tangerine
Tangerine (mandarin or mandarin orange); clementine; Mediterranean mandarin; satsuma mandarin; tangelo; tangor; cultivars, varieties,
and/or hybrids of these.
Tomato
Tomato, tomatillo.
Turnip tops or Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip greens).
turnip greens
Wheat
Wheat, triticale.

(h) Unless otherwise specified in this paragraph or in tolerance regulations prescribed in this part for specific pesticide
chemicals, the raw agricultural commodity or processed food to be examined for pesticide residues, shall consist of the
whole raw agricultural commodity or processed food.
(1) The raw agricultural commodity bananas, when examined for pesticide residues, shall not include any crown
tissue or stalk.
(2) Shell shall be removed and discarded from nuts before examination for pesticide residues.
(3) Caps (hulls) shall be removed and discarded from strawberries before examination for pesticide residues.
(4) Stems shall be removed and discarded from melons before examination for pesticide residues.
(5) Roots, stems, and outer sheaths (or husks) shall be removed and discarded from garlic bulbs and dry bulb onions,
and only the garlic cloves and onion bulbs shall be examined for pesticide residues.
(6) Where a tolerance is established on a root vegetable including tops and/or with tops, and the tops and the roots
are marketed together, they shall be analyzed separately and neither the pesticide residue on the roots nor the pesticide
residue on the tops shall exceed the tolerance level, except that in the case of carrots, parsnips, and rutabagas, the tops
shall be removed and discarded before analyzing roots for pesticide residues.

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(7) The crowns (leaves at the top of the fruit) shall be removed and discarded from pineapples before examination for
pesticide residues.
(8) The term lima beans means the beans and the pod.
(9) The term peanuts means the peanut meat after removal of the hulls.
(10) For processed foods consisting primarily of one ingredient and sold in a form requiring further preparation prior to
consumption (e.g., fruit juice concentrates, dehydrated vegetables, and powdered potatoes), the processed food to be
examined for residues shall be the whole processed commodity after compensating for or reconstituting to the
commodity's normal moisture content, unless a tolerance for the concentrated or dehydrated food form is included in this
part. If there exists a tolerance for a specific pesticide on the processed food in its concentrated or dehydrated food form,
for the purpose of determining whether the food is in compliance with that tolerance, the processed food to be examined
for residues shall be the whole processed commodity on an “as is” basis.
(i) The term pesticide chemical shall have the meaning specified in FFDCA section 201(q)(1), as amended, except as
provided in §180.4.
(j) The term negligible residue means any amount of a pesticide chemical remaining in or on a raw agricultural
commodity or group of raw agricultural commodities that would result in a daily intake regarded as toxicologically
insignificant on the basis of scientific judgment of adequate safety data. Ordinarily this will add to the diet an amount which
will be less than 1/2,000th of the amount that has been demonstrated to have no effect from feeding studies on the most
sensitive animal species tested. Such toxicity studies shall usually include at least 90-day feeding studies in two species of
mammals.
(k) The term nonperishable raw agricultural commodity means any raw agricultural commodity not subject to rapid
decay or deterioration that would render it unfit for consumption. Examples are cocoa beans, coffee beans, field-dried
beans, field-dried peas, grains, and nuts. Not included are eggs, milk, meat, poultry, fresh fruits, and vegetables such as
onions, parsnips, potatoes, and carrots.
(l) The term tolerance with regional registration means any tolerance which is established for pesticide residues
resulting from the use of the pesticide pursuant to a regional registration. Such a tolerance is supported by residue data
from specific growing regions for a raw agricultural commodity. Individual tolerances with regional registration are
designated in separate subsections in 40 CFR 180.101 through 180.999, as appropriate. Additional residue data which are
representative of the proposed use area are required to expand the geographical area of usage of a pesticide on a raw
agricultural commodity having an established “tolerance with regional registration.” Persons seeking geographically
broader registration of a crop having a “tolerance with regional registration” should contact the appropriate EPA product
manager concerning additional residue data required to expand the use area.
(m) The term pesticide chemical residue shall have the meaning specified in FFDCA section 201(q)(2), as amended,
except as provided in §180.4.
(n) The term food commodity means:
(1) Any raw agricultural commodity (food or feed) as defined in section 201(r) of the Federal Food, Drug, and
Cosmetic Act (FFDCA); and
(2) Any processed food or feed as defined in section 201(gg) of the FFDCA.
[36 FR 22540, Nov. 25, 1971]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.1, see the List of CFR Sections Affected, which appears in the
Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.3 Tolerances for related pesticide chemicals.
(a) Pesticide chemicals that cause related pharmacological effects will be regarded, in the absence of evidence to the
contrary, as having an additive deleterious action. (For example, many pesticide chemicals within each of the following
groups have related pharmacological effects: Chlorinated organic pesticides, arsenic-containing chemicals, metallic
dithiocarbamates, cholinesterase-inhibiting pesticides.)
(b) Tolerances established for such related pesticide chemicals may limit the amount of a common component (such
as As2O3) that may be present, or may limit the amount of biological activity (such as cholinesterase inhibition) that may
be present, or may limit the total amount of related pesticide chemicals (such as chlorinated organic pesticides) that may
be present.
(c)(1) Where tolerances for inorganic bromide in or on the same raw agricultural commodity are set in two or more
sections in this part (example: §§180.123 and 180.199), the overall quantity of inorganic bromide to be tolerated from use

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of the same pesticide in different modes of application or from two or more pesticide chemicals for which tolerances are
established is the highest of the separate applicable tolerances. For example, where the bromide tolerance on asparagus
from methyl bromide commodity fumigation is 100 parts per million (40 CFR 180.123) and on asparagus from methyl
bromide soil treatment is 300 parts per million (40 CFR 180.199), the overall inorganic bromide tolerance for asparagus
grown on methyl bromide-treated soil and also fumigated with methyl bromide after harvest is 300 parts per million.
(2) Where tolerances are established in terms of inorganic bromide residues only from use of organic bromide
fumigants on raw agricutural commodities, such tolerances are sufficient to protect the public health, and no additional
concurrent tolerances for the organic pesticide chemicals from such use are necessary. This conclusion is based on
evidence of the dissipation of the organic pesticide or its conversion to inorganic bromide residues in the food when ready
to eat.
(d)(1) Where tolerances are established for both calcium cyanide and hydrogen cyanide on the same raw agricultural
commodity, the total amount of such pesticides shall not yield more residue than that permitted by the larger of the two
tolerances, calculated as hydrogen cyanide.
(2) Where tolerances are established for residues of both O,O-diethyl S-[2-(ethylthio)ethyl] phosphorodithioate and
demeton (a mixture of O,O-diethyl O-(and S-) [2-(ethylthio)ethyl] phosphorothioates) on the same raw agricultural
commodity, the total amount of such pesticides shall not yield more residue than that permitted by the larger of the two
tolerances, calculated as demeton.
(3) Where tolerances are established for both terpene polychlorinates (chlorinated mixture of camphene, pinene, and
related terpenes, containing 65-66 percent chlorine) and toxaphene (chlorinated camphene containing 67-69 percent
chlorine) on the same raw agricultural commodities, the total amount of such pesticides shall not yield more residue than
that permitted by the larger of the two tolerances, calculated as a chlorinated terpene of molecular weight 396.6 containing
67 percent chlorine.
(4) Where a tolerance is established for more than one pesticide containing arsenic found in, or on a raw agricultural
commodity, the total amount of such pesticide shall not exceed the highest established tolerance calculated as As2O3.
(5) Where tolerances are established for more than one member of the class of dithiocarbamates listed in paragraph
(e)(3) of this section on the same raw agricultural commodity, the total residue of such pesticides shall not exceed that
permitted by the highest tolerance established for any one member of the class, calculated both as zinc
ethylenebisdithiocarbamate and carbon disulfide. The tolerance based on zinc ethylenebisdithiocarbamate shall first be
multiplied by 0.6 to convert it to the equivalent carbon disulfide tolerance, and then the carbon disulfide tolerance levels
will be compared to determine the highest tolerance level per raw agricultural commodity.
(6) Where tolerances are established for residues of both S,S,S-tributyl phosphorotrithioate and tributyl
phosphorotrithioite in or on the same raw agricultural commodity, the total amount of such pesticides shall not yield more
residue than that permitted by the higher of the two tolerances, calculated as S,S,S-tributyl phosphorotrithioate.
(7) Where tolerances are established for residues of O,S-dimethyl phosphoramidothioate, resulting from the use of
acephate (O,S-dimethyl acetylphos-phoramidothioate) and/or O,S - dimethylphosphoramidothioate on the same
agricultural commodity, the total amount of O,S-dimethyl-phosphoramidothioate shall not yield more residue than that
permitted by the higher of the two tolerances.
(8) Where a tolerance is established for more than one pesticide having the metabolites 1-(3,4-dichlorophenyl)-3methylurea (DCPMU) and 3,4-dichlorophenylurea (DCPU) found in or on a raw agricultural commodity, the total amount of
such residues shall not exceed the highest established tolerance for a pesticide having these metabolites.
(9) Where a tolerance is established for more than one pesticide having as metabolites compounds containing the
benzimidazole moiety found in or on a raw agricultural commodity, the total amount of such residues shall not exceed the
highest established tolerance for a pesticide having these metabolites.
(10) Where a tolerance is established for triclopyr, chloropyrifos, and chlorpyrifos-methyl having the common
metabolite 3,5,6-trichloro-2-pyridinol on the same raw agricultural commodity, the total amount of such residues shall not
exceed the highest established tolerance for any of the pesticides having the metabolites.
(11) Where tolerances are established for more than one pesticide having the metabolite 3,5,6-trichloro-2-pyridinol
found in or on the raw agricultural commodity, the total amount of such residues shall not exceed the highest established
tolerance for a pesticide having this metabolite.
(12) Where tolerances are established for residues of methomyl, resulting from the use of thiodicarb and/or methomyl
on the same raw agricultural commodity, the total amount of methomyl shall not yield more residue than that permitted by
the higher of the two tolerances.
(e) Except as noted in paragraphs (e)(1) and (2) of this section, where residues from two or more chemicals in the
same class are present in or on a raw agricultural commodity the tolerance for the total of such residues shall be the same
as that for the chemical having the lowest numerical tolerance in this class, unless a higher tolerance level is specifically
provided for the combined residues by a regulation in this part.

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(1) Where residues from two or more chemicals in the same class are present in or on a raw agricultural commodity
and there are available methods that permit quantitative determination of each residue, the quantity of combined residues
that are within the tolerance may be determined as follows:
(i) Determine the quantity of each residue present.
(ii) Divide the quantity of each residue by the tolerance that would apply if it occurred alone, and multiply by 100 to
determine the percentage of the permitted amount of residue present.
(iii) Add the percentages so obtained for all residues present.
(iv) The sum of the percentages shall not exceed 100 percent.
(2) Where residues from two or more chemicals in the same class are present in or on a raw agricultural commodity
and there are available methods that permit quantitative determinations of one or more, but not all, of the residues, the
amounts of such residues as may be determinable shall be deducted from the total amount of residues present and the
remainder shall have the same tolerance as that for the chemical having the lowest numerical tolerance in that class. The
quantity of combined residues that are within the tolerance may be determined as follows:
(i) Determine the quantity of each determinable residue present.
(ii) Deduct the amounts of such residues from the total amount of residues present and consider the remainder to
have the same tolerance as that for the chemical having the lowest numerical tolerance in that class.
(iii) Divide the quantity of each determinable residue by the tolerance that would apply if it occurred alone and the
quantity of the remaining residue by the tolerance for the chemical having the lowest numerical tolerance in that class and
multiply by 100 to determine the percentage of the permitted amount of residue present.
(iv) Add the percentages so obtained for all residues present.
(v) The sum of the percentages shall not exceed 100 percent.
(3) The following pesticides are members of the class of dithiocarbamates:
A mixture of 5.2 parts by weight of ammoniates of [ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis
[dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and disulfides.
2-Chloroallyl diethyldithiocarbamate.
Coordination product of zinc ion and maneb containing 20 percent manganese, 2.5 percent zinc, and 77.5 percent
ethylenebisdithiocarbamate.
Ferbam.
Maneb.
Manganous dimethyldithiocarbamate.
Sodium dimethyldithiocarbamate.
Thiram.
Zineb.
Ziram.

(4) The following are members of the class of chlorinated organic pesticides:
Aldrin.
BHC (benzene hexachloride).
1,1-Bis(p-chlorophenyl)-2,2,2-trichloroethanol.
Chlorbenside (p-chlorobenzyl p-chlorophenyl sulfide).
Chlordane.
Chlorobenzilate (ethyl 4,4′-dichlorobenzilate).
p-Chlorophenoxyacetic acid.
p-Chlorophenyl-2,4,5-trichlorophenyl sulfide.
2,4-D (2,4-dichlorophenoxyacetic acid).
DDD (TDE).

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DDT.
1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane.
2,6-Dichloro-4-nitroaniline.
2,4-Dichlorophenyl p-nitrophenyl ether.
Dieldrin.
Dodecachlorooctahydro-1,3,4-metheno-2H-cyclobuta[cd]pentalene.
Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, 6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3-oxide).
Endosulfan sulfate (6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide).
Heptachlor (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a-tetrahydro-4,7-methanoindene).
Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro-2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7-methanoindene).
Hexachlorophene (2,2′-methylenebis(3,4,6-trichlorophenol) and its monosodium salt.
Isopropyl 4,4′-dichlorobenzilate.
Lindane.
Methoxychlor.
Ovex (p-chlorophenyl p-chlorobenzenesulfonate).
Sesone (sodium 2,4-dichlorophenoxyethyl sulfate, SES).
Sodium 2,4-dichlorophenoxyacetate.
Sodium trichloroacetate.
Sulphenone (p-chlorophenyl phenyl sulfone).
Terpene polychlorinates (chlorinated mixture of camphene, pinene, and related terpenes 65-66 percent chlorine).
2,3,5,6-Tetrachloronitrobenzene.
Tetradifon (2,4,5,4′-tetrachlorodiphenyl sulfone).
Toxaphene (chlorinated camphene).
Trichlorobenzoic acid.
Trichlorobenzyl chloride.

(5) The following are members of the class of cholinesterase-inhibiting pesticides:
Acephate (O,S-dimethyl acetyl-phosphoramidothioate) and its cholinesterase-inhibiting metabolite O,S-dimethyl
phosphoramidothioate.
Aldicarb (2-methyl-2-(methylthio) propionaldehyde O-(methylcarbamoyl)oxime) and its chlorinesterase-inhibiting metabolites
2-methyl-2-(methylsulfinyl)propionaldehyde O-(methycarbamoyl) oxime and 2-methyl-2-(methylsulfonyl)propionaldehyde
O-(methylcarbamoyl)oxime.
4-tert-Butyl-2-chlorophenyl methyl methyl phosphoramidate.
S-[(tert-Butylthio)methyl] O,O-diethyl phosphorodithioate and its cholinesterase-inhibiting metabolites.
Carbaryl (1-naphthyl N-methylcarbamate).
Carbofuran (2,3,-dihydro-2,2-dimethyl-7-benzofuranyl-N-methylcarbamate).
Carbofuran metabolite (2,3-dihydro-2,2-dimethyl-3-hydroxy-7-benofuranyl N-methylcarbamate).
Carbophenothion (S-[(p-chlorophenyl) thiolmethyl] O,O-diethyl phosphorodithioate) and its cholinesterase-inhibiting metabolites.
Chlorpyrifos (O,O-diethyl O-(3,5,6-trichloro-2-pyridyl)phosphorothioate).
Chlorpyrifos-methyl (O,O-dimethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate.
2-Chloro-1-(2,4,5-trichlorophenyl)vinyl dimethyl phosphate.
2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl phosphate.
Coumaphos (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosran-7-yl phosphate).
Coumaphos oxygen analog (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyphorothioate).
Dialifor (S-(2-chloro-1-phthalimidoethyl) O,O-diethyl phosphorodithioate).

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Dialifor oxygen analog (S-(2-chloro-1-phthalimidoethyl) O,O-diethyl phosphorothioate).
Demeton (a mixture of O,O-diethyl O-(and S) [2-ethylthio)ethyl] phosphorothioates).
Ethiolate (S-ethyl diethylthiocarbamate).
2,2-Dichlorovinyl dimethyl phosphate.
O,O-Diethyl S-[2-(ethylthio)ethyl] phosphorodithioate and its cholinesterase-inhibiting metabolites.
O,O-Diethyl O-(2-diethylamino-6-methyl-4-pyrimidinyl) phosphorothioate and its oxygen analog diethyl 2-diethylamino-6-methyl-4pyrimidinyl phosphate.
O,O-Diethyl O-(2-isoprophyl-4-methyl-6-pyrimidinyl) phosphorothioate.
O,O-Diethyl O-[p-(methylsulfinyl)phenyl] phosphorothioate and its cholinesterase-inhibiting metabolites.
Diethyl 2-pyrazinyl phosphate.
O,O-Diethyl O-2-pyrazinyl phosphorothioate.
S-(O,O-Diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide
S-(O,O-Diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide
2-(Dimethylamino)-5.6-dimethyl-4-pyrimidinyl dimethylcarbamate and its metabolites 5,6-dimethyl-2-(formylmethylamino)-4pyrimidinyl dimethylcarbamate and 5,6-dimethyl-2-(methylamino)-4-pyrimidinyl dimethylcarbamate (both calculated as parent).
Dimethoate (O,O-dimethyl S-(N-methyl-carbamoylmethyl) phosphorodithioate).
Dimethoate oxygen analog (O,O-dimethyl S-(N-methylcarbamoylmethyl) phosphorothioate).
O,O-Dimethyl O-p-(dimethylsulfamoyl) phenyl phosphate.
O,O-Dimethyl O-p-(dimethylsulfamoyl) phenyl phosphorothioate.
3,5-Dimethyl-4-(methylthio) phenyl methylcarbamate.
O,O-Dimethyl S-[4-oxo-1,2,3-benzotriazin-3-(4H)-ylmethyl] phosphorodithioate.
Dimethyl phosphate of 3-hydroxy-N,N-dimethyl-cis-crotonamide.
Dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide.
Dimethyl phosphate of α-methylbenzyl 3-hydroxy-cis-crotonate.
O,O-Dimethyl 2,2,2-trichloro-1-hydroxyethyl phosphonate.
O,O-Dimethyl phosphorodithioate, S-ester with 4-(mercaptomethyl)-2-methozy-Δ2-1,3,4-thiadiazolin-5-one.
Dioxathion (2,3-p-dioxanedithiol S,S-bis (O,O-diethylphosphorodithioate)) containing approximately 70 percent cis and trans isomers
and approximately 30 percent related compounds.
EPN.
Ethephon ((2- - chloroethyl) phosphonic acid).
Ethion.
Ethion oxygen analog (S-[[(diethoxyphosphinothioyl)thio] methyl] O,O-diethyl phosphorothioate).
O- Ethyl O-[4-(methylthio) phenyl] S-propyl phosphorodithioate and its cholinesterase-inhibiting metabolites.
O-Ethyl S,S-dipropylphosphorodithioate.
Ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl) phosphoramidate and its cholinesterase-inhibiting metabolites.
O-Ethyl S-phenyl ethylphosphonodithioate.
O-Ethyl S-phenyl ethylphosphonothiolate.
m-(1-Ethylpropyl)phenyl methylcarbamate.
S-[2-Ethylsulfinyl)ethyl] O,O-dimethyl phosphorothioate and its cholinesterase-inhibiting metabolites, (primarily S-[2-(ethyl-sulfonyl)
ethyl] O,O-dimethyl phosphorothioate).
Fenthion (O,O-dimethyl O-[3-methyl-4-(methylthio)phenyl]phosphorothioate and its cholinesterase-inhibiting metabolites.
Malathion.
N-(Mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorodithioate).
N-(Mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorothioate).
Methomyl (S-methyl N-[(methylcarbamoyl)oxy]thioacetimidate).

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1-Methoxycarbonyl-1-propen-2-yl dimethyl phosphate and its beta isomer.
m-(1-Methylbutyl)phenyl methylcarbamate.
Methyl parathion.
Naled (1,2-dibromo-2,2-dichloroethyl dimethyl phosphate).
Oxamyl (methyl N′,N′-dimethyl-N-[(methylcarbamoyl)oxy]-1-thiooxamimidate)
Parathion.
Phorate (O,O-diethyl S-(ethylthio)methyl phosphorodithioate) and its cholinesterase-inhibiting metabolites.
Phosalone (S-(6-chloro-3-mercaptomethyl)-2-benzoxazolinone) O,O-diethyl phosphorodithioate).
Phosphamidon (2-chloro-2-diethylcarbamoyl-1-methylvinyl dimethyl phosphate) including all of its related cholinesterase-inhibiting
compounds.
Pirimiphos-methyl O-[2-diethylamino-6-methyl-pyrimidinyl) O,O-dimethyl phosphorothioate
Ronnel.
Schradan (octamethylpyrophosphoramide).
Tetraethyl pyrophosphate.
O,O,O′,O′-Tetramethyl O,O′-sulfinyldi-p-phenylene phosphorothioate.
O,O,O′,O′-Tetramethyl O,O′-thiodi-p-phenylene phosphorothioate.
Tributyl phosphorotritlioite.
S,S,S-Tributyl phosphorothrithioate.
3,4,5-Trimethylphenyl methylcarbamate and its isomer 2,3,5-trimethylphenyl methylcarbamate.

(6) The following pesticides are members of the class of dinitrophenols:
2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate, mixture of.
4,6-Dinitro-o-cresol and its sodium salt.
Dinoseb (2-sec-butyl-4,6-dinitrophenol) and its alkanolamine, ammonium, and sodium salts.
[41 FR 8969, Mar. 2, 1976]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.3, see the List of CFR Sections Affected, which appears in the
Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.4 Exceptions.
The substances listed in this section are excepted from the definitions of “pesticide chemical” and “pesticide chemical
residue” under FFDCA section 201(q)(3) and are therefore exempt from regulation under FFDCA section 402(a)(2)(B) and
408. These substances are subject to regulation by the Food and Drug Administration as food additives under FFDCA
section 409.
(a) Inert ingredients in food packaging treated with a pesticide, when such inert ingredients are the components of the
food packaging material (e.g. paper and paperboard, coatings, adhesives, and polymers).
(b) [Reserved]
[63 FR 10720, Mar. 4, 1998, as amended at 73 FR 54976, Sept. 24, 2008]

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§180.5 Zero tolerances.
A zero tolerance means that no amount of the pesticide chemical may remain on the raw agricultural commodity when
it is offered for shipment. A zero tolerance for a pesticide chemical in or on a raw agricultural commodity may be
established because, among other reasons:
(a) A safe level of the pesticide chemical in the diet of two different species of warm-blooded animals has not been
reliably determined.

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(b) The chemical is carcinogenic to or has other alarming physiological effects upon one or more of the species of the
test animals used, when fed in the diet of such animals.
(c) The pesticide chemical is toxic, but is normally used at times when, or in such manner that, fruit, vegetables, or
other raw agricultural commodities will not bear or contain it.
(d) All residue of the pesticide chemical is normally removed through good agricultural practice such as washing or
brushing or through weathering or other changes in the chemical itself, prior to introduction of the raw agricultural
commodity into interstate commerce.
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§180.6 Pesticide tolerances regarding milk, eggs, meat, and/or poultry; statement of policy.
(a) When establishing tolerances for pesticide residues in or on raw agricultural commodities, consideration is always
given to possible residues of those pesticide chemicals or their conversion products entering the diet of man through the
ingestion of milk, eggs, meat, and/or poultry produced by animals fed agricultural products bearing such pesticide
residues. In each instance an evaluation of all available data will result in a conclusion either:
(1) That finite residues will actually be incurred in these foods from feed use of the raw agricultural commodity
including its byproducts; or
(2) That it is not possible to establish with certainty whether finite residues will be incurred, but there is a reasonable
expectation of finite residues; or
(3) That it is not possible to establish with certainty whether finite residues will be incurred, but there is no reasonable
expectation of finite residues.
(b) When the data show that finite residues will actually be incurred in milk, eggs, meat, and/or poultry, a tolerance will
be established on the raw agricultural commodity used as feed provided that tolerances can be established at the same
time, on the basis of the toxicological and other data available, for the finite residues incurred in milk, eggs, meat, and/or
poultry. When it is not possible to determine with certainty whether finite residues will be incurred in milk, eggs, meat,
and/or poultry but there is a reasonable expectation of finite residues in light of data reflecting exaggerated pesticides
levels in feeding studies, a tolerance will be established on the raw agricultural commodity provided that appropriate
tolerances can be established at the same time, on the basis of the toxicological and other data available, for the finite
residues likely to be incurred in these foods through the feed use of the raw agricultural commodity or its byproducts.
When it is not possible to determine with certainty whether finite residues will be incurred in milk, eggs, meat, and/or
poultry but there is no reasonable expectation of finite residues in light of data such as those reflecting exaggerated
pesticide levels in feeding studies and those elucidating the biochemistry of the pesticide chemical in the animal, a
tolerance may be established on the raw agricultural commodity without the necessity of a tolerance on food products
derived from the animal.
(c) The principles outlined in paragraphs (a) and (b) of this section will also be followed with respect to tolerances for
residues which will actually be incurred or are reasonably to be expected in milk, eggs, meat, and/or poultry by the use of
pesticides directly on the animal or administered purposely in the feed or drinking water.
(d) Tolerances contemplated by paragraphs (a) and (b) of this section will in addition to toxicological considerations
be conditioned on the availability of a practicable analytical method to determine the pesticide residue; that is, the method
must be sensitive and reliable at the tolerance level or in special cases at a higher level where such level is deemed
satisfactory and safe in light of the toxicity of the pesticide residue and of the unlikelihood of such residue exceeding the
tolerance. The analytical methods to be used for enforcement purposes will be those set forth in the “Pesticide Analytical
Manual” (see §180.101(c)). The sensitivities of these methods are expressed in that manual.
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Subpart B—Procedural Regulations
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§180.7 Petitions proposing tolerances or exemptions for pesticide residues in or on raw agricultural
commodities or processed foods.
(a) Petitions to be filed with the Agency under the provisions of FFDCA section 408(d) shall be submitted in duplicate.
If any part of the material submitted is in a foreign language, it shall be accompanied by an accurate and complete English
translation. The petition shall be accompanied by an advance deposit for fees described in §180.33. The petition shall
state the petitioner's mail address to which notice of objection under FFDCA section 408(g)(2) may be sent. The petition
must be signed by the petitioner or by his attorney or agent, or (if a corporation) by an authorized official.
(b) Petitions shall include the following information:

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(1) An informative summary of the petition and of the data, information, and arguments submitted or cited in support
of the petition. Both a paper and electronic copy of the summary should be submitted. The electronic copy should be
formatted according to the Office of Pesticide Programs' current standard for electronic data submission as specified at
http://www.epa.gov/pesticides/regulating/registering/submissions/index.htm.
(2) A statement that the petitioner agrees that such summary or any information it contains may be published as a
part of the notice of filing of the petition to be published under FFDCA section 408(d)(3) and as a part of a proposed or
final regulation issued under FFDCA section 408.
(3) The name, chemical identity, and composition of the pesticide chemical residue and of the pesticide chemical that
produces the residue.
(4) Data showing the recommended amount, frequency, method, and time of application of the pesticide chemical.
(5) Full reports of tests and investigations made with respect to the safety of the pesticide chemical, including full
information as to the methods and controls used in conducting those tests and investigations.
(6) Full reports of tests and investigations made with respect to the nature and amount of the pesticide chemical
residue that is likely to remain in or on the food, including a description of the analytical methods used. (See §180.34 for
further information about residue tests.)
(7) Proposed tolerances for the pesticide chemical residue if tolerances are proposed.
(8) Practicable methods for removing any amount of the residue that would exceed any proposed tolerance.
(9) A practical method for detecting and measuring the levels of the pesticide chemical residue in or on the food, or for
exemptions, a statement why such a method is not needed.
(10) If the petition relates to a tolerance for a processed food, reports of investigations conducted using the
processing method(s) used to produce that food.
(11) Such information as the Administrator may require to make the determination under FFDCA section 408(b)(2)(C).
(12) Such information as the Administrator may require on whether the pesticide chemical may have an effect in
humans that is similar to an effect produced by a naturally occurring estrogen or other endocrine effects.
(13) Information regarding exposure to the pesticide chemical residue due to any tolerance or exemption already
granted for such residue.
(14) Information concerning any maximum residue level established by the Codex Alimentarius Commission for the
pesticide chemical residue addressed in the petition. If a Codex maximum residue level has been established for the
pesticide chemical residue and the petitioner does not propose that this level be adopted, a statement explaining the
reasons for this departure from the Codex level.
(15) Such other data and information as the Administrator requires by regulation to support the petition.
(16) Reasonable grounds in support of the petition.
(c) The data specified under paragraphs (b)(1) through (b)(16) of this section should be on separate sheets or sets of
sheets, suitably identified. If such data have already been submitted with an earlier application, the present petition may
incorporate it by reference to the earlier one.
(d) Except as noted in paragraph (e) of this section, a petition shall not be accepted for filing if any of the data
prescribed by FFDCA section 408(d) are lacking or are not set forth so as to be readily understood. The availability to the
public of information provided to, or otherwise obtained by, the Agency under this part shall be governed by part 2 of this
chapter. The Administrator shall make the full text of the summary referenced in paragraph (b)(1) of this section available
to the public in the public docket at http://www.regulations.gov no later than publication in the FEDERAL REGISTER of the
notice of the petition filing.
(e) The Administrator shall notify the petitioner within 15 days after its receipt of acceptance or nonacceptance of a
petition, and if not accepted the reasons therefor. If petitioner desires, the petitioner may supplement a deficient petition
after notification as to deficiencies. If the petitioner does not wish to supplement or explain the petition and requests in
writing that it be filed as submitted, the petition shall be filed and the petitioner so notified.
(f) A notice of the filing of a petition for a pesticide chemical residue tolerance that the Administrator determines has
met the requirements of paragraph (b) of this section shall be published in the FEDERAL REGISTER by the Administrator
within 30 days after such determination. The notice shall state the name of the pesticide chemical residue and the
commodities for which a tolerance is sought and announce the availability of a description of the analytical methods
available to the Administrator for the detection and measurement of the pesticide chemical residue with respect to which
the petition is filed or shall set forth the petitioner's statement of why such a method is not needed. The notice shall

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explicitly reference the specific docket identification number in the public docket at http://www.regulations.gov where the
full text of the summary required in paragraph (b) of this section is located, and refer interested parties to this document for
further information on the petition. The full text of the summary may be omitted from the notice.
(g) The Administrator may request a sample of the pesticide chemical at any time while a petition is under
consideration. The Administrator shall specify in its request for a sample of the pesticide chemical, a quantity which it
deems adequate to permit tests of analytical methods used to determine residues of the pesticide chemical and of
methods proposed by the petitioner for removing any residues of the chemical that exceed the tolerance proposed.
(h) The Administrator shall determine, in accordance with the Act, whether to issue an order that establishes,
modifies, or revokes a tolerance regulation (whether or not in accord with the action proposed by the petitioner), whether
to publish a proposed tolerance regulation and request public comment thereon under §180.29, or whether to deny the
petition. The Administrator shall publish in the FEDERAL REGISTER such order or proposed regulation. After receiving
comments on any proposed regulation, the Administrator may issue an order that establishes, modifies, or revokes a
tolerance regulation. An order published under this section shall describe briefly how to submit objections and requests for
a hearing under part 178 of this chapter. A regulation issued under this section shall be effective on the date of publication
in the FEDERAL REGISTER unless otherwise provided in the regulation.
[70 FR 33360, June 8, 2005, as amended at 73 FR 75600, Dec. 12, 2008]

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§180.8 Withdrawal of petitions without prejudice.
In some cases the Administrator will notify the petitioner that the petition, while technically complete, is inadequate to
justify the establishment of a tolerance or the tolerance requested by petitioner. This may be due to the fact that the data
are not sufficiently clear or complete. In such cases, the petitioner may withdraw the petition pending its clarification or the
obtaining of additional data. This withdrawal may be without prejudice to a future filing. A deposit for fees as specified in
§180.33 shall accompany the resubmission of the petition.
[70 FR 33361, June 8, 2005]

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§180.9 Substantive amendments to petitions.
After a petition has been filed, the petitioner may submit additional information or data in support thereof, but in such
cases the petition will be given a new filing date.
[70 FR 33361, June 8, 2005]

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§180.29 Establishment, modification, and revocation of tolerance on initiative of Administrator.
(a) Upon the Administrator's own initiative, the Administrator may propose, under FFDCA section 408(e), the issuance
of a regulation establishing a tolerance for a pesticide chemical or exempting it from the necessity of a tolerance, or a
regulation modifying or revoking an existing tolerance or exemption.
(b) The Administrator shall provide a period of not less than 60 days for persons to comment on the proposed
regulation, except that a shorter period for comment may be provided if the Administrator for good cause finds that it would
be in the public interest to do so and states the reasons for the finding in the notice of proposed rulemaking.
(c) After reviewing any timely comments received, the Administrator may by order establish, modify, or revoke a
tolerance regulation, which order and regulation shall be published in the FEDERAL REGISTER. An order published under
this section shall state that persons may submit objections and requests for a hearing in the manner described in part 178
of this chapter.
(d) Any final regulation issued under this section shall be effective on the date of publication in the FEDERAL REGISTER
unless otherwise provided in the regulation.
[70 FR 33361, June 8, 2005]

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§180.30 Judicial review.
(a) Under FFDCA section 408(h), judicial review is available in the United States Courts of Appeal as to the following
actions:
(1) Regulations establishing general procedures and requirements under FFDCA section 408(e)(1)(C).

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(2) Orders issued under FFDCA section 408(f)(1)(C) requiring the submission of data.
(3) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to establishment, modification, or revocation
of a tolerance or exemption under FFDCA section 408(d)(4), or any regulation that is the subject of such an order. The
underlying action here is Agency disposition of a petition seeking the establishment, modification, or revocation of a
tolerance or exemption.
(4) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the denial of a petition under FFDCA
section 408(d)(4).
(5) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the establishment, modification,
suspension, or revocation of a tolerance or exemption under FFDCA section 408(e)(1)(A) or (e)(1)(B). The underlying
action here is the establishment, modification, suspension, or revocation of a tolerance or exemption upon the initiative of
EPA including EPA actions pursuant to FFDCA sections 408(b)(2)(B)(v), 408(b)(2)(E)(ii), 408(d)(4)(C)(ii), 408(l)(4), and
408(q)(1).
(6) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the revocation or modification of a
tolerance or exemption under FFDCA section 408(f)(2) for noncompliance with requirements for the submission of data.
(7) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to rules issued under FFDCA sections 408
(n)(3) and 408(d) or (e) regarding determinations pertaining to State authority to establish regulatory limits on pesticide
chemical residues.
(8) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to orders issued under FFDCA section 408
(n)(5)(C) authorizing States to establish regulatory limits not identical to certain tolerances or exemptions.
(b) Any issue as to which review is or was obtainable under paragraph (a) of this section shall not be the subject of
judicial review under any other provision of law. In part, this means that, for the Agency actions subject to the objection
procedure in FFDCA section 408(g)(2), judicial review is not available unless an adversely affected party exhausts these
objection procedures, and any petition procedures preliminary thereto.
[70 FR 33362, June 8, 2005]

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§180.31 Temporary tolerances.
(a) A temporary tolerance (or exemption from a tolerance) established under the authority of FFDCA section 408(r)
shall be deemed to be a tolerance (or exemption from the requirement of a tolerance) for the purposes of FFDCA section
408(a)(1) or (a)(2) and for the purposes of §180.30.
(b) A request for a temporary tolerance or a temporary exemption from a tolerance by a person who has obtained or
is seeking an experimental permit for a pesticide chemical under the Federal Insecticide, Fungicide, and Rodenticide Act
shall be accompanied by such data as are available on subjects outlined in §180.7(b) and an advance deposit to cover
fees as provided in §180.33.
(c) To obtain a temporary tolerance, a requestor must comply with the petition procedures specified in FFDCA section
408(d) and §180.7 except as provided in this section.
(d) A temporary tolerance or exemption from a tolerance may be issued for a period designed to allow the orderly
marketing of the raw agricultural commodities produced while testing a pesticide chemical under an experimental permit
issued under authority of the Federal Insecticide, Fungicide, and Rodenticide Act if the Administrator concludes that the
safety standard in FFDCA section 408(b)(2) or (c), as applicable, is met. Subject to the requirements of FFDCA section
408(e), a temporary tolerance or exemption from a tolerance may be revoked if the experimental permit is revoked, or may
be revoked at any time if it develops that the application for a temporary tolerance contains a misstatement of a material
fact or that new scientific data or experience with the pesticide chemical indicates that it does not meet the safety standard
in FFDCA section 408(b)(2) or (c), as applicable.
(e) Conditions under which a temporary tolerance is established shall include:
(1) A limitation on the amount of the chemical to be used on the designated crops permitted under the experimental
permit.
(2) A limitation for the use of the chemical on the designated crops to bona fide experimental use by qualified persons
as indicated in the experimental permit.
(3) A requirement that the person or firm which obtains the experimental permit for which the temporary tolerance is
established will immediately inform the Environmental Protection Agency of any reports on findings from the experimental
use that have a bearing on safety.

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(4) A requirement that the person or firm which obtained the experimental permit for which the temporary tolerance is
established will keep records of production, distribution, and performance for a period of 2 years and, on request, at any
reasonable time, make these records available to any authorized officer or employee of the Environmental Protection
Agency.
[70 FR 33362, June 8, 2005]

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§180.32 Procedure for modifying and revoking tolerances or exemptions from tolerances.
(a) The Administrator on his/her own initiative may propose the issuance of a regulation modifying or revoking a
tolerance for a pesticide chemical residue on raw agricultural commodities or processed foods or modifying or revoking an
exemption from tolerance for such residue.
(b) Any person may file with the Administrator a petition proposing the issuance of a regulation modifying or revoking
a tolerance or exemption from a tolerance for a pesticide chemical residue. The petition shall furnish reasonable grounds
for the action sought. Reasonable grounds shall include an explanation showing wherein the person has a substantial
interest in such tolerance or exemption from tolerance and an assertion of facts (supported by data if available) showing
that new uses for the pesticide chemical have been developed or old uses abandoned, that new data are available as to
toxicity of the chemical, or that experience with the application of the tolerance or exemption from tolerance may justify its
modification or revocation. Evidence that a person has registered or has submitted an application for the registration of a
pesticide under the Federal Insecticide, Fungicide, and Rodenticide Act will be regarded as evidence that the person has a
substantial interest in a tolerance or exemption from the requirement of a tolerance for a pesticide chemical that consists
in whole or in part of the pesticide. New data should be furnished in the form specified in §180.7(b) for submitting petitions,
as applicable.
(c) The procedures for completing action on an Administrator initiated proposal or a petition shall be those specified in
§§180.29 and 180.7, as applicable.
[70 FR 33362, June 8, 2005]

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§180.33 Fees.
(a) Each petition for the establishment of a new tolerance or a tolerance higher than already established, shall be
accompanied by a fee of $80,950, plus $2,025 for each raw agricultural commodity more than nine on which the
establishment of a tolerance is requested, except as provided in paragraphs (b), (d), and (h) of this section.
(b) Each petition for the establishment of a tolerance at a lower numerical level or levels than a tolerance already
established for the same pesticide chemical, or for the establishment of a tolerance on additional raw agricultural
commodities at the same numerical level as a tolerance already established for the same pesticide chemical, shall be
accompanied by a fee of $18,500 plus $1,225 for each raw agricultural commodity on which a tolerance is requested.
(c) Each petition for an exemption from the requirement of a tolerance or repeal of an exemption shall be
accompanied by a fee of $14,925.
(d) Each petition or request for a temporary tolerance or a temporary exemption from the requirement of a tolerance
shall be accompanied by a fee of $32,325 except as provided in paragraph (e) of this section. A petition or request to
renew or extend such temporary tolerance or temporary exemption shall be accompanied by a fee of $4,600.
(e) A petition or request for a temporary tolerance for a pesticide chemical which has a tolerance for other uses at the
same numerical level or a higher numerical level shall be accompanied by a fee of $16,075, plus $1,225 for each raw
agricultural commodity on which the temporary tolerance is sought.
(f) Each petition for revocation of a tolerance shall be accompanied by a fee of $10,125. Such fee is not required
when, in connection with the change sought under this paragraph, a petition is filed for the establishment of new
tolerances to take the place of those sought to be revoked and a fee is paid as required by paragraph (a) of this section.
(g) If a petition or a request is not accepted for processing because it is technically incomplete, the fee, less $2,025
for handling and initial review, shall be returned. If a petition is withdrawn by the petitioner after initial processing, but
before significant Agency scientific review has begun, the fee, less $2,025 for handling and initial review, shall be returned.
If an unacceptable or withdrawn petition is resubmitted, it shall be accompanied by the fee that would be required if it were
being submitted for the first time.
(h) Each petition for a crop group tolerance, regardless of the number of raw agricultural commodities involved, shall
be accompanied by a fee equal to the fee required by the analogous category for a single tolerance that is not a crop
group tolerance, i.e., paragraphs (a) through (f) of this section, without a charge for each commodity where that would
otherwise apply.

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(i) Objections under section 408(d)(5) of the Act shall be accompanied by a filing fee of $4,050.
(j) The person who files a petition for judicial review of an order under section 408(h) of the Act shall pay the costs of
preparing the record on which the order is based unless the person has no financial interest in the petition for judicial
review.
(k) No fee under this section will be imposed on the Interregional Research Project Number 4 (IR-4 Program).
(l) The Administrator may waive or refund part or all of any fee imposed by this section if the Administrator determines
in his or her sole discretion that such a waiver or refund will promote the public interest or that payment of the fee would
work an unreasonable hardship on the person on whom the fee is imposed. A request for waiver or refund of a fee shall be
submitted to the Office of Pesticide Programs' Document Processing Desk at the appropriate address as set forth in 40
CFR 150.17(a) or (b). A fee of $2,025 shall accompany every request for a waiver or refund, as specified in paragraph (m)
of this section, except that the fee under this paragraph shall not be imposed on any person who has no financial interest
in any action requested by such person under paragraphs (a) through (j) of this section. The fee for requesting a waiver or
refund shall be refunded if the request is granted.
(m) All deposits and fees required by the regulations in this part shall be paid by money order, bank draft, or certified
check drawn to the order of the Environmental Protection Agency. All deposits and fees shall be forwarded to the
Environmental Protection Agency, Headquarters Accounting Operations Branch, Office of Pesticide Programs (Tolerance
Fees), P.O. Box 360277M, Pittsburgh, PA 15251. The payments should be specifically labeled “Tolerance Petition Fees”
and should be accompanied only by a copy of the letter or petition requesting the tolerance. The actual letter or petition,
along with supporting data, shall be forwarded within 30 days of payment to the Office of Pesticide Programs' Document
Processing Desk at the appropriate address as set forth in 40 CFR 150.17(a) or (b). A petition will not be accepted for
processing until the required fees have been submitted. A petition for which a waiver of fees has been requested will not
be accepted for processing until the fee has been waived or, if the waiver has been denied, the proper fee is submitted
after notice of denial. A request for waiver or refund will not be accepted after scientific review has begun on a petition.
(n) This fee schedule will be changed annually by the same percentage as the percent change in the Federal General
Schedule (GS) pay scale. In addition, processing costs and fees will periodically be reviewed and changes will be made to
the schedule as necessary. When automatic adjustments are made based on the GS pay scale, the new fee schedule will
be published in the FEDERAL REGISTER as a final rule to become effective 30 days or more after publication, as specified
in the rule. When changes are made based on periodic reviews, the changes will be subject to public comment.
(o) No fee required by this section shall be levied during the period beginning on October 1, 2003, and ending
September 30, 2008.
[68 FR 24371, May 7, 2003, as amended at 69 FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, 2005; 71 FR 35547, June 21, 2006]

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§180.34 Tests on the amount of residue remaining.
(a) Data in a petition on the amount of residue remaining in or on a raw agricultural commodity should establish the
residue that may remain when the pesticide chemical is applied according to directions registered under the Federal
Insecticide, Fungicide, and Rodenticide Act, or according to directions contained in an application for registration. These
data should establish the residues that may remain under conditions most likely to result in high residues on the
commodity.
(b) The petition should establish the reliability of the residue data reported in it. Sufficient information should be
submitted about the analytical method to permit competent analysts to apply it successfully.
(c) If the pesticide chemical is absorbed into a living plant or animal when applied (is systemic), residue data may be
needed on each plant or animal on which a tolerance or exemption is requested.
(d) If the pesticide chemical is not absorbed into the living plant or animal when applied (is not systemic), it may be
possible to make a reliable estimate of the residues to be expected on each commodity in a group of related commodities
on the basis of less data than would be required for each commodity in the group, considered separately.
(e) Each of the following groups of crops lists raw agricultural commodities that are considered to be related for the
purpose of paragraph (d) of this section. Commodities not listed in this paragraph are not considered to be related for the
purpose of paragraph (d) of this section.
(1) Apples, crabapples, pears, quinces.
(2) Avocados, papayas.
(3) Blackberries, boysenberries, dewberries, loganberries, raspberries.
(4) Blueberries, currants, gooseberries, huckleberries.

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(5) Cherries, plums, prunes.
(6) Oranges, citrus citron, grapefruit, kumquats, lemons, limes, tangelos, tangerines.
(7) Mangoes, persimmons.
(8) Peaches, apricots, nectarines.
(9) Beans, peas, soybeans (each in dry form).
(10) Beans, peas, soybeans (each in succulent form).
(11) Broccoli, brussels sprouts, cauliflower, kohlrabi.
(12) Cantaloups, honeydew melons, muskmelons, pumpkins, watermelons, winter squash.
(13) Carrots, garden beets, sugar beets, horseradish, parsnips, radishes, rutabagas, salsify roots, turnips.
(14) Celery, fennel.
(15) Cucumbers, summer squash.
(16) Lettuce, endive (escarole), Chinese cabbage, salsify tops.
(17) Onions, garlic, leeks, shallots (green, or in dry bulb form).
(18) Potatoes, Jerusalem-artichokes, sweetpotatoes, yams.
(19) Spinach, beet tops, collards, dandelion, kale, mustard greens, parsley, Swiss chard, turnip tops, watercress.
(20) Tomatoes, eggplants, peppers, pimentos.
(21) Pecans, almonds, brazil nuts, bush nuts, butternuts, chestnuts, filberts, hazelnuts, hickory nuts, walnuts.
(22) Field corn, popcorn, sweet corn (each in grain form).
(23) Milo, sorghum (each in grain form).
(24) Wheat, barley, oats, rice, rye (each in grain form).
(25) Alfalfa, Bermuda grass, bluegrass, brome grass, clovers, cowpea hay, fescue, lespedeza, lupines, orchard grass,
peanut hay, peavine hay, rye grass, soybean hay, sudan grass, timothy, and vetch.
(26) Corn forage, sorghum forage.
(27) Sugarcane, cane sorghum.
[36 FR 22540, Nov. 25, 1971, as amended at 39 FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, 1974; 40 FR 6972, Feb. 18, 1975;
45 FR 82928, Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR 26635, May 17, 1995; 73 FR 75600, Dec. 12, 2008]

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§180.35 Tests for potentiation.
Experiments have shown that certain cholinesterase-inhibiting pesticides when fed together to test animals are more
toxic than the sum of their individual toxicities when fed separately. One substance potentiates the toxicity of the other.
Important toxicological interactions also have been observed between pesticides and other substances. Wherever there is
reason to believe that a pesticide chemical for which a tolerance is proposed may interact with other pesticide chemicals
or other substances to which man is exposed, it may be necessary to require special experimental data regarding
potentiation capacities to evaluate the safety of the proposed tolerance. This necessarily will be determined on a case-bycase basis.
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§180.40 Tolerances for crop groups.
(a) Group or subgroup tolerances may be established as a result of:
(1) A petition from a person who has submitted an application for the registration of a pesticide under the Federal
Insecticide, Fungicide, and Rodenticide Act.
(2) On the initiative of the Administrator.

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(3) A petition by an interested person.
(b) The tables in §180.41 are to be used in conjunction with this section for the establishment of crop group
tolerances. Each table in §180.41 lists a group of raw agricultural commodities that are considered to be related for the
purposes of this section. Refer also to §180.1(g) for a listing of commodities for which established tolerances may be
applied to certain other related and similar commodities.
(c) When there is an established or proposed tolerance for all of the representative commodities for a specific group
or subgroup of related commodities, a tolerance may be established for all commodities in the associated group or
subgroup. Tolerances may be established for a crop group or, alternatively, tolerances may be established for one or more
of the subgroups of a crop group.
(d) The representative crops are given as an indication of the minimum residue chemistry data base acceptable to the
Agency for the purposes of establishing a group tolerance. The Agency may, at its discretion, allow group tolerances when
data on suitable substitutes for the representative crops are available (e.g., limes instead of lemons).
(e) Since a group tolerance reflects maximum residues likely to occur on all individual crops within a group, the
proposed or registered patterns of use for all crops in the group or subgroup must be similar before a group tolerance is
established. The pattern of use consists of the amount of pesticide applied, the number of times applied, the timing of the
first application, the interval between applications, and the interval between the last application and harvest. The pattern of
use will also include the type of application; for example, soil or foliar application, or application by ground or aerial
equipment.
(f) When the crop grouping contains commodities or byproducts that are utilized for animal feed, any needed
tolerance or exemption from a tolerance for the pesticide in meat, milk, poultry and/or eggs must be established before a
tolerance will be granted for the group as a whole. The representative crops include all crops in the group that could be
processed such that residues may concentrate in processed food and/or feed. Processing data will be required prior to
establishment of a group tolerance. Tolerances will not be granted on a group basis as to processed foods prepared from
crops covered by the group tolerance.
(g) If maximum residues (tolerances) for the representative crops vary by more than a factor of 5 from the maximum
value observed for any crop in the group, a group or subgroup tolerance will ordinarily not be established. In this case
individual crop tolerances, rather than group tolerances, will normally be established.
(h) Alternatively, a commodity with a residue level significantly higher or lower than the other commodities in a group
may be excluded from the group tolerance (e.g., cereal grains, except corn). In this case an individual tolerance at the
appropriate level for the unique commodity would be established, if necessary. The alternative approach of excluding a
commodity with a significantly higher or lower residue level will not be used to establish a tolerance for a commodity
subgroup. Most subgroups have only two representative commodities; to exclude one such commodity and its related
residue data would likely provide insufficient residue information to support the remainder of the subgroup. Residue data
from crops additional to those representative crops in a grouping may be required for systemic pesticides.
(i) The commodities included in the groups will be updated periodically either at the initiative of the Agency or at the
request of an interested party. Persons interested in updating this section should contact the Registration Division of the
Office of Pesticide Programs.
(j) When EPA amends a crop group in a manner that expands or contracts the commodities that are covered by the
group, EPA will initially retain the pre-existing as well as the revised crop group in the CFR. The revised crop group will
have the same number as the pre-existing crop group; however, the revised crop group number will be followed by a
hyphen and the final two digits of the year in which it was established (e.g., if Crop Group 1 is amended in 2007, the
revised group will be designated as Crop Group 1-07). If the pre-existing crop group had crop subgroups, these subgroups
will be numbered in a similar fashion in the revised crop group. The name of the revised crop group will not be changed
from the pre-existing crop group unless the revision so changes the composition of the crop group that the pre-existing
name is no longer accurate. Once a revised crop group is established, EPA will no longer establish tolerances under the
pre-existing crop group. At appropriate times, EPA will amend tolerances for crop groups that have been superseded by
revised crop groups to conform the pre-existing crop group to the revised crop group. Once all of the tolerances for the
pre-existing crop group have been updated, the pre-existing crop group will be removed from the CFR.
(k) Establishment of a tolerance does not substitute for the additional need to register the pesticide under a
companion law, the Federal Insecticide, Fungicide, and Rodenticide Act. The Registration Division of the Office of
Pesticide Programs should be contacted concerning procedures for registration of new uses of a pesticide.
[60 FR 26635, May 17, 1995, as amended at 70 FR 33363, June 8, 2005; 72 FR 69155, Dec. 7, 2007; 75 FR 56014, Sept. 15, 2010]

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§180.41 Crop group tables.
(a) The tables in this section are to be used in conjunction with §180.40 to establish crop group tolerances.

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(b) Commodities not listed are not considered as included in the groups for the purposes of this paragraph, and
individual tolerances must be established. Miscellaneous commodities intentionally not included in any group include
asparagus, avocado, banana, fig, globe artichoke, hops, mango, papaya, pawpaw, peanut, persimmon, pineapple, water
chestnut, and watercress.
(c) Each group is identified by a group name and consists of a list of representative commodities followed by a list of
all commodity members for the group. If the group includes subgroups, each subgroup lists the subgroup name, the
representative commodity or commodities, and the member commodities for the subgroup. Subgroups, which are a subset
of their associated crop group, are established for some but not all crops groups.
(1) Crop Group 1: Root and Tuber Vegetables Group.
(i) Representative commodities. Carrot, potato, radish, and sugar beet.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 1 and identifies the related crop
subgroups.
TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES
Commodities
Arracacha (Arracacia xanthorrhiza)
Arrowroot (Maranta arundinacea)
Artichoke, Chinese (Stachys affinis)
Artichoke, Jerusalem (Helianthus tuberosus)
Beet, garden (Beta vulgaris)
Beet, sugar (Beta vulgaris)
Burdock, edible (Arctium lappa)
Canna, edible (Queensland arrowroot) (Canna indica)
Carrot (Daucus carota)
Cassava, bitter and sweet (Manihot esculenta)
Celeriac (celery root) (Apium graveolens var. rapaceum)
Chayote (root) (Sechium edule)
Chervil, turnip-rooted (Chaerophyllum bulbosum).
Chicory (Cichorium intybus)
Chufa (Cyperus esculentus)
Dasheen (taro) (Colocasia esculenta)
Ginger (Zingiber officinale)
Ginseng (Panax quinquefolius)
Horseradish (Armoracia rusticana)
Leren (Calathea allouia)
Parsley, turnip-rooted (Petroselinum crispum var. tuberosum)
Parsnip (Pastinaca sativa)
Potato (Solanum tuberosum)
Radish (Raphanus sativus)
Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus)
Rutabaga (Brassica campestris var. napobrassica)
Salsify (oyster plant) (Tragopogon porrifolius).
Salsify, black (Scorzonera hispanica)
Salsify, Spanish (Scolymus hispanicus)
Skirret (Sium sisarum)
Sweet potato (Ipomoea batatas)
Tanier (cocoyam) (Xanthosoma sagittifolium)
Turmeric (Curcuma longa)
Turnip (Brassica rapa var. rapa)
Yam bean (jicama, manoic pea) (Pachyrhizus spp.)
Yam, true (Dioscorea spp.)

Related crop subgroups
1C, 1D
1C, 1D
1C, 1D
1C, 1D
1A, 1B
1A
1A, 1B
1C, 1D
1A, 1B
1C, 1D
1A, 1B
1C, 1D
1A, 1B
1A, 1B
1C, 1D
1C, 1D
1C, 1D
1A, 1B
1A, 1B
1C, 1D
1A, 1B
1A, 1B
1C
1A, 1B
1A, 1B
1A, 1B
1A, 1B
1A, 1B
1A, 1B
1A, 1B
1C, 1D
1C, 1D
1C, 1D
1A, 1B
1C, 1D
1C, 1D

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 1, specifies the representative
commodity(ies) for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 1 SUBGROUP LISTING
Representative commodities
Crop Subgroup 1A. Root vegetables
subgroup.
Carrot, radish, and sugar beet.

Crop Subgroup 1B. Root vegetables
(except sugar beet) subgroup.
Carrot and radish.

Commodities

Beet, garden; beet, sugar; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish;
parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret;
turnip.

Beet, garden; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley,
turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip.

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Crop Subgroup 1C. Tuberous and corm
vegetables subgroup.
Potato.
Crop Subgroup 1D. Tuberous and corm
vegetables (except potato) subgroup.
Sweet potato.

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Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet;
chayote (root); chufa; dasheen; ginger; leren; potato; sweet potato; tanier; turmeric; yam bean; yam, true.

Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet;
chayote (root); chufa; dasheen; ginger; leren; sweet potato; tanier; turmeric; yam bean; yam, true.

(2) Crop Group 2. Leaves of Root and Tuber Vegetables (Human Food or Animal Feed) Group (Human Food or
Animal Feed) Group.
(i) Representative commodities. Turnip and garden beet or sugar beet.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 2:
CROP GROUP 2: LEAVES OF ROOT AND TUBER VEGETABLES (HUMAN FOOD OR ANIMAL FEED) GROUP—COMMODITIES
Beet, garden (Beta vulgaris)
Beet, sugar (Beta vulgaris)
Burdock, edible (Arctium lappa)
Carrot (Daucus carota)
Cassava, bitter and sweet (Manihot esculenta)
Celeriac (celery root) (Apium graveolens var. rapaceum)
Chervil, turnip-rooted (Chaerophyllum bulbosum)
Chicory (Cichorium intybus)
Dasheen (taro) (Colocasia esculenta)
Parsnip (Pastinaca sativa)
Radish (Raphanus sativus)
Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus)
Rutabaga (Brassica campestris var. napobrassica)
Salsify, black (Scorzonera hispanica)
Sweet potato (Ipomoea batatas)
Tanier (cocoyam) (Xanthosoma sagittifolium)
Turnip (Brassica rapa var. rapa)
Yam, true (Dioscorea spp.)

(3) Crop Group 3. Bulb Vegetables (Allium spp.) Group.
(i) Representative commodities. Onion, green; and onion, dry bulb.
(ii) Commodities. The following is a list of all the commodities in Crop Group 3.
CROP GROUP 3: BULB VEGETABLE (ALLIUM SPP.) GROUP—COMMODITIES
Garlic, bulb (Allium sativum)
Garlic, great headed, (elephant) (Allium ampeloprasum var. ampeloprasum)
Leek (Allium ampeloprasum, A. porrum, A. tricoccum)
Onion, dry bulb and green (Allium cepa, A. fistulosum)
Onion, Welsh, (Allium fistulosum)
Shallot (Allium cepa var. cepa)

(4) Crop Group 3-07. Bulb Vegetable Group.
(i) Representative Commodities. Onion, bulb and onion, green.
(ii) Table. The following Table 1 lists all the commodities listed in Crop Group 3-07 and identifies the related crop
subgroups.
TABLE 1—CROP GROUP 3-07: BULB VEGETABLE GROUP

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Commodities
Chive, fresh leaves (Allium schoenoprasum L.)
Chive, Chinese, fresh leaves (Allium tuberosum Rottler ex Spreng)
Daylily, bulb (Hemerocallis fulva (L.) L. var. fulva)
Elegans hosta (Hosta Sieboldiana (Hook.) Engl)
Fritillaria, bulb (Fritillaria L. fritillary)
Fritillaria, leaves (Fritillaria L. fritillary)
Garlic, bulb (Allium sativum L. var. sativum) (A. sativum Common Garlic Group)
Garlic, great headed, bulb (Allium ampeloprasum L. var. ampeloprasum) (A. ampeloprasum Great Headed Garlic Group)
Garlic, Serpent, bulb (Allium sativum var. ophioscorodon or A. sativum Ophioscorodon Group)
Kurrat (Allium kurrat Schweinf. Ex. K. Krause or A. ampeloprasum Kurrat Group)
Lady's leek (Allium cernuum Roth)
Leek Allium porrum L. (syn: A. ampeloprasum L. var. porrum (L.) J. Gay) (A.ampeloprasum Leek Group)
Leek, wild (Allium tricoccum Aiton)
Lily, bulb (Lilium spp. (Lilium Leichtlinii var. maximowiczii, Lilium lancifolium))
Onion, Beltsville bunching (Allium x proliferum (Moench) Schrad.) (syn: Allium fistulosum L. x A. cepa L.)
Onion, bulb (Allium cepa L. var. cepa) (A. cepa Common Onion Group)
Onion, Chinese, bulb (Allium chinense G. Don.) (syn: A. bakeri Regel)
Onion, fresh (Allium fistulosum L. var. caespitosum Makino)
Onion, green (Allium cepa L. var. cepa) (A. cepa Common Onion Group)
Onion, macrostem (Allium macrostemom Bunge)
Onion, pearl (Allium porrum var. sectivum or A. ampeloprasum Pearl Onion Group)
Onion, potato, bulb (Allium cepa L. var. aggregatum G. Don.) (A. cepa Aggregatum Group)
Onion, tree, tops (Allium x proliferum (Moench) Schrad. ex Willd.) (syn: A. cepa var. proliferum (Moench) Regel; A. cepa L. var.
bulbiferum L.H. Bailey; A. cepa L. var. viviparum (Metz.) Alef.)
Onion, Welsh, tops (Allium fistulosum L.)
Shallot, bulb (Allium cepa var. aggregatum G. Don.)
Shallot, fresh leaves (Allium cepa var. aggregatum G. Don.)
Cultivars, varieties, and/or hybrids of these.

Related crop
subgroups
3-07B
3-07B
3-07A
3-07B
3-07A
3-07B
3-07A
3-07A
3-07A
3-07B
3-07B
3-07B
3-07B
3-07A
3-07B
3-07A
3-07A
3-07B
3-07B
3-07B
3-07A
3-07A
3-07B
3-07B
3-07A
3-07B

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 3-07, specifies the representative
commodities for each subgroup and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 3-07: SUBGROUP LISTING
Representative
commodities
Crop subgroup 3-07A.
Onion, bulb, subgroup.
Onion, bulb.
Crop subgroup 3-07B.
Onion, green, subgroup.
Onion, green.

Commodities
Daylily, bulb; fritillaria, bulb; garlic, bulb; garlic, great-headed, bulb; garlic, serpent, bulb; lily, bulb; onion, bulb; onion, Chinese,
bulb; onion, pearl; onion, potato, bulb; shallot, bulb; cultivars, varieties, and/or hybrids of these.
Chive, fresh leaves; chive, Chinese, fresh leaves; elegans hosta; fritillaria, leaves; kurrat; lady's leek; leek; leek, wild; Onion,
Beltsville bunching; onion, fresh; onion, green; onion, macrostem; onion, tree, tops; onion, Welsh, tops; shallot, fresh leaves;
cultivars, varieties, and/or hybrids of these.

(5) Crop Group 4. Leafy Vegetables (Except Brassica Vegetables) Group.
(i) Representative commodities. Celery, head lettuce, leaf lettuce, and spinach (Spinacia oleracea).
(ii) Table. The following table 1 lists all the commodities included in Crop Group 4 and identifies the related crop
subgroups.
TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP
Commodities
Amaranth (leafy amaranth, Chinese spinach, tampala) (Amaranthus spp.)
Arugula (Roquette) (Eruca sativa)
Cardoon (Cynara cardunculus)
Celery (Apium graveolens var. dulce)
Celery, Chinese (Apium graveolens var. secalinum)
Celtuce (Lactuca sativa var. angustana)
Chervil (Anthriscus cerefolium)
Chrysanthemum, edible-leaved (Chrysanthemum coronarium var. coronarium)
Chrysanthemum, garland (Chrysanthemum coronarium var. spatiosum)
Corn salad (Valerianella locusta)
Cress, garden (Lepidium sativum)
Cress, upland (yellow rocket, winter cress) (Barbarea vulgaris)
Dandelion (Taraxacum officinale)
Dock (sorrel) (Rumex spp.)
Endive (escarole) (Cichorium endivia)
Fennel, Florence (finochio) (Foeniculum vulgare Azoricum Group)
Lettuce, head and leaf (Lactuca sativa)

Related crop subgroups

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4A
4A
4B
4B
4B
4B
4A
4A
4A
4A
4A
4A
4A
4A
4A
4B
4A

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Orach (Atriplex hortensis)
Parsley (Petroselinum crispum)
Purslane, garden (Portulaca oleracea)
Purslane, winter (Montia perfoliata)
Radicchio (red chicory) (Cichorium intybus)
Rhubarb (Rheum rhabarbarum)
Spinach (Spinacia oleracea)
Spinach, New Zealand (Tetragonia tetragonioides, T. expansa)
Spinach, vine (Malabar spinach, Indian spinach) (Basella alba)
Swiss chard (Beta vulgaris var. cicla)

4A
4A
4A
4A
4A
4B
4A
4A
4A
4B

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 4, specifies the representative
commodities for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 4 SUBGROUP LISTING
Representative commodities
Commodities
Crop Subgroup 4A. Leafy greens
subgroup.
Head lettuce and leaf lettuce, and Amaranth; arugula; chervil; chrysanthemum, edible-leaved; chrysanthemum, garland; corn salad; cress, garden; cress,
spinach (Spinacia oleracea)
upland; dandelion; dock; endive; lettuce; orach; parsley; purslane, garden; purslane, winter; radicchio (red chicory);
spinach; spinach, New Zealand; spinach, vine.
Crop Subgroup 4B. Leaf petioles
subgroup.
Celery.
Cardoon; celery; celery, Chinese; celtuce; fennel, Florence; rhubarb; Swiss chard.

(6) Crop Group 5. Brassica (Cole) Leafy Vegetables Group.
(i) Representative commodities. Broccoli or cauliflower; cabbage; and mustard greens.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 5 and identifies the related crop
subgroups.
TABLE 1—CROP GROUP 5: BRASSICA (COLE) LEAFY VEGETABLES
Commodities
Broccoli (Brassica oleracea var. botrytis)
Broccoli, Chinese (gai lon) (Brassica alboglabra)
Broccoli raab (rapini) (Brassica campestris)
Brussels sprouts (Brassica oleracea var. gemmifera)
Cabbage (Brassica oleracea)
Cabbage, Chinese (bok choy) (Brassica chinensis)
Cabbage, Chinese (napa) (Brassica pekinensis)
Cabbage, Chinese mustard (gai choy) (Brassica campestris)
Cauliflower (Brassica oleracea var. botrytis)
Cavalo broccolo (Brassica oleracea var. botrytis)
Collards (Brassica oleracea var. acephala)
Kale (Brassica oleracea var. acephala)
Kohlrabi (Brassica oleracea var. gongylodes)
Mizuna (Brassica rapa Japonica Group)
Mustard greens (Brassica juncea)
Mustard spinach (Brassica rapa Perviridis Group)
Rape greens (Brassica napus)

Related crop subgroups
5A
5A
5B
5A
5A
5B
5A
5A
5A
5A
5B
5B
5A
5B
5B
5B
5B

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 5, specifies the representative
commodity(ies) for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 5 SUBGROUP LISTING
Representative commodities
Crop Subgroup 5A. Head and stem
Brassica subgroup
Broccoli or cauliflower; and cabbage

Commodities

Broccoli; broccoli, Chinese; brussels sprouts; cabbage; cabbage, Chinese (napa); cabbage, Chinese mustard;
cauliflower; cavalo broccolo; kohlrabi

Crop Subgroup 5B. Leafy Brassica greens
subgroup.
Mustard greens
Broccoli raab; cabbage, Chinese (bok choy); collards; kale; mizuna; mustard greens; mustard spinach; rape
greens

(7) Crop Group 6. Legume Vegetables (Succulent or Dried) Group.

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(i) Representative commodities. Bean (Phaseolus spp.; one succulent cultivar and one dried cultivar); pea (Pisum
spp.; one succulent cultivar and one dried cultivar); and soybean.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 6 and identifies the related crop
subgroups.
TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)

Commodities
Bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin)
Bean (Phaseolus spp.) (includes field bean, kidney bean, lima bean, navy bean, pinto bean, runner bean, snap bean, tepary bean, wax
bean)
Bean (Vigna spp.) (includes adzuki bean, asparagus bean, blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea, moth
bean, mung bean, rice bean, southern pea, urd bean, yardlong bean)
Broad bean (fava bean) (Vicia faba)
Chickpea (garbanzo bean) (Cicer arietinum)
Guar (Cyamopsis tetragonoloba)
Jackbean (Canavalia ensiformis)
Lablab bean (hyacinth bean) (Lablab purpureus)
Lentil (Lens esculenta)
Pea (Pisum spp.) (includes dwarf pea, edible-pod pea, En glish pea, field pea, garden pea, green pea, snow pea, sugar snap pea)
Pigeon pea (Cajanus cajan)
Soybean (Glycine max)
Soybean (immature seed) (Glycine max)
Sword bean (Canavalia gladiata)

Related crop
subgroups
6C
6A, 6B, 6C
6A, 6B, 6C
6B, 6C
6C
6C
6A
6C
6C
6A, 6B, 6C
6A, 6B, 6C
N/A
6A
6A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 6, specifies the representative
commodities for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 6 SUBGROUP LISTING
Representative commodities
Crop Subgroup 6A. Edible-podded
legume vegetables subgroup.
Any one succulent cultivar of ediblepodded bean (Phaseolus spp.) and any
one succulent cultivar of edible-podded
pea (Pisum spp.).
Crop Subgroup 6B. Succulent shelled
pea and bean subgroup.
Any succulent shelled cultivar of bean
(Phaseolus spp.) and garden pea (Pisum
spp.).
Crop Subgroup 6C. Dried shelled pea
and bean (except soybean) subgroup
Any one dried cultivar of bean (Phaseolus
spp.); and any one dried cultivar of pea
(Pisum spp.)

Commodities

Bean (Phaseolus spp.) (includes runner bean, snap bean, wax bean); bean (Vigna spp.) (includes asparagus
bean, Chinese longbean, moth bean, yardlong bean); jackbean; pea (Pisum spp.) (includes dwarf pea, edible-pod
pea, snow pea, sugar snap pea); pigeon pea; soybean (immature seed); sword bean.

Bean (Phaseolus spp.) (includes lima bean (green)); broad bean (succulent); bean (Vigna spp.) (includes
blackeyed pea, cowpea, southern pea); pea (Pisum spp.) (includes English pea, garden pea, green pea); pigeon
pea.

Dried cultivars of bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin);
(Phaseolus spp.) (includes field bean, kidney bean, lima bean (dry), navy bean, pinto bean; tepary bean; bean
(Vigna spp.) (includes adzuki bean, blackeyed pea, catjang, cowpea, Crowder pea, moth bean, mung bean, rice
bean, southern pea, urd bean); broad bean (dry); chickpea; guar; lablab bean; lentil; pea (Pisum spp.) (includes
field pea); pigeon pea.

(8) Crop Group 7. Foliage of Legume Vegetables Group.
(i) Representative commodities. Any cultivar of bean (Phaseolus spp.), field pea (Pisum spp.), and soybean.
(ii) Table. The following table 1 lists the commodities included in Crop Group 7.
TABLE 1—CROP GROUP 7: FOLIAGE OF LEGUME VEGETABLES GROUP
Representative commodities
Any cultivar of bean (Phaseolus spp.) and field pea (Pisum spp.), and
soybean (Glycine max)

Commodities
Plant parts of any legume vegetable included in the legume vegetables that will be
used as animal feed.

(iii) Table. The following table 2 identifies the crop subgroup for Crop Group 7 and specifies the representative
commodities for the subgroup, and lists all the commodities included in the subgroup.
TABLE 2—CROP GROUP 7 SUBGROUP LISTING
Representative commodities
Crop Subgroup 7A. Foliage of legume vegetables (except
soybeans) subgroup

Commodities

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Any cultivar of bean (Phaseolus spp.), and field pea (Pisum
spp.)

Plant parts of any legume vegetable (except soybeans) included in the legume vegetables
group that will be used as animal feed.

(9) Crop Group 8. Fruiting Vegetables Group.
(i) Representative commodities. Tomato, bell pepper, and one cultivar of non-bell pepper.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 8:
CROP GROUP 8: FRUITING VEGETABLES (EXCEPT CUCURBITS)—COMMODITIES
Eggplant (Solanum melongena)
Groundcherry (Physalis spp.)
Pepino (Solanum muricatum)
Pepper (Capsicum spp.) (includes bell pepper, chili pepper, cooking pepper, pimento, sweet pepper)
Tomatillo (Physalis ixocarpa)
Tomato (Lycopersicon esculentum)

(10) Crop Group 8-10. Fruiting Vegetable Group.
(i) Representative commodities. Tomato, standard size, and one cultivar of small tomato; bell pepper and one cultivar
of small nonbell pepper.
(ii) Commodities. The following is a list of all commodities included in the Crop group 8-10.
TABLE 1—CROP GROUP 8-10: FRUITING VEGETABLE GROUP
Related crop
subgroups
African eggplant, Solanum macrocarpon L
8-10B, 8-10C
Bush tomato, Solanum centrale J.M. Black
8-10A
Cocona, Solanum sessiliflorum Dunal
8-10A
Currant tomato, Lycopersicon pimpinellifolium L
8-10A
Eggplant, Solanum melongena L
8-10B, 8-10C
Garden huckleberry, Solanum scabrum Mill
8-10A
Goji berry, Lycium barbarum L
8-10A
Groundcherry, Physalis alkekengi L., P. grisea (Waterf.) M. Martinez, P. peruviana L., P. pubescens L
8-10A
Martynia, Proboscidea louisianica (Mill.) Thell
8-10B, 8-10C
Naranjilla, Solanum quitoense Lam
8-10A
Okra, Abelmoschus esculentus (L.) Moench
8-10B, 8-10C
Pea eggplant, Solanum torvum Sw.
8-10B, 8-10C
Pepino, Solanum muricatum Aiton
8-10B, 8-10C
Pepper, bell, Capsicum annuum L. var. annuum, Capsicum spp
8-10B
Pepper, nonbell, Capsicum chinese Jacq., C. annuum L. var. annuum, C. frutescens L., C. baccatum L., C. pubescens Ruiz & Pav., 8-10B, 8-10C
Capsicum spp
Roselle, Hibiscus sabdariffa L
8-10B, 8-10C
Scarlet eggplant, Solanum aethiopicum L
8-10B, 8-10C
Sunberry, Solanum retroflexum Dunal
8-10A
Tomatillo, Physalis philadelphica Lam
8-10A
Tomato, Solanum lycopersicum L., Solanum lycopersicum L. var. lycopersicum
8-10A
Tree tomato, Solanum betaceum Cav
8-10A
Cultivars, varieties and/or hybrids of these
Commodities

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 8-10, specifies the representative
commodities for each subgroup and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 8-10. SUBGROUP LISTING
Representative commodities
Crop subgroup 8-10A. Tomato subgroup
Tomato, standard size, and one cultivar of
small tomato
Crop subgroup 8-10B. Pepper/Eggplant
subgroup
Bell pepper and one cultivar of small nonbell
pepper
Crop subgroup 8-10C. Nonbell
pepper/Eggplant subgroup

Commodities
Bush tomato; cocona; currant tomato; garden huckleberry; goji berry; groundcherry; naranjilla; sunberry;
tomatillo; tomato; tree tomato; cultivars, varieties, and/or hybrids of these.

African eggplant; bell pepper; eggplant; Martynia; nonbell pepper; okra; pea eggplant; pepino; roselle; scarlet
eggplant; cultivars, varieties, and/or hybrids of these.

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African eggplant; eggplant; martynia; nonbell pepper; okra; pea eggplant; pepino; roselle; scarlet eggplant;
cultivars, varieties, and/or hybrids of these.

(11) Crop Group 9. Cucurbit Vegetables Group.
(i) Representative commodities. Cucumber, muskmelon, and summer squash.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 9 and identifies the related
subgroups.
TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES

Commodities
Chayote (fruit) (Sechium edule)
Chinese waxgourd (Chinese preserving melon) (Benincasa hispida)
Citron melon (Citrullus lanatus var. citroides)
Cucumber (Cucumis sativus)
Gherkin (Cucumis anguria)
Gourd, edible (Lagenaria spp.) (includes hyotan, cucuzza); (Luffa acutangula, L. cylindrica) (includes hechima, Chinese okra)
Momordica spp. (includes balsam apple, balsam pear, bitter melon, Chinese cucumber)
Muskmelon (hybrids and/or cultivars of Cucumis melo) (includes true cantaloupe, cantaloupe, casaba, crenshaw melon, golden pershaw
melon, honeydew melon, honey balls, mango melon, Persian melon, pineapple melon, Santa Claus melon, and snake melon)
Pumpkin (Cucurbita spp.)
Squash, summer (Cucurbita pepo var. melopepo) (includes crookneck squash, scallop squash, straightneck squash, vegetable marrow,
zucchini)
Squash, winter (Cucurbita maxima; C. moschata) (includes butternut squash, calabaza, hubbard squash); (C. mixta; C. pepo) (includes
acorn squash, spaghetti squash)
Watermelon (includes hybrids and/or varieties of Citrullus lanatus)

Related crop
subgroups
9B
9B
9A
9B
9B
9B
9B
9A
9B
9B
9B
9A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 9, specifies the representative
commodities for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 9 SUBGROUP LISTING
Representative commodities
Crop Subgroup 9A. Melon subgroup
Cantaloupes
Crop Subgroup 9B. Squash/cucumber
subgroup
One cultivar of summer squash and
cucumber.

Commodities
Citron melon; muskmelon; watermelon

Chayote (fruit); Chinese waxgourd; cucumber; gherkin; gourd, edible; Momordica spp.; pumpkin; squash,
summer; squash, winter.

(12) Crop Group 10. Citrus Fruit Group.
(i) Representative commodities. Sweet orange; lemon and grapefruit.
(ii) Commodities. The following is a list of all the commodities in Crop Group 10:
CROP GROUP 10: CITRUS FRUITS (CITRUS SPP., FORTUNELLA SPP.) GROUP—COMMODITIES
Calamondin (Citrus mitis × Citrofortunella mitis)
Citrus citron (Citrus medica)
Citrus hybrids (Citrus spp.) (includes chironja, tangelo, tangor)
Grapefruit (Citrus paradisi)
Kumquat (Fortunella spp.)
Lemon (Citrus jambhiri, Citrus limon)
Lime (Citrus aurantiifolia)
Mandarin (tangerine) (Citrus reticulata)
Orange, sour (Citrus aurantium)
Orange, sweet (Citrus sinensis)
Pummelo (Citrus grandis, Citrus maxima)
Satsuma mandarin (Citrus unshiu)

(13) Crop Group 10-10. Citrus Fruit Group.

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(i) Representative commodities. Orange or Tangerine/Mandarin, Lemon or Lime, and Grapefruit.
(ii) Commodities. The following is a list of all the commodities in Crop Group 10-10.
TABLE 1—CROP GROUP 10-10: CITRUS FRUIT GROUP
Commodities
Australian desert lime, Eremocitrus glauca (Lindl.) Swingle
Australian finger lime, Microcitrus australasica (F. Muell.) Swingle
Australian round lime, Microcitrus australis (A. Cunn. Ex Mudie) Swingle
Brown River finger lime, Microcitrus papuana Winters
Calamondin, Citrofortunella microcarpa (Bunge) Wijnands
Citron, Citrus medica L
Citrus hybrids, Citrus spp. Eremocitrus spp., Fortunella spp., Microcitrus spp., and Poncirus spp
Grapefruit, Citrus paradisi Macfad
Japanese summer grapefruit, Citrus natsudaidai Hayata
Kumquat, Fortunella spp
Lemon, Citrus limon (L.) Burm. f
Lime, Citrus aurantiifolia (Christm.) Swingle
Mediterranean mandarin, Citrus deliciosa Ten
Mount White lime, Microcitrus garrowayae (F.M. Bailey) Swingle
New Guinea wild lime, Microcitrus warburgiana (F.M. Bailey) Tanaka
Orange, sour, Citrus aurantium L
Orange, sweet, Citrus sinensis (L.) Osbeck
Pummelo, Citrus maxima (Burm.) Merr
Russell River lime, Microcitrus inodora (F.M. Bailey) Swingle
Satsuma mandarin, Citrus unshiu Marcow
Sweet lime, Citrus limetta Risso
Tachibana orange, Citrus tachibana (Makino) Tanaka
Tahiti lime, Citrus latifolia (Yu. Tanaka) Tanaka
Tangelo, Citrus xtangelo J.W. Ingram & H.E. Moore
Tangerine (Mandarin), Citrus reticulata Blanco
Tangor, Citrus nobilis Lour
Trifoliate orange, Poncirus trifoliata (L.) Raf
Uniq fruit, Citrus aurantium Tangelo group
Cultivars, varieties and/or hybrids of these

Related crop subgroups
10-10B
10-10B
10-10B
10-10B
10-10A
10-10A
10-10A
10-10C
10-10C
10-10B
10-10B
10-10B
10-10A
10-10B
10-10B
10-10A
10-10A
10-10C
10-10B
10-10A
10-10B
10-10A
10-10B
10-10A, 10-10C
10-10A
10-10A
10-10A
10-10C

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 10-10, specifies the representative
commodities for each subgroup and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 10-10: SUBGROUP LISTING
Representative commodities
Commodities
Crop Subgroup 10-10A. Orange
subgroup
Orange or tangerine/mandarin Calamondin; citron; citrus hybrids; mediterranean mandarin; orange, sour; orange, sweet; satsuma mandarin; tachibana
orange; tangerine (mandarin); tangelo; tangor; trifoliate orange; cultivars, varieties, and/or hybrids of these.
Crop Subgroup 10-10B.
Lemon/Lime subgroup
Lemon or lime
Australian desert lime; Australian finger lime; Australian round lime; brown river finger lime; kumquat; lemon; lime; mount
white lime; New Guinea wild lime; Russell River lime; sweet lime; Tahiti lime; cultivars , varieties, and/or hybrids of these.
Crop Subgroup 10-10C.
Grapefruit subgroup
Grapefruit
Grapefruit; Japanese summer grapefruit; pummelo; tangelo; uniq fruit; cultivars, varieties, and/or hybrids of these.

(14) Crop Group 11: Pome Fruits Group.
(i) Representative commodities. Apple and pear.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 11:
CROP GROUP 11: POME FRUITS GROUP—COMMODITIES
Apple (Malus domestica)
Crabapple (Malus spp.)
Loquat (Eriobotrya japonica)
Mayhaw (Crataegus aestivalis, C. opaca, and C. rufula)
Pear (Pyrus communis)
Pear, oriental (Pyrus pyrifolia)

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Quince (Cydonia oblonga)

(15) Crop group 11-10. Pome Fruit Group.
(i) Representative commodities. Apple and Pear
(ii) Commodities. The following is a list of all the commodities in Crop Group 11-10.
CROP GROUP 11-10: POME FRUIT GROUP—COMMODITIES
Apple, Malus domestica Borkh.
Azarole, Crataegus azarolus L.
Crabapple, Malus sylvestris (L.) Mill., M. prunifolia (Willd.) Borkh.
Loquat, Eriobotrya japonica (Thunb.) Lindl.
Mayhaw, Crataegus aestivalis (Walter) Torr. & A. Gray, C. opaca
Hook. & Arn., and C. rufula Sarg.
Medlar, Mespilus germanica L.
Pear, Pyrus communis L.
Pear, Asian, Pyrus pyrifolia (Burm. f.) Nakai var. culta (Makino) Nakai
Pseudocydonia sinensis (Thouin) C.K. Schneid.
Quince, Cydonia oblonga Mill.
Quince, Chinese, Chaenomeles speciosa (Sweet) Nakai,
Quince, Japanese, Chaenomeles japonica (Thunb.) Lindl. ex Spach
Tejocote, Crataegus mexicana DC.
Cultivars, varieties and/or hybrids of these.

(16) Crop Group 12. Stone Fruits Group.
(i) Representative commodities. Sweet cherry or tart cherry; peach; and plum or fresh prune (Prunus domestica,
Prunus spp.)
(ii) Commodities. The following is a list of all the commodities included in Crop Group 12:
CROP GROUP 12: STONE FRUITS GROUP—COMMODITIES
Apricot (Prunus armeniaca)
Cherry, sweet (Prunus avium),
Cherry, tart (Prunus cerasus)
Nectarine (Prunus persica)
Peach (Prunus persica)
Plum (Prunus domestica, Prunus spp.)
Plum, Chickasaw (Prunus angustifolia)
Plum, Damson (Prunus domestica spp. insititia)
Plum, Japanese (Prunus salicina)
Plumcot (Prunus. armeniaca × P. domestica)
Prune (fresh) (Prunus domestica, Prunus spp.)

(17) Crop Group 12-12: Stone Fruit Group.
(i) Representative commodities. Sweet cherry or Tart cherry; Peach; and Plum or Prune plum.
(ii) Commodities. The following Table 1 is a list of all commodities included in Crop Group 12-12.
TABLE 1—CROP GROUP 12-12: STONE FRUIT GROUP
Commodities

Related crop subgroup

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Apricot (Prunus armeniaca L.)
Apricot, Japanese (Prunus mume Siebold & Zucc.)
Capulin (Prunus serotina Ehrh. var. salicifolia (Kunth) Koehne)
Cherry, black (Prunus serotina Ehrh.)
Cherry, Nanking (Prunus tomentosa Thunb.)
Cherry, sweet (Prunus avium (L.) L.)
Cherry, tart (Prunus cerasus L.)
Jujube, Chinese (Ziziphus jujuba Mill.)
Nectarine (Prunuspersica (L.) Batsch var. nucipersica (Suckow) C.K. Schneid)
Peach (Prunus persica (L.) Batsch var. persica)
Plum (Prunus domestica L. subsp. domestica)
Plum, American (Prunus americana Marshall)
Plum, beach (Prunus maritima Marshall)
Plum, Canada (Prunus nigra Aiton)
Plum, cherry (Prunus cerasifera Ehrh.)
Plum, Chickasaw (Prunus angustifolia Marshall)
Plum, Damson (Prunus domestica L. subsp. insititia (L.) C.K. Schneid.)
Plum, Japanese (Prunus salicina Lindl.; P. salicina Lindl. var. salicina)
Plum, Klamath (Prunus subcordata Benth.)
Plum, prune (Prunus domestica L. subsp. domestica)
Plumcot (Prunus hybr.)
Sloe (Prunus spinosa L.)
Cultivars, varieties, and/or hybrids of these

12-12C
12-12C
12-12A
12-12A
12-12A
12-12A
12-12A
12-12C
12-12B
12-12B
12-12C
12-12C
12-12C
12-12C
12-12C
12-12C
12-12C
12-12C
12-12C
12-12C
12-12C
12-12C

(iii) Crop subgroups. The following Table 2 identifies the crop subgroups for Crop Group 12-12, specifies the
representative commodities for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 12-12: SUBGROUP LISTING
Representative
commodities
Cherry, sweet or
Cherry, tart
Peach
Plum or Prune plum

Commodities
Crop subgroup 12-12A. Cherry subgroup
Capulin; Cherry, black; Cherry, Nanking; Cherry, sweet; Cherry, tart; cultivars, varieties, and/or hybrids of these.
Crop subgroup 12-12B. Peach subgroup
Peach; Nectarine; cultivars, varieties, and/or hybrids of these.
Crop subgroup 12-12C. Plum subgroup
Apricot; Apricot, Japanese; Jujube, Chinese; Plum; Plum, American; Plum, beach; Plum, Canada; Plum, cherry; Plum, Chickasaw;
Plum, Damson; Plum, Japanese; Plum, Klamath; Plumcot; Plum, prune; Sloe; cultivars, varieties, and/or hybrids of these.

(18) Crop Group 13. Berries Group.
(i) Representative commodities. Any one blackberry or any one raspberry; and blueberry.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 13 and identifies the related
subgroups.
TABLE 1—CROP GROUP 13: BERRIES GROUP

Commodities
Blackberry (Rubus eubatus) (including bingleberry, black satin berry, boysenberry, Cherokee blackberry, Chesterberry, Cheyenne blackberry,
coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth
blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee
blackberry, youngberry, and varieties and/or hybrids of these)
Blueberry (Vaccinium spp.)
Currant (Ribes spp.)
Elderberry (Sambucus spp.)
Gooseberry (Ribes spp.)
Huckleberry (Gaylussacia spp.)
Loganberry (Rubus loganobaccus)
Raspberry, black and red (Rubus occidentalis, Rubus strigosus, Rubus idaeus)

Related crop
subgroups
13A

13B
13B
13B
13B
13B
13A
13A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 13, specifies the representative
commodities for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 13 SUBGROUPS LISTING
Representative commodities
Commodities
Crop Subgroup 13A. Caneberry (blackberry and raspberry) subgroup.
Any one blackberry or any one raspberry.
Blackberry; loganberry; red and black raspberry; cultivars and/or hybrids of these.
Crop Subgroup 13B. Bushberry subgroup.

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Blueberry, highbush.

Blueberry, highbush and lowbush; currant; elderberry; gooseberry; huckleberry.

(19) Crop Group 13-07. Berry and Small Fruit Crop Group
(i) Representative commodities. Any one blackberry or any one raspberry; highbush blueberry; elderberry or mulberry;
grape; fuzzy kiwifruit, and strawberry.
(ii) Table. The following Table 1 lists all the commodities listed in Crop Group 13-07 and identifies the related crop
subgroups.
TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP

Commodities
Amur river grape (Vitis amurensis Rupr)
Aronia berry (Aronia spp.)
Bayberry (Myrica spp.)
Bearberry (Arctostaphylos uva-ursi)
Bilberry (Vaccinium myrtillus L.)
Blackberry (Rubus spp.) (including Andean blackberry, arctic blackberry, bingleberry, black satin berry, boysenberry, brombeere, California
blackberry, Chesterberry, Cherokee blackberry, Cheyenne blackberry, common blackberry, coryberry, darrowberry, dewberry, Dirksen
thornless berry, evergreen blackberry, Himalayaberry, hullberry, lavacaberry, loganberry, lowberry, Lucretiaberry, mammoth blackberry,
marionberry, mora, mures deronce, nectarberry, Northern dewberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry,
ravenberry, rossberry, Shawnee blackberry, Southern dewberry, tayberry, youngberry, zarzamora, and cultivars, varieties and/or hybrids of
these.)
Blueberry, highbush (Vaccinium spp.)
Blueberry, lowbush (Vaccinium angustifolium Aiton)
Buffalo currant (Ribes aureum Pursh)
Buffaloberry (Shepherdia argentea (Pursh) Nutt.)
Che (Cudrania tricuspidata Bur. Ex Lavallee)
Chilean guava (Myrtus ugni Mol.)
Chokecherry (Prunus virginiana L.)
Cloudberry (Rubus chamaemorus L.)
Cranberry (Vaccinium macrocarpon Aiton)
Currant, black (Ribes nigrum L.)
Currant, red (Ribes rubrum L.)
Elderberry (Sambucus spp.)
European barberry (Berberis vulgaris L.)
Gooseberry (Ribes spp.)

Grape (Vitis spp.)
Highbush cranberry (Viburnum opulus L. var. Americanum Aiton)
Honeysuckle, edible (Lonicera caerula L. var. emphyllocalyx Nakai, Lonicera caerula L var . edulis Turcz. ex herder)
Huckleberry (Gaylussacia spp.)
Jostaberry (Ribes x nidigrolaria Rud. Bauer and A. Bauer)
Juneberry (Saskatoon berry) (Amelanchier spp.)
Kiwifruit, fuzzy (Actinidia deliciosa A. Chev.) (C.F. Liang and A.R. Fergusons, Actinida chinensis Planch.)
Kiwifruit, hardy (Actinidia arguta (Siebold and Zucc.) Planch. ex Miq)
Lingonberry (Vaccinium vitis-idaea L.)
Maypop (Passiflora incarnata L.)
Mountain pepper berries (Tasmannia lanceolata)(Poir.) A.C.Sm.
Mulberry (Morus spp.)
Muntries (Kunzea pomifera F. Muell.)
Native currant (Acrotriche depressa R. BR.)
Partridgeberry (Mitchella repens L.)
Phalsa (Grewia subinaequalis DC.)
Pincherry (Prunus pensylvanica L.f.)
Raspberry, black and red (Rubus spp.)
Riberry (Syzygium luehmannii)
Salal (Gaultheria shallon Pursh.)

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Related crop
subgroups
13-07D, 1307E, 13-07F
13-07B
13-07C
13-07G, 1307H
13-07G, 1307H
13-07A

13-07B
13-07B
13-07B
13-07C
13-07C
13-07B
13-07C
13-07G, 1307H
13-07G, 1307H
13-07B
13-07B
13-07B, 1307C
13-07B
13-07B, 1307D, 13-07E,
13-07F
13-07D, 1307F
13-07B
13-07B
13-07B
13-07B
13-07B, 1307C
13-07D, 1307E
13-07D, 1307E, 13-07F
13-07B, 1307G 13-07H
13-07E, 1307F
13-07C
13-07C
13-07G, 1307H
13-07B
13-07G, 1307H
13-07C
13-07C
13-07A
13-07C
13-07B, 1307C

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Schisandra berry (Schisandra chinensis (Turcz.) Baill.)
Sea buckthorn (Hippophae rhamnoides L.)
Serviceberry (Sorbus spp.)
Strawberry (Fragaria x ananassa Duchesne)
Wild raspberry (Rubus muelleri Lefevre ex P.J. Mull)
Cultivars, varieties, and/or hybrids of these.

13-07D, 1307E, 13-07F
13-07B
13-07C
13-07G
13-07A

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 13-07, specifies the representative
commodities for each subgroup and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING
Representative commodities
Commodities
Crop Subgroup 13-07A. Caneberry
subgroup
Any one blackberry or any one Blackberry; loganberry; raspberry, red and black; wild raspberry; cultivars, varieties, and/or hybrids of these.
raspberry.
Crop Subgroup 13-07B. Bushberry
subgroup.
Blueberry, highbush.
Aronia berry; blueberry, highbush; blueberry, lowbush; buffalo currant; Chilean guava; currant, black; currant, red;
elderberry; European, barberry; gooseberry; cranberry, highbush; honeysuckle, edible; huckleberry; jostaberry;
Juneberry; lingonberry; native currant; salal; sea buckthorn; cultivars, varieties, and/or hybrids of these.
Crop Subgroup 13-07C. Large
shrub/tree berry subgroup.
Elderberry or mulberry.
Bayberry; buffaloberry; che; chokecherry; elderberry; Juneberry; mountain pepper berries; mulberry; phalsa;
pincherry; riberry; salal; serviceberry; cultivars, varieties, and/or hybrids of these.
Crop Subgroup 13-07D. Small fruit
vine climbing subgroup.
Grape and fuzzy kiwifruit.
Amur river grape; gooseberry; grape; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties,
and /or hybrids of these.
Crop Subgroup 13-07E. Small fruit
vine climbing subgroup, except grape.
Fuzzy kiwifruit.
Amur river grape; gooseberry; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and/or
hybrids of these.
Crop Subgroup 13-07F. Small fruit
vine climbing subgroup except fuzzy
kiwifruit.
Grape.
Amur river grape; gooseberry; grape; kiwifruit, hardy; Maypop; schisandra berry; cultivars varieties, and/or hybrids of
these.
Crop Subgroup 13-07G. Low growing
berry subgroup.
Strawberry.
Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; strawberry;
cultivars, varieties, and/or hybrids of these.
Crop Subgroup 13-07H. Low growing
berry subgroup, except strawberry.
Cranberry
Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; cultivars,
varieties, and/or cultivars of these.

(20) Crop Group 14. Tree Nuts Group.
(i) Representative commodities. Almond and pecan.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 14:
CROP GROUP 14: TREE NUTS—COMMODITIES
Almond (Prunus dulcis)
Beech nut (Fagus spp.)
Brazil nut (Bertholletia excelsa)
Butternut (Juglans cinerea)
Cashew (Anacardium occidentale)
Chestnut (Castanea spp.)
Chinquapin (Castanea pumila)
Filbert (hazelnut) (Corylus spp.)
Hickory nut (Carya spp.)
Macadamia nut (bush nut) (Macadamia spp.)
Pecan (Carya illinoensis)

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Walnut, black and English (Persian) (Juglans spp.)

(21) Crop Group 14-12. Tree Nut Group.
(i) Representative commodities. Almond and Pecan.
(ii) Commodities. The following is a list of all commodities included in Crop Group 14-12.
CROP GROUP 14-12: TREE NUT GROUP
African nut-tree (Ricinodendron heudelotii (Baill.) Heckel)
Almond (Prunus dulcis (Mill.) D.A. Webb)
Beechnut (Fagus grandifolia Ehrh.; F. sylvatica L.)
Brazil nut (Bertholletia excelsa Humb. & Bonpl.)
Brazilian pine (Araucaria angustifolia (Bertol.) Kuntze)
Bunya (Araucaria bidwillii Hook.)
Bur oak (Quercus macrocarpa Michx.)
Butternut (Juglans cinerea L.)
Cajou nut (Anacardium giganteum Hance ex Engl.)
Candlenut (Aleurites moluccanus (L.) Willd.)
Cashew (Anacardium occidentale L.)
Chestnut (Castanea crenata Siebold & Zucc.; C. dentata (Marshall) Borkh.; C. mollissima Blume; C. sativa Mill.)
Chinquapin (Castaneapumila (L.) Mill.)
Coconut (Cocos nucifera L.)
Coquito nut (Jubaea chilensis (Molina) Baill.)
Dika nut (Irvingia gabonensis (Aubry-Lecomte ex O'Rorke) Baill.)
Ginkgo (Ginkgo biloba L.)
Guiana chestnut (Pachira aquatica Aubl.)
Hazelnut (Filbert) (Corylus americana Marshall; C. avellana L.; C. californica (A. DC.) Rose; C. chinensis Franch.)
Heartnut (Juglans ailantifolia Carrière var. cordiformis (Makino) Rehder)
Hickory nut (Carya cathayensis Sarg.; C. glabra (Mill.) Sweet; C. laciniosa (F. Michx.) W. P. C. Barton; C. myristiciformis (F. Michx.)
Elliott; C. ovata (Mill.) K. Koch; C. tomentosa (Lam.) Nutt.)
Japanese horse-chestnut (Aesculus turbinate Blume)
Macadamia nut (Macadamia integrifolia Maiden & Betche; M. tetraphylla L.A.S. Johnson)
Mongongo nut (Schinziophyton rautanenii (Schinz) Radcl.-Sm.)
Monkey-pot (Lecythis pisonis Cambess.)
Monkey puzzle nut (Araucaria araucana (Molina) K. Koch)
Okari nut (Terminalia kaernbachii Warb.)
Pachira nut (Pachira insignis (Sw.) Savigny)
Peach palm nut (Bactris gasipaes Kunth var. gasipaes)
Pecan (Carya illinoinensis (Wangenh.) K. Koch)
Pequi (Caryocar brasiliense Cambess.; C. villosum (Aubl.) Pers; C. nuciferum L.)
Pili nut (Canarium ovatum Engl.; C. vulgare Leenh.)
Pine nut (Pinus edulis Engelm.; P. koraiensis Siebold & Zucc.; P. sibirica Du Tour; P. pumila (Pall.) Regel; P. gerardiana Wall. ex D.
Don; P. monophylla Torr. & Frém.; P. quadrifolia Parl. ex Sudw.; P. pinea L.)
Pistachio (Pistacia vera L.)
Sapucaia nut (Lecythis zabucaja Aubl.)
Tropical almond (Terminalia catappa L.)

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Walnut, black (Juglans nigra L.; J. hindsii Jeps. ex R. E. Sm.; J. microcarpa Berland.)
Walnut, English (Juglans regia L.)
Yellowhorn (Xanthoceras sorbifolium Bunge)
Cultivars, varieties, and/or hybrids of these

(22) Crop Group 15. Cereal Grains Group.
(i) Representative commodities. Corn (fresh sweet corn and dried field corn), rice, sorghum, and wheat.
(ii) Commodities. The following is a list of all the commodities included in Crop Group 15:
CROP GROUP 15: CEREAL GRAINS—COMMODITIES
Barley (Hordeum spp.)
Buckwheat (Fagopyrum esculentum)
Corn (Zea mays)
Millet, pearl (Pennisetum glaucum)
Millet, proso (Panicum milliaceum)
Oats (Avena spp.)
Popcorn (Zea mays var. everta)
Rice (Oryza sativa)
Rye (Secale cereale)
Sorghum (milo) (Sorghum spp.)
Teosinte (Euchlaena mexicana)
Triticale (Triticum-Secale hybrids)
Wheat (Triticum spp.)
Wild rice (Zizania aquatica)

(23) Crop Group 16. Forage, Fodder and Straw of Cereal Grains Group.
(i) Representative commodities. Corn, wheat, and any other cereal grain crop.
(ii) Commodities. The commodities included in Crop Group 16 are: Forage, fodder, and straw of all commodities
included in the group cereal grains group.
(24) Crop Group 17. Grass Forage, Fodder, and Hay Group.
(i) Representative commodities. Bermuda grass; bluegrass; and bromegrass or fescue.
(ii) Commodities. The commodities included in Crop Group 17 are: Any grass, Gramineae family (either green or
cured) except sugarcane and those included in the cereal grains group, that will be fed to or grazed by livestock, all
pasture and range grasses and grasses grown for hay or silage.
(25) Crop Group 18. Nongrass Animal Feeds (Forage, Fodder, Straw, and Hay) Group.
(i) Representative commodities. Alfalfa and clover (Trifolium spp.)
(ii) Commodities. The following is a list of all the commodities included in Crop Group 18:
CROP GROUP 18: NONGRASS ANIMAL FEEDS (FORAGE, FODDER, STRAW, AND HAY) GROUP—COMMODITIES
Alfalfa (Medicago sativa subsp. sativa)
Bean, velvet (Mucuna pruriens var. utilis)
Clover (Trifolium spp., Melilotus spp.)
Kudzu (Pueraria lobata)
Lespedeza (Lespedeza spp.)
Lupin (Lupinus spp.)
Sainfoin (Onobrychis viciifolia);

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Trefoil (Lotus spp.)
Vetch (Vicia spp.)
Vetch, crown (Coronilla varia)
Vetch, milk (Astragalus spp).

(26) Crop Group 19. Herbs and Spices Group.
(i) Representative commodities. Basil (fresh and dried); black pepper; chive; and celery seed or dill seed.
(ii) Table. The following table 1 lists all the commodities included in Crop Group 19 and identifies the related
subgroups.
TABLE 1—CROP GROUP 19: HERBS AND SPICES GROUP
Commodities
Allspice (Pimenta dioica)
Angelica (Angelica archangelica)
Anise (anise seed) (Pimpinella anisum)
Anise, star (Illicium verum)
Annatto (seed)
Balm (lemon balm) (Melissa officinalis)
Basil (Ocimum basilicum)
Borage (Borago officinalis)
Burnet (Sanguisorba minor)
Camomile (Anthemis nobilis)
Caper buds (Capparis spinosa)
Caraway (Carum carvi)
Caraway, black (Nigella sativa)
Cardamom (Elettaria cardamomum)
Cassia bark (Cinnamomum aromaticum)
Cassia buds (Cinnamomum aromaticum)
Catnip (Nepeta cataria)
Celery seed (Apicum graveolens)
Chervil (dried) (Anthriscus cerefolium)
Chive (Allium schoenoprasum)
Chive, Chinese (Allium tuberosum)
Cinnamon (Cinnamomum verum)
Clary (Salvia sclarea)
Clove buds (Eugenia caryophyllata)
Coriander (cilantro or Chinese parsley) (leaf) (Coriandrum sativum)
Coriander (cilantro) (seed) (Coriandrum sativum)
Costmary (Chrysanthemum balsamita)
Culantro (leaf) (Eryngium foetidum)
Culantro (seed) (Eryngium foetidum)
Cumin (Cuminum cyminum)
Curry (leaf) (Murraya koenigii)
Dill (dillweed) (Anethum graveolens)
Dill (seed) (Anethum graveolens)
Fennel (common) (Foeniculum vulgare)
Fennel, Florence (seed) (Foeniculum vulgare Azoricum Group)
Fenugreek (Trigonella foenumgraecum)
Grains of paradise (Aframomum melegueta)
Horehound (Marrubium vulgare)
Hyssop (Hyssopus officinalis)
Juniper berry (Juniperus communis)
Lavender (Lavandula officinalis)
Lemongrass (Cymbopogon citratus)
Lovage (leaf) (Levisticum officinale)
Lovage (seed) (Levisticum officinale)
Mace (Myristica fragrans)
Marigold (Calendula officinalis)
Marjoram (Origanum spp.) (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram)
Mustard (seed) (Brassica juncea, B. hirta, B. nigra)
Nasturtium (Tropaeolum majus)
Nutmeg (Myristica fragrans)
Parsley (dried) (Petroselinum crispum)
Pennyroyal (Mentha pulegium)
Pepper, black (Piper nigrum)
Pepper, white
Poppy (seed) (Papaver somniferum)

Related crop subgroups
19B
19A
19B
19B
19B
19A
19A
19A
19A
19A
19B
19B
19B
19B
19B
19B
19A
19B
19A
19A
19A
19B
19A
19B
19A
19B
19A
19A
19B
19B
19A
19A
19B
19B
19B
19B
19B
19A
19A
19B
19A
19A
19A
19B
19B
19A
19A
19B
19A
19B
19A
19A
19B
19B
19B

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Rosemary (Rosemarinus officinalis)
Rue (Ruta graveolens)
Saffron (Crocus sativus)
Sage (Salvia officinalis)
Savory, summer and winter (Satureja spp.)
Sweet bay (bay leaf) (Laurus nobilis)
Tansy (Tanacetum vulgare)
Tarragon (Artemisia dracunculus)
Thyme (Thymus spp.)
Vanilla (Vanilla planifolia)
Wintergreen (Gaultheria procumbens)
Woodruff (Galium odorata)
Wormwood (Artemisia absinthium)

19A
19A
19B
19A
19A
19A
19A
19A
19A
19B
19A
19A
19A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 19, specifies the representative
commodities for each subgroup, and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 19 SUBGROUPS
Representative
commodities
Commodities
Crop Subgroup 19A.
Herb subgroup.
Basil (fresh and dried) Angelica; balm; basil; borage; burnet; camomile; catnip; chervil (dried); chive; chive, Chinese, clary; coriander (leaf); costmary;
and chive.
culantro (leaf); curry (leaf); dillweed; horehound; hyssop; lavender; lemongrass; lovage (leaf); marigold; marjoram (Origanum spp.);
nasturtium; parsley (dried); pennyroyal; rosemary; rue; sage; savory, summer and winter; sweet bay; tansy; tarragon; thyme;
wintergreen; woodruff; and wormwood.
Crop Subgroup 19B.
Spice subgroup.
Black pepper; and
Allspice; anise (seed); anise, star; annatto (seed); caper (buds); caraway; caraway, black; cardamom; cassia (buds); celery (seed);
celery seed or dill seed. cinnamon; clove (buds); coriander (seed); culantro (seed); cumin; dill (seed); fennel, common; fennel, Florence (seed); fenugreek;
grains of paradise; juniper (berry); lovage (seed); mace; mustard (seed); nutmeg; pepper, black; pepper, white; poppy (seed); saffron;
and vanilla.

(27) Crop Group 20. Oilseed Group.
(i) Representative commodities. Rapeseed (canola varieties only); sunflower, seed and cottonseed.
(ii) Table. The following Table 1 lists all the commodities listed in Crop Group 20 and identifies the related crop
subgroups and includes cultivars and/or varieties of these commodities.
TABLE 1—CROP GROUP 20: OILSEED GROUP
Commodities
Borage, Borago officinalis L
Calendula, Calendula officinalis L
Castor oil plant, Ricinus communis L
Chinese tallowtree, Triadica sebifera (L.) Small
Cottonseed, Gossypium hirsutum L. Gossypium spp
Crambe, Crambe hispanica L.; C. abyssinica Hochst. ex R.E. Fr
Cuphea, Cuphea hyssopifolia Kunth
Echium, Echium plantagineum L
Euphorbia, Euphorbia esula L
Evening primrose, Oenothera biennis L
Flax seed, Linum usitatissimum L
Gold of pleasure, Camelina sativa (L.) Crantz
Hare's ear mustard, Conringia orientalis (L.) Dumort
Jojoba, Simmondsia chinensis (Link) C.K. Schneid
Lesquerella, Lesquerella recurvata (Engelm. ex A. Gray) S. Watson
Lunaria, Lunaria annua L
Meadowfoam, Limnanthes alba Hartw. ex Benth
Milkweed, Asclepias spp
Mustard seed, Brassica hirta Moench, Sinapis alba L. subsp. Alba..
Niger seed, Guizotia abyssinica (L.f.) Cass
Oil radish, Raphanus sativus L. var. oleiformis Pers
Poppy seed, Papaver somniferum L. subsp. Somniferum
Rapeseed, Brassica spp.; B. napus L
Rose hip, Rosa rubiginosa L
Safflower, Carthamus tinctorious L
Sesame, Sesamum indicum L., S. radiatum Schumach. & honn
Stokes aster, Stokesia laevis (Hill) Greene
Sunflower, Helianthus annuus L
Sweet rocket, Hesperis matronalis L

Related crop subgroups
20A
20B
20B
20B
20C
20A
20A
20A
20B
20B
20A
20A
20A
20B
20A
20A
20A
20A
20A
20B
20A
20A
20A
20B
20B
20A
20B
20B
20A

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Tallowwood, Ximenia americana L
Tea oil plant, Camellia oleifera C. Abel
Vernonia, Vernonia galamensis (Cass.) Less
Cultivars, varieties, and/or hybrids of these

20B
20B
20B

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 20, specifies the representative
commodities for each subgroup and lists all the commodities included in each subgroup.
TABLE 2—CROP GROUP 20: SUBGROUP LISTING
Representative
commodities
Crop subgroup 20A.
Rapeseed subgroup
Rapeseed, canola varieties
only
Crop subgroup 20B.
Sunflower subgroup
Sunflower, seed
Crop subgroup 20C.
Cottonseed subgroup
Cottonseed

Commodities

Borage; crambe; cuphea; echium; flax seed; gold of pleasure; hare's ear mustard; lesquerella; lunaria; meadowfoam; milkweed;
mustard seed; oil radish; poppy seed; rapeseed; sesame; sweet rocket cultivars, varieties, and/or hybrids of these.

Calendula; castor oil plant; chinese tallowtree; euphorbia; evening primrose; jojoba; niger seed; rose hip; safflower; stokes
aster; sunflower; tallowwood; tea oil plant; vernonia; cultivars, varieties, and/or hybrids of these.

Cottonseed; cultivars, varieties, and/or hybrids of these.

(28) Crop Group 21. Edible fungi Group.
(i) Representative commodities. White button mushroom and any one oyster mushroom or any Shiitake mushroom.
(ii) Table. The following is a list of all the commodities in Crop Group 21. There are no related subgroups.
CROP GROUP 21—EDIBLE FUNGI GROUP—COMMODITIES
Blewitt (Lepista nuda)
Bunashimeji (Hypsizygus marrmoreus)
Chinese mushroom (Volvariella volvacea) (Bull.) Singer
Enoki (Flammulina velutipes) (Curt.) Singer
Hime-Matsutake (Agaricus blazei) Murill
Hirmeola (Auricularia auricular)
Maitake (Grifola frondosa)
Morel (Morchella spp.)
Nameko (Pholiota nameko)
Net Bearing (Dictyophora)
Oyster mushroom (Pleurotus spp.)
Pom Pom (Hericium erinaceus)
Reishi mushroom (Ganoderma lucidum (Leyss. Fr.) Karst.)
Rodman's agaricus (Agaricus bitorquis) (Quel.) Saccardo
Shiitake mushroom (Lentinula edodes (Berk.) Pegl.)
Shimeji (Tricholoma conglobatum)
Stropharia (Stropharia spp.)
Truffle (Tuber spp.)
White button mushroom (Agaricus bisporous (Lange) Imbach)
White Jelly Fungi (Tremella fuciformis)

[60 FR 26635, May 17, 1995, as amended at 72 FR 69156, 69157, Dec. 7, 2007; 73 FR 52, Jan. 2, 2008; 75 FR 76289, Dec. 8,
2010; 77 FR 50620, Aug. 22, 2012]

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Subpart C—Specific Tolerances
EDITORIAL NOTE: Nomenclature changes to subpart C of part 180 appear at 67 FR 41803, June 19, 2002; 67 FR 42393, June
21, 2002; 68 FR 39430, July 1, 2003; 71 FR 74804, Dec. 13, 2006; 72 FR 53137, Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; 73
FR 60155, Oct. 10, 2008; 75 FR 56014, Sept. 15, 2010; and 76 FR 34885, June 15, 2011.

Back to Top
§180.101 Specific tolerances; general provisions.
(a) The tolerances established for pesticide chemicals in this subpart C apply to residues resulting from their
application prior to harvest or slaughter, unless otherwise stated. Tolerances are expressed in terms of parts by weight of
the pesticide chemical per one million parts by weight of the raw agricultural commodity.

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(b) The poisonous and deleterious substances for which tolerances are established by the regulations in this subpart
C are named by their common names wherever practicable, otherwise by their chemical names.
(c) The analytical methods to be used for determining whether pesticide residues, including negligible residues, in or
on raw agricultural commodities are in compliance with the tolerances established in this part 180 are identified among the
methods contained or referenced in the Food and Drug Administration's “Pesticide Analytical Manual” which is available
from the Food and Drug Administration, Department of Health, Education, and Welfare, 200 C Street SW., Washington,
DC 20204.
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§180.103 Captan; tolerances for residues.
(a)(1) General. Tolerances are established for residues of the fungicide, captan (N-trichloromethylthio-4cyclohexene-1,2-dicarboximide) in or on the following commodities:
Commodity

Parts per million

Almond
Almond, hulls
Animal feed, nongrass, group 18
Apple
Apricot
Blueberry
Caneberry, subgroup 13A
Cherry, sweet
Cherry, tart
Cotton, undelinted seed
Dill, seed
Flax, seed
Grape
Grain, cereal, forage, fodder and straw, group 16
Grain, cereal, group 15
Grass, forage
Grass, hay
Nectarine
Okra
Peach
Peanut
Peanut, hay
Pear
Plum, prune, fresh
Rapeseed, forage
Rapeseed, seed
Safflower, seed
Sesame, seed
Strawberry
Sunflower, seed
Vegetable, brassica leafy, group 5
Vegetable, bulb, group 3
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root and tuber, group 1

0.25
75.0
0.05
25.0
10.0
20.0
25.0
50.0
50.0
0.05
0.05
0.05
25.0
0.05
0.05
0.05
0.05
25.0
0.05
15.0
0.05
0.05
25.0
10.0
0.05
0.05
0.05
0.05
20.0
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05

(2) Tolerances are established for the combined residues of the fungicide, captan (N-trichloromethylthio-4cyclohexene-1,2-dicarboximide) and its metabolite 1,2,3,6-tetrahydrophthalimide (THPI), measured at THPI, in or on the
following commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat

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0.15
0.20
0.30
0.15
0.20
0.30
0.15
0.20
0.30
0.15

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Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.20
0.30
0.10
0.15
0.20
0.30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 52016, Sept. 12, 2007]

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§180.106 Diuron; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide diuron, 3-(3,4-dichlorophenyl)
-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline in or on food commodities, as follows:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Apple
Artichoke, globe
Asparagus
Banana
Berry group 13
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Citrus, oil
Corn, field, grain
Corn, pop, grain
Cotton, undelinted seed
Fish - freshwater finfish, farm raised
Fruit, citrus, group 10, except lemon
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grape
Grass, forage, except bermudagrass
Grass, hay, except bermudagrass
Hazelnut
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Lemon
Nut, macadamia
Olive
Papaya
Peach
Pear
Pea, field, seed
Pea, field, vines
Pea, field, hay
Pecan
Peppermint, tops
Pineapple
Pineapple, process residue
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Spearmint, tops

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

3.0
2.0
0.1
1
7
0.1
0.1
1
1
1
3.0
0.1
0.1
0.2
2.0
0.05
1
1
1
5.0
0.05
2
2
0.1
1
1
1
1
1
1
0.5
0.05
1
0.5
0.1
1
0.1
2
2
0.05
1.5
0.1
0.4
1
1
1
2
0.5
2
1.5

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Sugarcane, cane
Sugarcane, molasses
Walnut
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.2
0.7
0.05
0.7
2
0.5
2
1.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in §180.1(l) are
established for the combined residues of the herbicide diuron (3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites
convertible to 3,4-dichloroaniline) in or on the raw agricultural commodities:
Commodity

Parts per million

Barley, bran
Barley, grain
Barley, hay
Barley, straw
Cactus
Clover, forage
Clover, hay
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Trefoil, forage
Trefoil, hay
Vetch, forage
Vetch, hay

0.7
0.2
2
1.5
0.05
0.1
1.0
2
0.1
2
1.5
0.1
1.5
0.1
1.5

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 2164, Jan. 14, 1998, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, 1999; 66 FR 28671, May 24, 2001;
67 FR 46883, July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR 32540, June 13, 2007; 72 FR 35666, June 29, 2007; 73 FR 54958,
Sept. 24, 2008; 76 FR 34885, June 15, 2011]

Back to Top
§180.108 Acephate; tolerances for residues.
(a) General. (1) Tolerances are established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate,
including its metabolites and degradates other than methamidophos, in or on the commodities in the following table.
Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate,
O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.
Commodity1

Parts per million

Bean, dry, seed
Bean, succulent
Brussels sprouts
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cauliflower
Celery
Cotton, hulls
Cotton, meal
Cotton, undelinted seed
Cranberry
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Lettuce, head
Milk

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3.0
3.0
3.0
0.1
0.1
0.1
2.0
10
1.0
1.0
0.5
0.5
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
10
0.1

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Peanut
Pepper
Peppermint, tops
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Spearmint, tops
Soybean, seed

0.2
4.0
27
0.1
0.1
0.1
0.1
0.1
0.1
27
1.0

1

Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from
methamidophos application are regulated under 40 CFR 180.315.
(2) A tolerance of 0.02 ppm is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate,
including its metabolites and degradates other than methamidophos, in or on all food items (other than those already
covered by a higher tolerance as a result of use on growing crops) in food handling establishments where food and food
products are held, processed, prepared and served, including food service, manufacturing and processing establishments,
such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and
canneries, where application of acephate shall be limited solely to spot and/or crack and crevice treatment (a coarse, lowpressure spray shall be used to avoid atomization or splashing of the spray for spot treatments; equipment capable of
delivering a pin-stream of insecticide shall be used for crack and crevice treatments). Spray concentration shall be limited
to a maximum of 1.0 percent active ingredient. Contamination of food or food-contact surfaces shall be avoided.
Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate,
O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.
(3) Tolerances are established for residues of methamidophos, O,S-dimethyl phosphoramidothioate, including its
metabolites and degradates, in or on the commodities in the following table as a result of the application of acephate.
Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methamidophos,
O,S-dimethyl phosphoramidothioate, in or on the commodity.
Commodity

Parts per million

Bean, dry, seed
Bean, succulent
Brussels sprouts
Cauliflower
Celery
Cranberry
Lettuce, head
Pepper
Peppermint, tops
Spearmint, tops

1
1
0.5
0.5
1
0.1
1
1
1
1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of
acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than
methamidophos, in or on the commodity in the following table. Compliance with the tolerance level specified in this
paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the
commodity.
Commodity1

Parts per million

Nut, macadamia

0.05

1
Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from
methamidophos application are regulated under 40 CFR 180.315.

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 13542, Mar. 20, 1998, as amended at 67 FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008; 75 FR 60237, Sept. 29, 2010]

Back to Top
§180.111 Malathion; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of
diethyl mercaptosuccinate) in or on the following food commodities:
Commodity

Parts per million

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Alfalfa, forage
Alfalfa, hay
Almond, hulls
Almond, postharvest
Apple
Apricot
Asparagus
Avocado
Barley, grain, postharvest
Bean, dry, seed
Bean, succulent
Beet, garden, roots
Beet, garden, tops
Beet, sugar, roots
Beet, sugar, tops
Blackberry
Blueberry
Boysenberry
Carrot, roots
Chayote, fruit
Chayote, roots
Cherry
Chestnut
Clover, forage
Clover, hay
Corn, field, forage
Corn, field, grain, postharvest
Corn, pop, grain, postharvest
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Cowpea, forage
Cowpea, hay
Cranberry
Cucumber
Currant
Date, dried fruit
Dewberry
Eggplant
Fig
Flax, seed
Garlic, bulb
Gooseberry
Grape
Grapefruit
Guava
Hazelnut
Hop, dried cones
Horseradish
Kumquat
Leek
Lemon
Lentil, seed
Lespedeza, hay
Lime
Loganberry
Lupin, seed
Mango
Melon
Mushroom
Nectarine
Nut, macadamia
Oat, grain, postharvest
Okra
Onion, bulb
Onion, green
Orange
Papaya
Parsnip
Passionfruit
Pea
Pea, field, hay
Pea, field, vines
Peach

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135
135
50
8
8
8
8
8
8
8
8
8
8
1
8
8
8
8
8
8
8
8
1
135
135
8
8
8
8
2
135
135
8
8
8
8
8
8
8
0.1
8
8
8
8
8
1
1
8
8
8
8
8
135
8
8
8
8
8
8
8
1
8
8
8
8
8
1
8
8
8
8
8
8

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Peanut, hay
Peanut, postharvest
Pear
Pecan
Pepper
Peppermint, tops
Pineapple
Plum
Plum, prune
Potato
Pumpkin
Quince
Radish
Raspberry
Rice, grain, postharvest
Rice, wild
Rutabaga
Rye, grain, postharvest
Safflower, seed
Salsify, roots
Salsify, tops
Shallot, bulb
Sorghum, grain, forage
Sorghum, grain, grain, postharvest
Soybean, forage
Soybean, hay
Soybean, seed
Soybean, vegetable, succulent
Spearmint, tops
Squash, summer
Squash, winter
Strawberry
Sunflower, seed, postharvest
Sweet potato, roots
Tangerine
Tomato
Trefoil, forage
Trefoil, hay
Turnip, greens
Turnip, roots
Vegetable, brassica, leafy, group 5
Vegetable, leafy, except brassica, group 4
Vetch, hay
Walnut
Wheat, grain, postharvest

135
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
0.2
8
8
8
8
8
135
135
8
8
8
8
8
8
8
1
8
8
135
135
8
8
8
8
135
8
8

(2) Tolerances are established for the combined residues of the insecticide malathion (O,O-dimethyl dithiophosphate
of diethyl mercaptosuccinate) and its metabolite, malaoxon (O,O-dimethyl thiophosphate of diethyl mercaptosuccinate), in
or on the following food commodities:
Commodity

Parts per million

Barley, straw
Corn, field, stover
Cotton, undelinted seed
Grass, forage
Grass, hay
Oat, forage
Oat, straw
Rye, forage
Rye, straw
Watercress
Wheat, forage
Wheat, straw

50
30.0
20.0
200
270
4.0
50
4.0
50
0.2
4.0
50

(3) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl
mercaptosuccinate), in or on the following food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat1
Cattle, meat byproducts1
Egg

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4
4
4
0.1

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Goat, fat

4
4

Goat, meat1

4

Goat, meat byproducts1
Hog, fat

4
4

Hog, meat1

4

Hog, meat byproducts1
Horse, fat

4
4

Horse, meat1
Horse, meat byproducts1
Milk, fat
Poultry, fat

4
0.5
4
4

Poultry, meat1
Poultry, meat byproducts1
Sheep, fat

4

Sheep, meat1

4
4

Sheep, meat byproducts1

4

1

The tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat, hog, horse,
poultry, or sheep.
(4) Malathion may be safely used in accordance with the following conditions:
(i) It is incorporated into paper trays in amounts not exceeding 100 milligrams per square foot.
(ii) Treated paper trays are intended for use only in the drying of grape (raisins).
(iii) Total residues of malathion resulting from drying of grape on treated trays and from application to grape before
harvest shall not exceed 12 parts per million on processed ready-to-eat raisins.
(5) Residues of malathion in safflower, refined oil from application to the growing safflower plant shall not exceed 0.6
parts per million.
(6) Malathion may be safely used for the control of insects during the drying of grape (raisins) in compliance with
paragraph (a)(4) of this section by incorporation into paper trays in amounts not exceeding 100 milligrams per square foot.
(7) Malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) may be safely used in feed in accordance
with the following conditions.
(i) A tolerance of 50 parts per million is established for residues of malathion in citrus, dried pulp for cattle feed, when
present as the result of the application of the pesticide to bagged citrus pulp during storage. Whether or not tolerances for
residues of malathion on the fresh fruit have been established under section 408 of the Act, the total residue of malathion
in the citrus, dried pulp shall not exceed 50 parts per million.
(ii) A tolerance of 10 parts per million is established for malathion in nonmedicated cattle feed concentrate blocks
resulting from its application as a pesticide to paper used in packaging the nonmedicated cattle feed concentrate blocks.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[43 FR 22974, May 30, 1978, as amended at 43 FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, 1979; 45 FR 76145, Nov. 18, 1980;
47 FR 42738, Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, 1997; 65 FR
33694, May 24, 2000; 72 FR 35665, June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR 47455, Sept. 16, 2009; 75 FR 60238, Sept.
29, 2010]

Back to Top
§180.114 Ferbam; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate),
calculated as carbon disulfide, in or on the following food commodities:
Commodity

Parts per million

Expiration/Revocation Date

Apple

4.01

None

Bean

7.01

10/27/07

Cabbage

7.01

10/27/07

Cherry

4.01

None

Cranberry

4.01

None

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Fruit, citrus, group 10

4.01

Grape

4.01

None

Lettuce

7.01

10/27/07

None

Nectarine

4.01

None

Peach

4.01

None

Pear

4.01

None

Raspberry

7.01

10/27/07

1

Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950
(formerly §180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure
specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are
established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on
the following food commodities:
Commodity

Parts per million
4.01

Mango
1

This tolerance was established on the basis of data acquired at the public hearings held in 1950 (formerly §180.101)
and the remainder was established on the basis of pesticide petitions presented under the procedure specified in the
amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 57072, Oct. 26, 1998, as amended at 72 FR 53453, Sept. 19, 2007]

Back to Top
§180.116 Ziram; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide ziram (zinc dimethyldithiocarbamate), calculated
as zinc ethylenebisdithiocarbamate, in or on the following food commodities:
Commodity

Parts per million

Expiration/revocation date

Almond

1

0.1

None

Apple

1

7.0

None

Apricot

1

7.0

None

Blackberry

1

7.0

5/11/13

Blueberry

1

7.0

None

Cherry, sweet

1

7.0

None

Cherry, tart

1

Grape
Huckleberry
Peach
Pear
Pecan
Quince
Strawberry
Tomato

7.0
7.0
7.0
7.0

1

7.0
0.1

1

7.0
7.0

1

7.0

None
None
None
None
None
None
None
None
None

1

Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950
(formerly §180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure
specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Public Law 518, 83d Congress (68 Stat. 511).
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39437, July 1, 2003, as amended at 71 FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, 2008; 77 FR 59123, Sept. 26,
2012]

Back to Top

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§180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide S-ethyl dipropylthiocarbamate, including its
metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified
in this paragraph is to be determined by measuring only the sum of S-ethyl dipropylthiocarbamate, S-ethyl
(2-hydroxypropyl)propylcarbamothioate, S-(2-hydroxyethyl)dipropylcarbamothioate, and S-ethyl (3-hydroxypropyl)
propylcarbamothioate, calculated as the stoichiometric equivalent of S-ethyl dipropylthiocarbamate, in or on the
commodity.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond
Almond, hulls
Bean, dry, seed
Bean, succulent
Beet, garden, tops
Beet, sugar, molasses
Beet, sugar, tops
Clover, forage
Clover, hay
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, citrus, group 10
Lespedeza, forage
Lespedeza, hay
Pea, succulent
Safflower, seed
Sunflower, seed
Tomato
Trefoil, forage
Trefoil, hay
Vegetable, root
Walnut

0.2
0.6
0.08
0.08
0.08
0.08
0.5
0.4
0.5
0.1
0.1
0.08
0.08
0.08
0.08
0.08
0.08
0.08
0.08
0.20
0.08
0.1
0.1
0.1
0.08
0.08
0.08
0.08
0.1
0.1
0.1
0.08

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[75 FR 60239, Sept. 29, 2010]

Back to Top
§180.121 Methyl parathion; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide methyl parathion, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only methyl parathion, O,O-dimethyl O-(4-nitrophenyl) phosphorothioate, in
or on the commodity.

Commodity
Alfalfa, forage
Alfalfa, hay
Almond
Almond, hulls
Barley
Corn, field, forage
Corn, field, grain
Corn, pop, grain
Corn, sweet, forage

Parts per
million
1.25
5.0
0.1
3.0
1.0
1.0
1.0
1.0
1.0

Expiration/
Revocation
date
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13

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Corn, sweet, kernel plus cob with husks removed
Cotton, undelinted seed
Grass, forage
Oat
Onion
Pea, field, vines
Potato
Rapeseed, seed
Rice, grain
Soybean, hay
Soybean, seed
Sunflower, seed
Sweet potato, roots
Walnut
Wheat

1.0
0.75
1.0
1.0
1.0
1.0
0.1
0.2
1.0
1.0
0.1
0.2
0.1
0.1
1.0

12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 1245, Jan. 5, 2001, as amended at 66 FR 38955, July 26, 2001; 67 FR 38603, June 5, 2002; 72 FR 35666, June 29, 2007;
73 FR 54959, Sept. 24, 2008; 74 FR 46372, Sept. 9, 2009; 76 FR 56652, Sept. 14, 2011; 78 FR 60721, Oct. 2, 2013]

Back to Top
§180.123 Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of inorganic bromides (calculated as Br) in or on the following
food commodities which have been fumigated with the antimicrobial agent and insecticide methyl bromide after harvest
(with the exception of strawberry):
Commodity
Alfalfa, hay, postharvest
Almond, postharvest
Apple, postharvest
Apricot, postharvest
Artichoke, jerusalem, postharvest
Asparagus, postharvest
Avocado, postharvest
Barley, grain, postharvest
Bean, lima, postharvest
Bean, postharvest
Bean, snap, succulent, postharvest
Bean, succulent, postharvest
Beet, garden, roots, postharvest
Beet, sugar, roots, postharvest
Blueberry, postharvest
Butternut, postharvest
Cabbage, postharvest
Cacao bean, roasted bean, postharvest
Cantaloupe, postharvest
Carrot, roots, postharvest
Cashew, postharvest
Cherry, sweet, postharvest
Cherry, tart, postharvest
Chestnut, postharvest
Cippolini, bulb, postharvest
Citron, citrus, postharvest
Coconut, copra, postharvest
Coffee, bean, green, postharvest
Corn, field, grain, postharvest
Corn, pop, postharvest
Corn, sweet, kernel plus cob with husks removed, postharvest
Cotton, undelinted seed, postharvest
Cucumber, postharvest
Cumin, seed, postharvest
Eggplant, postharvest
Garlic, postharvest
Ginger, postharvest
Grape, postharvest

Parts per million
50.0
200.0
5.0
20.0
30.0
100.0
75.0
50.0
50.0
50.0
50.0
50.0
30.0
30.0
20.0
200.0
50.0
50.0
20.0
30.0
200.0
20.0
20
200.0
50.0
30.0
100.0
75.0
50.0
240.0
50.0
200.0
30.0
100.0
20.0
50.0
100.0
20.0

Expiration/Revocation Date
10/31/11
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
10/31/11
None
None
None
None
None
None

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Grapefruit, postharvest
Hazelnut, postharvest
Horseradish, postharvest
Kumquat, postharvest
Lemon, postharvest
Lime, postharvest
Melon, honeydew, postharvest
Muskmelon, postharvest
Nectarine, postharvest
Nut, brazil, postharvest
Nut, hickory, postharvest
Nut, macadamia, postharvest
Oat, postharvest
Okra, postharvest
Onion, bulb, postharvest
Onion, green, postharvest
Orange, postharvest
Parsnip, roots, postharvest
Peach, postharvest
Peanut, postharvest
Pear, postharvest
Pea, blackeyed, postharvest
Pea, postharvest
Pecan, postharvest
Pepper, postharvest
Pimento, postharvest
Pineapple, postharvest
Pistachio, postharvest
Plum, postharvest
Pomegranate, postharvest
Potato, postharvest
Pumpkin, postharvest
Quince, postharvest
Radish, postharvest
Rice, grain, postharvest
Rutabaga, roots, postharvest
Rutabaga, tops, postharvest
Rye, grain, postharvest
Salsify, roots, postharvest
Sorghum, grain, grain, postharvest
Soybean, postharvest
Squash, summer, postharvest
Squash, winter, postharvest
Squash, zucchini, postharvest
Strawberry, postharvest
Sweet potato, postharvest
Tangerine, postharvest
Timothy, hay, postharvest
Tomato, postharvest
Turnip, roots, postharvest
Walnut, postharvest
Watermelon, postharvest
Wheat

Page 55 of 441

30.0
200.0
30.0
30.0
30.0
30.0
20.0
20.0
20.0
200.0
200.0
200.0
50.0
30.0
20.0
20.0
30.0
30.0
20.0
200.0
5.0
50.0
50.0
200.0
30.0
30.0
20.0
200.0
20.0
100.0
75.0
20.0
5.0
30.0
50.0
30.0
30.0
50.0
30.0
50.0
200.0
30.0
20.0
20.0
60.0
75.0
30.0
50.0
20.0
30.0
200.0
20.0
50.0

None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
10/19/10
None
None
None
None
None

(2) Inorganic bromide may be present as a residue in certain processed food in accordance with the following
conditions:
(i) When inorganic bromide residues are present as a result of fumigation of the processed food with methyl bromide
or from such fumigation in addition to the authorized use of methyl bromide on the source raw agricultural commodity, as
provided for in this part, the total residues of inorganic bromides (calculated as Br) shall not exceed the following levels:
(A) 400 parts per million in or on egg, dried and herb, processed and spice.
(B) 325 parts per million in or on cheese, parmesan and cheese, roquefort cheese.
(C) 250 parts per million in or on tomato, concentrated products and fig, dried fruit.
(D) 125 parts per million in or on processed food other than those listed above.
(ii) When inorganic bromide residues are present in malt beverage, fermented in accordance with 21 CFR 172.730(a)
(2), the amount shall not exceed 25 parts per million (calculated as Br).

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(iii) Where tolerances are established on both the raw agricultural commodities and processed food made therefrom,
the total residues of inorganic bromides in or on the processed food shall not be greater than those designated in
paragraph (a)(2) of this section, unless a higher level is established elsewhere in this part.
(3) Tolerances are established for residues of inorganic bromides (calculated as Br) as follows:
(i) 400 parts per million for residues in or on dog food, resulting from fumigation with methyl bromide.
(ii) 125 parts per million for residues in or on processed commodities for animal feedstuffs from barley, corn, grain
sorghum, oat, rice, rye and wheat, resulting directly from fumigation with methyl bromide or from carryover and
concentration of residues of inorganic bromides from fumigation of the grains with methyl bromide.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established
for residues of inorganic bromides (calculated as Br) in or on the following food commodity grown in soil fumigated with
methyl bromide.
Commodity

Parts per million

Ginger, postharvest

100

(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74812, Dec. 13, 2006, as amended at 75 FR 60239, Sept. 29, 2010]

Back to Top
§180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.
(a) Investigations by the Food and Drug Administration show that peanut hay and peanut shells have been used as
feed for meat and dairy animals. While many growers now harvest peanuts with combines and leave the hay on the
ground to be incorporated into the soil, some growers follow the practice of curing peanuts on the vines in a stack and
save the hay for animal feed. Peanut shells or hulls have been used to a minor extent as roughage for cattle feed. It has
been established that the feeding to cattle of peanut hay and peanut hulls containing residues of inorganic bromides will
contribute considerable residues of inorganic bromides to the meat and milk.
(b) There are no tolerances for inorganic bromides in meat and milk to cover residues from use of such peanut hulls
as animal feed. Peanut hulls containing residues of inorganic bromides from the use of methyl bromide are unsuitable as
an ingredient in the feed of meat and dairy animals and should not be represented, sold, or used for that purpose.
[58 FR 65555, Dec. 15, 1993]

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§180.124 Methyl bromide; tolerances for residues.
(a) General. A tolerance is established for residues of the fumigant methyl bromide, including metabolites and
degradates, in or on the commodity in the table below. Compliance with the tolerance level specified below is to be
determined by measuring only methyl bromide.
Commodity

Parts per
million

Cotton, undelinted seed

150

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 35298, June 13, 2012]

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§180.127 Piperonyl butoxide; tolerances for residues.
(a) General. (1) Tolerances for residues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl piperonyl)ether]
are established in or on the following food commodities:
Commodity

Parts per million

Almond, postharvest
Apple, postharvest

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8
8

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Barley, postharvest
Bean, postharvest
Birdseed, mixtures, postharvest
Blackberry, postharvest
Blueberry, postharvest
Boysenberry, postharvest
Buckwheat, grain, postharvest
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherry, sweet, postharvest
Cherry, tart, postharvest
Cacoa bean, roasted bean, postharvest
Coconut, copra, postharvest
Corn, field, grain, postharvest
Corn, pop, postharvest
Cotton, undelinted seed, postharvest
Crabapple, postharvest
Currant, postharvest
Dewberry, postharvest
Egg
Fig, postharvest
Flax, seed, postharvest
Goat, fat
Goat, meat
Goat, meat byproducts
Gooseberry, postharvest
Grape, postharvest
Guava, postharvest
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Loganberry, postharvest
Mango, postharvest
Milk, fat
Muskmelon, postharvest
Oat, postharvest
Orange, postharvest
Peach, postharvest
Peanut, postharvest
Pea, postharvest
Pear, postharvest
Pineapple, postharvest
Plum, prune, fresh, postharvest
Potato, postharvest
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Raspberry, postharvest
Rice, postharvest
Rye, postharvest
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, postharvest
Sweet potato, postharvest
Tomato, postharvest
Walnut, postharvest
Wheat, postharvest

20
8
20
8
8
8
20
0.1
0.1
0.1
8
8
8
8
20
20
8
8
8
8
1
8
8
0.1
0.1
0.1
8
8
8
0.1
0.1
0.1
0.1
0.1
0.1
8
8
0.25
8
8
8
8
8
8
8
8
8
0.25
3
3
3
8
20
20
0.1
0.1
0.1
8
0.25
8
8
20

(2) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:
(i) It is used or intended for use in combination with pyrethrins for control of insects:
(A) In cereal grain mills and in storage areas for milled cereal grain products, whereby the amount of piperonyl
butoxide is at least equal to but not more than 10 times the amount of pyrethrins in the formulation.

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(B) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams
per square foot, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation.
Such treated bags are to be used only for food, dried.
(C) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth,
whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated
bags are constructed with waxed paper liners and are to be used only for food, dried that contain 4 percent fat or less.
(D) In two-ply bags consisting of cellophane/polyolefin sheets bound together by an adhesive layer when it is
incorporated in the adhesive. The treated sheets shall contain not more than 50 milligrams of piperonyl butoxide per
square foot (538 milligrams per square meter). Such treated bags are to be used only for packaging plum, prune, dried;
grape, raisin; and other fruit, dried and are to have a maximum ratio of 3.12 milligrams of piperonyl butoxide per ounce of
fruit (0.10 milligram of piperonyl butoxide per gram of product).
(E) In food processing and food storage areas: Provided, That the food is removed or covered prior to such use.
(ii) It is used or intended for use in combination with pyrethrins and N-octylbicycloheptene dicarboximide for insect
control in accordance with 21 CFR 178.3730.
(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide in or on:
(A) Grain, cereal, milled fractions when present therein as a result of its use in cereal grain mills and in storage areas
for milled cereal grain products.
(B) Food, dried when present as a result of migration from its use on the outer ply of multiwall paper bags of 50
pounds or more capacity.
(C) Food treated in accordance with 21 CFR 178.3730.
(D) Food, dried that contain 4 percent fat, or less, when present as a result of migration from its use on the cloth of
cotton bags of 50 pounds or more capacity constructed with waxed paper liners.
(E) Food treated in accordance with paragraph (a)(2)(i)(D) and (E) of this section.
(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(v) Where tolerances are established on both raw agricultural commodities and processed food made therefrom, the
total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the
two tolerances.
(3) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:
(i) It is used or intended for use in combination with pyrethrins for control of insects:
(A) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams
per square foot.
(B) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth.
Such treated bags are constructed with waxed paper liners and are to be used only for feed, dried that contain 4 percent
fat or less.
(ii) It is used in combination with pyrethrins, whereby the amount of piperonyl butoxide is equal to 10 times the amount
of pyrethrins in the formulation. Such treated bags are to be used only for feed, dried.
(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide when present as the result of
migration:
(A) In or on feed, dried from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.
(B) In or on feed, dried that contain 4 percent fat, or less, from its use on cotton bags of 50 pounds or more capacity
constructed with waxed paper liners.
(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency.
(v) Where tolerances are established on both the raw agricultural commodities and food, processed made therefrom,
the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of
the two tolerances.
(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74813, Dec. 13, 2006]

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§180.128 Pyrethrins; tolerances for residues.
(a) General. (1) Tolerances for residues of the insecticide pyrethrins ((1S)-2-methyl-4-oxo-3-(2Z)
-2,4-pentadienylcyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (pyrethrin 1), (1S)
-2-methyl-4-oxo-3-(2Z)-2,4-pentadienyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]
-2,2-dimethylcyclopropane-carboxylate (pyrethrin 2), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)
-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (cinerin 1), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (cinerin 2),
(1S)-2-methyl-4-oxo-3-(2Z)-2-pentenyl-2-cyclopenten-1-yl (1R, 3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)
cyclopropanecarboxylate (jasmolin 1), and (1S)-2-methyl-4-oxo-3-(2Z)-pentenyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (jasmolin 2)), the insecticidally active principles
of Chrysanthemum cinerariaefolium, which are measured as cumulative residues of pyrethrin 1, cinerin 1, and jasmolin 1
are not to exceed the following:
Commodity

Parts per million

Almond, postharvest
Apple, postharvest
Barley, grain, postharvest
Bean, succulent, postharvest
Birdseed, mixtures, postharvest
Blackberry, postharvest
Blueberry, postharvest
Boysenberry, postharvest
Buckwheat, grain, postharvest
Cacao bean, roasted bean, postharvest
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherry, sweet, postharvest
Cherry, tart, postharvest
Coconut, copra, postharvest
Corn, field, grain, postharvest
Corn, pop, grain, postharvest
Cotton, undelinted seed, postharvest
Crabapple, postharvest
Currant, postharvest
Dewberry, postharvest
Fig, postharvest
Flax, seed, postharvest
Goat, fat
Goat, meat
Goat, meat byproducts
Gooseberry, postharvest
Grape, postharvest
Guava, postharvest
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Loganberry, postharvest
Mango, postharvest
Milk, fat (reflecting negligible residues in milk)
Muskmelon, postharvest
Oat, grain, postharvest
Orange, postharvest
Pea, dry, seed, postharvest
Peach, postharvest
Peanut, postharvest
Pear, postharvest
Pineapple, postharvest
Plum, prune, fresh, postharvest
Potato, postharvest

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1.0
1.0
3.0
1.0
3.0
1.0
1.0
1.0
3.0
1.0
1.0
0.05
0.05
1.0
1.0
1.0
3.0
3.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.05
0.05
1.0
1.0
1.0
1.0
0.05
0.05
1.0
0.05
0.05
1.0
1.0
0.05
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.05

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Raspberry, postharvest
Rice, grain, postharvest
Rye, grain, postharvest
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, grain, postharvest
Sweet potato, postharvest
Tomato, postharvest
Walnut, postharvest
Wheat, grain, postharvest

1.0
3.0
3.0
1.0
0.05
0.05
1.0
0.05
1.0
1.0
3.0

(2) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on milled fractions derived
from grain, cereal when present as a result of its use in cereal grain mills and in storage areas for milled cereal grain
products.
(3) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on all food items in food
handling establishments where food and food products are held, processed, prepared and/or served. Food must be
removed or covered prior to use.
(4) Where tolerances are established on both the raw agricultural commodities and processed foods made there-from,
the total residues of pyrethrins in or on the processed food shall not be greater than that permitted by the larger of the two
tolerances.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74814, Dec. 13, 2006, as amended at 73 FR 5108, Jan. 29, 2008]

Back to Top
§180.129 o-Phenylphenol and its sodium salt; tolerances for residues.
(a) General. Tolerances are established for combined residues of the fungicide o-phenylphenol and sodium
o-phenylphenate, each expressed as o-phenylphenol, from postharvest application of either in or on the following food
commodities:
Commodity

Parts per million

Apple
Cantaloupe (NMT 10 ppm in edible portion)
Carrot, roots
Cherry
Citrus fruits
Cucumber
Lemon
Nectarine
Orange
Pepper, bell
Peach
Pear
Pineapple
Plum, prune, fresh
Sweet potato, roots
Tomato

25
125
20
5
10
10
10
5
10
10
20
25.0
10
20
15
10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54960, Sept. 24, 2008]

Back to Top
§180.130 Hydrogen Cyanide; tolerances for residues.
(a) General. A tolerance for residues of the insecticide hydrogen cyanide from postharvest fumigation as a result of
application of sodium cyanide is established as follows: 50 parts per million in or on Fruit, citrus.

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 39077, July 21, 1999]

Back to Top
§180.132 Thiram; tolerances for residues.
Link to an amendment published at 80 FR 72597, November 20, 2015.
(a) General. Tolerances for residues of the fungicide thiram (tetramethyl thiuram disulfide), including its metabolites
and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified is to be
determined by measuring only thiram.
Commodity

Parts per million

Apple

7.0
15

Avocado1

0.80

Banana1
Peach
Strawberry

7.0
20

1

No U.S. registrations as of September 23, 2009.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 49615, July 31, 2002, as amended at 74 FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, 2014; 79 FR 18822, Apr. 4, 2014;
80 FR 16306, Mar. 27, 2015; 80 FR 35252, June 19, 2015]

Back to Top
§180.142 2,4-D; tolerances for residues.
Link to an amendment published at 80 FR 72597, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including
its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be
determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the
acid, in or on the following commodities:
Commodity

Parts per million

Almond hulls
Asparagus
Barley, bran
Barley, grain
Barley, straw
Berry, group 13
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cranberry
Fish
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat

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0.1
5.0
4.0
2.0
50
0.2
0.3
4.0
0.3
0.3
6.0
0.05
50
0.05
50
6.0
0.05
50
0.5
0.1
3.0
0.05
0.05
0.3

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Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Grain, aspirated fractions
Grape
Grass, forage
Grass, hay
Hop, dried cones
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Millet, forage
Millet, grain
Millet, straw
Milk
Nut, tree, group 14
Oat, forage
Oat, grain
Oat, straw
Pistachio
Potato
Rice, grain
Rice, hulls
Rice, straw
Rye, bran
Rye, forage
Rye, grain
Rye, straw
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Shellfish
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Strawberry
Sugarcane, cane
Sugarcane, molasses
Teff, bran
Teff, forage
Teff, grain
Teff, straw
Vegetable, leaves of root and tuber, group 2
Vegetable, root and tuber, except potato, group 1
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, straw

4.0
0.3
0.3
40
0.05
360
300
0.2
0.3
4.0
0.3
0.3
25
2.0
50
0.05
0.2
25
2.0
50
0.05
0.4
0.5
2.0
10
4.0
25
2.0
50
0.3
4.0
0.3
0.3
1.0
0.2
0.2
0.2
0.02
2.0
0.02
0.05
0.05
0.2
4.0
25.0
2.0
50.0
0.1
0.1
4.0
25
2.0
50

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues
of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the follow
commodities:
Commodity

Parts per million

Rice, wild, grain

0.05

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide,
plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below.
Compliance with the tolerances levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic
acid), both free and conjugated, determined as the acid, in or on the following commodities:
Commodity

Parts per million

Animal feed, nongrass, group 18

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0.2

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Avocado
Cotton, undelinted seed
Dill, seed
Okra
Vegetable, brassica leafy, group 5
Vegetable, bulb, group 3
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, legume, group 6

0.05
0.05
0.05
0.05
0.4
0.05
0.05
0.2
0.05
0.4
0.05

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, 2009; 76 FR 55817, Sept. 9,
2011]

Back to Top
§180.145 Fluorine compounds; tolerances for residues.
(a) General. (1) Tolerances are established for combined residues of the insecticidal fluorine compounds cryolite and
synthetic cryolite (sodium aluminum fluoride) in or on the following agricultural commodities:
Commodity

Parts per million

Apricot
Blackberry
Blueberry
Boysenberry
Broccoli
Brussels sprouts
Cabbage
Cauliflower
Collards
Cranberry
Cucumber
Dewberry
Eggplant
Fruit, citrus
Grape
Kale
Kohlrabi
Lettuce, head
Lettuce, leaf
Loganberry
Melon
Nectarine
Peach
Pepper
Plum, prune, fresh
Pumpkin
Raspberry
Squash, summer
Squash, winter
Strawberry
Tomato
Youngberry

7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7

(2) Tolerances are established for residues of fluoride in or on the following commodities from the postharvest
fumigation with sulfuryl fluoride for the control of insects:
Commodity

Parts per million

All processed food commodities not otherwise listed
Barley, bran, postharvest
Barley, flour, postharvest
Barley, grain, postharvest
Barley, pearled barley, postharvest
Cattle, meat, dried
Cheese
Cacao bean, roasted bean, postharvest
Coconut, postharvest
Coffee, bean, green, postharvest
Corn, field, flour, postharvest
Corn, field, grain, postharvest

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

70
45.0
45.0
15.0
45.0
40
5.0
20
40
15
35.0
10.0

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Corn, field, grits, postharvest
Corn, field, meal, postharvest
Corn, pop, grain, postharvest
Cotton, undelinted seed, postharvest
Egg, dried
Fruit, dried, except grape, raisin, postharvest
Ginger, postharvest
Grain, aspirated fractions, postharvest
Grape, raisin, postharvest
Hog, meat
Herbs and spices group 19, postharvest
Milk, powdered
Millet, grain, postharvest
Nut, pine, postharvest
Nut, tree, Group 14, postharvest
Oat, flour, postharvest
Oat, grain, postharvest
Oat, groats/rolled oats
Peanut, postharvest
Pistachio, postharvest
Rice, bran, postharvest
Rice, flour, postharvest
Rice, grain, postharvest
Rice, hulls, postharvest
Rice, polished rice, postharvest
Rice, wild, grain, postharvest
Sorghum, grain, postharvest
Triticale, grain, postharvest
Vegetable, legume, group 6, postharvest
Wheat, bran, postharvest
Wheat, flour, postharvest
Wheat, germ, postharvest
Wheat, grain, postharvest
Wheat, milled byproducts, postharvest
Wheat, shorts, postharvest

10.0
30.0
10.0
70
900
3.0
70
55.0
7.0
20
70
5.0
40.0
20
10.0
75.0
25.0
75.0
15
10.0
31.0
45
12.0
35.0
25.0
25.0
40.0
40.0
70
40.0
125.0
130.0
40.0
130.0
40.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined by §180.1(l), are
established for the combined residues of the insecticidal fluorine compounds, cryolite and synthetic cryolite (sodium
aluminum fluoride), in or on the following raw agricultural commodities:
Commodity

Parts per million

Kiwifruit

15

(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74815, Dec. 13, 2006, as amended at 76 FR 34885, June 15, 2011]

Back to Top
§180.151 Ethylene oxide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the antimicrobial agent and insecticide ethylene oxide,
when used as a postharvest fumigant in or on the following food commodities:
Commodity

Parts per million

Herb and spice, group 19, dried, except basil
Licorice, roots
Peppermint, tops, dried
Sesame, seed
Spearmint, tops, dried
Vegetable, dried
Walnut

7
7
7
7
7
7
50

(2) Tolerances are established for residues of the ethylene oxide reaction product, 2-chloroethanol, commonly
referred to as ethylene chlorohydrin, when ethylene oxide is used as a postharvest fumigant in or on food commodities as
follows:
Commodity

Parts per million

Herb and spice, group 19, dried, except basil
Licorice, roots

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

940
940

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Peppermint, tops, dried
Sesame, seed
Spearmint, tops, dried
Vegetable, dried

940
940
940
940

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33695, May 24, 2000, as amended at 74 FR 46696, Sept. 11, 2009]

Back to Top
§180.153 Diazinon; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide diazinon, O,O-diethyl O-[6-methyl2-(1-methylethyl)-4-pyrimidinyl]phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:
Commodity

Parts per million

Almond, hulls
Apple
Apricot
Bean, lima
Bean, snap, succulent
Beet, garden, roots
Beet, garden, tops
Blueberry
Caneberry subgroup 13-07A
Carrot, roots
Cattle, fat
Cherry, sweet
Cherry, tart
Cranberry
Endive
Fig
Ginseng
Grape

3.0
0.50
0.20
0.50
0.50
0.75
0.70
0.50
0.75
0.75
0.50
0.20
0.20
0.50
0.70
0.50
0.75
0.752
0.50
0.75

Hazelnut
Kiwifruit1
Lettuce
Melon
Mushroom

0.70
0.75
0.752
0.20
0.75
0.75
0.50
0.20
0.50
0.50
0.20
0.50
0.75
0.70
0.50
0.75
0.70
0.05

Nectarine
Onion, bulb
Onion, green
Pea, succulent
Peach
Pear
Pineapple
Plum, prune, fresh
Radish
Rutabaga
Spinach
Strawberry
Tomato
Vegetable, brassica, leafy, group 5
Watercress
1

There are no domestic registrations for kiwifruit as of March 6, 2002.

2

The expiration/revocation date for this tolerance is 9/10/2010.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the insecticide diazinon, O, O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]
-phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:
Commodity

Parts per million

Almond

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.50

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Banana
Celery
Cucumber
Parsley, leaves
Parsnip
Pepper
Potato
Squash, summer
Squash, winter
Sweet potato, roots
Swiss chard
Turnip, roots
Turnip, tops

0.20
0.70
0.75
0.75
0.50
0.5
0.10
0.50
0.75
0.10
0.70
0.50
0.75

(d) Indirect or inadvertent residues. [Reserved]
[47 FR 42738, Sept. 29, 1982]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.153, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.154 Azinphos-methyl; tolerances for residues.
(a) General. Tolerances for residues of the insecticide O,O-dimethyl S-[(4-oxo-1,2,3-benzotriazin-3(4H)-yl)methyl]
phosphorodithioate in or on the following raw agricultural commodities:
Commodity

Parts per million

Expiration/Revocation Date

Almond1

0.2

None

Almond, hulls1

5.0

None

Apple2

1.5

None

Blackberry3

2.0

None

Blueberry2

5.0

None

Boysenberry3

2.0

None

Brussels sprouts4

2.0

None

Cherry2

2.0

None

Crabapple2

1.5

None

Cranberry3

0.5

12/31/12

Loganberry3

2.0

None

Parsley, leaves2

5.0

None

Parsley, turnip rooted, roots2

2.0

None

Peach3

2.0

None

Pear2

1.5

None

Pistachio1

0.3

None

Plum, prune5

2.0

None

Quince5

1.5

None

Raspberry3

2.0

None

Walnut1

0.3

None

1

There are no U.S. registrations as of October 30, 2009.

2

There are no U.S. registrations as of September 30, 2012.

3

There are no U.S. registrations since September 30, 2006.

4

There are no U.S. registrations since September 30, 2008.

5

There are no U.S. registrations since December 28, 2005.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 38752, June 22, 2000, as amended at 74 FR 46697, Sept. 11, 2009]

Back to Top

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§180.155 1-Naphthaleneacetic acid; tolerances for residues.
(a) General. Tolerances are established for the residues of 1-naphthaleneacetic acid, including its metabolites and
degradates in or on the commodities in the following table. Compliance with the tolerance levels specified is to be
determined by measuring only 1-naphthaleneacetic acid and its conjugates, calculated as the Stoichiometric equivalent of
1-naphthaleneacetic acid, in or on the commodity.
Parts per
million

Commodity
Avocado
Cherry, sweet
Fruit, pome, group 11-10
Mango
Olive
Orange

0.05
0.1
0.15
0.05
0.7
0.1
0.05

Pineapple1
Potato
Rambutan
Sapote, mamey
Tangerine

0.01
2.0
0.05
0.1

1

There are no U.S. registrations since 1988.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[78 FR 30218, May 22, 2013]

Back to Top
§180.163 Dicofol; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide dicofol, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only dicofol as the sum of its p,p-dicofol and o,p-dicofol isomers: 4-chloroα-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)
benzenemethanol, in or on the commodity.
Commodity
Apple, wet pomace
Bean, dry, seed
Bean, succulent
Butternut
Caneberry subgroup 13A
Chestnut
Citrus, dried pulp
Citrus oil
Cotton, refined oil
Cotton, undelinted seed
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grape
Grape, raisin
Hazelnut
Hop, dried cones
Nut, hickory
Nut, macadamia
Pecan
Peppermint, oil
Peppermint, tops
Spearmint, oil
Spearmint, tops
Strawberry
Tea, dried
Tea, plucked leaves
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Walnut

Parts per million

Expiration/revocation date
38.0
0.5
3.0
0.1
5.0
0.1
12.0
200.0
0.5
0.1
6.0
10.0
5.0
5.0
20.0
0.1
65.0
0.1
0.1
0.1
30.0
25.0
30.0
25.0
10.0
50.0
30.0
2.0
2.0
0.1

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
None
None
10/31/16
10/31/16
10/31/16

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(2) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or
on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be
determined by measuring only the sum of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, its
isomer o,p-dicofol, 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, and its metabolites 4-chloroα-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)
benzenemethanol, calculated as the stoichiometric equivalent of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)
-α-(trichloromethyl)benzenemethanol, in or on the commodity.
Commodity
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Egg
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk, fat (reflecting 0.75 ppm in whole milk)
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver

Parts per million

Expiration/Revocation Date
50.0
5.0
3.0
3.0
0.05
50.0
5.0
3.0
3.0
50.0
5.0
3.0
3.0
50.0
5.0
3.0
3.0
22.0
0.1
0.1
0.1
50.0
5.0
3.0
3.0

10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16
10/31/16

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34826, June 26, 1998, as amended at 72 FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, 2007; 77 FR 59124, Sept. 26,
2012]

Back to Top
§180.169 Carbaryl; tolerances for residues.
Link to an amendment published at 80 FR 72597, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per
se, in or on the following food commodities:
Commodity
Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple, wet pomace
Asparagus
Banana
Beet, sugar, roots
Beet, sugar, tops
Bushberry subgroup 13-07B
Cabbage
Cactus, fruit
Cactus, pads
Caneberry subgroup 13-07A
Citrus, oil
Clover, forage
Clover, hay
Corn, field, forage
Corn, field, grain

Parts per million
50
75
50
15
15
5.0
0.5
25
3.0
21
5.0
12
12.0
20
50
70
30
0.02

Expiration/revocation date
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None

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Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Cranberry
Dandelion, leaves
Endive
Flax, seed
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grain, aspirated fractions
Grape
Grape, raisin
Grass, forage
Grass, hay
Leaf petiole subgroup 4B
Lettuce
Millet, proso, grain
Millet, proso, straw
Nut, tree group 14, except walnut
Okra
Olive
Oyster
Parsley, leaves
Pea and bean, dried shelled, except soybean, subgroup 6C
Peanut
Peanut, hay
Pineapple
Pistachio
Rice, grain
Rice, hulls
Rice, straw
Sorghum grain, forage
Sorghum grain, grain
Sorghum grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Spinach
Strawberry
Sunflower, seed
Sweet potato, roots
Trefoil, forage
Trefoil, hay
Vegetable, brassica, leafy, group 5, except cabbage
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, subgroup 7A, except soybean
Vegetable, fruiting, group 8
Vegetable, leaves of root and tuber, group 2, except sugar beet tops
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root and tuber, group 1, except sugar beet and sweet potato
Walnut
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

20
0.02
20
185
0.1
215
5.0
3.0
22
10
0.5
10
12
10
70
10
12
100
15
3.0
10
1.0
20
0.1
4.0
10
0.25
22
1.0
0.05
20
2.0
0.1
15
30
60
30
10
30
15
15
0.5
22
4.0
0.5
0.2
15
25
10
3.0
60
5.0
75
10
2.0
1.0
30
1.0
30
20

None
None
None
None
None
None
10/31/09
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None

(2) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate, including its
metabolites: 1-naphthol (naphthyl-sulfate); 5,6-dihydrodihydroxycarbaryl; and 5,6-dihydrodihydroxy naphthol, calculated as
1-naphthyl N-methylcarbamate and the free and conjugated residues of carbaryl: 5,6-dihydro-5,6-dihydroxy carbaryl and
5-methoxy-6-hydroxy carbaryl, in or on the following food commodities:
Commodity
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat

Parts per million

Expiration/revocation date
0.5
1.0
3.0
0.5
0.5

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

None
None
None
10/31/09
None

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eCFR — Code of Federal Regulations

Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Sheep, fat
Sheep, meat
Sheep, meat byproducts

Page 70 of 441

1.0
3.0
0.5
1.0
3.0
0.5
1.0
3.0
1.0
5.0
5.0
0.5
1.0
3.0

None
None
None
None
None
None
None
None
None
10/31/09
10/31/09
None
None
None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are
established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food
commodities:
Commodity

Parts per million

Dillweed, fresh leaves

0.2

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33695, May 24, 2000, as amended at 66 FR 38955, July 26, 2001; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005;
73 FR 52611, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009]

Back to Top
§180.172 Dodine; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide dodine, including its metabolites and degradates,
in or on the commodities listed in the table below. Compliance with the tolerance levels specified in the table is to be
determined by measuring only dodine, N-dodecylguanidine acetate; in or on the following commodities.
Commodity

Parts per million

Almond, hull
Apple
Apple, wet pomace
Banana
Fruit, stone, crop group 12
Nuts, tree, crop group 14
Peanut
Pear
Strawberry

30.0
5.0
15.0
0.50
5.0
0.3
0.013
5.0
5.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, 2012]

Back to Top
§180.175 Maleic hydrazide; tolerances for residues.
(a) General. (1) Tolerances for residues of the herbicide and plant regulator maleic hydrazide
(1,2-dihydro-3,6-pyridazinedione) are established in or on the following raw agricultural commodities:
Commodity

Parts per million

Onion, bulb
Potato

15.0
50.0

(2) A food additive known as maleic hydrazide (1,2-dihydro-3,6-pyridazinedione) may be present in potato, chips
when used in accordance with the following conditions:
(i) The food additive is present as a result of the application of a pesticide formulation containing maleic hydrazide to
the growing potato plant in accordance with directions registered by the U.S. Environmental Protection Agency.

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(ii) The label of the pesticide formulation containing the food additive conforms to labeling registered by the U.S.
Environmental Protection Agency.
(iii) The food additive is present in an amount not to exceed 160 parts per million by weight of the finished food.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 64293, Dec. 5, 1997, as amended at 64 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, 2002]

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§180.176 Mancozeb; tolerances for residues.
Link to an amendment published at 80 FR 72597, November 20, 2015.
(a) General. Tolerances are established for residues of mancozeb (a coordination product of zinc ion and maneb
(manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodities in the
following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only
those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.
Commodity

Parts per million

Almond
Almond, hulls
Apple
Asparagus
Atemoya
Banana
Barley, bran
Barley, flour
Barley, grain
Barley, pearled barley
Barley, straw
Beet, sugar, dried pulp
Beet, sugar, roots
Beet, sugar, tops
Broccoli
Cabbage
Canistel
Cattle, kidney
Cattle, liver
Cherimoya
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Crabapple
Cranberry
Custard apple
Fennel
Flax, seed
Ginseng
Goat, kidney
Goat, liver
Grape
Hog, kidney
Hog, liver
Horse, kidney
Horse, liver
Lettuce, head
Lettuce, leaf
Mango
Oat, flour
Oat, grain

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0.1
4
0.6
0.1
3.0
2
20
20
5
20
25
3.0
1.2
60
7
9
15.0
0.5
0.5
3.0
40
0.1
15
0.1
40
70
0.1
40
0.5
0.6
5
3.0
2.5
0.15
1.2
0.5
0.5
1.5
0.5
0.5
0.5
0.5
3.5
18
15.0
20
5

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Oat, groats/rolled oats
Oat, straw
Onion, bulb
Papaya
Peanut
Peanut, hay
Pear
Pepper
Potato
Poultry, kidney
Poultry, liver
Quince
Rice, grain
Rye, bran
Rye, grain
Rye, straw
Sapodilla
Sapote, mamey
Sapote, white
Sheep, kidney
Sheep, liver
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Star apple
Sugar apple

20
25
1.5
10
0.1
65
0.6
12
0.2
0.5
0.5
0.6
0.06
20
5
25
15.0
15.0
15.0
0.5
0.5
0.15
0.25
0.15
15.0
3.0
10

Tangerine1
Tomato
Vegetable, cucurbit, group 9
Walnut
Wheat, bran
Wheat, flour
Wheat, germ
Wheat, grain
Wheat, middlings
Wheat, shorts
Wheat, straw

2.5
2.0
0.70
20
20
20
5
20
20
25

1

There are no U.S. registrations for use of mancozeb on tangerine.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registrations, as defined in §180.1(l), is
established for residues of the fungicide mancozeb, (a coordination product of zinc ion and maneb (manganese
ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodity in the following table in this
paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those
mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.
Commodity
Carrot, roots

Parts per million
1

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33708, May 24, 2000, as amended at 65 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003;
69 FR 29458, May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 50913, Aug.
18, 2010; 76 FR 18915, Apr. 6, 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, May 14, 2014]

Back to Top
§180.178 Ethoxyquin; tolerances for residues.
(a) General. A tolerance is established for residues of the plant regulator ethoxyquin (1,2-dihydro-6ethoxy-2,2,4-trimethylquinoline) from preharvest or postharvest use in or on the following commodity:
Commodity

Parts per million

Pear

3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[63 FR 57073, Oct. 26, 1998]

Back to Top
§180.181 Chlorpropham; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the plant regulator and herbicide chlorpropham (isopropyl
m-chlorocarbanilate (CIPC) in or on the following food commodities:
Commodity

Parts per million

Potato
Potato, wet peel

30
40

(2) Tolerances are established for the combined residues of the plant regulator and herbicide chlorpropham (isopropyl
m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham-O-sulfonic acid (4-HSA) in or on the following food
commodities:
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts except kidney
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts except kidney
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts except kidney
Milk
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts except kidney

0.20
0.30
0.06
0.06
0.20
0.30
0.06
0.06
0.20
0.30
0.06
0.06
0.20
0.30
0.06
0.06
0.30
0.20
0.30
0.06
0.06

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[43 FR 52487, Nov. 13, 1978, as amended at 63 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007]

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§180.182 Endosulfan; tolerances for residues.
(a)(1) General. Tolerances are established for residues of the insecticide endosulfan, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9ahexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate,
6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the
stoichiometric equivalent of endosulfan, in or on the commodity.

Commodity
Almond
Almond, hulls
Apricot
Bean
Broccoli
Brussels sprouts
Cabbage
Cantaloupe
Carrot, roots
Cattle, fat

Expiration/
revocation
date

Parts per million
0.3
1.0
2.0
2.0
3.0
2.0
4.0
1.0
0.2
13.0

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7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/16

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Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Cauliflower
Celery
Cherry, sweet
Cherry, tart
Collards
Cotton, gin byproducts
Cotton, undelinted seed
Cucumber
Eggplant
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hazelnut
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Kale
Lettuce, head
Lettuce, leaf
Milk, fat
Muskmelon
Mustard greens
Mustard, seed
Nectarine
Nut, macadamia
Peach
Pear
Pineapple
Pineapple, process residue
Plum
Plum, prune
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver
Squash, summer
Strawberry
Sweet potato, roots
Walnut
Watermelon

5.0
2.0
1.0
2.0
8.0
2.0
2.0
2.0
30.0
1.0
1.0
1.0
13.0
5.0
2.0
1.0
0.2
13.0
5.0
2.0
1.0
13.0
5.0
2.0
1.0
2.0
11.0
6.0
2.0
1.0
2.0
0.2
2.0
0.2
2.0
2.0
1.0
20.0
2.0
2.0
13.0
5.0
2.0
1.0
1.0
2.0
0.15
0.2
1.0

7/31/16
7/31/16
7/31/16
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/16
7/31/16
7/31/16
7/31/16
7/31/12
7/31/16
7/31/16
7/31/16
7/31/16
7/31/16
7/31/16
7/31/16
7/31/16
7/31/12
7/31/12
7/31/12
7/31/16
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/12
7/31/13
7/31/16
7/31/16
7/31/12
7/31/12
7/31/16
7/31/16
7/31/16
7/31/16
7/31/12
7/31/16
7/31/12
7/31/12
7/31/12

(2) A tolerance is established for the combined residues of the insecticide endosulfan, 6,7,8,9,10,10hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2, 4,3-benzodioxathiepin-3-oxide (alpha and beta isomers), and its
metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,
4,3-benzodioxathiepin-3,3-dioxide in or on the commodity in the following table:
Commodity
Parts per million
Tea, dried
24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide to growing tea

Expiration/
revocation date
7/31/16

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. (1) Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities
in the table in this paragraph, when endosulfan is used in the state of Florida. Compliance with the tolerance levels
specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its
metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9ahexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in
or on the commodity.
Commodity

Parts per million

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Apple
Apple, wet pomace
Blueberry
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Pepper
Potato
Pumpkin
Squash, winter
Tomato

1.0
5.0
0.3
12.0
0.2
14.0
2.0
0.2
1.0
1.0
1.0

Expiration/
revocation
date
12/31/14
12/31/14
12/31/14
12/31/14
12/31/14
12/31/14
12/31/14
12/31/14
12/31/14
12/31/14
12/31/14

(2) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities
in the table in this paragraph, when endosulfan is used in the United States (except Florida). Compliance with the
tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its
metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9ahexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in
or on the commodity.

Commodity

Parts per million

Apple
Apple, wet pomace
Blueberry
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Pepper
Potato
Pumpkin
Squash, winter
Tomato

1.0
5.0
0.3
12.0
0.2
14.0
2.0
0.2
1.0
1.0
1.0

Expiration/
revocation
date
7/31/15
7/31/15
7/31/15
7/31/15
7/31/15
7/31/15
7/31/15
7/31/15
7/31/15
7/31/15
7/31/15

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33696, May 24, 2000, as amended at 71 FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, 2011; 78 FR 8409, Feb. 6, 2013]

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§180.183 Disulfoton; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl)
phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance
with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of disulfoton,
O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl)
phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog
sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl)
phosphorodithioate; and disulfoton oxygen analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate;
calculated as the stoichiometric equivalent of disulfoton, in or on the commodity.
Commodity
Bean, lima
Bean, snap, succulent
Broccoli
Brussels sprouts
Cabbage
Cauliflower
Coffee, green bean
Cotton, undelinted seed
Lettuce, head
Lettuce, leaf

Parts per million

Expiration/Revocation Date
0.75
0.75
0.75
0.75
0.75
0.75
0.2
0.75
0.75
2

12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
12/31/13
6/30/14
12/31/13
12/31/14
12/31/14

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration is established for residues of the
insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, including its metabolites and degradates, in or

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on the commodity in the following table. Compliance with the tolerance levels specified in this paragraph is to be
determined by measuring only the sum of disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its
metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorothioate; disulfoton sulfoxide, O,O-diethyl
S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl)
phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorodithioate; and disulfoton oxygen
analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate; calculated as the stoichiometric equivalent of
disulfoton, in or on the commodity.
Commodity
Asparagus

Parts per million

Expiration/Revocation Date
0.1

12/31/13

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, 2001; 67 FR 41806, June 19, 2002;
67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, 2009; 75 FR 60240,
Sept. 29, 2010]

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§180.184 Linuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the
tolerance levels specified below is to be determined by measuring only those linuron residues convertible to
3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity:
Commodity

Parts per million

Asparagus
Carrot, roots
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts except kidney and liver
Celeriac
Cilantro, dried leaves
Cilantro, fresh leaves
Coriander, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Dill, oil
Dill, seed
Dillweed, dried leaves
Dillweed, fresh leaves
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts except kidney and liver
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts except kidney and liver
Horseradish
Milk
Parsley, dried leaves
Parsley, leaves
Parsnip, roots
Parsnip, tops
Pea, dry, seed
Rhubarb
Sheep, fat

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7.0
1.0
0.2
2.0
2.0
0.1
0.1
1.0
10
3.0
0.01
1.0
0.1
6.0
1.0
0.25
6.0
5.0
0.25
2.0
0.5
5.0
1.5
0.2
2.0
2.0
0.1
0.1
0.05
0.05
0.1
0.2
2.0
2.0
0.1
0.1
0.05
0.05
9.0
4.0
0.05
0.05
0.09
0.5
0.2

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Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts except kidney and liver
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Soybean, vegetable

2.0
2.0
0.1
0.1
1.0
0.25
1.0
1.0
1.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide linuron
[3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea], including its metabolites and degradates, in or on the commodities in the
table below, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the
tolerance levels specified below is to be determined by measuring only those linuron residues convertible to
3.4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity. The tolerance expires
and is revoked on the date specified in the table.
Parts per
million

Commodity
Lentil

Expiration/revocation date
0.1

12/31/14

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are
established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites
and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric
equivalent of linuron, in or on the commodity.
Commodity

Parts per million

Celery
Potato
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.5
0.2
0.5
0.05
0.5
2.0

(d) Indirect or inadvertent residues. [Reserved]
[64 FR 41822, Aug. 2, 1999, as amended at 72 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, 2008; 76 FR 81396, Dec. 28, 2011;
79 FR 8307, Feb. 12, 2014]

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§180.185 DCPA; tolerances for residues.
(a) General. Tolerances for the combined residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its
metabolites monomethyltetrachloroterephthalate (MTP) and tetrachloroterephthalic acid (TCP) (calculated as dimethyl
tetrachloroterephthalate) are established in or on the following food commodities:
Commodity

Parts per million

Cantaloupe
Garlic
Ginseng
Horseradish
Muskmelon
Onion, bulb
Onion, green
Strawberry
Tomato
Vegetable, brassica, leafy, group 5
Watermelon

1.0
1.0
2.0
2.0
1.0
1.0
1.0
2.0
1.0
5.0
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for the combined inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its
metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or
on the following food commodities:
Commodity

Parts per million

Radish, roots
Radish, tops

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

2.0
15.0

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(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of
the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid
(MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:
Commodity

Parts per million

Basil, dried leaves
Basil, fresh leaves
Bean, dry
Bean, mung, seed
Bean, snap, succulent
Celeriac
Chicory, roots
Chicory, tops
Chive
Coriander, leaves
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, forage
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Cucumber
Dill
Eggplant
Lettuce
Marjoram
Parsley, dried leaves
Parsley, leaves
Pea, blackeyed, seed
Pepper
Pimento
Potato
Radicchio
Radish, oriental, roots
Radish, oriental, tops
Rutabaga
Soybean
Squash, summer
Squash, winter
Sweet potato
Turnip, roots
Turnip, tops
Yam, true, tuber

20.0
5.0
2.0
2.0
2.0
2.0
2.0
5.0
5.0
5.0
0.4
0.05
0.4
0.4
0.05
0.4
0.4
0.05
0.4
0.2
1.0
5.0
1.0
2.0
5.0
20.0
5.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
2.0
2.0
1.0
1.0
2.0
2.0
5.0
2.0

[72 FR 52018, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, 2008; 74 FR 14744, Apr. 1,
2009]

Back to Top
§180.189 Coumaphos; tolerances for residues.
(a) General. Tolerances for residues of the insecticide coumaphos (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1benzopyran-7-yl phosphorothioate and its oxygen analog (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl
phosphate) in or on food commodities as follows:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Honey
Honeycomb
Horse, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.15
45.0
1.0

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Horse, meat
Horse, meat byproducts
Milk, fat ( = n in whole milk)
Sheep, fat
Sheep, meat
Sheep, meat byproducts

1.0
1.0
0.5
1.0
1.0
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 39077, July 21, 1999, as amended at 65 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, 2002; 69 FR 29458, May 24, 2004;
72 FR 28876, May 23, 2007]

Back to Top
§180.190 Diphenylamine; tolerances for residues.
(a) General. Tolerances for residues of the plant regulator diphenylamine are established in or on the following
commodities:
Commodity
Apple, wet pomace
Apple from preharvest or postharvest use, including use of impregnated wraps
Cattle, fat
Cattle, liver
Cattle, meat byproducts, except liver
Cattle, meat
Goat, fat
Goat, liver
Goat, meat byproducts, except liver
Goat, meat
Horse, fat
Horse, liver
Horse, meat byproducts, except liver
Horse, meat
Milk
Pear (post harvest)
Sheep, fat
Sheep, liver
Sheep, meat byproducts, except liver
Sheep, meat

Parts per million
30.0
10.0
0.01
0.1
0.01
0.01
0.01
0.1
0.01
0.01
0.01
0.1
0.01
0.01
0.01
5.0
0.01
0.1
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 25848, May 13, 1999, as amended at 66 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, 2007; 76 FR 34885, June 15, 2011]

Back to Top
§180.191 Folpet; tolerances for residues.
(a) General. Tolerances are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on raw
agricultural commodities as follows:
Commodity

Parts per million

Apple1
Cranberry1
Cucumber1
Grape1
Grape, raisin1
Hop, dried cones
Lettuce1

5.0
15.0
2.0
50.0
80.0
120.0
50.0

Melon1

3.0

Onion,bulb1

2.0

Strawberry1

5.0

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Tomato1
1

25.0

No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations as defined in §180.1(l) are
established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on the following raw agricultural commodity:
Commodity

Parts per million

Avocado

25.0

(d) Indirect or inadvertent residues. [Reserved]
[61 FR 37222, July 17, 1996, as amended at 68 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, 2004; 72 FR 41928, Aug. 1, 2007]

Back to Top
§180.198 Trichlorfon; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide trichlorfon (dimethyl (2,2,2-trichloro-1hydroxyethyl) phosphonate) in or on the following food commodities:
Commodity

Parts per million

Cattle, fat1

0.5

Cattle, meat1

0.2

Cattle, meat byproducts1

0.1

1

There are no U.S. registrations for cattle commodities as of June 24, 1999.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 54578, Sept. 26, 2007]

Back to Top
§180.200 Dicloran; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide dicloran, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only dicloran, 2,6-dichloro-4-nitroaniline, in or on the commodity.
Commodity

Parts per
million

Apricot
Bean, snap, succulent
Carrot, roots
Celery
Cherry, sweet
Cucumber
Endive
Garlic
Grape
Lettuce
Nectarine
Onion
Peach
Plum, prune, fresh
Potato
Rhubarb
Sweet potato, roots
Tomato

Expiration/revocation date
20
20
10
15
20
5
10
5
10
10
20
10
20
15
0.25
10
10
5

None
None
11/2/11
None
None
None
None
None
None
None
None
None
None
None
12/31/14
None
None
None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[77 FR 40815, July 11, 2012]

Back to Top
§180.202 p-Chlorophenoxyacetic acid; tolerances for residues.
(a) General. A tolerance is established for the combined residues of the plant regulator p-chlorophenoxyacetic acid
and its metabolite p-chlorophenol to inhibit embryonic root development in or on the following food commodity:
Commodity

Parts per million

Bean, mung, sprouts

0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003, as amended at 71 FR 56398, Sept. 27, 2006]

Back to Top
§180.204 Dimethoate; tolerances for residues.
(a) General. Tolerances are established for total residues of the insecticide dimethoate (O,O-dimethyl S-(Nmethylcarbamoylmethyl) phosphorodithioate) including its oxygen analog (O,O-dimethyl S-(N- methylcarbamoylmethyl)
phosphorothioate) in or on the following food commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Bean, dry, seed
Bean, lima
Bean, snap, succulent
Blueberry1
Broccoli
Cattle, meat byproducts
Cauliflower
Celery
Citrus, dried pulp
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Cotton, undelinted seed
Egg
Endive
Goat, meat byproducts
Grapefruit
Hog, meat byproducts
Horse, meat byproducts
Kale
Lemon
Lettuce, leaf
Melon
Milk
Mustard greens
Orange
Pea
Pear
Pecan
Pepper
Potato
Poultry, meat byproducts
Safflower, seed
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

2.0
2.0
2.0
2.0
2.0
1.0
2.0
0.02
2.0
2.0
5.0
1.0
0.1
1.0
0.1
1.0
1.0
0.1
0.02
2.0
0.02
2.0
0.02
0.02
2.0
2.0
2.0
1.0
0.002
2.0
2.0
2.0
2.0
0.1
2.0
0.2
0.02
0.1
0.02
0.1
0.1

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Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Swiss chard
Tangerine
Tomato
Turnip, roots
Turnip, tops
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw
1

0.1
2.0
2.0
0.05
2.0
2.0
2.0
0.2
2.0
2.0
0.04
2.0
2.0

There are U.S. registrations as of August 16, 1996.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for total residues of dimethoate including its oxygen analog in or on the following food commodities:
Commodity

Parts per million

Asparagus
Brussels sprouts
Cherry, sweet
Cherry, tart

0.15
5.0
2.0
2.0

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33697, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, 2008]

Back to Top
§180.205 Paraquat; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for residues of the desiccant, defoliant, and herbicide paraquat (1,1′
-dimethyl-4,4′-bipyridinium-ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both
calculated as the cation) in or on the following food commodities:
Commodity

Parts per million

Acerola
Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Artichoke, globe
Asparagus
Atemoya
Avocado
Banana
Barley, grain
Barley, hay
Barley, straw
Beet, sugar, roots
Beet, sugar, tops
Berry group 13
Biriba
Cacao bean, bean
Canistel
Carrot, roots
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Cherimoya
Coffee, bean, green
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
0.5
75.0
210.0
0.05
0.5
0.05
0.05
0.05
0.05
3.5
1.0
0.5
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.5
0.05
0.05
0.05
0.05
3.0
0.1
10.0
0.1
10.0

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Corn, sweet, kernel plus cob with husks removed
Cotton, gin byproducts
Cotton, undelinted seed
Cowpea, forage
Cowpea, hay
Cranberry
Custard apple
Egg
Endive
Feijoa
Fig
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Grain, aspirated fractions
Grape
Grass, forage
Grass, hay
Guar, seed
Guava
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts, except kidney
Hop, dried cones
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Ilama
Jaboticaba
Kiwifruit
Lentil, seed
Lettuce
Longan
Lychee
Mango
Milk
Nut, tree, group 14
Okra
Olive
Onion, bulb
Onion, green
Papaya
Passionfruit
Pawpaw
Pea and bean, dried shelled, except soybean, subgroup 6C, except guar bean
Pea and bean, succulent shelled, subgroup 6B
Pea, field, hay
Pea, field, vines
Peanut
Peanut, hay
Peppermint, tops
Persimmon
Pineapple
Pineapple, process residue
Pistachio
Pomegranate
Pulasan
Rambutan
Rhubarb
Rice, grain
Rice, straw
Safflower, seed
Sapodilla
Sapote, black
Sapote, mamey
Sapote, white
Sheep, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
110.0
3.5
0.1
0.4
0.05
0.05
0.01
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.5
0.05
0.05
65.0
0.05
90.0
40.0
0.5
0.05
0.05
0.5
0.05
0.05
0.5
0.05
0.5
0.05
0.05
0.05
0.05
0.05
0.3
0.05
0.05
0.05
0.05
0.01
0.05
0.05
0.05
0.1
0.05
0.05
0.2
0.05
0.3
0.05
0.8
0.2
0.05
0.5
0.5
0.05
0.05
0.25
0.05
0.05
0.05
0.05
0.05
0.05
0.06
0.05
0.05
0.05
0.05
0.05
0.05

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Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Sorghum, forage, forage
Sorghum, grain, forage
Sorghum, grain, grain
Soursop
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Spanish lime
Spearmint, tops
Star apple
Starfruit
Strawberry
Sugar apple
Sugarcane, cane
Sugarcane, molasses
Sunflower, seed
Turnip, greens
Turnip, roots
Vegetable, brassica, leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, legume, edible podded, subgroup 6A
Vegetable, tuberous and corm, subgroup 1C
Wax jambu
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.5
0.05
0.05
0.1
0.1
0.05
0.05
0.4
10.0
4.5
0.7
0.05
0.5
0.05
0.05
0.25
0.05
0.5
3.0
2.0
0.05
0.05
0.05
0.05
0.05
0.05
0.50
0.05
0.5
1.1
3.5
50.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(l), are established
for residues of the pesticide paraquat (1,1′-dimethyl-4,4′ bipyridinium ion) derived from application of either the bis(methyl
sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:
Commodity

Parts per million

Pea, pigeon, seed
Taro, corm
Tyfon

0.05
0.1
0.05

(d) Indirect or inadvertent residues. [Reserved]
[46 FR 51614, Oct. 21, 1981]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.205, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.206 Phorate; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide phorate (O,O-diethyl S (ethylthio)
methyl]phosphorodithioate), phorate sulfoxide, phorate sulfone, phorate oxygen analog, phorate oxygen analog sulfoxide,
and phorate oxygen analog sulfone in or on the following food commodities:
Commodity

Parts per million

Bean, dry, seed
Bean, succulent
Beet, sugar, roots
Beet, sugar, tops
Coffee, green bean1
Corn, field, forage
Corn, field, grain
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Cotton, undelinted seed
Hop, dried cones
Peanut

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
0.05
0.3
3.0
0.02
0.5
0.05
0.5
0.05
0.05
2.0
0.1

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Potato
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Sugarcane, cane
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw
1

0.2
0.05
0.1
0.05
0.05
1.5
0.05
1.5
0.05

There are no U.S. registrations as of September 1, 1993 for the use of phorate on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001;
67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR 53738, Sept. 17, 2008]

Back to Top
§180.207 Trifluralin; tolerances for residues.
(a) General. Tolerances are established for residues of trifluralin, including its metabolites and degradates, in or on
the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by only trifluralin α,α,α-trifluoro-2,6-dinitro-N,N-dipropyl-p-toluidine, in or on the commodity.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Asparagus
Barley, grain
Barley, hay
Barley, straw
Bean, mung, sprouts
Carrot, roots
Celery
Corn, field, forage
Corn, field, grain
Corn, field, stover
Cotton, gin byproducts
Endive
Fruit, citrus, group 10
Fruit, stone, group 12
Grape
Hop, dried cones
Nut, tree, group 14
Oilseed, crop group 20
Okra
Peanut
Peanut, hay
Peppermint, oil
Peppermint, tops
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Spearmint, oil
Spearmint, tops
Sugarcane, cane
Vegetable, brassica, leafy group 5
Vegetable, bulb, group 3
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root and tuber, group 1, except carrot
Wheat, grain
Wheat, straw

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

3.0
2.0
0.05
0.05
0.05
0.05
0.05
2.0
1.0
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
2.0
0.05
0.05
0.05
0.05
2.0
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 42619, June 25, 1980, as amended at 45 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, 1980; 46 FR 37250, July 20,
1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR
21643, Apr. 27, 2005; 71 FR 54433, Sept. 15, 2006; 78 FR 46274, July 31, 2013]

Back to Top
§180.208 Benfluralin; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide benfluralin, N-butyl-N-ethyl-αααtrifluoro-2,6-dinitro-p-toluidine, in or on the following food commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Clover, forage
Clover, hay
Lettuce
Trefoil, forage
Trefoil, hay

0.05
0.05
0.05
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003, as amended at 73 FR 52613, Sept. 10, 2008]

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§180.209 Terbacil; tolerances for residues.
(a) General. Tolerances are established for combined residues of the herbicide terbacil, (3-tert-butyl-5-chloro-6methyluracil) and its metabolites [3-tert-butyl-5-chloro-6-hydroxymethyluracil], [6-chloro-2,3-dihydro-7-hydroxymethyl
3,3-dimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], and [6-chloro-2,3-dihydro-3,3,7-trimethyl-5H-oxazolo(3,2-a) pyrimidin-5one], calculated as terbacil, in or on the following raw agricultural commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Apple
Asparagus
Blueberry
Caneberry subgroup 13A
Peach
Peppermint, tops
Spearmint, tops
Strawberry
Sugarcane, cane
Watermelon

1.0
2.0
0.3
0.4
0.2
0.2
0.2
2.0
2.0
0.1
0.4
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 30818, May 31, 2006]

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§180.210 Bromacil; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide bromacil (5-bromo-3-sec-butyl-6-methyluracil) in
or on the following food commodities:

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Commodity

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Parts per million

Fruit, citrus
Pineapple

0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003]

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§180.211 Propachlor; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide propachlor (2-chloro-Nisopropylacetanilide) and its metabolites containing the N-isopropylaniline moiety, calculated as 2-chloro-Nisopropylacetanilide, in or on the following raw agricultural commodities:
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Milk
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Sorghum, forage, forage
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover

0.05
0.2
0.02
0.05
3.0
0.2
1.0
3.0
0.05
0.2
0.02
0.05
0.02
0.02
0.02
0.05
0.2
0.02
0.05
0.02
0.05
0.2
0.02
0.05
8.0
8.0
0.25
12.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 25959, June 16, 1982, as amended at 47 FR 28381, June 30, 1982; 47 FR 28626, July 1, 1982; 47 FR 46701, Oct. 20, 1982;
63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007]

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§180.212 S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide S-ethyl cyclohexylethylthiocarbamate in or on
the following food commodities:
Commodity

Parts per million

Beet, garden, roots
Beet, garden, tops
Beet, sugar, roots
Beet, sugar, tops
Spinach

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0.05(N)
0.05(N)
0.05(N)
0.05(N)
0.05(N)

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003]

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§180.213 Simazine; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide simazine (2-chloro-4,6-bis
(ethylamino)-s-triazine) and its two chlorinated degradates (2-amino-4-chloro-6-ethylamino-s-triazine and 2,4-diamino-6chloro-s-triazine), the total residue to be measured in or on the following food commodities:
Commodity

Parts per million

Almond
Almond, hulls
Apple
Avocado
Blackberry
Blueberry
Cattle, meat
Cattle, meat byproducts
Cherry
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cranberry
Currant
Egg
Goat, meat
Goat, meat byproducts
Grape
Grapefruit
Hazelnut
Horse, meat
Horse, meat byproducts
Lemon
Loganberry
Milk
Nut, macadamia
Olive
Orange
Peach
Pear
Pecan
Plum
Raspberry
Sheep, meat
Sheep, meat byproducts
Strawberry
Walnut

0.25
0.25
0.20
0.20
0.20
0.20
0.03
0.03
0.25
0.20
0.20
0.25
0.20
0.25
0.20
0.25
0.25
0.25
0.25
0.03
0.03
0.03
0.20
0.25
0.20
0.03
0.03
0.25
0.20
0.03
0.25
0.20
0.25
0.20
0.25
0.20
0.20
0.20
0.03
0.03
0.25
0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, 2007; 72 FR 53454, Sept. 19,
2007]

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§180.215 Naled; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide naled (1,2-dibromo-2,2-dichloro-ethyl
dimethyl phosphate) and its conversion product 2,2-dichlorovinyl dimethyl phosphate, expressed as naled, resulting from
the application of the pesticide to growing crops or from direct application to livestock and poultry, in or on the following
raw agricultural commodities:
Commodity

Parts per million

Almond, hulls
Almond
Bean, dry, seed
Bean, succulent
Beet, sugar, roots
Beet, sugar, tops
Broccoli
Brussels sprouts
Cabbage
Cauliflower
Celery
Collards
Cotton, undelinted seed
Cucumber
Eggplant
Grape
Grapefruit
Grass, forage
Hop, dried cones
Kale
Legume, forage
Lemon
Melon
Orange, sweet
Peach
Pea, succulent
Pepper
Pumpkin
Safflower, seed
Spinach
Squash, summer
Squash, winter
Strawberry
Swiss chard
Tangerine
Tomato
Turnip, greens
Walnut

0.5
0.5
0.5
0.5
0.5
0.5
1
1
1
1
3
3
0.5
0.5
0.5
0.5
3
10
0.5
3
10
3
0.5
3
0.5
0.5
0.5
0.5
0.5
3
0.5
0.5
1
3
3
0.5
3
0.5

(2) A tolerance of 0.5 part per million is established for the pesticide naled in or on all raw agricultural commodities,
except those otherwise listed in this section, from use of the pesticide for area pest (mosquito and fly) control.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[42 FR 46304, Sept. 15, 1977, as amended at 54 FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001;
77 FR 59124, Sept. 26, 2012]

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§180.217 Metiram; tolerances for residues.
(a) General. Tolerances are established for residues of a metiram (a mixture of 5.2 parts by weight of ammoniates of
[ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis [dithiocarbamic acid] bimolecular and trimolecular
cyclic anhydrosulfides and disulfides), including its metabolites and degradates, in or on the commodities in the following
table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those
metiram residues convertible to and expressed in terms of the degradate carbon disulfide.
Commodity

Parts per million

Apple
Apple, pomace, wet

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0.5
2

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Banana1

3
5

Grape, wine1
Potato

0.2

1

There are no U.S. registrations on bananas and grape, wine as of April 29, 2011.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 57074, Oct. 26, 1998, as amended at 76 FR 23891, Apr. 29, 2011]

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§180.220 Atrazine; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide atrazine (2-chloro-4-ethylamino-6isopropylamino-s-triazine) and its chlorinated metabolites 2-amino-4-chloro-6-isopropylamino-s-triazine, 2-amino-4-chloro6-ethylamino-s-triazine, and 2,4-diamino-6-chloro-s-triazine, in or on the following food commodities:
Commodity

Parts per
million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, forage
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Goat, fat
Goat, meat
Goat, meat byproducts
Grass, forage
Grass, hay
Guava
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Nut, macadamia
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, forage, forage
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Sugarcane, cane
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.02
0.02
0.02
1.5
0.20
0.5
1.5
0.20
0.5
15
0.20
2.0
0.02
0.02
0.02
4.0
4.0
0.05
0.02
0.02
0.02
0.02
0.20
0.02
0.02
0.02
0.25
0.25
0.20
0.50
0.20
1.5
0.10
5.0
0.50

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertant residues of atrazine,
2-chloro-4-ethylamino-6-isopropylamino-s-triazine, in or on the following raw agricultural commodity when present therein
as a result of application of atrazine to the growing crops in paragraph (a) of this section:
Commodity

Parts per million

Vegetable, leafy, except brassica, group 4

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0.25

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[43 FR 29121, July 6, 1978, as amended at 44 FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 1982; 47 FR 8012, Feb. 24, 1982; 63
FR 57075, Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; 72 FR 53454,
Sept. 19, 2007; 73 FR 37852, July 2, 2008; 76 FR 56654, Sept. 14, 2011]

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§180.222 Prometryn; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide prometryn, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the
following raw agricultural commodities:
Commodity

Parts per million

Bean, snap, succulent
Carrot, roots
Celeriac, roots
Celeriac, tops
Cilantro, leaves
Coriander, dried leaves
Cotton, gin byproducts
Cotton, undelinted seed
Dill, oil
Dillweed, dried leaves
Dillweed, fresh leaves
Leaf petioles subgroup 4B
Okra
Parsley, dried leaves
Parsley, leaves
Pea, pigeon, seed

0.05
0.45
0.05
0.20
3.5
9.0
1.0
0.25
1.3
1.1
0.30
0.50
0.05
1.5
0.60
0.25

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional exemptions. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide
prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the
tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)
-6-methylthio-s-triazine, in or on the following raw agricultural commodities.
Commodity

Parts per million

Barley, forage
Barley, hay
Barley, straw
Oat, forage
Oat, hay
Oat, straw
Rye, forage
Rye, hay
Rye, straw
Triticale, forage
Triticale, hay
Triticale, straw
Wheat, forage
Wheat, hay
Wheat, straw

0.3
1.0
0.3
0.3
1.0
0.3
0.3
1.0
0.3
0.3
1.0
0.3
0.3
1.0
0.3

[43 FR 29121, July 6, 1978, as amended at 45 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, 1989; 60 FR 20434, Apr. 26, 1995; 63
FR 17692, Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; 74 FR 67108,
Dec. 18, 2009; 76 FR 34885, June 15, 2011; 78 FR 55640, Sept. 11, 2013]

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§180.225 Phosphine; tolerances for residues.
(a) General. (1) Tolerances are established for residues of phosphine in or on the following raw agricultural
commodities (RACs) resulting from post-harvest fumigation for the control of insects with phosphine gas or phosphide
compounds that produce phosphine gas.
Commodity

Parts per million

Almond
Avocado

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0.1
0.01

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Banana
Barley, grain
Cabbage, Chinese, bok choy
Cabbage, Chinese, napa
Cacao bean, dried bean
Cashew
Citron, citrus
Coffee, bean, green
Corn, field, grain
Corn, pop, grain
Cotton, undelinted seed
Date, dried fruit
Dill, seed
Eggplant
Endive
Grapefruit
Hazelnut
Kumquat
Lemon
Lettuce
Lime
Mango
Millet, grain
Mushroom
Nut, brazil
Oat, grain
Okra
Orange, sweet
Papaya
Peanut
Pecan
Pepper
Persimmon
Pistachio
Rice, grain
Rye, grain
Safflower, seed
Salsify, tops
Sesame, seed
Sorghum, grain
Soybean, seed
Sunflower, seed
Sweet potato, roots
Tangelo
Tangerine
Tomato
Vegetable, legume, group 6, except soybean
Walnut
Wheat, grain

0.01
0.1
0.01
0.01
0.1
0.1
0.01
0.1
0.1
0.1
0.1
0.1
0.01
0.01
0.01
0.01
0.1
0.01
0.01
0.01
0.01
0.01
0.1
0.01
0.1
0.1
0.01
0.01
0.01
0.1
0.1
0.01
0.01
0.1
0.1
0.1
0.1
0.01
0.1
0.1
0.1
0.1
0.01
0.01
0.01
0.01
0.01
0.1
0.1

(2) Tolerances are established for residues of the fumigant in or on all RACs resulting from preharvest treatment of
pest burrows in agricultural and non-crop land areas.
Commodity
All raw agricultural commodities resulting from preharvest treatment of pest burrows

Parts per million
0.01

(3) Residues resulting from fumigation of processed food:
Commodity

Parts per million

Processed food

0.01

(4) Residues resulting from fumigation of animal feed:
Commodity

Parts per million

Animal feed

0.1

(5) To assure safe use of this pesticide, it must be used in compliance with the labeling conforming to that registered
by the U.S. Environmental Protection Agency (EPA) under FIFRA. Labeling shall bear a restriction to aerate the finished
food/feed for 48 hours before it is offered to the consumer, unless EPA specifically determines that a different time period
is appropriate. Where appropriate, a warning shall state that under no condition should any formulation containing

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aluminum or magnesium phosphide be used so that it will come in contact with any processed food, except processed
brewer's rice, malt, and corn grits stored in breweries for use in the manufacture of beer.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[64 FR 72950, Dec. 29, 1999, as amended at 71 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, 2007; 74 FR 46372, Sept. 9, 2009]

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§180.226 Diquat; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the plant growth regulator and herbicide diquat,
(6,7-dihydrodipyrido (1,2-a:2′1′-c)pyrazinediium) derived from application of the dibromide salt and calculated as the cation
in or on the following food commodities:
Commodity

Parts per million

Alfalfa, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Canola, meal
Canola, seed
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Potato
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

3.0
0.05
0.05
0.05
6.0
2.0
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.02
0.1
0.05
0.05
0.05
0.05
0.05
0.05

(2)(i) Tolerances are established for residues of the herbicide diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium)
(calculated as the cation) derived from the application of the dibromide salt to ponds, lakes, reservoirs, marshes, drainage
ditches, canals, streams, and rivers which are slow-moving or quiescent in programs of the Corp of Engineers or other
Federal or State public agencies and to ponds, lakes and drainage ditches only where there is little or no outflow of water
and which are totally under the control of the user, in or on the following food commodities:
Commodity

Parts per million

Avocado
Berry group 13
Cotton, undelinted seed
Cranberry
Fish
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grain, cereal, forage, fodder and straw, group 16
Grain, cereal, group 15
Grape
Grass, forage, fodder and hay, group 17
Hop, dried cones
Nut, tree, group 14
Shellfish
Strawberry
Sugarcane, cane
Vegetable, brassica, leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7

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0.2
0.05
0.2
0.05
2.0
0.05
0.02
0.02
0.02
0.02
0.05
0.2
0.2
0.02
20.0
0.05
0.2
0.05
0.02
0.2

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Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, root and tuber, group 1
Vegetable, seed and pod

0.05
0.05
0.02
0.05

(ii) Where tolerances are established at higher levels from other uses of diquat on the subject crops, the higher
tolerances applies also to residues of the aquatic uses cited in this paragraph.
(3) Tolerances are established for the plant growth regulator diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium)
derived from application of the dibromide salt and calculated as the cation in or on the following food commodites:
Commodity

Parts per million

Banana1

0.05

Coffee, bean, green1
Soybean, hulls

0.05
0.6

1

There are no U.S. registrations as of May 26, 2010.

(4) A tolerance of 0.5 part per million is established for residues of diquat in potato, granules/flakes and potato, chips.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33709, May 24, 2000, as amended at 72 FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, 2010; 75 FR 60241, Sept. 29,
2010]

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§180.227 Dicamba; tolerances for residues.
(a) General. (1) Tolerances are established for the residues of the herbicide dicamba (3,6-dichloro-o-anisic acid),
including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels
is to be determined by measuring only the sum of the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite,
3,6-dichloro-5-hydroxy-o-anisic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following
commodities:
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Grass, forage, fodder and hay, group 17, forage
Grass, forage, fodder and hay, group 17, hay
Millet, proso, forage
Millet, proso, grain
Millet, proso, hay
Millet, proso, straw
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Rye, forage
Rye, grain
Rye, straw
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Sugarcane, cane
Sugarcane, molasses
Teff, forage
Teff, grain

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6.0
2.0
15.0
3.0
0.1
3.0
0.1
3.0
0.50
0.04
0.50
0.2
125.0
200.0
90.0
2.0
40.0
30.0
90.0
2.0
40.0
30.0
90.0
2.0
30.0
3.0
4.0
10.0
0.3
5.0
90.0
6.0

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Teff, hay
Teff, straw
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

40.0
30.0
90.0
2.0
40.0
30.0

(2) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its
metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be
determined by measuring only the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-2hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:
Commodity

Parts per million

Asparagus
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Milk
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney

4.0
0.3
25.0
0.25
3.0
0.3
25.0
0.25
3.0
0.3
25.0
0.25
3.0
0.3
25.0
0.25
3.0
0.2
0.3
25.0
0.25
3.0

(3) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its
metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be
determined by measuring only the residues of dicamba, 3,6-dichloro-o-anisic acid, and its metabolites, 3,6-dichloro-5hydroxy-o-anisic acid, and 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in
or on the following commodities:
Commodity

Parts per million

Grain, aspirated fractions
Soybean, hulls
Soybean, seed

1000
30.0
10.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33709, May 24, 2000, as amended at 72 FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, 2008; 73 FR 54960, Sept. 24,
2008; 75 FR 60241, Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011]

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§180.229 Fluometuron; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethylN'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the
following food commodities:
Commodity

Parts per million

Cotton, gin byproducts
Cotton, undelinted seed

3.5
1.0

(2) Tolerances are established for the combined residues of the herbicide fluometuron, N,N-dimethylN'-[3-(trifluoromethyl)phenyl]urea, and its metabolites determined as TFMA and the hydroxylated metabolites: CGA-

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236431, 1-(4-hydroxy-3-trifluoromethylphenyl)urea; CGA-236432, 1-methyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea; and
CGA-13211, 1,1-dimethyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea, in or on the following food commodities:
Commodity

Parts per million

Cattle, meat byproducts
Egg
Goat, meat byproducts
Hog, meat byproducts
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, meat byproducts

0.1
0.1
0.1
0.1
0.1
0.02
0.1
0.1
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the herbicide
fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined
as TFMA, in or on the following food commodities.
Commodity
Grain, cereal, forage, fodder, and straw group 16, forage
Grain, cereal, forage, fodder, and straw, group 16, stover
Grain, cereal, group 15
Peanut
Peanut, hay
Peanut, meal
Soybean, forage
Soybean, hay
Soybean, seed
Rice, hulls
Wheat, milled byproducts

Parts per million
3.0
6.0
0.5
0.1
4.0
0.2
3.0
3.0
2.0
1.0
1.0

[73 FR 52613, Sept. 10, 2008]

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§180.231 Dichlobenil; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide dichlobenil
(2,6-dichlorobenzonitrile) and its metabolite 2,6-dichlorobenzamide in or on the following raw agricultural commodities:
Commodity

Parts per million

Apple
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Cranberry
Fruit, stone, group 12
Grape
Hazelnut
Pear
Rhubarb

0.5
0.15
0.10
0.1
0.15
0.15
0.1
0.5
0.06

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[36 FR 22540, Nov. 25, 1971, as amended at 63 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, 2001; 73 FR 50570, Aug. 27, 2008]

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§180.232 Butylate; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide butylate, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only butylate, S-ethyl bis (2-methylpropyl) carbamothioate, in or on the
commodity.

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Commodity
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed

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Parts per
million

Expiration/revocation date
0.1
0.1
0.1
0.1
0.1
0.1
0.1

3/23/13
3/23/13
3/23/13
3/23/13
3/23/13
3/23/13
3/23/13

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39439, July 1, 2003, as amended at 76 FR 23493, Apr. 27, 2011; 77 FR 59125, Sept. 26, 2012]

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§180.235 Dichlorvos; tolerances for residues.
(a) General. (1) Tolerances for residues of the insecticide 2,2-dichlorovinyl dimethyl phosphate are established as
follows:
Commodity
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Mushroom (residues expressed as naled)
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Raw agricultural commodities, nonperishable, bulk stored regardless of fat content, postharvest
Raw agricultural commodities nonperishable, packaged or bagged, containing 6 percent fat or less, postharvest
Raw agricultural commodities, nonperishable, packaged or bagged, containing more than 6 percent fat, postharvest
Sheep, fat
Sheep, meat
Sheep, meat byproducts

Parts per million
0.02(N)
0.02(N)
0.02(N)
0.05(N)
0.02(N)
0.02(N)
0.02(N)
0.02(N)
0.02(N)
0.02(N)
0.02(N)
0.5
0.05(N)
0.05(N)
0.05(N)
0.5
0.5
2
0.02(N)
0.02(N)
0.02(N)

(2) The tolerance of 0.1 part per million prescribed by 21 CFR 556.180 for negligible residues of 2,2-dichlorovinyl
dimethyl phosphate in hog, fat; hog, meat; hog, meat byproducts; and hog, skin covers both its use as an anthelmintic in
swine feed and as an insecticide applied directly to swine.
(3) Dichlorvos may be present as a residue from application as an insecticide on packaged or bagged nonperishable
processed food (see: 21 CFR 170.3(j)) in an amount in such food not in excess of 0.5 part per million (ppm). To assure
safe use of the insecticide, its label and labeling shall conform to the label and labeling registered by the U.S.
Environmental Protection Agency, and the usage employed shall conform with such label or labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, 1991; 63 FR 57075, Oct. 26,
1998; 65 FR 33697, May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR 59125, Sept. 26, 2012]

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§180.236 Triphenyltin hydroxide; tolerances for residues.

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(a) General. Tolerances are established for the combined residues of the fungicide triphenyltin hydroxide (TPTH) and
its monophenyltin (MPTH) and diphenyltin (DPTH) hydroxide and oxide metabolites, expressed in terms of parent TPTH,
in or on the following raw agricultural commodities:
Commodity

Parts per million

Beet, sugar, roots
Beet, sugar, tops
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Milk
Pecan
Potato
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat

0.05
10.0
0.2
2.0
4.0
0.5
0.2
2.0
4.0
0.5
0.3
0.06
0.3
0.2
2.0
4.0
0.5
0.06
0.05
0.05
0.2
2.0
4.0
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 41929, Aug. 1, 2007]

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§180.241 Bensulide; tolerances for residues.
(a) General. Tolerances are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of
N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of
N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:
Commodity

Parts per million

Onion, bulb
Vegetable, brassica, leafy group 5
Vegetable, cucurbits group 9
Vegetable, fruiting group 8
Vegetable, leafy except brassica group 4

0.10
0.15
0.15
0.10
0.15

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide
including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the
following food commodities:
Commodity

Parts per million

Carrot, roots

0.10

(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003, as amended at 73 FR 53738, Sept. 17, 2008]

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§180.242 Thiabendazole; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and
conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or on the commodity.
Parts per
million

Commodity
Alfalfa, forage
Alfalfa, hay
Apple, wet pomace

0.02
0.02
12.0
10.0

Avocado1
Banana, postharvest
Barley, grain
Barley, hay
Barley, straw
Bean, dry, seed
Brassica, head and stem, subgroup 5A

3.0
0.05
0.30
0.30
0.1
0.02
15.0

Cantaloupe1
Carrot, roots, postharvest
Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, forage
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernels plus cop with husks removed
Corn, sweet, stover
Fruit, citrus, group 10, postharvest
Fruit, pome, group 11, postharvest
Mango
Mushroom
Oats, forage
Oats, grain
Oats, hay
Oats, straw
Onion, bulb, subgroup 3-07A
Papaya, postharvest
Potato, postharvest
Radish, tops
Rye, forage
Rye, grain
Rye, straw
Soybean
Spinach

10.0
15.0
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
10.0
5.0
10.0
40.0
0.30
0.05
0.30
0.30
0.02
5.0
10.0
0.02
0.30
0.05
0.30
0.1
0.02
5.0

Strawberry1
Sweet potato (postharvest to sweet potato intended only for use as seed)
Triticale, forage
Triticale, grain
Triticale, hay
Triticale, straw
Vegetable, cucurbit, group 9
Vegetable, root (except sugarbeet), subgroup 1B
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.30
0.05
0.30
0.30
0.02
0.02
0.30
0.05
0.30
0.30

1

There are no U.S. registrations on the indicated commodity.

(2) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolites 5-hydroxythiabendazole (free and
conjugated) and benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or
on the commodity.
Commodity

Parts per million

Cattle, meat
Cattle, meat byproducts
Goat, meat byproducts

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0.1
0.4
0.4

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Hog, meat byproducts
Horse, meat byproducts
Milk
Sheep, meat byproducts

0.3
0.4
0.1
0.4

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for
residues of the thiabendazole, including its metabolites and degradates, in or on the specified agricultural commodities,
resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance
levels specified below is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and
its metabolite benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole. The
tolerances expire on the date specified in the table.
Commodity
Pea, succulent shelled

Parts per
million

Expiration date
0.02

12/31/18

(c) Tolerances with regional exemptions. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[42 FR 32783, June 28, 1977]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.242, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.243 Propazine; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide propazine, 2-chloro-4,6-bis(isopropylamino)
-s-triazine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the
tolerance levels specified in this paragraph is to be determined by measuring only the sum of propazine, 2-chloro-4,6-bis
(isopropylamino)-s-triazine, and its two chlorinated degradates, 2-amino-4-chloro-6-isopropylamino-s-triazine and
2,4-diamino-6-chloro-s-triazine, calculated as the stoichiometric equivalent of propazine, in or on the commodity.
Commodity

Parts per million

Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover

0.25
0.25
0.25

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[75 FR 60242, Sept. 29, 2010]

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§180.245 Streptomycin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide streptomycin in or on food commodities as
follows:
Commodity

Parts per million

Bean, dry, seed
Bean, succulent
Fruit, pome, group 11

0.5
0.5
0.25

(2) Tolerances are established for residues of the fungicide streptomycin from treatment of seedling plants before
transplanting in or on the following food commodities:
Commodity

Parts per million

Celery
Pepper
Tomato

0.25
0.25
0.25

(3) Tolerances are established for residues of the fungicide streptomycin from treatment of seed pieces in or on the
following food commodity:

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Commodity

Parts per million

Potato

0.25

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of streptomycin, in or on
the agricultural commodities, as specified in the following table, resulting from use of the pesticide pursuant to FIFRA
section 18 emergency exemptions. Compliance with the tolerance levels listed in the following table is to be determined by
measuring the levels of streptomycin only, in or on the commodities listed in the table. The tolerances expire on the dates
specified in the table.
Commodity

Parts per million

Grapefruit
Grapefruit, dried pulp

Expiration date
0.15
0.40

12/31/2015
12/31/2015

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003, as amended at 73 FR 54960, Sept. 24, 2008; 78 FR 29055, May 17, 2013]

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§180.249 Alachlor; tolerances for residues.
(a) General. Tolerances are established for combined residues of alachlor (2-chloro-2′,6″-diethyl-N-(methoxymethyl)
acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline
(1-HEEA) upon basic hydrolysis, calculated as alachlor in or on the following raw agricultural commodities.
Commodity

Parts per million

Beans, dry
Beans, succulent lima
Cattle, fat
Cattle, meat byproducts
Cattle, meat
Corn, field, forage
Corn, field, grain
Corn, field, pop
Corn, field, stover
Corn, pop, stover
Corn, sweet (K + CWHR)
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Cowpea, forage
Cowpea, hay
Egg
Goat, fat
Goat, meat byproducts
Goat, meat
Hog, fat
Hog meat byproducts
Hog, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Milk
Peanut
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Sheep, fat
Sheep, meat byproducts
Sheep, meat
Sorghum grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybeans, seed
Sunflower, meal
Sunflower, seed

0.1
0.1
0.02
0.02
0.02
2.0
0.2
0.2
2.0
2.0
0.05
2.0
0.7
0.03
5.0
5.0
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.5
0.02
0.02
0.02
0.02
0.02
0.02
2.0
0.1
1.0
1.0
3.4
2.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of alachlor
(2-chloro-2′,6′-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline
(DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor, in or on the following
raw agricultural commodities when present therein as a result of the application of alachlor to the growing crops in
paragraph (a) of this section:
Commodity
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Grain, cereal, forage, and straw, group 16 except corn, sorghum, rice, straw
Grain, cereal, forage, fodder and straw, group 16 except corn, sorghum, rice, forage
Grain, cereal, forage, fodder, and straw, group 16 except for corn, sorghum, rice, hay
Grain, cereal, group 15 except corn, sorghum, rice

Parts per million
1.4
1.2
0.8
0.6
0.8
0.05

[72 FR 54584, Sept. 26, 2007]

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§180.252 Tetrachlorvinphos; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide tetrachlorvinphos [(Z)-2-chloro1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate], including its metabolites, 1-(2,4,5-trichlorophenyl)-ethanol (free and
conjugated forms), 2,4,5-trichloroacetophenone, and 1-(2,4,5-trichlorophenyl)-ethanediol, in or on the following
commodities:
Parts per
million
0.2
1.0
0.5
2.0
1.0
0.2
0.2
1.0
0.5
2.0
1.0
0.05
7.0
2.0
3.0
2.0

Commodity
Cattle, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se)
Cattle, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se)
Cattle, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)
Cattle, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se)
Cattle, meat byproducts, except kidney and liver
Egg (of which no more than 0.05 ppm is tetrachlorvinphos per se)
Hog, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se)
Hog, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se)
Hog, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)
Hog, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se)
Hog, meat byproducts, except kidney and liver
Milk, fat (reflecting negligible residues in whole milk and of which no more than 0.05 ppm is tetrachlorvinphos per se)
Poultry, fat (of which no more than 7.0 ppm is tetrachlorvinphos per se)
Poultry, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)
Poultry, meat (of which no more than 3.0 ppm is tetrachlorvinphos per se)
Poultry, meat byproducts, except liver

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 57659, Sept. 16, 2011, as amended at 78 FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, 2013]

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§180.253 Methomyl; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide methomyl, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in
or on the commodity.
Commodity
Alfalfa, forage
Alfalfa, hay
Apple
Asparagus
Avocado
Barley, grain
Barley, hay
Barley, straw
Bean, dry, seed
Bean, forage

Parts per million

Expiration/revocation date
10
10
1
2
2
1
10
10
0.1
10

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

None
None
None
None
None
None
None
None
None
None

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Bean, succulent
Beet, garden, tops
Bermudagrass, forage
Bermudagrass, hay
Blueberry
Broccoli
Brussels sprouts
Cabbage
Cabbage, Chinese, bok choy
Cabbage, Chinese, napa
Cauliflower
Celery
Collards
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Dandelion, leaves
Endive
Grape
Grapefruit
Hop, dried cones1
Kale
Lemon
Lentil, seed
Lettuce
Mustard greens
Nectarine
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Onion, dry bulb
Onion, green
Orange
Parsley, leaves
Pea
Pea, field, vines
Peach
Peanut
Pecan
Pepper, bell
Pepper, nonbell
Peppermint, tops
Pomegranate
Rye, forage
Rye, grain
Rye, straw
Sorghum, grain, forage
Sorghum, grain, grain
Soybean, forage
Soybean, seed
Spearmint, tops
Spinach
Swiss chard
Tangerine
Tomato
Turnip, greens
Vegetable, brassica, leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetables, leafy2
Vegetable, root and tuber, group 1
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

Page 103 of 441

2
6
10
40
6
3
2
5
5
5
2
3
6
10
0.1
10
0.1
10
10
0.1
10
0.1
6
5
5
2
12

None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
12/31/16
None
None

6
2
0.1
5
6
5
10
1
10
10
0.2
3
2
6
5
10
5
0.1
0.1
2
2
2
0.2
10
1
10
1
0.2
10
0.2
2
6
6
2
1
6
6.0
0.2
0.2
0.2

None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None

0.2
10
1
10
10

None
None
None
None
None

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

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1

There are no U.S. registrations for use of methomyl on hop, dried cone, as of February 14, 1990.

2

Except for Beet (tops), broccoli, Brussels sprouts, cabbage, cabbage, Chinese, cauliflower, celery, collards,
dandelions, endive (escarole), kale, lettuce, mustard greens, parsley, spinach, Swiss chard, turnip, greens (tops), and
watercress.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established
for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodity in the table in
this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only
methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.
Parts
per million

Commodity
Pear

4

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33697, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29,
2010; 76 FR 34885, June 15, 2011; 77 FR 59125, Sept. 26, 2012; 80 FR 72598, Nov. 20, 2015]

Back to Top
§180.254 Carbofuran; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide carbofuran
(2,3-dihydro-2,2-dimethyl-7-benzofuranyl-N-methylcarbamate), its carbamate metabolite-2,3-dihydro-2,2-dimethyl-3hydroxy-7-benzofuranyl-N-methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7-benzofuranol,
2,3-dihydro-2,2-dimethyl-3,-oxo-7-benzofuranol and 2,3-dihydro-2,2-dimethyl-3,7-benzofurandiol in or on the following raw
agricultural commodities:
Commodity

Parts per million

Banana1

0.1

Coffee, bean, green1

0.1

Rice, grain1

0.2

Sugarcane, cane1

0.1

1

There are no U.S. registrations for use of carbofuran on these commodities.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[39 FR 20597, June 12, 1974]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.254, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.257 Chloroneb; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide chloroneb, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of chloroneb, 1,4-dichloro-2,5-dimethoxybenzene, and its
metabolite 2,5-dichloro-4-methoxyphenol (free and conjugated), calculated as the stoichiometric equivalent of chloroneb,
in or on the commodity.

Commodity
Bean, dry, seed
Bean, succulent
Beet, sugar, roots
Beet, sugar, tops
Cowpea, forage
Cowpea, hay
Cattle, fat

Expiration/
revocation
date

Parts per
million
0.2
0.2
0.2
0.2
2.0
2.0
0.2

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12

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Cattle, meat
Cattle, meat byproducts
Cotton, gin byproducts
Cotton, undelinted seed
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, seed

0.2
0.2
1.0
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.05
0.2
0.2
0.2
2.0
2.0
0.2

4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12
4/16/12

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003, as amended at 72 FR 53460, Sept. 19, 2007; 76 FR 56654, Sept. 14, 2011]

Back to Top
§180.258 Ametryn; tolerances for residues.
(a) General. Tolerances are established for residues of the desiccant and herbicide (2-ethylamino)-4-(isopropylamino)
-6-(methylthio)-s-triazine in or on the following raw agricultural commodities:
Commodity
Banana
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Pineapple
Sugarcane, cane

Parts per million

Expiration/Revocation Date
0.25
0.1
0.05
0.05
0.05
0.05
0.5
0.25
0.5
0.05
0.05

6/16/10
None
None
None
None
None
6/16/10
6/16/10
6/16/10
None
None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[43 FR 29121, July 6, 1978, as amended at 48 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, 1983; 52 FR 33237, Sept. 2, 1987;
63 FR 57075, Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009]

Back to Top
§180.259 Propargite; tolerances for residues.
(a) General. Tolerances are established for residues of the pesticide propargite (2-(p-tert-butylphenoxy) cyclohexyl
2-propynyl sulfite) in or on the following food commodities.
Commodity

Parts per million

Almond
Almond, hulls
Bean, dry, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1
55.0
0.2
0.1
0.1
0.1

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Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, stover
Cotton, undelinted seed
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grape
Grapefruit
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Lemon
Milk, fat (0.08 ppm in milk)
Nectarine
Orange
Peanut
Peppermint, tops
Poultry, fat
Potato
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Spearmint, tops
Tea, dried
Walnut

30.0
10.0
0.1
10.0
0.1
10.0
10.0
10.0
0.1
0.1
0.1
0.1
0.1
0.4
10.0
5.0
0.1
0.1
0.1
100.0
0.1
0.1
0.1
5.0
2.0
4.0
10.0
0.1
50.0
0.1
0.1
0.1
0.1
0.1
10.0
5.0
10.0
50.0
10.0
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of propargite in or on the following raw agricultural commodities:
Commodity

Parts per million

Corn, sweet, kernel plus cob with husks removed

0.1

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33710, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 76 FR 34885, June 15,
2011]

Back to Top
§180.261 Phosmet; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide
S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following
table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of
phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog,
N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of
phosmet, in or on the commodity.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple
Apricot
Blueberry

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

20
40
10
10
5
10

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Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherry
Cranberry
Fruit, citrus, group 10
Goat, fat
Goat, meat
Goat, meat byproducts
Grape
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Kiwifruit
Milk
Nectarine
Nut, tree, group 14
Pea, dry, seed
Pea, field, hay
Pea, field, vines
Pea, succulent
Peach
Pear
Plum, prune, fresh
Potato
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sweet potato, roots

0.2
0.1
0.1
10
10
5
0.1
0.1
0.1
10
0.2
0.04
0.04
0.1
0.1
0.1
25
0.1
5
0.1
0.5
20
10
1
10
10
5
0.1
0.1
0.1
0.1
12

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the
insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl
phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate,
calculated as the stoichiometric equivalent of phosmet, in or on the commodity.
Commodity

Parts per million

Crabapple
Pistachio

20
0.1

(d) Indirect or inadvertent residues. [Reserved]
[43 FR 46538, Oct. 10, 1978, as amended at 45 FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, 1983; 52 FR 48539, Dec. 23, 1987;
53 FR 657, Jan. 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR 46698, Sept.
11, 2009; 75 FR 60242, Sept. 29, 2010]

Back to Top
§180.262 Ethoprop; tolerances for residues.
(a) General. Tolerances are established for residues of the nematocide and insecticide ethoprop, O-ethyl S,S-dipropyl
phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance
with the tolerance levels specified in this paragraph is to be determined by measuring only ethoprop, O-ethyl S,S-dipropyl
phosphorodithioate, in or on the commodity.
Commodity

Parts per million

Banana
Bean, lima
Bean, snap, succulent
Cabbage
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02

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Cucumber
Hop, dried cones
Peppermint, tops

0.02
0.02
0.02
0.02

Pineapple1
Potato
Spearmint, tops
Sugarcane, cane
Sweet potato, roots

0.02
0.02
0.02
0.02

1
There are no U.S. registrations as of July 23, 2009, except for existing stocks bearing old labeling whose sale,
distribution, and use is allowed, provided it is consistent with the terms of the cancellation order of July 9, 2009; i.e., the
EPA will allow the technical registrant to continue to sell and distribute existing stocks of the amended registered product
bearing old labeling for use on pineapple for 18 months (until January 9, 2011) and persons other than the registrant may
continue to sell and/or use existing stocks of product bearing the old labeling until such stocks are exhausted, provided
that such use is consistent with the terms of the previously approved labeling on, or that accompanied, the modified
product.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 53004, Nov. 24, 1982, as amended at 48 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 1987; 53 FR 30053, Aug. 10, 1988;
63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR 38955, July 26, 2001; 67 FR 49616, July 31, 2002; 73 FR 53731,
Sept. 17, 2008; 73 FR 54961, Sept. 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010]

Back to Top
§180.263 Phosalone; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide phosalone, S-(6-chloro-3-(mercaptomethyl)-2benzoxazolinone) O,O-diethyl phosphorodithioate, in or on the following food commodities:
Commodity

Parts per million

Expiration/Revocation Date

Apple1

10.0

9/30/13

Cherry1

15.0

9/30/13

Grape1

10.0

9/30/13

Peach1

15.0

9/30/13

Pear1

10.0

9/30/13

Plum, prune, fresh1

15.0

9/30/13

1

There are no U.S. registrations since 1992.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[74 FR 46698, Sept. 11, 2009]

Back to Top
§180.269 Aldicarb; tolerances for residues.
(a) General. Tolerances are established for combined residues of the insecticide and nematocide aldicarb (2-methyl2-(methylthio)propionaldehyde O-(methylcarbamoyl) oxime and its cholinesterase-inhibiting metabolites 2-methyl
2-(methylsulfinyl) propionaldehyde O-(methylcarbamoyl) oxime and 2-methyl-2-(methylsulfonyl) propionaldehyde
O-(methylcarbamoyl) oxime in or on the following food commodities:
Commodity

Parts per million

Bean, dry, seed
Beet, sugar, roots
Beet, sugar, tops
Citrus, dried pulp
Coffee, bean, green
Cotton, undelinted seed
Cotton, hulls
Grapefruit
Lemon

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1
0.05
1
0.6
0.1
0.1
0.3
0.3
0.3

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Lime
Orange, sweet
Peanut
Pecan
Potato
Sorghum, grain, bran
Sorghum, grain, grain
Sorghum, grain, stover
Soybean
Sugarcane, cane
Sweet potato, roots

0.3
0.3
0.05
0.5
1
0.5
0.2
0.5
0.02
0.02
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33710, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, 2008]

Back to Top
§180.272 Tribuphos; tolerances for residues.
(a) General. Tolerances are established for residues of the defoliant tribuphos (S,S,S-tributyl phosphorotrithioate) in
or on food commodities as follows:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cotton, gin byproducts
Cotton, undelinted seed
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.15
0.02
0.02
40.0
4.0
0.15
0.02
0.02
0.15
0.02
0.02
0.15
0.02
0.02
0.01
0.15
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33698, May 24, 2000, as amended at 67 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, 2007]

Back to Top
§180.274 Propanil; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for the combined residues of the herbicide propanil (3′, 4′
-dichloropropionanilide) and its metabolites convertible to 3, 4-dichloroaniline (3, 4-DCA) in or on the following food
commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Crayfish
Egg
Goat, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.10
0.05
1.0
0.05
0.30
0.10

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Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, bran
Rice, grain
Rice, hulls
Rice, straw
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.05
1.0
0.10
0.05
1.0
0.10
0.05
1.0
0.05
0.05
0.10
0.50
40
10
30
75
0.10
0.05
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34827, June 26, 1998, as amended at 72 FR 28888, May 23, 2007]

Back to Top
§180.275 Chlorothalonil; tolerances for residues.
(a) General. (1) Tolerances are established for the fungicide chlorothalonil (tetrachloroisophthalonitrile) and its
metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.
Commodity

Parts per million

Almond
Almond, hulls
Apricot
Asparagus
Banana (NMT 0.05 ppm in edible pulp)
Bean, dry, seed
Bean, snap, succulent
Blueberry
Brassica, head and stem, subgroup 5A
Carrot, roots
Celery
Cherry, sweet
Cherry, tart
Cocoa bean, dried bean
Coffee, bean, green
Corn, sweet, kernel plus cob with husks removed
Cranberry
Ginseng
Horseradish
Lentil
Lychee
Mango
Mushroom
Nectarine
Okra
Onion, bulb
Onion, green
Papaya
Parsnip, roots
Passionfruit
Pea, edible podded
Peach
Peanut
Pistachio
Plum
Plum, prune
Potato

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
1.0
0.5
0.1
0.5
0.1
5
1.0
5.0
1
15
0.5
0.5
0.05
0.20
1
5.0
4.0
4.0
0.10
15
1.0
1.0
0.5
6.0
0.5
5
15
1
3
5
0.5
0.3
0.2
0.2
0.2
0.1

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Rhubarb
Soybean
Starfruit
Tomato
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8, except tomato
Yam, true

4.0
0.2
3.0
5
5.0
6.0
0.10

(2) Tolerances are established for the metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food
commodities.
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat byproducts, except kidney
Cattle, meat
Goat, fat
Goat, kidney
Goat, meat byproducts, except kidney
Goat, meat
Hog, fat
Hog, kidney
Hog, meat byproducts, except kidney
Hog, meat
Horse, fat
Horse, kidney
Horse, meat byproducts, except kidney
Horse, meat
Milk
Sheep, fat
Sheep, kidney
Sheep, meat byproducts, except kidney
Sheep, meat

0.1
0.5
0.05
0.03
0.1
0.5
0.05
0.03
0.1
0.5
0.05
0.03
0.1
0.5
0.05
0.03
0.1
0.1
0.5
0.05
0.03

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for the combined residues of chlorothalonil and its metabolite in or on the following raw agricultural
commodities:
Commodity

Parts per million

Hazelnut
Peppermint, tops
Persimmon
Spearmint, tops

0.1
2
1.5
2

(d) Indirect or inadvertent residues. [Reserved]
[42 FR 56114, Oct. 21, 1977]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.275, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.276 Formetanate hydrochloride; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide formetanate hydrochloride, including its
metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels
specified in this paragraph is to be determined by measuring only formetanate hydrochloride, N,N-dimethylN'-[3-[(methylamino)carbonyl]oxy]phenyl]methanimidamide hydrochloride, in or on the commodity.
Commodity
Apple
Apple, wet pomace
Grapefruit
Lemon
Lime
Nectarine
Orange
Peach

Parts per
million

Expiration/revocation date
0.50
1.5
1.5
0.60
0.03
0.40
1.5
0.40

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

12/31/13
12/31/13
None
None
None
None
None
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Tangelo
Tangerine

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0.50
0.03
0.03

12/31/13
None
None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 40815, July 11, 2012]

Back to Top
§180.278 Phenmedipham; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide phenmedipham
(3-methoxycarbonylaminophenyl-3′-methylcarbanilate) in or on the following food commodities:
Commodity

Parts per million

Beet, garden, roots
Beet, garden, tops
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Spinach

0.2
0.2
0.5
0.2
0.1
0.1
4.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 28888, May 23, 2007]

Back to Top
§180.284 Zinc phosphide; tolerances for residues.
(a) General. Tolerances are established for residues of the phosphine resulting from the use of the rodenticide zinc
phosphide in or on the raw agricultural commodities as follows:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Barley, grain
Barley, hay
Barley, straw
Bean, dry, seed
Beet, sugar, roots
Beet, sugar, tops
Grape
Grass, rangeland, forage
Grass, rangeland, hay
Potato
Sugarcane, cane
Timothy, hay
Timothy, forage
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.2
0.2
0.05
0.2
0.2
0.05
0.05
0.2
0.01
0.1
0.1
0.05
0.01
0.5
0.5
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of phosphine resulting from the use of the rodenticide zinc phosphide in or on the following raw
agricultural commodities as follows:
Commodity

Parts per million

Artichoke, globe

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.01

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Beet, sugar, roots
Beet, sugar, tops

0.04
0.02

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 45182, Aug. 25, 1998, as amended at 63 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, 1999; 64 FR 61791, Nov. 15, 1999;
65 FR 8874, Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247,
Jan. 16, 2003; 68 FR 56195, Sept. 30, 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Sept. 9, 2009; 76 FR 34885, June 15, 2011]

Back to Top
§180.287 Amitraz; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for residues of the insecticide amitraz (N'-[2,4-dimethylphenyl]-N[[(2,4-dimethylphenyl)imino]methyl]]-N-methylmethanimidamide), including its metabolites and degradates, in or on the
commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring
amitraz residues convertible to 2,4-dimethylaniline, expressed as the stoichiometric equivalent of amitraz, in or on the
following raw agricultural commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts

0.1
0.02
0.2
1.0

Cotton, undelinted seed1
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts
Honey
Honeycomb
Milk
Milk, fat

0.1
0.1
0.1
0.05
0.3
0.2
9
0.03
0.2

1

There are no U.S. registrations on cottonseed as of May 3, 2006.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[44 FR 70145, Dec. 6, 1979, as amended at 51 FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992;
58 FR 14316, Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; 74 FR 47456,
Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013]

Back to Top
§180.288 2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for residues of the fungicide 2-(thiocyanomethylthio)benzothiazole in or on
the following food commodities:
Commodity

Parts per million

Barley, grain
Barley, straw
Beet, sugar, roots
Beet, sugar, tops
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Cotton, forage
Cotton, undelinted seed
Oat, forage
Oat, grain
Oat, hay

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1
0.1
0.1
0.1
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)

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Oat, straw
Rice, grain
Rice, straw
Safflower, seed
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)
0.1(N)

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39440, July 1, 2003, as amended at 74 FR 46374, Sept. 9, 2009]

Back to Top
§180.289 Methanearsonic acid; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide methanearsonic acid, including its metabolites
and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in
this paragraph is to be determined by measuring only methanearsonic acid, from application of the disodium and
monosodium salts of methanearsonic acid, calculated as the stoichiometric equivalent of As2O3, in or on the commodity.
Commodity
Cotton, undelinted seed
Cotton, hulls
Fruit, citrus

Parts per million

Expiration/Revocation Date
0.7
0.9
0.35

None
None
12/31/12

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34828, June 26, 1998, as amended at 77 FR 59126, Sept. 26, 2012]

Back to Top
§180.291 Pentachloronitrobenzene; tolerance for residues.
(a) General. Tolerances are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB)
and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:
Commodity

Parts per million

Bean
Brassica, head and stem, subgroup 5A
Cotton, undelinted seed
Garlic, bulb
Peanut
Potato
Soybean, forage
Soybean, hay
Soybean, seed
Vegetable, fruiting, group 8

0.1
0.1
0.1
0.1
1.0
0.1
0.02
0.02
0.02
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are
established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites
pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:
Commodity

Parts per million

Collards
Kale
Mustard, greens

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.2
0.2
0.2

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(d) Indirect or inadvertent residues. [Reserved]
[74 FR 47456, Sept. 16, 2009]

Back to Top
§180.292 Picloram; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide picloram, 4-amino-3,5,6-trichloropicolinic acid,
including its metabolites and degradates, in or on the commodities in the following table from its application in the acid
form or in the form of its salts. Compliance with the tolerance levels specified in this paragraph is to be determined by
measuring only picloram, 4-amino-3,5,6-trichloropicolinic acid, in or on the commodity.
Commodity

Parts per million

Barley, grain
Barley, pearled barley
Barley, straw
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grass, forage
Grass, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Oat, forage
Oat, grain
Oat, groats/rolled oats
Oat, straw
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Wheat, bran
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, middlings
Wheat, shorts
Wheat, straw

0.5
3.0
1.0
0.4
0.4
15
0.05
0.4
0.4
15
4.0
400
225
0.05
0.05
0.05
0.4
0.4
15
0.25
1.0
0.5
3.0
1.0
0.05
0.05
0.05
0.4
0.4
15
3.0
1.0
3.0
0.5
3.0
3.0
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[41 FR 19221, May 11, 1976, as amended at 47 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; 64 FR 39082, July 21, 1999; 72
FR 41930, Aug. 1, 2007; 75 FR 60243, Sept. 29, 2010]

Back to Top
§180.293 Endothall; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. (1) Tolerances are established for the residues of endothall, including its metabolites and degradates, in
or on the commodities in the table, below. Compliance with the tolerance levels specified, below, is to be determined by
measuring only endothall (7-oxabicylco [2.2.1] heptanes-2,3-dicarboxylic acid) and its mono-methyl ester.
Commodity

Parts per million

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

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Apple
Apple, wet pomace
Cotton, undelinted seed
Fish
Hop, dried cones
Potato
Rice, grain
Rice, straw

0.05
0.15
0.1
0.1
0.1
0.1
0.05
0.05

(2) An interim tolerance of 0.2 parts per million is established for residues of the herbicide endothall (7 - oxabicyclo
[2.2.1] heptane-2,3-dicarboxylic acid) in water, potable from use of its potassium, sodium, di-N, N-dimethylalkylamine, and
mono-N-N,-dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other
potential sources of water, potable.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent combined residues of
the herbicide, endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in potable water from use of its potassium,
sodium, di-N, N -dimethylalkylamine, and mono- N-N, -dimethylalkylamine salts as algicides or herbicides to control
aquatic plants in canals, lakes, ponds, and other potable water sources that may lead to endothall residues in or on the
following commodities:
Commodity

Parts per million

Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Apple, wet pomace
Beet, sugar, molasses
Brassica, head and stem subgroup 5A
Brassica, leafy, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Corn, field, grain
Corn, pop, grain
Corn, sweet, kernel plus cob with husks removed
Citrus, dried pulp
Egg
Feed commodities not otherwise listed
Food commodities not otherwise listed
Fruit, citrus group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Grain, aspirated fractions
Grain cereal, forage, fodder and straw, group 16
Grain, cereal, group 15, except corn
Grape
Grape, raisin
Grass, forage, fodder, and hay group 17, forage
Grass, forage, fodder, and hay group 17, hay
Herb and spice, group 19
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Milk
Nut, tree, group 14
Okra
Pea and bean, dried shelled, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peppermint, tops
Pistachio
Poultry, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

15.0
4.0
10
0.15
1.5
0.1
2.0
0.6
0.6
0.01
0.20
0.10
0.03
0.07
0.07
0.3
0.1
0.05
10.0
5.0
0.05
0.05
0.3
0.005
0.15
0.05
0.015
35.0
10.0
4.0
1.0
5.0
3.5
18.0
5.0
0.005
0.10
0.05
0.01
0.03
0.05
0.05
0.2
2.0
5.0
0.05
0.015

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Poultry, liver
Poultry, meat
Poultry, meat byproducts
Rice, hulls
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Soybean, hulls
Soybean, seed
Spearmint, tops
Tomato, paste
Tomato, puree
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, edible, podded, subgroup 6A
Vegetable, root and tuber, group 1
Wheat, milled byproducts

0.05
0.015
0.20
8.0
0.005
0.15
0.05
0.015
0.5
0.2
5.0
0.1
0.1
0.5
1.5
4.0
0.05
2.0
3.0
2.0
1.0
5.0

[41 FR 23717, June 11, 1976, as amended at 51 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, 1997; 63 FR 42249, Aug. 7, 1998;
67 FR 35048, May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; 74 FR 67097,
Dec. 18, 2009; 78 FR 76566, Dec. 18, 2013]

Back to Top
§180.297 N-1-Naphthyl phthalamic acid; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide N-1-naphthyl phthalamic acid from application of
its sodium salt in or on the following raw agricultural commodities:
Commodity

Parts per million

Cantaloupe
Cucumber
Muskmelon
Watermelon

0.1(N)
0.1(N)
0.1(N)
0.1(N)

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 32306, May 16, 1980, as amended at 63 FR 57075, Oct. 26, 1998]

Back to Top
§180.298 Methidathion; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide methidathion, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl]
O,O-dimethyl phosphorodithioate, in or on the commodity.
Commodity
Almond, hulls
Artichoke, globe
Citrus, oil
Cotton, undelinted seed
Fruit, citrus, group 10, except tangerine
Fruit, pome, group 11
Fruit, stone, group 12
Mango
Nut, tree, group 14
Olive
Safflower, seed
Sorghum, forage, forage
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover

Parts per million

Expiration/revocation date
6.0
0.05
420.0
0.2
4.0
0.05
0.05
0.05
0.05
0.05
0.5
2.0
2.0
0.2
2.0

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16
12/31/16

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Sunflower, seed
Tangerine

0.5
6.0

12/31/16
12/31/16

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the insecticide methidathion, including its metabolites and degradates, in or on the commodities
in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by
measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl] O,O-dimethyl phosphorodithioate, in
or on the commodity.
Expiration/
revocation
date

Parts per
million

Commodity
Kiwifruit
Longan
Starfruit
Sugar apple

0.1
0.1
0.1
0.2

12/31/16
12/31/16
12/31/16
12/31/16

(d) Indirect or inadvertent residues. [Reserved]
[43 FR 44845, Sept. 29, 1978]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.298, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.299 Dicrotophos; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide dicrotophos, dimethyl phosphate of
3-hydroxy-N,N-dimethyl-cis-crotonamide, in or on the following food commodities:
Commodity

Parts per million

Cotton, gin byproducts
Cotton, undelinted seed

2.0
0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 52613, Sept. 10, 2008]

Back to Top
§180.300 Ethephon; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for residues of the plant regulator ethephon [(2-chloroethyl) phosphonic acid]
in or on food commodities as follows:
Commodity

Parts per million

Apple
Apple, juice
Barley, bran
Barley, grain
Barley, straw
Blackberry
Blueberry
Cantaloupe
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Cherry
Coffee, bean, green
Cotton, gin byproducts
Cotton, undelinted seed
Cucumber

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

5.0
10.0
5.0
2.0
10.0
30.0
20.0
2.0
0.02
1.0
0.02
0.2
10.0
0.5
180.0
6.0
0.1

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Egg
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Grape
Grape, raisin
Hazelnut
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Milk
Nut, macadamia
Pepper
Pineapple
Poultry, fat
Poultry, liver
Poultry, meat
Poultry, meat byproducts, except liver
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Sugarcane, molasses
Tomato
Walnut
Wheat, bran
Wheat, germ
Wheat, grain
Wheat, middlings
Wheat, shorts
Wheat, straw

0.002
0.02
1.0
0.02
0.2
2.0
12.0
0.80
0.02
1.0
0.02
0.2
0.02
1.0
0.02
0.2
0.01
0.5
30.0
2.0
0.02
0.05
0.01
0.01
0.02
1.0
0.02
0.2
1.5
2.0
0.5
5.0
5.0
2.0
5.0
5.0
10.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(m), of 0.1 part
per million is established for residues of the plant regulator ethephon [(2-chloroethyl)phosphonic acid] in or on the food
commodity sugarcane.
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33710, May 24, 2000, as amended at 72 FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, 2010]

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§180.301 Carboxin; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for the combined residues of the fungicide carboxin (5,6-dihydro-2methyl-1,4-oxathiin-3-carboxanilide) and its metabolites determined as aniline and expressed as parent compound, in or
on food commodities as follows:
Commodity

Parts per million

Barley, grain
Barley, straw
Bean, dry, seed
Bean, succulent
Canola, seed
Cattle, fat
Cattle, meat byproducts
Cattle, meat
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover

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0.2
0.2
0.2
0.2
0.03
0.05
0.1
0.05
0.2
0.2
0.2
0.2
0.2

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Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Egg
Goat, fat
Goat, meat byproducts
Goat, meat
Hog, fat
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Milk
Oat, forage
Oat, grain
Oat, straw
Onion, bulb
Peanut
Peanut, hay
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Rice, grain
Rice, straw
Safflower, seed
Sheep, fat
Sheep, meat byproducts
Sheep, meat
Soybean, seed
Wheat, forage
Wheat, grain
Wheat, straw

0.2
0.2
0.2
0.2
0.05
0.05
0.1
0.05
0.05
0.1
0.05
0.05
0.1
0.05
0.05
0.5
0.2
0.2
0.2
0.2
0.2
0.1
0.1
0.1
0.2
0.2
0.2
0.05
0.1
0.05
0.2
0.5
0.2
0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 FR 4586, Jan. 30, 1998; 64 FR
11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR 72853, Dec. 9,
2002; 71 FR 56383, Sept. 27, 2006]

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§180.303 Oxamyl; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for the combined residues of the insecticide oxamyl, methyl
N,N-dimethyl-N-[(methylcarbamoyl)-oxy]-1-thiooxamimidate, and its oxime metabolite methyl N,N-dimethyl-N-hydroxy-1thiooxamimidate calculated as oxamyl in or on the following food commodities:
Commodity

Parts per million

Apple
Banana
Cantaloupe
Carrot
Celery
Cotton, undelinted seed
Cucumber
Eggplant
Fruit, citrus, group 10
Garlic, bulb
Melon, honeydew
Onion, bulb
Peanut
Peanut, hay
Pear
Peppermint, tops
Pepper, bell

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2
0.3
2.0
0.1
10.0
0.2
2.0
2.0
3
0.2
2.0
0.2
0.05
2.0
2.0
10.0
2.0

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Pepper, nonbell
Pineapple
Pineapple, process residue
Pumpkin
Soybean, seed
Spearmint, tops
Squash, summer
Squash, winter
Tomato
Vegetable, tuberous and corm, subgroup 1C
Watermelon

5.0
1
2.0
2.0
0.1
10.0
2.0
2.0
2
0.1
2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54961, Sept. 24, 2008]

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§180.304 Oryzalin; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide,
in or on the following raw agricultural commodities:
Commodity

Parts per million

Almond, hulls
Avocado
Berry group 13
Cranberry
Fig
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grape
Kiwifruit
Nut, tree, group 14
Olive
Pistachio
Pomegranate
Strawberry

0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural
commodities:
Commodity

Parts per million

Guava
Papaya

0.05
0.05

(d) Indirect or inadvertent residues. [Reserved]
[71 FR 54434, Sept. 15, 2006, as amended at 76 FR 34885, June 15, 2011]

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§180.311 Cacodylic acid; tolerances for residues.
(a) General. A tolerance is established for residues of the defoliant cacodylic acid, dimethylarsinic acid, including its
metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in
this paragraph is to be determined by measuring only those cacodylic acid residues convertible to As2O3, expressed as
the stoichiometric equivalent of cacodylic acid, in or on the commodity.
Commodity
Cotton, undelinted seed

Parts per million

Expiration/Revocation Date
2.8

1/1/12

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 6567, Feb. 11, 2004, as amended at 75 FR 60243, Sept. 29, 2010]

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§180.314 Triallate; tolerances for residues.
(a) General. Tolerances are established for residues of triallate, S-2,3,4-trichloroallyl diisopropylthiocarbamate and its
metabolite 2,3,3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodity:
Commodity

Parts per million

Bermudagrass, hay

0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in 180.1(l),are
established for residues of the herbicide (S-2, 3, 4-trichloroallyl diisopropylthiocarbamate) and its metabolite 2, 3,
3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodities:
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Beet, sugar, dried pulp
Beet, sugar, roots
Beet, sugar, tops
Pea, dry
Pea, field, hay
Pea, field, vines
Pea, succulent
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
1.0
0.3
0.2
0.1
0.5
0.2
1.0
0.5
0.2
0.5
0.05
1.0
1.0

(d) Indirect or inadvertent residues. [Reserved]
[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, 2008; 74 FR 29963, June 24,
2009]

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§180.315 Methamidophos; tolerances for residues.
(a) General. Tolerances are established for residues of methamidophos, O,S-dimethyl phosphoramidothioate,
including its metabolites and degradates, in or on the commodities in the following table as a result of the application of
methamidophos. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only
methamidophos, O,S-dimethyl phosphoramidothioate, in or on the commodity.
Commodity

Parts per million

Expiration/Revocation Date

Broccoli1

1.0

Cabbage2
Cotton, undelinted seed
Potato

1.0

12/31/12
12/31/12

0.1
0.1

12/31/13
12/31/13

1

There are no U.S. registrations since 1989.

2

There are no U.S. registrations since 2001.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of
methamidophos, O,S-dimethyl phosphoramidothioate, including its metabolites and degradates, in or on the commodity in
the following table as a result of the application of methamidophos. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only methamidophos, O,S-dimethyl phosphoramidothioate, in or on the
commodity.
Commodity

Parts per million

Expiration/Revocation Date

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2.0

12/31/13

(d) Indirect or inadvertent residues. [Reserved]
[75 FR 60243, Sept. 29, 2010]

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§180.316 Pyrazon; tolerances for residues.
(a) General. Tolerances are established for combined residues of the herbicide pyrazon (5-amino-4-chloro-2-phenyl-3
(2H)-pyridazinone) and its metabolites (calculated as pyrazon) in or on the following food commodities:
Commodity

Parts per million

Beet, garden, roots
Beet, garden, tops
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver

0.9
7.0
1.5
0.2
3.0
0.10
0.15
0.10
0.10
0.10
0.15
0.10
0.10
0.10
0.15
0.10
0.10
0.02
0.10
0.15
0.10
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for combined residues of the herbicide pyrazon,
5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone, and its metabolites (calculated as pyrazon), in or on the following food
commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, stover
Soybean, forage
Soybean, hay
Wheat, forage
Wheat, hay
Wheat, straw

0.5
0.5
0.5
0.5
0.3
0.2
0.1

[68 FR 39441, July 1, 2003, as amended at 73 FR 52614, Sept. 10, 2008]

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§180.317 Propyzamide; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide propyzamide, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate,
expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on
the commodity.
Commodity

Parts per million

Alfalfa, seed
Animal feed, nongrass, group 18
Apple
Artichoke, globe
Blackberry

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10.0
10.0
0.1
0.01
0.05

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Blueberry
Boysenberry
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Egg
Endive
Fruit, stone, group 12
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except kidney and liver
Grape
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts, except kidney and liver
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except kidney and liver
Lettuce, head
Milk
Pear
Poultry, fat
Poultry, liver
Poultry, meat
Poultry, meat byproducts, except liver
Radicchio
Raspberry
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except kidney and liver

0.05
0.05
0.2
0.4
0.4
0.02
0.02
0.02
1.0
0.1
0.2
0.4
0.4
0.02
0.02
0.1
0.2
0.4
0.4
0.02
0.02
0.2
0.4
0.4
0.02
0.02
1.0
0.02
0.1
0.02
0.2
0.02
0.02
2.0
0.05
0.2
0.4
0.4
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities
in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by
measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric
equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.
Commodity

Parts per million

Pea, field, seed
Rhubarb

0.05
0.1

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide
propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph.
Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide
residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide,
3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.
Commodity

Parts per million

Grain, cereal, forage, group 16
Grain, cereal, hay, group 16
Grain, cereal, straw, group 16

0.6
0.2
0.3

[72 FR 52018, Sept. 12, 2007, as amended at 76 FR 23493, Apr. 27, 2011]

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§180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.
(a) General. (1) A tolerance is established for the herbicide 4-(2-methyl-4-chlorophenoxy) butyric acid in or on the
following food commodity:

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Commodity

Parts per million

Pea

0.1(N)

(2) Tolerances are established for the combined residues, free and conjugated, of the herbicide MCPB, 4-(4-chloro-2methylphenoxy)butanoic acid, and its metabolite MCPA, (4-chloro-2-methylphenoxy)acetic acid, in or on the following food
commodities:
Commodity

Parts per million

Peppermint, tops
Spearmint, tops

0.20
0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39441, July 1, 2003, as amended at 73 FR 66785, Nov. 12, 2008]

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§180.319 Interim tolerances.
(a) General. While petitions for tolerances for negligible residues are pending and until action is completed on these
petitions, interim tolerances are established for residues of the listed pesticide chemicals in or on the following raw
agricultural commodities:

Substances
Endothall (7-oxabicyclo-(2,2,1)heptane 2,3-dicarboxylic acid
Methyl parathion

Uses
Herbicide
Herbicide

Tolerance in parts per million
0.2
0.5

Raw
agricultural
commodity
Beet, sugar
Rye

Expiration/
revocation
date
None
12/31/13

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 59126, Sept. 26, 2012, as amended at 79 FR 27502, May 14, 2014]

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§180.324 Bromoxynil; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide bromoxynil, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by
measuring only bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, resulting from application of its octanoic and/or heptanoic
acid ester, in or on the commodities.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Barley, grain
Barley, hay
Barley, straw
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Flax, seed
Garlic
Grain, aspirated fractions
Grass, forage
Grass, hay
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Onion, bulb
Peppermint, hay

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0.1
0.5
0.05
9.0
4.0
0.3
0.05
0.2
0.05
0.2
0.1
0.1
1.2
18
5.0
0.3
0.05
9.0
4.0
0.1
0.1

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Rye, forage
Rye, grain
Rye, straw
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Spearmint, hay
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

1.0
0.05
2.0
0.8
0.2
0.2
0.1
1.0
0.05
4.0
2.0

(2) Tolerances are established for residues of the herbicide bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, including
its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be
determined by measuring only bromoxynil and its metabolite, 3,5-dibromo-4-hydroxybenzoic acid (DBHA), resulting from
application of its octanoic and/or heptanoic acid ester, in or on the commodities.
Commodity

Parts per million

Cattle, fat
Cattle, meat byproducts
Cattle, meat
Cotton, gin byproducts
Cotton, hulls
Cotton, undelinted seed
Egg
Goat, fat
Goat, meat byproducts
Goat, meat
Hog, fat
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Milk
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Sheep, fat
Sheep, meat byproducts
Sheep, meat

1
3.5
0.5
7.0
5.0
1.5
0.05
1
3.5
0.5
1
3.5
0.5
1
3.5
0.5
0.4
0.05
0.3
0.05
1
3.5
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 33023, June 18, 1997, as amended at 63 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, 2001; 70 FR 7046, Feb. 10,
2005; 72 FR 35666, June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR 31491, June 1, 2011]

Back to Top
§180.328 Napropamide; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide napropamide, N,N-diethyl-2-(1-napthalenyloxy)
propionamide, in or on the following food commodities:
Commodity
Almond, hulls
Asparagus
Basil
Berry group 13
Coffee, green bean
Cranberry
Grape
Kiwifruit
Marjoram
Nut, tree, group 14
Peppermint, tops
Persimmon
Rhubarb

Parts per million

Expiration/revocation date
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

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None
None
None
None
None
None
None
None
None
None
None
None
None

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Rosemary
Savory, summer
Savory, winter
Spearmint, tops
Strawberry
Sweet potato, roots
Vegetable, brassica, leafy, group 5
Vegetable, fruiting, group 8

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0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

None
None
None
None
None
None
None
None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 52614, Sept. 10, 2008, as amended at 76 FR 34885, June 15, 2011]

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§180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl
(S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the
following food commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Bean, lima
Beet, sugar, roots
Beet, sugar, tops
Broccoli
Brussels sprouts
Cabbage
Cauliflower
Clover, forage
Clover, hay
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Cucumber
Eggplant
Grapefruit
Hazelnut
Lemon
Lettuce, head
Melon
Onion, bulb
Orange
Pepper
Peppermint, tops
Pumpkin
Safflower, seed
Sorghum, forage, forage
Sorghum, grain, forage
Sorghum, grain, grain
Spearmint, tops
Squash, summer
Squash, winter
Strawberry
Walnut

5.0
11.0
0.2
0.3
0.5
1.0
1.0
2.0
1.0
5.0
10.0
1.0
0.5
3.0
0.02
1.0
1.0
1.0
0.05
1.0
2.0
0.2
0.05
1.0
0.75
12.5
0.2
1.0
2.0
2.0
0.75
12.5
1.0
0.3
2.0
0.05

(2) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)
ethyl) O,O-dimethyl phosphorothioate) and its cholinesterase-inhibiting metabolites in or on the following food
commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg

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0.01
0.01
0.01
0.01

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Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are
established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)-ethyl) O,O-dimethyl
phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:
Commodity

Parts per million

Broccoli raab

2.0

(d) Indirect or inadvertent residues. [Reserved]
[72 FR 54578, Sept. 26, 2007]

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§180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide 4-(2,4-dichlorophenoxy) butyric acid (2,4-DB),
both free and conjugated, determined as the acid, in or on food commodities, as follows:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Cattle, meat byproducts
Clover, forage
Clover, hay
Goat, meat byproducts
Hog, meat byproducts
Horse, meat byproducts
Peanut
Peppermint, tops
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, seed
Spearmint, tops
Trefoil, forage
Trefoil, hay

0.7
2.0
0.05
0.2
0.2
0.05
0.05
0.05
0.2
0.2
0.05
0.7
2.0
0.5
0.2
0.7
2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54961, Sept. 24, 2008, as amended at 74 FR 46374, Sept. 9, 2009]

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§180.332 Metribuzin; tolerances for residues.
(a) General. Tolerances are established for combined residues of the herbicide metribuzin (4-amino-6-(1,1-dimethylethyl)-3-(methylthio)-;1,2,4-triazin-5(4H)-one) and its triazinone metabolites in or on food commodities:
Commodity

Parts per million

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Alfalfa, forage
Alfalfa, hay
Asparagus
Barley, grain
Barley, hay
Barley, pearled barley
Barley, straw
Carrot, roots
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Grass, forage
Grass, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Lentil
Milk
Pea, dry, seed
Pea, field, hay
Pea, field, vines
Pea, succulent
Potato
Potato, chips
Potato, processed potato waste
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sainfoin, forage
Sainfoin, hay
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, seed
Soybean, forage
Soybean, hay
Sugarcane, cane
Sugarcane, molasses
Tomato
Wheat, bran
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, hay
Wheat, middlings
Wheat, shorts
Wheat, straw

2.0
7.0
0.1
0.75
7.0
3.0
1.0
0.3
0.7
0.7
0.7
0.1
0.05
0.1
0.05
0.1
0.05
0.1
0.01
0.7
0.7
0.7
2.0
7.0
0.7
0.7
0.7
0.7
0.7
0.7
0.05
0.05
0.05
4.0
0.5
0.1
0.6
3.0
3.0
0.7
0.7
0.7
2.0
7.0
0.7
0.7
0.7
0.3
4.0
4.0
0.1
2.0
0.1
3.0
2.0
3.0
0.75
7.0
3.0
3.0
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, 1979; 44 FR 45387, Aug. 2, 1979;
52 FR 23654, June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, 2000; 66 FR
63198, Dec. 5, 2001; 67 FR 49617, July 31, 2002]

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§180.337 Oxytetracycline; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide/bactericide oxytetracycline, including its
metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels
specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)
-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2naphthacenecarboxamide, in or on the commodity.
Commodity

Parts per million

Apple
Peach
Pear

0.35
0.35
0.35

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 23493, Apr. 27, 2011]

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§180.339 MCPA; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic
acid), both free and conjugated, resulting from the direct application of MCPA or its sodium or dimethylamine salts, or its
2-ethylhexyl ester in or on the following food commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Barley, grain
Barley, hay
Barley, straw
Clover, forage
Clover, hay
Flax, seed
Grain, aspirated fractions
Grass, forage
Grass, hay
Lespedeza, forage
Lespedeza, hay
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Pea, dry
Pea, field, hay
Pea, succulent
Pea, field, vines
Rye, forage
Rye, grain
Rye, straw
Trefoil, forage
Trefoil, hay
Vetch, forage
Vetch, hay
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.5
2.0
1.0
40
25
0.5
2.0
0.1
3.0
300
20
0.5
2.0
20
1.0
115
25
0.1
0.1
0.1
0.1
20
1.0
25
0.5
2.0
0.5
2.0
20
1.0
115
25

(2) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic acid) resulting
from the direct application of MCPA or its sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the following
food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1
0.1
0.1
0.1

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Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep meat
Sheep meat byproducts

0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008]

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§180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.
(a) General. Tolerances are established for combined negligible residues of a fungicide and insecticide that is a
mixture of 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate in or on raw agricultural commodities
as follows:
Commodity

Parts per million

Apple1

0.1

Grape1

0.1

1

There are no U.S. registrations on apple and grape as of October 24, 2002.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[40 FR 29715, July 15, 1975, as amended at 63 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, 2004]

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§180.342 Chlorpyrifos; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the pesticide chlorpyrifos per se
(O,O-diethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond
Almond, hulls
Apple
Apple, wet pomace
Banana
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherry, sweet
Cherry, tart
Citrus, dried pulp
Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, refined oil

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

3.0
13
0.2
12
0.01
0.02
0.1
5.0
15
1.0
8.0
0.3
0.05
0.05
1.0
1.0
5.0
20
8.0
0.05
0.25

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Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husk removed
Corn, sweet, stover
Cotton, undelinted seed
Cranberry
Cucumber
Egg
Fig
Fruit, citrus, group 10
Goat, fat
Goat, meat
Goat, meat byproducts
Hazelnut
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Kiwifruit
Milk, fat (Reflecting 0.01 ppm in whole milk)
Nectarine
Onion, bulb
Peach
Peanut
Peanut, refined oil
Pear
Pecan
Pepper
Peppermint, tops
Peppermint, oil
Plum, prune, fresh
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Pumpkin
Radish
Rutabaga
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Spearmint, tops
Spearmint, oil
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Strawberry
Sunflower, seed
Sweet potato, roots
Turnip, roots
Turnip, tops
Vegetable, brassica, leafy, group 5
Vegetable, legume, group 6. except soybean
Walnut
Wheat, forage
Wheat, grain
Wheat, straw

8.0
8.0
0.05
8.0
0.2
1.0
0.05
0.01
0.01
1.0
0.2
0.05
0.05
0.2
0.2
0.05
0.05
0.25
0.25
0.25
2.0
0.25
0.05
0.5
0.05
0.2
0.2
0.05
0.2
1.0
0.8
8.0
0.05
0.1
0.1
0.1
0.05
2.0
0.5
0.2
0.05
0.05
0.8
8.0
0.5
0.5
2.0
0.3
0.2
0.1
0.05
1.0
0.3
1.0
0.05
0.2
3.0
0.5
6.0

(2) Chlorpyrifos [O,O-diethyl O-(3,5,6-trichloro-2-pyridyl) phosphorothioate] may be safely used in accordance with the
following prescribed conditions.
(i) Application shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where
food and food products are held, processed, prepared or served. Contamination of food or food contact surfaces shall be
avoided. Food must be removed or covered during treatment.
(ii) Spray concentration for spot treatment shall be limited to a maximum of 0.5 percent of the active ingredient by
weight. A course, low-pressure spray shall be used to avoid atomization or splashing of the spray.
(iii) Paint-on application for spot treatment shall be limited to a maximum of 2 percent of the active ingredient by
weight.

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(iv) Crack and crevice treatment shall be limited to a maximum of 2 percent of the active ingredient by weight.
Equipment capable of delivering a pin-stream of insecticide shall be used.
(v) Application via adhesive strips shall contain a maximum of 10% by weight of the controlled-release product in
food-handling establishments where food and food products are held, processed, prepared, or served. A maximum of 36
strips (or 5.15 grams of chlorpyrifos) is to be used per 100 square feet of floor space. The strips are not to be placed in
exposed areas where direct contact with food, utensils, and food-contact surfaces would be likely to occur.
(vi) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(3) A tolerance of 0.1 part per million is established for residues of chlorpyrifos, per se, in or on food commodities
(other than those already covered by a higher tolerance as a result of use on growing crops) in food service
establishments where food and food products are prepared and served, as a result of the application of chlorpyrifos in
microencapsulated form.
(i) Application of a microencapsulated product shall be limited solely to spot and/or crack and crevice treatment in
food handling establishments where food and food products are prepared and served. All treatments shall be applied in
such a manner as to avoid contamination of food or food contact surfaces.
(ii) Spray concentrations shall be limited to a maximum of 0.5 percent of the active ingredient by weight.
(iii) For crack and crevice treatment, equipment capable of delivering a pin stream of spray directly into cracks and
crevices or capable of applying small amounts of insecticide into cracks and crevices shall be used.
(iv) For spot treatment, an individual spot shall not exceed 2 square feet.
(v) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in 180.1(l), are established
for residues of the pesticide chlorpyrifos per se (O,O-diethyl- O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the
following food commodities:
Commodity

Parts per million

Asparagus
Grape

5.0
0.01

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33711, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006; 73 FR 53739, Sept. 17,
2008; 76 FR 56656, Sept. 14, 2011]

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§180.345 Ethofumesate; tolerances for residues.
(a) General. Tolerances for the combined residues of the herbicide ethofumesate (2-ethoxy-2,3-dihydro-3,3-dimethyl5-benzofuranyl methanesulfonate) and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl
methanesulfonate and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranyl methanesulfonate both calculated as parent
compound in or on the following food commodities:
Commodity

Parts per million

Beet, garden, roots
Beet, garden, tops
Beet, sugar, molasses
Beet, sugar, refined sugar
Beet, sugar, roots
Beet, sugar, tops
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Garlic
Goat, fat
Goat, meat
Goat, meat byproducts
Grass, straw
Horse, fat
Horse, meat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.5
5.0
0.5
0.2
0.3
4.0
0.05
0.05
0.05
0.25
0.05
0.05
0.05
1.0
0.05
0.05

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Horse, meat byproducts
Onion, bulb
Shallot, bulb
Shallot, fresh leaves
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.05
0.25
0.25
0.25
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. Tolerances with regional registration as defined in 40 CFR 180.1(l) are
established for the combined residues of ethofumesate,(2-ethoxy -2, 3-dihydro-3, 3-dimethyl-5-benzofuranyl
methanesulfonate) and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate and
2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranyl methanesulfonate (both calculated as the parent compound) in or on the
raw agricultural commodities:
Commodity

Parts per million

Carrot, roots

7.0

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34828, June 26, 1998, as amended at 71 FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007]

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§180.349 Fenamiphos; tolerances for residues.
(a) General. Tolerances are established for residues of the nematicide/insecticide fenamiphos, ethyl 3-methyl4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, including its metabolites and degradates, in or on the commodities
in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring
only the sum of fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, and its cholinesterase
inhibiting metabolites ethyl 3-methyl-4-(methylsulfinyl)phenyl 1-(methylethyl)phosphoramidate and ethyl 3-methyl4-(methylsulfonyl)phenyl 1-(methylethyl)phosphoramidate, calculated as the stoichiometric equivalent of fenamiphos, in or
on the commodity.
Commodity

Parts per million

Banana1

0.1

Grape1

0.1

Grape, raisin1

0.3

Pineapple1

0.3

1

There are no U.S. registrations as of May 31, 2007.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33712, May 24, 2000, as amended at 73 FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, 2010]

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§180.350 Nitrapyrin; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the soil microbiocide nitrapyrin [2-chloro6-(trichloromethyl) pyridine] and its metabolite, 6-chloropicolinic acid in or on the following raw agricultural commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, milled byproducts
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Sorghum, forage, forage
Sorghum, grain, forage
Sorghum, grain, grain

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

1.0
0.1
0.2
1.0
0.1
1.0
1.0
0.1
1.0
0.5
0.5
0.1

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Sorghum, grain, stover
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, milled byproducts, except flour
Wheat, straw

0.5
3.0
2.0
0.5
2.0
6.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[46 FR 58315, Dec. 1, 1981, as amended at 47 FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, 1987; 58 FR 32304, June 9, 1993;
63 FR 57076, Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007]

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§180.352 Terbufos; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide terbufos (phosphorodithioic acid,
S-(t-butylthio)methyl O,O-diethyl ester) and its phosphorylated (cholinesterase-inhibiting) metabolites (phosphorothioic
acid, S-(t-butylthio)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester;
phosphorothioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester; phosphorodithioic acid, S-(t-butylsulfinyl)methyl
O,O-diethyl ester; and phosphorodithioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester) in or on food commodities:
Commodity

Parts per million

Banana
Beet, sugar, roots
Beet, sugar, tops

0.025
0.05
0.1
0.05

Coffee, green bean1
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, forage
Corn, sweet, stover
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
1

0.5
0.5
0.5
0.5
0.5
0.05
0.5
0.5
0.5
0.05
0.5

There are no U. S. registrations as of August 2, 1995, for the use of terbufos on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 53740, Sept. 17, 2008]

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§180.353 Desmedipham; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide desmedipham, (ethyl-m-hydroxycarbanilate
carbanilate) in or on the following raw agricultural commodities in the table that follows:
Commodity

Parts per million

Beet, garden, roots
Beet, garden, tops
Beet, sugar, roots
Beet, sugar, tops
Spinach

0.05
1.0
0.1
5.0
6.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[40 FR 4658, Jan. 31, 1975, as amended at 62 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, 1998; 64 FR 46292, Aug. 25,
1999; 65 FR 82293, Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; 72 FR
53449, Sept. 19, 2007; 73 FR 53740, Sept. 17, 2008]

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§180.355 Bentazon; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. (1) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food
commodities:
Commodity

Parts per million

Bean, dry, seed
Bean, succulent
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, sweet, kernel plus cob with husks removed
Cowpea, forage
Cowpea, hay
Flax, seed
Pea, dry, seed
Pea, field, hay
Pea, field, vines
Pea, succulent
Peanut
Peanut, hay
Pepper, nonbell
Peppermint, tops
Rice, grain
Rice, hulls
Rice, straw
Sorghum, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Spearmint, tops

0.05
0.5
3.0
0.05
3.0
0.05
0.05
10.0
3.0
1.0
1.0
8.0
3.0
3.0
0.05
3.0
0.05
1.0
0.05
0.25
3.0
0.20
0.05
0.05
8.0
8.0
0.05
1.0

(2) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its metabolite 2-amino-N-isopropyl benzamide (AIBA) in or on the
following food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat byproducts
Cattle, meat
Egg
Goat, fat
Goat, meat byproducts
Goat, meat
Hog, fat
Hog, meat byproducts
Hog, meat
Milk
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Sheep, fat
Sheep, meat byproducts
Sheep, meat

0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.02
0.05
0.05
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(m), are
established for combined residues of the herbicide, bentazon (3-isopropyl-1H-2, 1,3-benzothiadiazin-4(3H)
-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food commodities:

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Parts per million

Clover, forage
Clover, hay

1.0
2.0

(d) Indirect or inadvertent residues. [Reserved]
[42 FR 26979, May 26, 1977]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.355, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.356 Norflurazon; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide norflurazon (4-chloro5-(methylamino)-2-(alpha, alpha, alpha-trifluoro-m-tolyl)-3-(2H)-pyridazinone) and its desmethyl metabolite 4-chloro5-(amino)-2-alpha, alpha, alpha-trifluoro-m-tolyl)-3(2H)-pyridazinone in or on the following raw agricultural commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Alfalfa, seed
Almond, hulls
Almond
Apple
Apricot
Asparagus
Avocado
Blackberry
Blueberry
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Cherry
Citrus, dried pulp
Citrus, molasses
Cotton, undelinted seed
Cranberry
Fruit, citrus
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Grape
Hazelnut
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Hop, dried cones
Hop, vines
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Nectarine
Peach
Peanut
Peanut, hay
Peanut, hay
Pear
Pecan
Plum, prune, fresh
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Raspberry
Sheep, fat
Sheep, liver

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3.0
5.0
0.1
1.0
0.1
0.1
0.1
0.05
0.20
0.1
0.2
0.1
0.50
0.1
0.1
0.1
0.4
1.0
0.1
0.1
0.2
0.1
0.50
0.1
0.1
0.1
0.1
0.1
0.50
0.1
0.1
3.0
1.0
0.1
0.50
0.1
0.1
0.1
0.1
0.1
0.05
5.50
1.5
0.1
0.1
0.1
0.1
0.1
0.1
0.2
0.1
0.50

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Sheep, meat
Sheep, meat byproducts, except liver
Soybean
Soybean, forage
Soybean, hay
Walnut

0.1
0.1
0.1
1.0
1.0
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 14909, Apr. 7, 1982]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.356, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.360 Asulam; tolerance for residues.
(a) General. Tolerances are established for the combined residues of asulam (methyl sulfanilylcarbamate) and its
sulfanilamide containing metabolites in or on the following food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sugarcane, cane
Sugarcane, molasses

0.05
0.05
0.2
0.05
0.05
0.2
0.05
0.05
0.2
0.05
0.05
0.2
0.05
0.05
0.05
0.2
1.0
30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 39441, July 1, 2003, as amended at 72 FR 37654, July 11, 2007]

Back to Top
§180.361 Pendimethalin; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and
degradates, in or on the commodities. Compliance with the tolerance levels specified in the following table below is to be
determined by measuring only pendimethalin, [N- (1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine], and its metabolite,
4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, calculated as the stoichiometric equivalent of pendimethalin, in
or on the following commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Alfalfa, seed
Almond, hulls
Apple, wet pomace
Artichoke, globe

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3.5
4.0
0.10
6.0
0.20
0.1

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Asparagus
Beans
Beans, forage
Beans, hay
Berry, low growing subgroup 13-07G
Brassica head and stem, subgroup 5-A
Brassica, leafy greens, subgroup 5B
Carrot
Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Crayfish
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small vine climbing, except grape, subgroup 13-07E
Fruit, stone, group 12-12
Grape
Grass forage, fodder, and hay crop group 17, forage
Grass forage, fodder, and hay crop group 17, hay
Grass forage, fodder, and hay crop group 17, straw
Hop, dried cones
Juneberry
Lettuce, leaf
Melon subgroup 9A
Nut, tree, group 14
Olive
Onion, bulb subgroup 3-07A
Onion, green subgroup 3-07B
Peanut
Peanut, hay
Peas (except field peas)
Peppermint, oil
Peppermint, tops
Pistachio
Pomegranate
Potato
Rice, grain
Rice, straw
Sorghum, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Spearmint, oil
Spearmint, tops
Sugarcane, cane
Sunflower subgroup 20B
Turnip greens
Vegetable, fruiting, group 8-10
Vegetable, soybean, succulent
Wheat, grain
Wheat, forage
Wheat, hay
Wheat, straw

0.15
0.10
0.10
0.10
0.1
0.1
0.20
0.5
0.5
0.1
0.1
0.1
0.1
0.1
0.1
0.1
3.0
0.1
0.05
0.1
0.1
0.10
0.1
0.1
20
13
4.0
0.1
0.10
4.0
0.10
0.1
0.1
0.1
0.2
0.1
0.1
0.10
1.0
0.2
0.1
0.10
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
1.0
0.2
0.1
0.1
0.20
0.1
0.10
0.10
3.0
0.60
0.30

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for
combined residues of the herbicide pendimethalin, [N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine], and its
metabolite 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, in or on the specified agricultural commodities,
resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire and are
revoked on the date specified in the table.
Commodity
Bermuda grass, forage
Bermuda grass, hay

Parts per million

Expiration/revocation date
25
60

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[49 FR 15293, Apr. 18, 1984]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.361, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.362 Fenbutatin-oxide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its
metabolites and degradates, in or on the plant commodities in the table in this paragraph. Compliance with the tolerance
levels specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2phenylpropyl) distannoxane, in or on the commodity.
Commodity

Parts per million

Almond, hulls
Apple
Apple, wet pomace
Cherry, sweet
Cherry, tart
Citrus, dried pulp
Citrus, oil
Cucumber
Eggplant
Fruit, citrus, group 10
Grape
Grape, raisin
Nut, tree, group 14
Papaya
Peach
Pear
Pistachio
Plum, prune, fresh
Plum, prune, dried
Strawberry

80.0
15.0
100.0
6.0
6.0
100.0
140.0
4.0
6.0
20.0
5.0
20.0
0.5
2.0
10.0
15.0
0.5
4.0
20.0
10.0

(2) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and
degradates, in or on the animal commodities in the table in this paragraph. Compliance with the tolerance levels specified
in this paragraph is to be determined by measuring only the sum of fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl)
distannoxane, and its organotin metabolites, dihydroxybis(2-methyl-2-phenylpropyl) stannane and 2-methyl-2phenylpropylstannoic acid, calculated as the stoichiometric equivalent of fenbutatin-oxide, in or on the commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk, fat
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.5
0.5
0.5
0.1
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.1
0.1
0.1
0.1
0.5
0.5
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established
for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant

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commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be
determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.
Commodity

Parts per million

Raspberry

10.0

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33713, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, 2008; 76 FR 23494, Apr. 27, 2011]

Back to Top
§180.364 Glyphosate; tolerances for residues.
(a) General. (1) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or
on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the
ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the
potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only
glyphosate (N-(phosphonomethyl)glycine).
Commodity
Acerola
Alfalfa, seed
Almond, hulls
Aloe vera
Ambarella
Animal feed, nongrass, group 18
Artichoke, globe
Asparagus
Atemoya
Avocado
Bamboo, shoots
Banana
Barley, bran
Beet, sugar, dried pulp
Beet, sugar, roots
Beet, sugar, tops
Berry and small fruit, group 13-07
Betelnut
Biriba
Blimbe
Breadfruit
Cacao bean, bean
Cactus, fruit
Cactus, pads
Canistel
Carrot
Chaya
Cherimoya
Citrus, dried pulp
Coconut
Coffee, bean, green
Corn, pop, grain
Corn, sweet, kernel plus cob with husk removed
Cotton, gin byproducts
Custard apple
Date, dried fruit
Dokudami
Durian
Epazote
Feijoa
Fig
Fish
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, stone, group 12
Galangal, roots
Ginger, white, flower
Gourd, buffalo, seed
Governor's plum
Gow kee, leaves
Grain, cereal, forage, fodder and straw, group 16, except field corn, forage and field corn, stover

Parts per million

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0.2
0.5
25
0.5
0.2
400
0.2
0.5
0.2
0.2
0.2
0.2
30
25
10
10
0.20
1.0
0.2
0.2
0.2
0.2
0.5
0.5
0.2
5.0
1.0
0.2
1.5
0.1
1.0
0.1
3.5
210
0.2
0.2
2.0
0.2
1.3
0.2
0.2
0.25
0.50
0.20
0.2
0.2
0.2
0.1
0.2
0.2
100

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Grain, cereal, group 15 except field corn, popcorn, rice, sweet corn, and wild rice
Grass, forage, fodder and hay, group 17
Guava
Herbs subgroup 19A
Hop, dried cones
Ilama
Imbe
Imbu
Jaboticaba
Jackfruit
Kava, roots
Kenaf, forage
Leucaena, forage
Longan
Lychee
Mamey apple
Mango
Mangosteen
Marmaladebox
Mioga, flower
Noni
Nut, pine
Nut, tree, group 14
Oilseeds, group 20, except canola
Okra
Olive
Oregano, Mexican, leaves
Palm heart
Palm heart, leaves
Palm, oil
Papaya
Papaya, mountain
Passionfruit
Pawpaw
Pea, dry
Peanut
Peanut, hay
Pepper leaf, fresh leaves
Peppermint, tops
Perilla, tops
Persimmon
Pineapple
Pistachio
Pomegranate
Pulasan
Quinoa, grain
Rambutan
Rice, grain
Rice, wild, grain
Rose apple
Sapodilla
Sapote, black
Sapote, mamey
Sapote, white
Shellfish
Soursop
Spanish lime
Spearmint, tops
Spice subgroup 19B
Star apple
Starfruit
Stevia, dried leaves
Sugar apple
Sugarcane, cane
Sugarcane, molasses
Surinam cherry
Sweet potato
Tamarind
Tea, dried
Tea, instant
Teff, forage
Teff, grain
Teff, hay

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30
300
0.2
0.2
7.0
0.2
0.2
0.2
0.2
0.2
0.2
200
200
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.20
1.0
1.0
40
0.5
0.2
2.0
0.2
0.2
0.1
0.2
0.2
0.2
0.2
8.0
0.1
0.5
0.2
200
1.8
0.2
0.1
1.0
0.2
0.2
5.0
0.2
0.1
0.1
0.2
0.2
0.2
0.2
0.2
3.0
0.2
0.2
200
7.0
0.2
0.2
1.0
0.2
2.0
30
0.2
3.0
0.2
1.0
7.0
100
5.0
100

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Ti, leaves
Ti, roots
Ugli fruit
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, subgroup 7A, except soybean
Vegetable, fruiting, group 8-10 (except okra)
Vegetable, leafy, brassica, group 5
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2, except sugar beet tops
Vegetable, legume, group 6 except soybean and dry pea
Vegetables, root and tuber, group 1, except carrot, sweet potato, and sugar beet
Wasabi, roots
Water spinach, tops
Watercress, upland
Wax jambu
Yacon, tuber

0.2
0.2
0.5
0.20
0.5
0.2
0.10
0.2
0.2
0.2
5.0
0.20
0.2
0.2
0.2
0.2
0.2

(2) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the
commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the
ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the
potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only
glyphosate (N-(phosphonomethyl)glycine) and its metabolite N-acetyl-glyphosate (N-acetyl-N-(phosphonomethyl)glycine;
calculated as the stoichiometric equivalent of glyphosate).
Commodity

Parts per Million

Canola, seed
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Egg
Goat, meat byproducts
Grain aspirated fractions
Hog, meat byproducts
Horse, meat byproducts
Poultry, meat
Poultry, meat byproducts
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed

20
5.0
13
5.0
100
0.05
5.0
310.0
5.0
5.0
0.10
1.0
5.0
100.0
200.0
120.0
20.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 64911, Oct. 1, 1980]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.364, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.367 n-Octyl bicycloheptenedicarboximide; tolerances for residues.
(a) General. A tolerance of 5 parts per million is established for residues of the insecticide synergist N-octyl
bicycloheptene dicarboximide, including its metabolites and degradates, in or on all food items in food handling
establishments where food and food products are held, processed, prepared and/or served, provided that the food is
removed or covered prior to such use, except for bagged food in warehouse storage which need not be removed or
covered prior to applications of formulations containing N-octyl bicycloheptene dicarboximide. Compliance with the
tolerance level specified in this paragraph is to be determined by measuring only N-octyl bicycloheptene dicarboximide, in
or on the commodity.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[65 FR 33713, May 24, 2000, as amended at 75 FR 60243, Sept. 29, 2010]

Back to Top
§180.368 Metolachlor; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues (free and bound) of the herbicide metolachlor,
2-chloro-N-(2- ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the
derivatives, 2- [(2-ethyl-6- methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3morpholinone, each expressed as the parent compound in the following raw agricultural commodities:
Commodity
Almond, hulls
Animal feed, nongrass, group 18
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Dillweed
Egg
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except kidney and liver
Grass, forage
Grass, hay
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except kidney and liver
Milk
Nut, tree, group 14
Okra
Peanut
Peanut, hay
Peanut, meal
Potato
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Safflower, seed
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except kidney and liver
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Tomato
Vegetable, foliage of legume, subgroup 7A, except soybean
Vegetable, legume, group 6

Parts per million
0.30
1.0
0.02
0.20
0.05
0.02
0.04
6.0
0.10
6.0
0.10
6.0
6.0
0.10
6.0
4.0
0.10
0.50
0.02
0.02
0.20
0.05
0.02
0.04
10
0.20
0.02
0.20
0.05
0.02
0.04
0.02
0.10
0.50
0.20
20
0.40
0.20
0.02
0.02
0.05
0.10
0.02
0.20
0.05
0.02
0.04
1.0
0.30
4.0
5.0
8.0
0.20
0.10
15.0
0.30

(2) Tolerances are established for residues of S-metolachlor, including its metabolites and degradates, in or on the
commodity(s), as defined. Compliance with the tolerance levels specified in the following table below is to be determined
by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-

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methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)
amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric
equivalent of S-metolachlor, in or on the commodity.
Commodity

Parts per million

Asparagus
Beet, garden, leaves
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Carrot, roots
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Cilantro, leaves
Coriander, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Egg
Grain, aspirated fractions
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except kidney and liver
Grass, forage
Grass, hay
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except kidney and liver
Leaf petioles, subgroup 4B
Lettuce
Low growing berry subgroup 13-07G, except cranberry
Milk
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Peanut
Peanut, hay
Peanut, meal
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Safflower, seed
Sesame, seed
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except kidney and liver
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Sorghum, sweet, stalk
Soybean, forage
Soybean, hay
Soybean, seed

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0.10
1.8
2.0
0.5
15.0
0.60
1.8
0.15
0.10
0.40
0.02
0.20
0.05
0.02
0.04
8.0
0.13
40
0.10
40
0.10
40
40
0.10
40
4.0
0.10
0.02
0.70
0.02
0.20
0.05
0.02
0.04
10.0
0.20
0.02
0.20
0.05
0.02
0.04
0.10
1.5
0.40
0.02
0.10
2.0
0.20
20.0
0.40
0.02
0.02
0.05
0.10
0.13
0.02
0.20
0.05
0.02
0.04
1.0
0.3
4.0
4.0
5.0
8.0
0.20

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Spinach
Sunflower, meal
Sunflower subgroup 20B
Tomato, paste
Turnip, greens
Vegetable, cucurbit group 9
Vegetable, foliage of legume, except soybean, subgroup 7A
Vegetable, fruiting, group 8-10, except tabasco pepper
Vegetable, legume, group 6
Vegetable, root, except sugar beet, subgroup 1B, except carrot
Vegetable, tuberous and corm, subgroup 1C

0.50
1.0
1.0
0.30
1.8
0.50
15.0
0.10
0.30
0.30
0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. (1) Tolerances with regional registration as defined in 180.1(l) are
established for the combined residues (free and bound) of the herbicide metolachlor [2-chloro-N-(2-ethyl-6-methylphenyl)
-N-(2-methoxy-1-methylethyl)acetamide] and its metabolites, determined as the derivatives, 2-[2-ethyl-6-methylphenyl)
amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, each expressed as the parent
compound, in or on the following raw agricultural commodities:
Commodity

Parts per million

Pepper, nonbell

0.50

(2) Tolerances with regional registration are established for residues of S-metolachlor, including its metabolites and
degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified
in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloroN-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as
the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.
Commodity

Parts per million

Pepper, tabasco

0.50

(d) Indirect or inadvertent residues. (1) Tolerances are established for the indirect or inadvertent combined residues
(free and bound) of the herbicide metolachlor, 2-chloro-N-(2-ethyl-6- methylphenyl)-N-(2-methoxy-1-methylethyl)
acetamide, and its metabolites, determined as the derivatives, 2-[(2-ethyl-6-methylphenyl)amino]-1-propanol and
4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following
raw agricultural commodities:
Commodity

Parts per million

Animal feed, nongrass, group 18
Barley, grain
Barley, hay
Barley, straw
Buckwheat, grain
Millet, forage
Millet, grain
Millet, hay
Millet, straw
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Rice, grain
Rye, forage
Rye, grain
Rye, straw
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

1.0
0.10
0.80
0.80
0.10
0.50
0.10
0.80
0.80
0.50
0.10
0.80
0.80
0.10
0.50
0.10
0.80
0.50
0.10
0.80
0.80

(2) Tolerances for are established for the indirect or inadvertent residues of S-metolachlor, including its metabolites
and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels
specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor,
S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites,
determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.
Commodity

Parts per million

Animal feed, nongrass, group 18

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1.0

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Barley, grain
Barley, hay
Barley, straw
Buckwheat, grain
Millet, forage
Millet, grain
Millet, hay
Millet, straw
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Rice, grain
Rye, forage
Rye, grain
Rye, straw
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.10
0.50
0.50
0.10
0.50
0.10
0.50
0.50
0.50
0.10
0.50
0.50
0.10
0.50
0.10
0.50
0.50
0.10
0.50
0.50

[73 FR 53740, Sept. 17, 2008, as amended at 74 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, 2010; 77 FR 48906, Aug. 15,
2012; 77 FR 59127, Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014; 80 FR 38986, July 8, 2015]

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§180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide 5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole
and its monoacid metabolite 3-carboxy-5-ethoxy-1,2,4-thiadiazole in or on the following raw agricultural commodities:
Commodity

Parts per million

Barley, grain
Barley, hay
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Peanut
Peanut, hay
Safflower, seed
Sorghum, grain, forage
Sorghum, grain, grain
Tomato
Vegetable, foliage of legume, group 7
Vegetable, legume, group 6
Wheat, forage
Wheat, grain
Wheat, straw

0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.15
0.1
0.1
0.1
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[47 FR 49845, Nov. 3, 1982, as amended at 48 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007;
73 FR 54961, Sept. 24, 2008]

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§180.371 Thiophanate-methyl; tolerances for residues.
(a) General. Tolerances are established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis
(iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodities in the following
table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of
thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl
2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the
commodity.

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Commodity

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Parts per million

Almond
Almond, hulls
Apple
Apricot
Banana
Bean, dry, seed
Bean, snap, succulent
Beet, sugar, roots
Cherry, sweet
Cherry, tart
Grain, aspirated fractions
Grape
Onion, bulb
Onion, green
Peach
Peanut
Peanut, hay
Pear
Pecan
Pistachio
Plum
Potato
Soybean, hulls
Soybean, seed
Strawberry
Vegetable, cucurbit, group 9
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.1
0.5
2.0
15.0
2.0
0.2
2.0
0.2
20.0
20.0
12
5.0
0.5
3.0
3.0
0.1
5.0
3.0
0.1
0.1
0.5
0.1
1.5
0.2
7.0
1.0
1.1
0.1
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of
thiophanate-methyl, dimethyl ((1,2-phenylene) bis(iminocarbonothioyl)) bis(carbamate), including its metabolites and
degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph
is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl))
bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent
of thiophanate-methyl, in or on the commodity.
Commodity

Parts per million

Canola, seed

0.1

(d) Indirect or inadvertent residues. [Reserved]
[75 FR 60244, Sept. 29, 2010]

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§180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.
(a) General. A tolerance is established for residues of the fungicide 2,6-dimethyl-4-tridecylmorpholine in or on the
following food commodity:
Commodity

Parts per million

Banana1

1.0

1

There are no U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54961, Sept. 24, 2008]

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§180.373 [Reserved]

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§180.377 Diflubenzuron; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. (1) Tolerances are established for residues of diflubenzuron, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide).
Commodity

Parts per million

Artichoke, globe
Cattle, fat
Cattle, meat
Cotton, undelinted seed
Egg
Goat, fat
Goat, meat
Hog, fat
Hog, meat
Horse, fat
Horse, meat
Milk
Mushroom
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Sheep, fat
Sheep, meat
Soybean
Soybean, hulls

6.0
0.05
0.05
0.2
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.2
0.05
0.05
0.05
0.05
0.05
0.05
0.5

(2) Tolerances are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]
-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below
is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]
-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of
diflubenzuron, in or on the commodity.
Commodity

Parts per million

Almond, hulls
Barley, grain
Barley, hay
Barley, straw
Brassica, leafy greens, subgroup 5B
Cattle, meat byproducts
Citrus, oil
Fruit, citrus, group 10-10
Fruit, stone, group 12, except cherry
Goat, meat byproducts
Grain, aspirated fractions
Grass, forage, fodder, and hay, group 17
Hog, meat byproducts
Horse, meat byproducts
Nut, tree, group 14
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Peanut
Peanut, hay
Peanut, refined oil
Pear
Pepper
Pistachio
Rice, grain
Rice, straw
Sheep, meat byproducts
Turnip greens
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

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6.0
0.06
3.0
1.8
9.0
0.15
32
3.0
0.07
0.15
11
6.0
0.15
0.15
0.06
7.0
0.06
6.0
3.5
0.10
55
0.20
0.50
1.0
0.06
0.02
0.8
0.15
9.0
7.0
0.06
6.0
3.5

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(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide
diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6- difluorobenzamide) and its metabolites, in connection with use of
the pesticide under section 18 emergency exemptions granted by EPA. Compliance with the tolerance levels specified
below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]
-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of
diflubenzuron, in or on the commodity. The tolerances are specified in the following table, and will expire and are revoked
on the dates specified.
Commodity
Alfalfa, forage
Alfalfa, hay
Lemon

Parts per million

Expiration/revocation date
6.0
6.0
0.8

12/31/17
12/31/17
12/31/10

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33699, May 24, 2000]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.377, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.378 Permethrin; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide cis- and trans-permethrin
isomers [cis-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] and
[trans-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] in/on the following food
commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond
Almond, hulls
Artichoke, globe
Asparagus
Avocado
Broccoli
Brussels sprouts
Cabbage
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cauliflower
Cherry, sweet
Cherry, tart
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Egg
Eggplant
Fruit, pome, group 11
Garlic, bulb
Grain, aspirated fractions
Goat, fat
Goat, meat
Goat, meat byproducts
Hazelnut
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Horseradish

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20
45
0.05
20
5.0
2.0
1.0
2.0
1.0
6.0
1.5
0.10
0.10
0.5
4.0
4.0
50
0.05
30
0.05
30
50
0.10
30
0.10
0.50
0.05
0.10
0.50
1.5
0.10
0.10
0.05
0.05
0.05
0.05
1.5
0.10
0.10
0.50

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Kiwifruit
Leaf petioles subgroup 4B
Leafy greens subgroup 4A
Lettuce, head
Milk, fat (reflecting 0.88 ppm in whole milk)
Mushroom
Onion, bulb
Peach
Pepper, bell
Pistachio
Potato
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, seed
Spinach
Tomato
Vegetable, cucurbit, group 9
Walnut
Watercress

2.0
5.0
20
20
3.0
5.0
0.10
1.0
0.50
0.10
0.05
0.15
0.05
0.05
1.5
0.10
0.10
0.05
20
2.0
1.5
0.05
5.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l) are established
for the combined residues of the insecticide cis- and trans-permethrin isomers [cis-(3-phenoxyphenyl)methyl
3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] and [trans-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)
-2,2-dimethylcyclopropane carboxylate] in/on the following food commodities:
Commodity

Parts per million

Collards
Grass, forage
Grass, hay
Papaya
Turnip, tops
Turnip, roots

15
15
15
1.0
10
0.20

(d) Indirect or inadvertent residues. [Reserved]
[72 FR 52019, Sept. 12, 2007]

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§180.380 Vinclozolin; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the fungicide vinclozolin (3-(3,5-dichlorophenyl)
-5-ethenyl-5-methyl-2,4-oxazolidinedione) and its metabolites containing the 3,5-dichloroaniline moiety in or on the food
commodities in the table below. There are no U.S. registrations for grape (wine) as of July 30, 1997.
Commodity
Bean, succulent
Canola, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Grape, wine
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Lettuce, head
Lettuce, leaf
Milk
Poultry, fat

Parts per million

Expiration/Revocation Date
2.0
1.0
0.05
0.05
0.05
0.05
0.05
0.05
0.05
6. 0
0.05
0.05
0.05
0.05
0.05
0.05
10.0
10.0
0.05
0.1

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11/30/05
11/30/08
11/30/08
11/30/08
11/30/08
11/30/08
11/30/08
11/30/08
11/30/08
None
11/30/08
11/30/08
11/30/08
11/30/08
11/30/08
11/30/08
11/30/05
11/30/05
11/30/08
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Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

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0.1
0.1
0.05
0.05
0.05

11/30/08
11/30/08
11/30/08
11/30/08
11/30/08

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
(e) Revoked tolerances subject to the channel of trade provisions. The following table lists commodities with residues
of vinclozolin resulting from lawful use are subject to the channels of trade provisions of section 408(l)(5) of the FFDCA:
Commodity

Parts per million

Cucumber
Fruit, stone, except plum, prune, fresh
Pepper, bell
Strawberry

1.0
25.0
3.0
10.0

[62 FR 38474, July 18, 1997, as amended at 63 FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, 2000; 67 FR 40189, June 12, 2002;
68 FR 56189, Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR 55268, Sept. 21, 2005]

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§180.381 Oxyfluorfen; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:
Commodity

Parts per million

Almond, hulls
Artichoke, globe
Avocado
Banana
Broccoli
Cabbage
Cacao bean, dried bean
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cauliflower
Coffee, bean, green
Corn, field, grain
Cotton, undelinted seed
Date, dried fruit
Egg
Feijoa
Fig
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grape
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Horseradish
Kiwifruit
Milk
Nut, tree, group 14
Olive
Onion, bulb
Peppermint, tops
Persimmon
Pistachio
Pomegranate

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1
0.05
0.05
0.05
0.05
0.05
0.05
0.01
0.01
0.01
0.05
0.05
0.05
0.05
0.05
0.03
0.05
0.05
0.05
0.05
0.01
0.01
0.01
0.05
0.01
0.01
0.01
0.01
0.01
0.01
0.05
0.05
0.01
0.05
0.05
0.05
0.05
0.05
0.05
0.05

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Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean
Spearmint, tops

0.2
0.01
0.01
0.01
0.01
0.01
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the
herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food
commodities:
Commodity

Parts per million

Blackberry
Chickpea, seed
Grass, forage
Grass, hay
Grass, seed screenings
Guava
Papaya
Raspberry
Taro, corm
Taro, leaves

0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05

(d) Indirect or inadvertent residues. [Reserved]
[45 FR 85022, Dec. 24, 1980]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.381, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.383 Sodium salt of acifluorfen; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. Tolerances are established for combined residues of the herbicide sodium salt of acifluorfen, sodium
5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, and its metabolites (the corresponding acid, methyl ester, and
amino analogues) in or on the following raw agricultural commodities:
Commodity

Parts per million

Peanut
Rice, grain
Rice, straw
Soybean, seed
Strawberry

0.1
0.1
0.2
0.1
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional restrictions. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 24877, Apr. 11, 1980, as amended at 46 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982; 61 FR 30165, June 14,
1996; 62 FR 39974, July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006]

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§180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the plant growth regulator mepiquat
(N,N-dimethylpiperidinium) in or on the following commodities:
Commodity

Parts per million

Cattle, meat byproducts
Cotton, gin byproducts

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1
6.0

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Cotton, undelinted seed
Goat, meat byproducts
Hog, meat byproducts
Horse, meat byproducts
Sheep, meat byproducts

2.0
0.1
0.1
0.1
0.1

(2) Tolerances are established for residues of the plant growth regulator mepiquat chloride (N,N-dimethylpiperidinium
chloride) in or on the following commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Goat, fat
Goat, meat
Grape
Grape, raisin
Hog, fat
Hog, meat
Horse, fat
Horse, meat
Sheep, fat
Sheep, meat

0.1
0.1
0.1
0.1
1.0
5.0
0.1
0.1
0.1
0.1
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 3118, Jan. 23, 2002]

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§180.385 Diclofop-methyl; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide diclofop-methyl (methyl
2-[4-(2,4-dichlorophenoxy)phenoxy]propanoate) and its metabolites, 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoic acid
and 2-[4-(2,4-dichloro-5-hydroxyphenoxy)phenoxy]propanoic acid, in or on the following raw agricultural commodities:
Commodity

Parts per million

Barley, grain
Barley, straw
Wheat, grain
Wheat, straw

0.1
0.1
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, 1986; 51 FR 19176, May 28, 1986;
63 FR 57077, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007]

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§§180.388-180.389 [Reserved]
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§180.390 Tebuthiuron; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the herbicide tebuthiuron
(N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(2-hydroxy-1,1-dimethylethyl)
-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, and
N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural
commodities:
Commodity

Parts per million

Grass, forage
Grass, hay

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10.0
10.0

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(2) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)
-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea,
N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, 2-dimethylethyl-5-amino-1,3,4-thiadiazole, and N-(5-(1,1-dimethylethyl)
-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

1.0
1.0
5.0
1.0
1.0
5.0
1.0
1.0
5.0
1.0
1.0
5.0

(3) A tolerance is established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)
-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea,
N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea,
N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea, and N-(5-(2-hydroxy-1,1-dimethylethyl)
-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:
Commodity

Parts per million

Milk

0.8

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 53461, Sept. 19, 2007]

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§180.395 Hydramethylnon; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone
(3-(4-(trifluoromethyl)phenyl)-1-(2-(4-(trifluoromethyl)phenyl)ethenyl)-2-propenylidene)hydrazone in or on the following raw
agricultural commodities:
Commodity

Parts per million

Grass, forage
Grass, hay
Pineapple

2.0
2.0
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[45 FR 55198, Aug. 19, 1980, as amended at 63 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, 1998; 66 FR 28672, May 24, 2001;
68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR 41931, Aug. 1, 2007]

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§180.396 Hexazinone; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)
-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the
following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the
sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its plant metabolites:
metabolite A, 3-(4-hydroxycyclohexyl)-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite B,
3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)
-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite D, 3-cyclohexyl-1-methyl-1,3,5-triazine-2,4,6-(1H,
3H, 5H)-trione, and metabolite E, 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, calculated as
the stoichiometric equivalent of hexazinone, in or on the commodity.

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Parts per million

Alfalfa, forage
Alfalfa, hay
Alfalfa, seed
Blueberry
Grass, forage
Grass, hay
Pineapple
Sugarcane, cane
Sugarcane, molasses

2.0
4.0
2.0
0.6
250
230
0.6
0.6
4.0

(2) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the
following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the
sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its animal tissue
metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F,
3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of
hexazinone, in or on the commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.1
0.5
4.0
0.1
0.5
4.0
0.1
0.5
4.0
0.1
0.5
4.0
0.1
0.5
4.0

(3) A tolerance is established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodity in the following
table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of
hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its metabolites: metabolite B,
3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)
-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C-2, 3-(3-hydroxycyclohexyl)-6-(methylamino)-1methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)
-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.
Commodity

Parts per million

Milk

11

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33713, May 24, 2000, as amended at 71 FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, 2010]

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§180.399 Iprodione; tolerances for residues.
Link to an amendment published at 80 FR 72598, November 20, 2015.
(a) General. (1) Tolerances are established for the combined residues of the fungicide iprodione
[3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer 3-(1-methylethyl)
-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolite 3-(3,5-dichlorophenyl)-2,4-dioxo-1imidazolidine-carboxamide in or on the following food commodities:
Commodity

Parts per million

Almond, hulls
Almond
Apricot

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

2.0
0.3
20.0

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Bean, dry, seed
Bean, forage
Bean, succulent
Blueberry
Boysenberry
Broccoli
Caneberry subgroup 13A
Carrot, roots
Cherry, sweet, postharvest
Cherry, tart
Cotton, undelinted seed
Cowpea, hay
Currant
Garlic
Ginseng
Ginseng, dried root
Grape
Grape, raisin
Kiwifruit
Lettuce
Nectarine, postharvest
Onion, bulb
Peach, postharvest
Peanut
Peanut, hay
Plum, postharvest
Plum, prune
Potato
Raspberry
Rice, bran
Rice, grain
Rice, hulls
Rice, straw
Strawberry

2.0
90.0
2.0
15.0
15.0
25.0
25.0
5.0
20.0
20.0
0.10
90.0
15.0
0.1
2.0
4.0
60.0
300
10.0
25.0
20.0
0.5
20.0
0.5
150.0
20.0
20.0
0.5
15.0
30.0
10.0
50.0
20.0
15.0

(2) Tolerances are established for the combined residues of iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)
-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1imidazolidinecarboxamide, and its metabolites [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide] and
[N-(3,5-dichloro-4-hydroxyphenyl)-ureido-carboxamide], all expressed as iprodione equivalents in or on the following food
commodities of animal origin:
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Egg
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except kidney and liver
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts, except kidney and liver
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except kidney and liver
Milk
Poultry, fat
Poultry, liver
Poultry, meat
Poultry, meat byproducts, except liver
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.5
3.0
3.0
0.5
0.5
1.5
0.5
3.0
3.0
0.5
0.5
0.5
3.0
3.0
0.5
0.5
0.5
3.0
3.0
0.5
0.5
0.5
3.5
5.0
1.0
1.0
0.5
3.0
3.0
0.5

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Sheep, meat byproducts, except kidney and liver

0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide],
and its metabolite [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide] in or on the following food commodity:
Commodity

Parts per million

Mustard greens

15.0

(d) Indirect or inadvertent residues. [Reserved]
[48 FR 40385, Sept. 7, 1983]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.399, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.401 Thiobencarb; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for the combined residues of the herbicide thiobencarb (S-[(4-chlorophenyl)
methyl]diethyl-carbamothioate) and its chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following
raw agricultural commodities:
Commodity

Part per million

Cattle, fat
Cattle, meat byproducts
Cattle, meat
Egg
Goat, fat
Goat, meat byproducts
Goat, meat
Hog, fat
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Milk
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Rice, grain
Rice, straw
Sheep, fat
Sheep, meat byproducts
Sheep, meat

0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.05
0.2
0.2
0.2
0.2
1.0
0.2
0.2
0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the herbicide thiobencarb (S-[(4-chloro-phenyl)methyl]diethylcarbamothioate) and its
chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following raw agricultural commodities:
Commodity

Parts per million

Celery
Endive
Lettuce

0.2
0.2
0.2

(d) Indirect or inadvertent residues. [Reserved]
[47 FR 6833, Feb. 17, 1982, as amended at 56 FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, 2011]

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§180.403 Thidiazuron; tolerances for residues.

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(a) General. Tolerances are established for the combined residues of the defoliant thidiazuron (N-phenylN-1,2,3-thiadiazol-5-ylurea) and its aniline containing metabolites in or on the following food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cotton, gin byproducts
Cotton, undelinted seed
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.4
0.4
0.4
24.0
0.3
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.05
0.4
0.4
0.4

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33700, May 24, 2000, as amended at 72 FR 53462, Sept. 19, 2007]

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§180.404 Profenofos; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide profenofos (O-(4-bromo-2-chlorophenyl)-Oethyl-S-propyl phosphorothioate) in or on the following food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cotton, gin byproducts
Cotton, undelinted seed
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.05
0.05
0.05
55.0
2.0
0.05
0.05
0.05
0.05
0.05
0.05
0.01
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, 2002; 72 FR 54579, Sept. 26, 2007]

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§180.405 Chlorsulfuron; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6methyl-1,3,5-triazin-2-yl)aminocarbonyl]benzenesulfonamide) and its metabolite, 2-chloro-5-hydroxy-N-[(4-methoxy-6methyl-1,3,5-triazin-2-yl)aminocarbonyl] benzenesulfonamide in or on the following raw agricultural commodities:
Commodity

Parts per million

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Barley, grain
Barley, straw
Oat, forage
Oat, grain
Oat, straw
Wheat, forage
Wheat, grain
Wheat, straw

0.1
0.5
20.0
0.1
0.5
20.0
0.1
0.5

(2) Tolerances are established for residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2- yl)
aminocarbonyl] benzenesulfonamide) in or on the following raw agricultural commodities.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Grass, forage
Grass, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.3
0.3
0.3
0.3
0.3
0.3
11.0
19.0
0.3
0.3
0.3
0.3
0.3
0.3
0.1
0.3
0.3
0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 52873, Aug. 14, 2002]

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§180.407 Thiodicarb; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide thiodicarb (dimethyl N,N′-[thiobis
[[(methylimino)carbonyloxy]]
bis[ethanimidothioate]) and its metabolite methomyl (S-methyl
N-[(methylcarbamoyl)
oxy]thioacetimidate) in or on the following food commodities or groups. The time-limited
tolerances expire and are revoked on the dates listed in the following table:
Commodity
Broccoli
Cabbage
Cauliflower
Corn, sweet, kernel plus cob with husks removed
Cotton, undelinted seed
Soybean, hulls
Soybean
Vegetable, leafy, except brassica, group 4

Parts per million

Expiration/revocation date
7.0
7.0
7.0
2.0
0.4
0.8
0.2
35

None
None
None
None
None
None
None
None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 44595, Aug. 22, 1997, as amended at 75 FR 60245, Sept. 29, 2010]

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§180.408 Metalaxyl; tolerances for residues.

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(a) General. Tolerances are established for the combined residues of the fungicide metalaxyl [N-(2,6-dmethylphyenyl)
-N-(methoxyacetyl) alanine methylester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy
methyl-6-methylphenyl)-N-(methoxyacetyl)-alanine methyl ester, each expressed as metalaxyl equivalents, in or on the
following food commodities:
Commodity
Alfalfa, forage
Alfalfa, hay
Almond
Almond, hulls
Apple
Apple, wet pomace
Apricot, dried
Asparagus
Avocado
Beet, garden, roots
Beet, garden, tops
Beet, sugar
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Blueberry
Broccoli
Brussels sprouts
Cabbage
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Cauliflower
Citrus, oil
Citrus, dried pulp
Clover, forage
Clover, hay
Cotton, undelinted seed
Cranberry
Egg
Fruit, citrus
Fruit, stone, group 12
Ginseng
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except kidney and liver
Grain, cereal, group 15, except barley, oat and wheat
Grain, crop
Grape
Grape, raisin
Grass, forage
Grass, hay
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts, except kidney and liver
Hop, dried cones
Hop, vines
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except kidney and liver
Lettuce, head
Milk
Mustard greens
Onion, bulb
Onion, green
Peanut
Peanut, hay
Peanut, meal

Parts per million
6.0
20.0
0.5
10.0
0.2
0.4
4.0
7.0
4.0
0.1
0.1
0.1
1.0
0.5
10.0
2.0
2.0
2.0
1.0
0.4
0.4
0.4
0.05
0.05
1.0
7.0
7.0
1.0
2.5
0.1
4.0
0.05
1.0
1.0
3.0
0.4
0.4
0.4
0.05
0.05
0.1
0.1
2.0
6.0
10.0
25.0
0.4
0.4
0.4
0.05
0.05
20
2.0
0.4
0.4
0.4
0.05
0.05
5.0
0.02
5.0
3.0
10.0
0.2
20.0
1.0

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Peanut, hulls
Pineapple
Pineapple, fodder
Pineapple, forage
Plum, prune, dried
Potato, chips
Potato, granules, flakes
Potato, processed potato waste
Potato, wet peel
Poultry, fat
Poultry, kidney
Poultry, liver
Poultry, meat
Poultry, meat byproducts, except kidney and liver
Potato
Raspberry
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except kidney and liver
Soybean, hulls
Soybean, meal
Soybean, seed
Spinach
Strawberry
Sunflower, seed
Sunflower, forage
Tomato, paste
Tomato, puree
Vegetable, brassica, leafy, group 5, except broccoli, cabbage, cauliflower, brussels sprouts, and mustard greens
Vegetable, cucurbit, group 9
Vegetable, foilage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4, except spinach
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, cannery waste
Vegetable, legume, group 6
Vegetable, root and tuber, group 1
Walnut

2.0
0.1
0.1
0.1
4.0
4.0
4.0
4.0
4.0
0.4
0.4
0.4
0.05
0.05
0.5
0.5
0.4
0.4
0.4
0.05
0.05
2.0
2.0
1.0
10.0
10.0
0.1
0.1
3.0
3.0
0.1
1.0
8.0
1.0
5.0
15.0
5.0
0.2
0.5
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration (refer to §180.1(m)) are established for
the combined residues of the fungicide metalaxyl [N-(2,6-dimethylphenyl)-N-(methoxyacetyl) alanine methyl ester] and its
metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methyl)-N-(methoxyacetyl)-alanine
methylester, each expressed as metalaxyl, in or on the following raw agricultural commodity:
Commodity

Parts per million

Papaya

0.1

(d) Indirect or inadvertent tolerances. Tolerances are established for indirect or inadvertent residues of metalaxyl in or
on the food commodities when present therein as a result of the application of metalaxyl to growing crops listed in
paragraph (a) of this section and other non-food crops to read as follows:
Commodity
Barley, bran
Barley, flour
Barley, grain
Barley, pearled barley
Barley, straw
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; forage
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; stover
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; straw
Oat, flour
Oat, forage
Oat, grain
Oat, groats, rolled oats
Oat, straw
Wheat, bran
Wheat, flour
Wheat, forage

Part per million

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1.0
1.0
0.2
1.0
2.0
1.0
1.0
1.0
1.0
2.0
0.2
1.0
2.0
1.0
1.0
2.0

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Wheat, germ
Wheat, grain
Wheat, middlings
Wheat, shorts
Wheat, straw

1.0
0.2
1.0
1.0
2.0

[65 FR 33700, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, 2009; 75 FR 56015, Sept. 15,
2010]

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§180.409 Pirimiphos-methyl; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide pirimiphos-methyl (O-(2-diethylamino-6-methyl4-pyrimidinyl) O,O-dimethyl phosphorothioate) in or on the following raw agricultural commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat byproducts
Corn, field, grain
Corn, pop, grain
Goat, fat
Goat, meat byproducts
Grain, aspirated fractions
Hog, fat
Hog, meat byproducts
Horse, fat
Horse, meat byproducts
Poultry, fat
Sheep, fat
Sheep, meat byproducts
Sorghum, grain, grain

0.02
0.02
8.0
8.0
0.02
0.02
20.0
0.02
0.02
0.02
0.02
0.02
0.02
0.02
8.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33714, May 24, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 49617, July 31, 2002; 70 FR 44492, Aug. 3, 2005;
72 FR 53462, Sept. 19, 2007]

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§180.410 Triadimefon; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the fungicide triadimefon, 1-(4-chlorophenoxy)
-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone, and triadimenol, β-(4-chlorophenoxy)-α-(1,1-dimethylethyl)
-1H-1,2,4-triazole-1-ethanol, expressed as triadimefon, in or on the following food commodities:
Commodity

Parts per million

Pineapple

Expiration/Revocation Date
2.0

None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54962, Sept. 24, 2008, as amended at 76 FR 34885, June 15, 2011]

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§180.411 Fluazifop-P-butyl; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide fluazifop-P-butyl, including its metabolites and
degradates, in or on the following commodities in the table. Compliance with the tolerance levels specified in the table
below is to be determined by measuring only the sum of fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]
phenoxy]propanoate, and the free and conjugated forms of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2pyridinyl]oxy]phenoxy]propanoic acid, calculated as the stoichiometric equivalent of fluazifop, in or on the commodity.
Commodity

Parts per million

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Banana
Beans, dry, seed
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Carrot, roots
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Citrus, dried pulp
Citrus, juice
Citrus, oil
Cotton, gin byproducts
Cotton, refined oil
Cotton, undelinted seed
Egg
Endive
Fruit, citrus, group 10
Fruit, stone
Goat, fat
Goat, meat
Goat, meat byproducts
Grape
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Nut, macadamia
Onion, bulb
Peanut
Peanut, meal
Pecans
Poultry, fat
Poultry, meat
Poultry, meat byproducts

0.01
50
1.0
3.5
0.25
2.0
0.05
0.05
0.05
0.40
0.06
30.0
1.5
1.3
1.0
0.05
6.0
0.03
0.05
0.05
0.05
0.05
0.01
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.1
0.5
1.5
2.2
0.05
0.05
0.05
0.05
1.0

Potato1

2.0

Potato, chips1

4.0

Potato, granules/flakes1
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, seed
Sweet potato, roots

0.05
0.05
0.05
2.5
1.5

1

No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the
herbicide fluazifop-P-butyl, including its metabolites and degradates, in or on the following commodities in the table.
Compliance with the tolerance levels specified in the table below is to be determined by measuring only the sum of
fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, and the free and conjugated forms
of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, calculated as the
stoichiometric equivalent of fluazifop, in or on the commodity.
Commodity

Parts per million

Asparagus
Coffee, bean
Pepper, tabasco
Rhubarb

3.0
0.1
1.0
0.5

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33714, May 24, 2000, as amended at 74 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, 2009; 74 FR 47457, Sept. 16, 2009;
76 FR 5703, Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011; 80 FR 46822, Aug. 6, 2015]

Back to Top

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§180.412 Sethoxydim; tolerances for residues.
(a) Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one (CAS Reg. No.
74051-80-2) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of
sethoxydim, in or on the commodity.
Commodity

Parts per
million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apricot
Apple, wet pomace
Asparagus
Bean, succulent
Beet, sugar, molasses
Beet, sugar, tops
Berry, low growing, subgroup 13-07H, except strawberry
Borage, meal
Buckwheat, flour
Buckwheat, grain
Bushberry subgroup 13-07B
Calendula, meal
Caneberry subgroup 13-07A
Canola, meal
Castor oil plant, meal
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherry, sweet
Cherry, tart
Chinese tallowtree, meal
Citrus, dried pulp
Clover, forage
Clover, hay
Coriander, leaves
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husk removed
Corn, sweet, stover
Cottonseed subgroup 20C
Cowpea, forage
Cowpea, hay
Crambe, meal
Cuphea, meal
Dillweed, fresh leaves
Echium, meal
Egg
Euphorbia, meal
Evening primrose, meal
Flax seed, meal
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Goat, fat
Goat, meat
Goat, meat byproducts
Gold of pleasure, meal
Grape, raisin
Hare's ear mustard, meal
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Jojoba, meal
Juneberry1

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40
40
2.0
0.2
0.8
4.0
15
10
3.0
2.5
40
25
19
4.0
20
5.0
40
20
0.2
0.2
1.0
0.2
0.2
20
1.5
35
55
4.0
2.0
0.5
2.5
3.0
0.4
3.5
5.0
15
50
40
40
10
40
2.0
20
20
40
0.5
0.2
1.0
0.2
0.2
1.0
40
2.0
40
0.2
0.2
1.0
0.2
0.2
1.0
20
5.0

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Lesquerella, meal

40
5.0

Lingonberry1
Lunaria, meal
Meadowfoam, meal
Milk
Milkweed, meal
Mustard, meal
Nectarine
Niger seed, meal
Nut, tree, group 14
Oil radish, meal
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea, field, hay
Pea, field, vines
Pea, succulent
Peach
Peanut
Peppermint, tops
Pistachio
Poppy seed, meal
Potato granules/flakes
Potato waste, processed
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Radish, tops
Rapeseed, meal
Rapeseed subgroup 20A
Rose hip, meal
Safflower, seed

40
40
0.5
40
40
0.2
20
0.2
40
25
40
20
10
0.2
25
30
0.2
40
8.0
8.0
0.2
0.2
2.0
4.5
40
35
20
15
5.0

Salal1
Sesame, meal
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, hay
Soybean, seed
Spearmint, tops
Strawberry
Stokes aster, meal
Sunflower, meal
Sunflower subgroup 20B, except safflower
Sweet rocket, meal
Tallowwood, meal
Tea oil plant, meal
Turnip, tops
Vegetable, brassica, leafy, group 5
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy, except brassica, group 4
Vegetable, root and tuber, group 1
Vernonia, meal

40
0.2
0.2
1.0
10
16
30
10
20
20
7.0
40
20
20
5.0
5.0
1.0
4.0
4.0
4.0
4.0
20

1

The individual tolerances for Juneberry, Lingonberry, and Salal expire on December 15, 2015.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. Tolerances are established for the herbicide sethoxydim, including its
metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3hydroxy-2-cyclohexen-1-one) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the
stoichiometric equivalent of sethoxydim, in or on the commodity.
Commodity

Parts per
million

Artichoke, globe
Fescue, forage
Fescue, hay
Rhubarb

5.0
7.0
4.0
0.3

(d) Indirect and inadvertent residues. [Reserved]

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[80 FR 34077, June 15, 2015]

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§180.413 Imazalil; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the fungicide imazalil,
1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolite, 1-(2,4-dichlorophenyl)-2-(1H-imidazole1-yl)-1-ethanol, in or on the following food commodities:
Commodity

Parts per million

Banana
Barley, grain
Barley, hay
Barley, straw
Citrus, dried pulp
Citrus, oil
Fruit, citrus, postharvest
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

3.0
0.1
0.5
0.5
25.0
200.0
10.0
0.5
0.1
0.5
0.5

(2) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)
-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolites, 3-[2-(2,4-dichlorophenyl)-2-(2,3-dihydroxypropoxy)ethyl]
-2,4-imidazolidinedione (FK772) and 3-[2-(2,4-dichlorophenyl)-2-(hydroxy)]-2,4-imidazolidinedione (FK284), in or on the
following food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.01
0.01
0.2
0.01
0.01
0.2
0.01
0.01
0.2
0.02
0.01
0.01
0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33715, May 24, 2000, as amended at 67 FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006]

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§180.414 Cyromazine; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide cyromazine, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the
commodity.
Commodity

Parts per million

Bean, dry, except cowpea
Bean, lima
Bean, succulent
Broccoli
Cabbage, abyssinian
Cabbage, seakale
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Egg

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3.0
1.0
2.0
1.0
10.0
10.0
0.05
0.2
0.05
0.05
0.25

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Garlic
Garlic, great-headed, bulb
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Hanover salad, leaves
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Leek

0.2
0.2
0.05
0.2
0.05
0.05
10.0
0.05
0.2
0.05
0.05
0.05
0.2
0.05
0.05
3.0
0.3

Mango1
Milk
Mushroom
Onion, bulb
Onion, green
Onion, potato
Onion, tree
Onion, welsh
Pepper
Potato
Poultry, fat (from chicken layer hens and chicken breeder hens only)
Poultry, meat (from chicken layer hens and chicken breeder hens only)
Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only)
Rakkyo, bulb
Shallot, bulb
Shallot, fresh leaves
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Tomato
Turnip, greens
Vegetable, brassica, leafy, group 5, except broccoli
Vegetable, leafy, except brassica, group 4
Vegetable, cucurbit, group 9

0.05
1.0
0.2
3.0
3.0
3.0
3.0
1.0
0.8
0.05
0.05
0.05
0.2
0.2
3.0
0.05
0.2
0.05
0.05
0.5
10.0
10.0
7.0
1.0

1

There are no U.S. registrations on mango as of May 4, 2000.

(2) A tolerance of 5.0 parts per million is established for residues of the insecticide cyromazine, including its
metabolites and degradates, in or on poultry feed when used as a feed additive only in feed for chicken layer hens and
chicken breeder hens at the rate of not more than 0.01 pound of cyromazine per ton of poultry feed for control of flies in
manure of treated chicken layer hens and chicken breeder hens, provided the feeding of cyromazine-treated feed must
stop at least 3 days (72 hours) before slaughter. If the feed is formulated by any person other than the end user, the
formulator must inform the end user, in writing, of the 3-day (72 hours) pre-slaughter interval. Compliance with the
tolerance level specified in this paragraph is to be determined by measuring only cyromazine,
N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide
cyromazine, including its metabolites and degradates, in or on the commodities in the table in this paragraph when present
therein as a result of the application of cyromazine to growing crops listed in paragraph (a)(1) of this section. Compliance
with the tolerance levels specified in this paragraph is to be determined by measuring only cyromazine,
N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.
Commodity

Parts per million

Cotton, undelinted seed
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, forage
Corn, sweet, stover
Radish, roots
Radish, tops

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1
0.5
0.5
0.5
0.5
0.5

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[65 FR 25860, May 4, 2000, as amended at 67 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, 2003; 75 FR 22256, Apr. 28, 2010;
76 FR 23494, Apr. 27, 2011]

Back to Top
§180.415 Aluminum tris (O-ethylphosphonate); tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its
metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels
specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the
commodity.
Commodity

Parts per million

Avocado
Banana
Bushberry subgroup 13B
Caneberry subgroup 13A
Cranberry
Fruit, citrus, group 10
Fruit, pome, group 11
Ginseng
Hop, dried cones
Juneberry
Lingonberry
Nut, macadamia
Onion, bulb
Onion, green
Pea, succulent

25
3.0
40
0.1
0.5
5.0
10
0.1
45
40
40
0.20
0.5
10.0
0.3
0.01

Pepper/eggplant, subgroup 8-10B1
Pineapple
Salal
Strawberry
Tomato
Turnip, greens
Turnip, roots
Vegetable, brassica, leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, leafy, except brassica, group 4

0.1
40
75
3
40
15
60
15
100

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in
or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to
be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.
Commodity

Parts per million

Asparagus
Grape

0.1
10

(d) Indirect or inadvertent residues. [Reserved]
[64 FR 36801, July 8, 1999, as amended at 64 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, 2000; 67 FR 55346, Aug. 29, 2002;
68 FR 11335, Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015]

Back to Top
§180.416 Ethalfluralin; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide ethalfluralin, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only the residues of ethalfluralin, N-ethyl-N-(2-methyl-2-propenyl)-2,6-dinitro4-(trifluoromethyl)benzenamine.
Commodity

Parts per million

Bean, dry, seed
Dill, dried leaves
Dill, fresh leaves
Peanut
Pea, dry, seed
Potato
Rapeseed subgroup 20A

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
0.05
0.05
0.05
0.05
0.05
0.05

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Soybean
Sunflower subgroup 20B
Vegetable, cucurbit, group 9

0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[49 FR 391, Jan. 4, 1984, as amended at 50 FR 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 FR 66014, Dec. 17, 1997; 64 FR
5191, Feb. 3, 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR 2342, Jan. 17,
2002; 67 FR 49617, July 31, 2002; 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, 2013]

Back to Top
§180.417 Triclopyr; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances for residues of the herbicide triclopyr per se, as a result of the application/use of
butoxyethyl ester of triclopyr and triethyylamine salt of triclopyr, are established in or on the following raw agricultural
commodities:
Commodity

Parts per million

Egg
Fish
Grass, forage
Grass, hay
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts, except kidney
Rice, grain
Rice, straw
Shellfish

0.05
3.0
700.0
200.0
0.01
0.1
0.1
0.1
0.3
10.0
3.5

(2) Tolerances for the combined residues of the herbicide triclopyr ((3,5,6-trichloro-2-pyridinyl)oxy) acetic acid and its
metabolite 3,5,6-trichloro-2-pyridinol (TCP), as a result of the application/use of butoxyethyl ester of triclopyr or the
triethylamine salt of triclopyr, are established in or on the following raw agricultural commodities:
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except kidney and liver
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts, except kidney and liver
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except kidney and liver
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except kidney and liver

0.05
0.5
0.5
0.05
0.05
0.05
0.5
0.5
0.05
0.05
0.05
0.5
0.5
0.05
0.05
0.05
0.5
0.5
0.05
0.05
0.05
0.5
0.5
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[50 FR 18486, May 1, 1985, as amended at 55 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, 1995; 62 FR 46894, Sept. 5, 1997;
63 FR 45406, Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR 58725, Sept. 18, 2002; 72 FR 41931, Aug. 1, 2007]

Back to Top
§180.418 Cypermethrin and isomers alpha-cypermethrin and zeta-cypermethrin; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the insecticide cypermethrin (±)alpha
cyano-(3-phenoxyphenyl)methyl(±)cis,trans-3(2,2-dichloroethenyl-2,2-dimethylcyclopropanecarboxylate in or on the
following commodities:
Commodity

Parts per million

Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cotton, gin byproducts
Cotton, undelinted seed
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Horse, fat
Horse, meat
Horse, meat byproducts
Lettuce, head
Milk, fat (reflecting 0.10 in whole milk)
Onion, bulb
Onion, green
Pecan
Poultry, fat
Poultry, meat
Sheep, fat
Sheep, meat
Sheep, meat byproducts

2.0
14.0
1.0
0.2
0.05
11.0
0.5
0.05
1.0
0.2
0.05
0.1
0.05
1.0
0.2
0.05
4.0
2.5
0.1
6.0
0.05
0.05
0.05
1.0
0.2
0.05

(2) Tolerances are established for residues of zeta-cypermethrin, (S-cyano(3-phenoxyphenyl) methyl (±))(cis-trans
3-(2,2-dichloroethenyl)-2,2 dimethylcyclopropanecarboxylate), including its metabolites and degradates, in or on the
commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined
by measuring only total cypermethrin, cyano(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane
carboxylate, in or on the commodity.
Commodity
Alfalfa, forage
Alfalfa, hay
Alfalfa, seed
Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Artichoke, globe
Avocado
Barley, grain
Barley, hay
Barley, straw
Beet, sugar, roots
Beet, sugar, tops
Berry group 13
Borage, seed
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Buckwheat, grain
Buckwheat, hay
Buckwheat, straw
Cabbage

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

Parts per
million
15
30
0.50
6
8
40
0.60
0.50
3.0
6.0
20.0
0.05
0.20
0.8
0.2
2.00
14.00
3.0
6.0
20.0
2.00

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Canistel
Castor oil plant, refined oil
Castor oil plant, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Chinese tallowtree, refined oil
Chinese tallowtree, seed
Cilantro, leaves
Citrus, dried pulp
Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Crambe, seed
Cuphea, seed
Echium, seed
Egg
Euphorbia, refined oil
Euphorbia, seed
Evening primrose, refined oil
Evening primrose, seed
Flax, seed
Food commodities/feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed
handling establishments
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Gold of pleasure, seed
Grain, aspirated fractions
Grape
Grass, forage, fodder, and hay, group 17, forage
Grass, forage, fodder and hay, group 17, hay
Hare's-ear mustard, seed
Hog, fat
Hog, meat
Horse, fat
Horse, meat
Horse, meat byproducts
Jojoba, refined oil
Jojoba, seed
Lesquerella, seed
Lunaria, seed
Mango
Meadowfoam, seed
Milk, fat (reflecting 0.10 in whole milk)
Milkweed, seed
Mustard, seed
Niger seed, refined oil
Niger seed, seed
Nut, tree, group 14
Oat, grain
Oat, hay
Oat, straw
Oil radish, seed
Okra
Onion, bulb
Onion, green
Papaya
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut
Pecan
Pistachio

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.50
0.4
0.2
1.00
0.2
0.05
0.4
0.2
10
1.8
4.0
9.0
0.05
30
0.05
30
15.00
0.05
15.00
0.5
0.2
0.2
0.2
0.05
0.4
0.2
0.4
0.2
0.2
0.05
0.35
2
1
1.00
0.2
0.05
0.2
10.0
2
10
35
0.2
0.1
0.05
1.00
0.2
0.05
0.4
0.2
0.2
0.2
0.70
0.2
2.50
0.2
0.2
0.4
0.2
0.05
3.0
6.0
20.0
0.2
0.2
0.10
3.00
0.50
0.05
0.1
0.05
0.05
0.05

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Poppy, seed
Poultry, fat
Poultry, meat
Rapeseed
Rice, grain
Rice, hulls
Rice, straw
Rice, wild, grain
Rose hip, refined oil
Rose hip, seed
Rye, grain
Rye, hay
Rye, straw
Safflower, seed
Sapodilla
Sapote, black
Sapote, mamey
Sesame, seed
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Star apple
Stokes aster, refined oil
Stokes aster, seed
Sugarcane, cane
Sunflower, refined oil
Sunflower, seed
Sweet rocket, seed
Tallowwood, refined oil
Tallowwood, seed
Tea oil plant, refined oil
Tea oil plant, seed
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root and tuber, group 1, except sugar beet
Vernonia, refined oil
Vernonia, seed
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.2
0.05
0.05
0.2
1.50
6.00
2.00
1.5
0.4
0.2
3.0
6.0
20.0
0.2
0.50
0.50
0.50
0.2
1.00
0.2
0.05
0.1
0.5
5.0
0.05
0.50
0.4
0.2
0.60
0.5
0.2
0.2
0.4
0.2
0.4
0.2
14
0.2
0.2
10.00
0.5
0.1
0.4
0.2
3.0
0.2
6.0
7.0

(3) Tolerances are established for residues of the insecticide, alpha-cypermethrin, (R)-cyano(3-phenoxyphenyl)methyl
(1S,3S)-rel-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only total cypermethrin, cyano(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane
carboxylate, in or on the commodity.
Commodity

Parts per
million

Alfalfa, hay
Beet, sugar, roots
Beet, sugar, tops
Brassica, head and stem, subgroup 5A
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Citrus, dried pulp
Citrus, oil
Corn, field, grain
Corn, pop, grain
Corn, sweet, kernel plus cob with husks removed
Cotton, undelinted seed
Egg
Food commodities/feed commodities (other than those covered by a higher tolerance as a results of use on growing crops) in food/feed
handling establishments

15
0.05
0.20
2.0
1.0
0.20
0.05
1.8
4.0
0.05
0.05
0.05
0.50
0.05
0.05

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Fruit, citrus, group 10-10
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Horse, fat
Horse, meat
Horse, meat byproducts
Milk, fat, reflecting 0.10 ppm in whole milk
Nut, tree, group 14-12
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Poultry, fat
Poultry, meat
Rice, grain
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, grain
Soybean, seed
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy, group 4
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root and tuber, group 1, except sugar beet
Wheat, grain

10
1.0
0.20
0.05
1.0
0.05
1.0
0.20
0.05
2.5
0.05
0.05
0.10
0.05
0.05
1.5
1.0
0.20
0.05
0.50
0.05
0.20
0.20
10
0.50
0.10
0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63235, 63243, Nov. 26, 1997, as amended at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, Sept. 17, 2001; 67 FR 6430, Feb.
12, 2002; 67 FR 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; 71 FR 78382, Dec. 29, 2006; 72 FR 53462, Sept. 19, 2007; 72
FR 71801, Dec. 19, 2007; 73 FR 1525, Jan. 9, 2008; 77 FR 72984, Dec. 7, 2012; 78 FR 7275, Feb. 1, 2013; 79 FR 73213, Dec. 10,
2014; 79 FR 77394, Dec. 24, 2014; 80 FR 45438, July 30, 2015]

Back to Top
§180.419 Chlorpyrifos-methyl; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the insecticide chlorpyrifos-methyl
[O,-O,-dimethyl O-(3,5,6-trichloro-2-pyridyl)] phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or on the
following food commodities:
Commodity

Parts per million

Barley, grain
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk, fat (0.05 ppm (N) in whole milk
Oat, grain
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, grain
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

6.0
0.5
0.5
0.5
0.1
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1.25
6.0
0.5
.5
.5
6.0
0.5
0.5
0.5
6.0

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Wheat, grain

6.0

(2) Tolerances are established for the combined residues of the insecticide chlorpyrifos-methyl (O,-O- dimethylO-(3,5,6-trichloro-2-pyridyl) phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or on the following food
commodities when present therein as a result of application to stored grains:
Commodity

Parts per million

Barley, bran
Barley, pearled barley
Rice, bran
Rice, hulls
Rice, polished rice
Sorghum, grain, bran
Wheat, bran
Wheat, germ
Wheat, middlings
Wheat, shorts

90
90
30
30
30
90
30
30
30
30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33715, May 24, 2000, as amended at 74 FR 46374, Sept. 9, 2009]

Back to Top
§180.420 Fluridone; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide fluridone, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4
(1H)-pyridinone, and its bound residues, calculated as the stoichiometric equivalent of fluridone, in or on the commodity.
Commodity

Parts per million

Crayfish
Fish

0.5
0.5

(2) Tolerances are established for residues of the herbicide fluridone, including its metabolites and degradates, in or
on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be
determined by measuring only fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, in or on the
commodity.
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, kidney
Poultry, liver
Poultry, meat
Poultry, meat byproducts

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
0.1
0.1
0.05
0.05
0.05
0.05
0.1
0.1
0.05
0.05
0.05
0.1
0.1
0.05
0.05
0.05
0.1
0.1
0.05
0.05
0.05
0.05
0.01
0.01
0.05
0.05

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Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts

0.05
0.1
0.1
0.05
0.05

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for
residues of the herbicide fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, including its
metabolites and degradates in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to
the Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA) section 18 emergency exemptions. Compliance with the
tolerance levels specified below is to be determined by measuring only fluridone. The tolerances expire on the date
specified in the table.
Commodity
Cotton, undelinted seed

Parts per million

Expiration/revocation date
0.1

12/31/17

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide
fluridone, including its metabolites and degradates, in or on the irrigated crop commodities and crop groupings in the table
in this paragraph, resulting from use of irrigation water containing residues of 0.15 parts per million following applications
of fluridone on or around aquatic sites. Where tolerances are established at higher levels from other uses of fluridone on
the crops in the table in this paragraph, the higher tolerance also applies to residues in or on the irrigated commodity.
Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only fluridone,
1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, in or on the commodity.
Commodity

Parts per million

Animal feed, nongrass, group 18
Avocado
Berry, group 13
Cotton, undelinted seed
Cranberry
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grain, cereal, forage, fodder and straw, group 16
Grain, cereal, group 15
Grape
Grass, forage
Hop, dried cones
Nut, tree, group 14
Okra
Strawberry
Vegetable, brassica, leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root and tuber, group 1

0.15
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.15
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

[76 FR 23495, Apr. 27, 2011, as amended at 77 FR 66720, Nov. 7, 2012; 80 FR 18143, Apr. 3, 2015]

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§180.421 Fenarimol; tolerances for residues.
(a) General. Tolerances are established for residues of fenarimol, including its metabolites and degradates, in or on
the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only fenarimol alpha-(2 chlorophenyl)-alpha-(4-chlorophenyl)-5-pyrimidinemethanol.
Commodity

Parts per million

Apple
Apple, wet pomace
Banana
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Cherry, sweet
Cherry, tart
Goat, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.3
0.3
0.25
0.01
0.01
0.01
0.05
1.0
1.0
0.01

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Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Grape
Hazelnut
Hop, dried cones
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Pear
Pecan
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Vegetable, cucurbit, group 9*

0.01
0.01
0.05
0.1.
0.02
5.0
0.01
0.01
0.01
0.05
0.1
0.02
0.01
0.01
0.01
0.05
0.20

*There are no U.S. registrations as of August 27, 2010.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[51 FR 39662, Oct. 30, 1986, as amended at 53 FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, 1988; 54 FR 45734, Oct. 31, 1989;
60 FR 33354, June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; 67 FR
41807, June 19, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, Sept. 15, 2006; 74 FR 68173, Dec.
23, 2009; 75 FR 56897, Sept. 17, 2010]

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§180.422 Tralomethrin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide tralomethrin, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of tralomethrin, (S)-cyano(3-phenoxyphenyl)methyl (1R,3S)
-2,2-dimethyl-3-(1,2,2,2-tetrabromoethyl)cyclopropanecarboxylate, and its metabolites (S)-cyano(3-phenoxyphenyl)methyl
(1R,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate and (S)-cyano(3-phenoxyphenyl)methyl (1S,3R)
-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate, calculated as the stoichiometric equivalent of tralomethrin,
in or on the commodity.
Commodity
Broccoli
Cotton, undelinted seed
Cotton, oil
Lettuce, head
Lettuce, leaf
Soybean, seed
Sunflower, seed

Parts per million

Expiration/revocation date
0.5
0.02
0.20
1.00
3.00
0.05
0.05

7/9/13
7/9/13
7/9/13
7/9/13
7/9/13
7/9/13
7/9/13

(2) A tolerance of 0.02 part per million with an expiration/revocation date of July 9, 2013 is established for residues of
the insecticide tralomethrin, including its metabolites and degradates, in or on food commodities (other than those covered
by a higher tolerance as a result of use on growing crops) in food-handling establishments. Compliance with the tolerance
level specified in this paragraph is to be determined by measuring only the sum of tralomethrin, (S)-cyano
(3-phenoxyphenyl)methyl (1R,3S)-2,2-dimethyl-3-(1,2,2,2-tetrabromoethyl)cyclopropanecarboxylate, and its metabolites
(S)-cyano(3-phenoxyphenyl)methyl (1R,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate and (S)-cyano
(3-phenoxyphenyl)methyl (1S,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate, calculated as the
stoichiometric equivalent of tralomethrin, in or on the commodity.
(i) The insecticide may be present as a residue from application of tralomethrin in food-handling establishments,
including food service, manufacturing, and processing establishments, such as restaurants, cafeterias, supermarkets,
bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries.
(ii) The application shall be made in accordance with the following prescribed conditions: Application shall be limited
to a general surface and spot and/or crack and crevice treatment in food-handling establishments where food and food
products are held, processed, prepared, and served. General surface application may be used only when the facility is not
in operation provided exposed food has been covered or removed from the area being treated. All food-contact surfaces
and equipment must be thoroughly cleaned after general surface applications. Spot and/or crack and crevice application
may be used while the facility is in operation provided exposed food is covered or removed from the area being treated

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prior to application. Spray concentration shall be limited to a maximum of 0.06 percent active ingredient. Contamination of
food and food-contact surfaces shall be avoided.
(3) A tolerance of 0.02 part per million with an expiration/revocation date of July 9, 2013 is established for residues of
the insecticide tralomethrin, including its metabolites and degradates, in or on feed commodities (other than those covered
by a higher tolerance as a result of use on growing crops) in feed-handling establishments. Compliance with the tolerance
level specified in this paragraph is to be determined by measuring only the sum of tralomethrin, (S)-cyano
(3-phenoxyphenyl)methyl (1R,3S)-2,2-dimethyl-3-(1,2,2,2-tetrabromoethyl)cyclopropanecarboxylate, and its metabolites
(S)-cyano(3-phenoxyphenyl)methyl (1R,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate and (S)-cyano
(3-phenoxyphenyl)methyl (1S,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate, calculated as the
stoichiometric equivalent of tralomethrin, in or on the commodity.
(i) The insecticide may be present as a residue from application of tralomethrin in feed-handling establishments,
including feed manufacturing and processing establishments.
(ii) The application shall be made in accordance with the following prescribed conditions: Application shall be limited
to a general surface and spot and/or crack and crevice treatment in feed-handling establishments where feed and feed
products are held or processed. General surface application may be used only when the facility is not in operation
provided exposed feed has been covered or removed from the area being treated. All feed-contact surfaces and
equipment must be thoroughly cleaned after general surface applications. Spot and/or crack and crevice application may
be used while the facility is in operation provided exposed feed is covered or removed from the area being treated prior to
application. Spray concentration shall be limited to a maximum of 0.06 percent active ingredient. Contamination of feed
and feed-contact surfaces shall be avoided.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63001, Nov. 26, 1997, as amended at 62 FR 66025, Dec. 17, 1997; 65 FR 33701, May 24, 2000; 71 FR 74817, Dec. 13,
2006; 77 FR 59127, Sept. 26, 2012]

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§180.425 Clomazone; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide clomazone, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only clomazone, 2-[(2-chlorophenyl)methyl]-4,4-dimethyl-3-isoxazolidinone,
in or on the commodity.
Commodity
Bean, snap, succulent
Brassica, head and stem, subgroup 5A
Cotton, undelinted seed
Cowpea, forage
Cowpea, hay
Cucumber
Pea, southern, dry seed
Pea, southern, succulent seed
Pea, succulent
Pepper
Peppermint, tops
Pumpkin
Rhubarb
Rice, grain
Rice, straw
Soybean
Spearmint, tops
Squash, summer
Squash, winter
Sugarcane, cane
Sweet potato, roots
Vegetable, cucurbit, group 9
Vegetable, tuberous and corm, except potato, subgroup 1D

Parts per million
0.05
0.10
0.05
0.05
0.05
0.1
0.05
0.05
0.05
0.05
0.05
0.1
0.30
0.02
0.02
0.05
0.05
0.1
0.1
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[51 FR 9446, Mar. 19, 1986]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.425, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.426 2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-quinoline carboxylic acid; tolerance
for residues.
A tolerance is established for residues of the herbicide 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2yl]-3-quinoline carboxylic acid, in or on the raw agricultural commodity soybean at 0.05 part per million.
[51 FR 13309, Apr. 2, 1986]

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§180.427 Tau-Fluvalinate; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide tau-fluvalinate, cyano-(3-phenoxyphenyl)methyl
N-[2-chloro-4-(trifluoromethyl)phenyl]-D-valinate, in or on the following food commodities:
Commodity

Parts per million

Honey

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertent residues. [Reserved]
[65 FR 33701, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, 2008]

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§180.428 Metsulfuron methyl; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the herbicide metsulfuron methyl (methyl
2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- 2-yl)amino]carbonyl]amino] sulfonyl] benzoate) and its metabolite methyl
2-[[[[(4-methoxy-6-methyl-1-,3,5- triazin-2-yl)amino]carbonyl]amino] sulfonyl]-4-hydroxybenzoate in or on the following raw
material agricultural commodities:
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Grass, forage
Grass, hay
Grass, straw
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Sugarcane, cane
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.1
20.0
0.3
15.0
15.0
15.0
0.2
0.1
0.2
0.05
5.0
0.1
20.0
0.3

(2) Tolerances are established for residues of metsulfuron methyl (methyl-2[[[[(4-methoxy- 6-methyl-1,3,5-triazin-2- yl)
amino]carbonyl]amino] sulfonyl] benzoate) in or on the following raw agricultural commodities:
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, kidney

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.1
0.5
0.1
0.1
0.1
0.5

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Goat, meat
Goat, meat byproducts
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts

0.1
0.1
0.1
0.5
0.1
0.1
0.1
0.5
0.1
0.1
0.05
0.1
0.5
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 70191, Dec. 16, 1999, as amended at 66 FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, 2002]

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§180.429 Chlorimuron ethyl; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide chlorimuron ethyl, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only chlorimuron ethyl, ethyl 2-[[[[(4-chloro-6-methoxypyrimidin-2yl)amino]carbonyl]
sulfonyl]benzoate] in or on the following commodities:
Commodity
Berry, low growing, except strawberry, subgroup 13-07H
Corn, field, forage
Corn, field, grain
Corn, field, stover
Grain, aspirated fractions
Peanut
Soybean, forage
Soybean, hay
Soybean, seed

Parts per million
0.02
0.5
0.01
2.0
3.0
0.02
0.45
1.8
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[74 FR 10494, Mar. 11, 2009, as amended at 74 FR 67087, Dec. 18, 2009]

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§180.430 Fenoxaprop-ethyl; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide fenoxaprop-ethyl, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of fenoxaprop-ethyl, (±)-ethyl 2-[4-[(6-chloro-2-benzoxazolyl)
oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoic acid and
6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of fenoxaprop-ethyl, in or on the
commodity.
Commodity

Parts per million

Barley, grain
Barley, straw
Cattle, fat
Cattle, meat byproducts
Cattle, meat
Cotton, undelinted seed
Goat, fat
Goat, meat byproducts

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
0.1
0.05
0.05
0.05
0.05
0.05
0.05

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Goat, meat
Hog, fat
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Milk
Peanut
Peanut, hulls
Rice, grain
Sheep, fat
Sheep, meat byproducts
Sheep, meat
Soybean
Wheat, grain
Wheat, straw

0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.02
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.50

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide
fenoxaprop-ethyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph in
connection with use of fenoxaprop-ethyl under section 18 emergency exemptions granted by EPA. Compliance with the
tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenoxaprop-ethyl, (±)-ethyl
2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]
propanoic acid and 6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of fenoxaprop-ethyl,
in or on the commodity. The tolerances expire and are revoked on the dates specified in the table in this paragraph.
Commodity

Expiration/
revocation date

Parts per million

Grass, forage
Grass, hay

0.05
0.05

12/31/16
12/31/16

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the herbicide fenoxaprop-ethyl, including its metabolites and degradates, in or on the
commodities in the table in this paragraph when fenoxaprop-ethyl is used in the states of Oregon, Washington, and Utah.
Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of
fenoxaprop-ethyl, (±)-ethyl 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2benzoxazolyl)oxy]phenoxy]propanoic acid and 6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric
equivalent of fenoxaprop-ethyl, in or on the commodity
Parts per
million

Commodity
Grass, hay

0.09

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 1377, Jan. 9, 1998, as amended at 63 FR 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008; 75 FR 80346, Dec. 22, 2010;
76 FR 23495, Apr. 27, 2011; 78 FR 78748, Dec. 27, 2013; 79 FR 26164, May 7, 2014]

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§180.431 Clopyralid; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide clopyralid, including its metabolites and
degradates, in or on the commodities in the table below from its application in the acid form or in the form of its salts.
Compliance with the tolerance levels specified below is to be determined by measuring only clopyralid, (3,6-dichloro-2pyridinecarboxylic acid), in or on the following commodities:
Commodity

Parts per million

Apple
Asparagus
Barley, bran
Barley, grain
Barley, hay
Barley, pearled barley
Barley, straw
Beet, garden, tops
Beet, garden, roots
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

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0.05
1.0
12
3.0
9.0
12
9.0
3.0
4.0
10
2.0
3.0
2.0
5.0

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Bushberry subgroup 13-07B
Canola, meal
Canola, seed
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Corn, field, forage
Corn, field, grain
Corn, field, milled byproducts
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cranberry
Egg
Flax, meal
Fruit, stone, group 12
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Grass, forage
Grass, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Oat, forage
Oat, grain
Oat, groats/rolled oats
Oat, straw
Peppermint, tops
Plum, prune, dried
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rapeseed, forage
Rapeseed, meal
Rapeseed, subgroup 20A, except gold of pleasure
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver
Spearmint, tops
Spinach
Strawberry
Swiss chard
Teff, forage
Teff, grain
Teff, hay
Teff, straw
Turnip, greens
Turnip, roots
Wheat, bran
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, middling
Wheat, shorts
Wheat, straw

0.50
6.0
3.0
1.0
3.0
1.0
36.0
3.0
1.0
1.5
10.0
1.0
10.0
7.0
1.0
10.0
4.0
0.1
6.0
0.5
1.0
3.0
1.0
36.0
500.0
500.0
0.2
0.2
0.2
5.0
1.0
3.0
1.0
36.0
0.2
9.0
3.0
12
9.0
3.0
1.5
0.2
0.2
0.2
3.0
6.0
3.0
1.0
3.0
1.0
36.0
3.0
5.0
4.0
3.0
9.0
3.0
9.0
9.0
4.0
1.0
12
9.0
12
3.0
12
12
9.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[52 FR 10566, Apr. 2, 1987]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.431, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.432 Lactofen; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide lactofen, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only lactofen, 2-ethoxy-1-methyl-2-oxoethyl 5-[2-chloro-4-(trifluoromethyl)
phenoxy]-2-nitrobenzoate, in or on the commodity.
Commodity

Parts per million

Beans, snap, succulent, except lima bean
Cotton, gin byproducts
Cotton, undelinted seed
Peanut
Soybean, seed

0.01
0.02
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of the herbicide lactofen, including its metabolites and degradates, in or on the commodities in the
table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring
only lactofen, 2-ethoxy-1-methyl-2-oxoethyl 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, in or on the
commodity.
Commodity

Parts per million

Okra
Vegetables, fruiting, group 08

0.02
0.02

(d) Indirect or inadvertent residues. [Reserved]
[69 FR 57216, Sept. 24, 2004, as amended at 72 FR 33906, June 20, 2007; 76 FR 23496, Apr. 27, 2011]

Back to Top
§180.433 Fomesafen; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide fomesafen, including its metabolites and
degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table below
is to be determined by measuring only fomesafen, 5-[2-chloro-4-(trifluoromethyl)phenoxy]-N-(methylsulfonyl)-2nitrobenzamide, in or on the commodity.
Commodity

Parts per million

Bean, dry
Bean, lima, succulent
Bean, snap, succulent
Cantaloupe
Cotton, gin byproducts
Cotton, undelinted seed
Cucumber
Pea, succulent
Pepper, bell
Pepper, non-bell
Potato
Pumpkin
Soybean
Soybean, vegetable, succulent
Squash, summer
Squash, winter
Tomato
Watermelon

0.05
0.05
0.05
0.025
0.025
0.025
0.025
0.025
0.025
0.025
0.025
0.025
0.05
0.05
0.025
0.025
0.025
0.025

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[71 FR 25951, May 3, 2006, as amended at 72 FR 52020, Sept. 12, 2007; 76 FR 12882, Mar. 9, 2011; 78 FR 65570, Nov. 1, 2013;
80 FR 9391, Feb. 23, 2015]

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§180.434 Propiconazole; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of propiconazole, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only those propiconazole residues convertible to 2,4-dichlorobenzoic acid (2,4-DCBA), expressed as the
stoichiometric equivalent of propiconazole, in or on the commodity in the table below:
Commodity
Almond, hulls
Banana
Barley, bran
Barley, grain
Barley, hay
Barley, straw
Bean, dry seed
Bean, snap
Bean, succulent shelled
Beet, garden, roots
Beet, garden, tops
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Bushberry, subgroup 13-07B
Caneberry, subgroup 13-07A
Carrot, roots
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver and kidney
Cilantro, leaves
Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Fruit, citrus, group 10-10
Fruit, stone, group 12, except plum
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except liver and kidney
Grain, aspirated fractions
Grass, forage
Grass, hay
Grass, straw
Hog, kidney
Hog, liver
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except liver and kidney
Leaf petioles subgroup 4B
Low growing berry subgroup 13-07G, except cranberry
Milk
Mushroom

Parts per million

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7.0
0.2
6.0
3.0
30
20
0.40
0.70
0.10
0.30
5.5
1.0
1.5
0.3
10
1.0
1.0
0.25
0.05
2.0
2.0
0.05
0.05
13
1000
12
0.2
30
0.2
30
6.0
0.1
30
8.0
4.0
0.05
2.0
2.0
0.05
0.05
110
0.5
0.5
40
0.2
0.2
0.05
2.0
2.0
0.05
0.05
5.0
1.3
0.05
0.1

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Nut, tree, group 14
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Onion, bulb subgroup 3-07A
Onion, green, subgroup 3-07B
Parsley, fresh leaves
Parsley, dried leaves
Peanut
Peanut, hay
Peppermint, tops
Pineapple
Pineapple, process residue
Pistachio
Plum
Rapeseed subgroup 20A
Rice, bran
Rice, grain
Rice, hulls
Rice, straw
Rye, bran
Rye, forage
Rye, grain
Rye, straw
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver and kidney
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Spearmint, tops
Sugarcane, cane
Tomato
Vegetable, foliage of legume, group 7
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.1
4.0
3.0
15
10
0.2
9.0
13
35
0.2
20
10.0
4.5
7.0
0.1
0.60
0.30
15
7.0
20
18
0.6
9.0
0.3
10
0.05
2.0
2.0
0.05
0.05
12
3.5
15
11
30
2.0
10.0
0.4
3.0
30
0.6
15
0.3
30
20

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of propiconazole
(1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole) and its metabolites determined as
2,4-dichlorobenzoic acid and expressed as parent compound, in connection with use of the pesticide under section 18
emergency exemptions granted by EPA. The tolerances will expire and are revoked on the dates specified in the following
table:
Commodity

Parts per million

Avocado
Nectarine
Peach

Expiration/revocation date
10
2.0
2.0

12/31/16
12/31/13
12/31/13

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established
for residues of 1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl]methyl]-1H-1,2,4-triazole and its metabolites
determined as 2,4-dichlorobenzoic acid and expressed as parent compound, in or on the following commodities:
Commodity

Parts per million

Cranberry
Rice, wild, grain

1.0
0.5

(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the fungicide
1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole and its metabolites determined as
2,4-dichlorobenzoic acid and expressed as parent compound in or on the following commodities when present therein as a
result of application of propiconazole to growing crops in paragraphs (a) and (c) of this section:
Commodity

Parts per million

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Alfalfa, forage
Alfalfa, hay

0.1
0.1

[71 FR 55306, Sept. 22, 2006, as amended at 72 FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, 2009; 75 FR 80346, Dec. 22,
2010; 76 FR 27268, May 11, 2011; 77 FR 38204, June 27, 2012; 77 FR 75044, Dec. 19, 2012; 78 FR 23503, Apr. 19, 2013; 78 FR
78748, Dec. 27, 2013; 79 FR 18467, Apr. 2, 2014]

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§180.435 Deltamethrin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of deltamethrin, including its metabolites and degradates, in
or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by
measuring only deltamethrin, (1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylic acid (S)-alpha-cyano-3phenoxybenzyl ester, and its major metabolites, trans-deltamethrin, (S)-alpha-cyano-m-phenoxybenzyl(1R,3S)
-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, and alpha-R-deltamethrin, (R)
-alpha-cyano-m-phenoxybenzyl-(1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, in or on the
commodity.
Commodity

Parts per million

Almond, hulls
Apple, wet pomace
Artichoke, globe
Barley, bran
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, forage
Corn, field, refined oil
Corn, field, stover
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, refined oil
Cotton, undelinted seed
Egg
Fish—freshwater finfish
Fish—freshwater finfish, farm raised
Fish—saltwater finfish, other
Fish—saltwater finfish, tuna
Fruit, pome, Group 11
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grain, cereal, Group 15, except sweet corn
Hog, fat
Horse, fat
Horse, meat
Horse, meat byproducts
Lychee*
Milk, fat (reflecting 0.02 ppm in whole milk)
Nut, tree, Group 14
Onion, bulb
Onion, green
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Radish, tops
Rapeseed
Rice, hulls
Rye, bran
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, stover
Soybean, seed
Soybean, hulls
Starfruit*
Sunflower, seed

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2.5
1.0
0.5
5.0
0.05
0.02
0.05
0.7
2.5
5.0
5.0
10
0.03
15
0.2
0.04
0.02
0.01
0.01
0.01
0.01
0.2
0.05
0.02
0.05
65
1.0
0.05
0.05
0.02
0.05
0.2
0.1
0.1
0.1
1.5
0.05
0.02
0.02
4.0
0.2
2.5
5.0
0.05
0.02
0.05
0.5
1.0
0.1
0.2
0.2
0.1

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Tomato
Tomato, paste
Tomato, puree
Vegetable, cucurbit, Group 9
Vegetable, fruiting, Group 8
Vegetable, root, except sugar beet, Subgroup IB
Vegetable, tuberous and corm, Subgroup IC
Wheat, bran

0.2
1.0
1.0
0.2
0.3
0.2
0.04
5.0

*There are no U.S. registrations for use of deltamethrin on starfruit and lychee.
(2) A tolerance of 0.05 ppm is established for residues of the insecticide deltamethrin, including its metabolites and
degradates, in or on all food/feed items (other than those covered by a higher tolerance as a result of use on growing
crops) when deltamethrin is used in food/feed handling establishments or as a wide-area mosquito adulticide. Compliance
with the tolerance levels specified is to be determined by measuring only deltamethrin, (1R,3R)-3-(2,2-dibromovinyl)
-2,2-dimethylcyclopropanecarboxylic acid (S)-alpha-cyano-3-phenoxybenzyl ester, and its major metabolites,
trans-deltamethrin, (S)-alpha-cyano-m-phenoxybenzyl(1R,3S)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate,
and alpha-R-deltamethrin, (R)-alpha-cyano-m-phenoxybenzyl-(1R,3R)-3-(2,2-dibromovinyl)
-2,2-dimethylcyclopropanecarboxylate, in or on the commodity.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63001, Nov. 26, 1997, as amended at 63 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, 2004; 74 FR 46375, Sept. 9,
2009; 76 FR 34885, June 15, 2011; 79 FR 66301, Nov. 7, 2014; 80 FR 16302, Mar. 27, 2015]

Back to Top
§180.436 Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3-phenoxyphenyl)
methyl-3-(2,2-dichloroethenyl)-2,2dimethyl-cyclopropane-carboxylate; CAS No. 68359-37-5) in or on the following raw
agricultural commodities:
Commodity
Alfalfa
Alfalfa, forage
Alfalfa, hay
Almond, hulls
Barley, bran
Barley, grain
Beet, sugar, dried pulp
Beet, sugar, roots
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Buckwheat, grain
Carrot, roots
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Citrus, dried pulp
Citrus, oil
Corn, field, grain
Corn, pop, grain
Corn, sweet, kernel plus cob with husks removed
Cotton, hulls
Cotton, refined oil
Cotton, undelinted seed
Egg
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grain, cereal, forage, fodder and hay, group 16, forage, except rice
Grain, cereal, forage, fodder and hay, group 16, hay, except rice
Grain, cereal, forage, fodder and hay, group 16, stover, except rice

Parts per million

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5.0
5.0
13
0.5
0.5
0.15
1.0
0.10
2.5
7.0
0.15
0.20
2.0
0.10
0.10
0.3
0.3
0.05
0.05
0.05
2.0
2.0
1.0
0.01
0.2
0.5
0.3
2.0
0.05
0.05
150
25
6.0
30

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Grain, cereal, forage, fodder and hay, group 16, straw, except rice
Grape
Grape, raisin
Grass, forage, fodder and hay, group 17, forage
Grass, forage, fodder and hay, group 17, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Hop, vines
Horse, fat
Horse, meat
Horse, meat byproducts
Lettuce, head
Lettuce, leaf
Milk
Milk, fat
Millet, grain
Mustard greens
Nut, tree, group 14
Oat, bran
Oat, grain
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea, dry, seed
Pea, southern, succulent
Peanut
Peanut, hay
Pepper
Pistachio
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Radish, roots
Rye, bran
Rye, grain
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, grain
Soybean, forage
Soybean, hay
Soybean, seed
Sugarcane, cane
Sugarcane, molasses
Sunflower, forage
Sunflower, seed
Teosinte, grain
Tomato
Tomato, dry pomace
Tomato, paste
Tomato, wet pomace
Triticale, grain
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, tuberous and corm, subgroup 1C
Wheat, bran
Wheat, grain
Wheat, shorts

7.0
1.0
3.5
12
50
0.5
0.01
0.01
20.0
4.0
2.0
0.05
0.05
2.0
3.0
0.2
5.0
0.15
7.0
0.01
0.5
0.15
0.15
0.15
0.25
0.01
6.0
0.50
0.01
0.01
0.01
0.01
1.0
0.5
0.15
2.0
0.05
0.05
3.5
8.0
4.0
0.03
0.05
0.20
5.0
0.02
0.05
0.20
5.0
0.5
5.0
0.15
7.0
0.1
0.5
6.0
0.01
0.5
0.15
0.5

(2) A tolerance of 0.05 ppm is established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3-phenoxyphenyl)
methyl-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate; CAS Reg. No. 69359-37-5) in food commodities
exposed to the insecticide during treatment of food-handling establishments where food and food products are held,
processed, prepared, or served. Treatments may be made by general surface, spot, and/or crack and crevice applications.
(i) General surface treatments shall be limited to a maximum of 3.8 grams of active ingredient per 1,000 square feet,
applying to walls, floors, and ceilings with a low-pressure system. Cover or remove all food processing and/or handling
equipment during application. Do not apply directly to food products. Reapplications may be made at 10-day intervals.
(ii) Crack and crevice or spot treatments shall be limited to a maximum of 0.1 percent of the active ingredient weight,
applied with a low-pressure system with a pinpoint or variable-pattern nozzle. Dust formulation shall be limited to a

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maximum of 0.1 percent of the active ingredient by weight, applied using a hand duster, power duster, or other equipment
capable of applying dust insecticide directly into voids and cracks and crevices. Dust applications should be made in a
manner to avoid deposits on exposed surfaces or introducing the material into the air. Cover exposed food or remove food
from premises. Do not apply directly to food. Reapplications may be made at 10-day intervals.
(iii) To ensure safe use of the insecticide, its label and labeling shall conform to that registered by the Environmental
Protection Agency, and it shall be used in accordance with such label and labeling.
(3) A tolerance of 0.05 part per million is established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate; CAS Reg. No. 68359-37-5) in feed
commodities exposed to the insecticide during treatment of feed-handling establishments where feed and feed products
are held, processed, prepared, or served. Treatments may be made by general surface, spot, and/or crack and crevice
applications.
(i) General surface tratments shall be limited to a maximum of 3.8 grams of active ingredient per 1,000 square feet,
applying to walls, floors, and ceilings with a low-pressure system. Cover or remove all feed processing and/or handling
equipment during application. Do not apply directly to feed products. Reapplications may be made at 10-day intervals.
(ii) Crack and crevice or spot treatments shall be limited to a maximum of 0.1 percent of the active ingredient by
weight, applied with a low-pressure system with a pinpoint or variable-pattern nozzle. Dust formulation shall be limited to a
maximum of 0.1 percent of the active ingredient by weight, applied using a hand duster, power duster, or other equipment
capable of applying dust insecticide directly into voids and cracks and crevices. Dust applications should be made in a
manner to avoid deposits on exposed surfaces or introducing the material into the air. Cover exposed feed or remove feed
from premises. Do not apply directly to feed. Reapplications may be made at 10-day intervals.
(iii) To ensure safe use of the insecticide, its label and labeling shall conform to that registered by EPA, and it shall be
used in accordance with such label and labeling.
(4) Tolerances are established for residues of the isomer, beta-cyfluthrin, cyano(4-fluoro-3-phenoxyphenyl)methyl3-(2,2-dichloroethenyl)-2,2-dimethyl-cyclopropanecarboxylate [mixture comprising the enantiomeric pair (R)-α-cyano-4fluoro-3-phenoxybenzyl (1S,3S)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate and (S)-α-cyano-4-fluoro-3phenoxybenzyl (1R,3R)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate with the enantiomeric pair (R)-α-cyano4-fluoro-3-phenoxybenzyl (1S,3R)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate and (S)-α-cyano-4-fluoro-3phenoxybenzyl (1R,3S)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate], in or on the following raw agricultural
commodities:
Commodity
Alfalfa
Alfalfa, forage
Alfalfa, hay
Almond, hulls
Barley, bran
Barley, grain
Beet, sugar, dried pulp
Beet, sugar, roots
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Buckwheat, grain
Carrot, roots
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Citrus, dried pulp
Citrus, oil
Corn, field, grain
Corn, pop, grain
Corn, sweet, kernel plus cob with husks removed
Cotton, hulls
Cotton, refined oil
Cotton, undelinted seed
Egg
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grain, cereal, forage, fodder and hay, group 16, forage, except rice
Grain, cereal, forage, fodder and hay, group 16, hay, except rice
Grain, cereal, forage, fodder and hay, group 16, stover, except rice

Parts per million

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5.0
5.0
13
0.5
0.5
0.15
1.0
0.10
2.5
7.0
0.15
0.20
2.0
0.10
0.10
0.3
0.3
0.05
0.05
0.05
2.0
2.0
1.0
0.01
0.2
0.5
0.3
2.0
0.05
0.05
150
25
6.0
30

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Grain, cereal, forage, fodder and hay, group 16, straw, except rice
Grape
Grape, raisin
Grass, forage, fodder and hay, group 17, forage
Grass, forage, fodder and hay, group 17, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Hop, vines
Horse, fat
Horse, meat
Horse, meat byproducts
Lettuce, head
Lettuce, leaf
Milk
Milk, fat
Millet, grain
Mustard greens
Nut, tree, group 14
Oat, bran
Oat, grain
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea, dry, seed
Pea, southern, succulent
Peanut
Peanut, hay
Pepper
Pistachio
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Radish, roots
Rye, bran
Rye, grain
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, grain
Soybean, forage
Soybean, hay
Soybean, seed
Sugarcane, cane
Sugarcane, molasses
Sunflower, forage
Sunflower, seed
Teosinte, grain
Tomato
Tomato, paste
Tomato, pomace
Triticale, grain
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy greens, except Brassica, group 4
Vegetable, tuberous and corm, subgroup 1C
Wheat, bran
Wheat, grain
Wheat, shorts

7.0
1.0
3.5
12
50
0.5
0.01
0.01
20.0
4.0
2.0
0.05
0.05
2.0
3.0
0.2
5.0
0.15
7.0
0.01
0.5
0.15
0.15
0.15
0.25
0.01
6.0
0.50
0.01
0.01
0.01
0.01
1.0
0.5
0.15
2.0
0.05
0.05
3.5
8.0
4.0
0.03
0.05
0.20
5.0
0.02
0.05
0.20
0.5
5.0
0.15
7.0
0.1
0.5
6.0
0.01
0.5
0.15
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[53 FR 1924, Jan. 25, 1988]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.436, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.437 Methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-p-toluate and methyl 6-(4-isopropyl-4-methyl-5oxo-2-imidazolin-2-yl)-m-toluate; tolerances for residues.
Tolerances are established for the combined residues of the herbicide methyl 2-(4-isopropyl-4-methyl-5-oxo-2imidazolin-2-yl)-p-toluate and methyl 6-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-m-toluate in or on the following raw
agricultural commodities:
Commodity

Parts per million

Barley, grain
Barley, straw
Sunflower, seed
Wheat, grain
Wheat, straw

0.10
2.00
0.10
0.10
2.00

[53 FR 24069, June 27, 1988]

Back to Top
§180.438 Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for the combined residues of the pyrethroid lambda-cyhalothrin, 1:1
mixture of (S)-α-cyano-3-phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)
-2,2-dimethylcyclopropanecarboxylate and (R)-α-cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1enyl)-2,2-dimethylcyclopropanecarboxylate and its epimer expressed as epimer of lambda-cyhalothrin, a 1:1 mixture of (S)
-α-cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and
(R)-α-cyano-3-phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate, on
plants and livestocks, as indicated in the following table.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple, wet pomace
Avocado, imported
Barley, bran
Barley, grain
Barley, hay
Barley, straw
Brassica, head and stem, subgroup 5A
Buckwheat, grain
Canola, refined oil
Canola, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, flour
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, grain, flour
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, stover
Corn, sweet, kernel plus cob with husks removed
Cotton, undelinted seed
Egg
Fruit, pome, group 11
Fruit, stone, group 12
Garlic
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grass, forage, fodder and hay, group 17
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

5.0
6.0
1.5
2.50
0.20
0.2
0.05
2.0
2.0
0.4
0.05
2.0
1.0
3.0
0.2
0.2
0.15
6.0
0.05
1.0
0.05
0.05
1.0
6.0
1.0
0.05
0.05
0.01
0.30
0.50
0.1
3.0
0.2
0.2
2.0
7.0
0.2
0.01
0.02
10.0
3.0

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Horse, meat
Horse, meat byproducts
Lettuce, head
Lettuce, leaf
Milk, fat (reflecting 0.4 ppm in whole milk)
Nut, tree, group 14
Oat, grain
Oat, forage
Oat, hay
Oat, straw
Onion, bulb
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut
Peanut, hay
Pistachio
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, grain
Rice, hulls
Rice, straw
Rice, wild, grain
Rye, bran
Rye, grain
Rye, forage
Rye, straw
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean
Sorghum, grain, grain
Sorghum, grain, forage
Sorghum, grain, stover
Sugarcane, cane
Sunflower, forage
Sunflower, seed, hulls
Sunflower, refined oil
Sunflower, seed
Tomato
Tomato, dry pomace
Tomato, wet pomace
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, legume, edible podded, subgroup 6A
Vegetable, tuberous and corm, subgroup 1C
Wheat, grain
Wheat, forage
Wheat, hay
Wheat, straw
Wheat, bran

0.2
0.2
2.0
2.0
10.0
0.05
0.05
2.0
2.0
2.0
0.1
0.10
0.01
0.05
3.0
0.05
0.03
0.01
0.01
1.0
5.0
1.8
1.0
0.2
0.05
2.0
2.0
3.0
0.2
0.2
0.01
0.2
0.30
0.50
0.05
0.2
0.50
0.30
0.2
0.1
6.0
6.0
0.05
0.20
0.20
0.02
0.05
2.0
2.0
2.0
0.2

(2) Tolerances1 are established for the combined residues of the pyrethroid [gamma-cyhalothrin (the isolated active
isomer of lambda-cyhalothrin) (S)-′-cyano-3-phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)
-2,2-dimethylcyclopropanecarboxylate)) and its epimer (R)-′-cyano-3-phenoxybenzyl (Z)-(1R,3R)
-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate in/on the following commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple, pomace, wet
Avocado, imported
Brassica, head and stem, subgroup 5A
Canola, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, flour
Corn, field, forage
Corn, field, grain
Corn, field, stover

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

5
6
1.5
2.50
0.20
0.4
0.15
3
0.2
0.2
0.15
6.0
0.05
1.0

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Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Egg
Fruit, pome, group 11
Fruit, stone, group 12
Garlic
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Lettuce, head
Lettuce, leaf
Milk, fat (reflecting 0.20 ppm in whole milk)
Nut, tree, group 14
Okra
Onion, bulb
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut
Peanut, hay
Pistachio
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, grain
Rice, hulls
Rice, straw
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean
Sugarcane
Sunflower, forage
Sunflower, refined oil
Sunflower, seed
Sunflower, seed, hulls
Tomato
Tomato, dry pomace
Tomato, wet pomace
Vegetables, fruiting, group 8
Vegetable, legume, edible podded, subgroup 6A
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
1.0
6.0
0.05
1.0
0.05
0.01
0.30
0.50
0.10
3.0
0.2
0.2
2.0
3.0
0.2
0.2
3.0
0.2
0.2
2.0
2.0
5.0
0.05
0.20
0.1
0.10
0.01
0.05
3.0
0.05
0.03
0.01
0.01
1.0
5.0
1.8
3.0
0.2
0.2
0.30
0.20
0.50
0.01
0.05
0.20
0.30
0.20
0.50
0.10
6.0
6.0
0.20
0.20
2.0
2.0
0.05
2.0
2.0

1
The analytical enforcement methods for lambda-cyhalothrin are applicable for determination of gamma-cyhalothrin
residues in plant and animal commodities.

(3) A tolerance of 0.01 part per million is established for residues of the insecticide lamba-cyhalothrin and an isomer
gamma-cyhalothrin in or on all food commodities (other than those already covered by a higher tolerance as a result of
use on growing crops) in food-handling establishments where food products are held, processed, or prepared.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[71 FR 74817, Dec. 13, 2006, as amended at 72 FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, 2008; 76 FR 34885, June 15, 2011]

Back to Top
§180.439 Thifensulfuron methyl; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of thifensulfuron methyl, including its metabolites and
degradates, in or on the commodities listed in the following table [below]. Compliance with the tolerance levels specified in
the following table [below] is to be determined by measuring only thifensulfuron methyl (methyl 3-[[[[(4-methoxy-6methyl-1,3,5-triazin-2-yl)amino]carbonyl]amino] sulfonyl]-2-thiophenecarboxylate).
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Canola, seed
Chicory, roots
Chicory, tops
Corn, field, forage
Corn, field, grain
Corn, field, stover
Cotton, gin byproducts
Cotton, undelinted seed
Flax, seed
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Rice, grain
Rice, straw
Sorghum, grain, forage.
Sorghum, grain, grain
Sorghum, grain, stover
Soybean
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.8
0.10
0.02
0.01
0.01
0.10
0.05
0.10
0.02
0.02
0.02
0.2
0.05
0.05
0.10
0.05
0.05
0.05
0.05
0.05
0.10
2.5
0.05
0.7
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances are established for residues of thifensulfuron methyl, including
its metabolites and degradates, in or on the commodities listed in the following table [below]. Compliance with the
tolerance levels specified in the following table [below] is to be determined by measuring only thifensulfuron methyl
(methyl 3-[[[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)amino]carbonyl]amino] sulfonyl]-2-thiophenecarboxylate).
Commodity

Parts per million

Safflower, seed

0.05

(d) Indirect or inadvertent residues. [Reserved]
[69 FR 55982, Sept. 17, 2004, as amended at 69 FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, 2007; 73 FR 47075, Aug. 13,
2008; 75 FR 19277, Apr. 14, 2010; 77 FR 52240, Aug. 29, 2012]

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§180.440 Tefluthrin; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide tefluthrin (2,3,5,6 tetrafluroro-4methylphenyl)methyl-(1 alpha, 3 alpha)-(Z)-(±)-3(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-diemthylcyclopropanecarboxylate)
and its metabolite (Z)-3-(2-chloro-3,3,3-trifluroro-1-propenyl)-2,2-dimethylcyclopropanecarboxylic acid in or on the
following commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.06
0.06
0.06
0.06
0.06
0.06

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Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.06
0.06

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 62961, Nov. 26, 1997, as amended at 74 FR 46375, Sept. 9, 2009]

Back to Top
§180.441 Quizalofop ethyl; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the herbicide quizalofop ethyl, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only those quizalofop ethyl residues convertible to 2-methoxy-6-chloroquinoxaline,
expressed as the stoichiometric equivalent of quizalofop ethyl, in or on the commodity.
Parts per
million

Commodity
Barley, grain
Barley, hay
Barley, straw
Bean, dry, seed
Bean, succulent
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Cotton, undelinted seed
Cowpea, forage
Cowpea, hay
Crambe, meal
Flax, seed
Gold of pleasure, meal
Lentil, seed
Pea, dry
Pea, field, hay
Pea, field, vines
Pea, succulent
Peppermint, tops
Rapeseed, meal
Rapeseed subgroup 20A, except flax, seed
Sorghum, grain, aspirated grain fractions
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, flour
Soybean, hulls
Soybean, meal
Soybean, seed
Soybean, soapstock
Spearmint, tops
Sunflower, seed
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.05
0.05
0.4
0.25
0.2
0.1
0.5
0.1
3.0
3.0
2.0
0.05
2.0
0.05
0.25
3.0
3.0
0.3
2.0
2.0
1.5
1.0
0.20
0.20
0.30
0.5
0.02
0.5
0.05
1.0
2.0
1.9
0.05
0.05
0.05
0.05

(2) Tolerances are established for residues of the herbicide quizalofop ethyl, including its metabolites and degradates,
in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only those quizalofop ethyl residues convertible to quizalofop (2-[4-(6-chloroquinoxalin-2-yl-oxy)
phenoxy]propanoic acid), expressed as quizalofop, in or on the commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.05
0.02
0.05
0.02

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Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Milk, fat
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.05
0.02
0.05
0.05
0.02
0.05
0.05
0.02
0.05
0.01
0.25
0.05
0.02
0.05
0.05
0.02
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the
herbicide quizalofop ethyl, including its metabolites and degradates, in or on the commodities in the following table.
Compliance with the tolerance levels specified in the following table is to be determined by measuring only those
quizalofop ethyl residues convertible to 2-methoxy-6-chloroquinoxaline, expressed as the stoichiometric equivalent of
quizalofop ethyl, in or on the commodity.
Commodity

Parts per million

Pineapple

0.1

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 32759, June 16, 1998, as amended at 70 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, 2006; 76 FR 56045, Sept. 15,
2010; 77 FR 23630, Apr. 20, 2012]

Back to Top
§180.442 Bifenthrin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide bifenthrin, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)
-2,2-dimethylcyclopropanecarboxylate.
Commodity

Parts per million

Almond, hulls
Artichoke, globe
Banana1
Beet, garden, roots
Beet, garden, tops
Brassica, head and stem, subgroup 5A, except cabbage
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Cabbage
Caneberry subgroup 13A
Cattle, fat
Cattle, meat byproducts
Cattle, meat
Coriander, dried leaves
Coriander, leaves
Coriander, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husk removed
Corn, sweet, stover
Cotton, undelinted seed
Eggplant
Egg
Fruit, citrus, group 10

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

2.0
1.0
0.1
0.45
15
0.6
3.5
1.8
4.0
1.0
1.0
0.10
0.5
25
6.0
5.0
3.0
0.05
5.0
0.05
5.0
3.0
0.05
5.0
0.5
0.05
0.05
0.05

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Goat, fat
Goat, meat byproducts
Goat, meat
Grain, aspirated fractions
Grape
Groundcherry
Herb subgroup 19A
Hog, fat
Hog, meat byproducts
Hog, meat
Hop, dried cones
Horse, fat
Horse, meat byproducts
Horse, meat
Leafy petioles subgroup 4B
Lettuce, head
Mayhaw
Milk, fat (reflecting 0.1 ppm in whole milk)
Nut, tree, group 14
Okra
Pea and bean, dried shelled, expect soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut
Pear
Pepino
Pepper, bell
Pepper, nonbell
Pistachio
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Radish, tops
Rapeseed, seed
Sheep, fat
Sheep, meat byproducts
Sheep, meat
Soybean, hulls
Soybean, refined oil
Soybean, seed
Spinach
Strawberry

1.0
0.10
0.5
70
0.2
0.5
0.05
1.0
0.10
0.5
10.0
1.0
0.10
0.5
3.0
3.0
1.4
1.0
0.05
0.50
0.15
0.05
0.05
0.5
0.5
0.5
0.5
0.05
0.05
0.05
0.05
4.5
0.05
1.0
0.1
0.5
0.50
0.30
0.2
0.2
3.0
30

Tea, dried1
Tomato
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root, subgroup 1B except sugar beet and garden beet
Vegetable, tuberous and corm, subgroup 1C

0.15
3.5
0.4
0.6
0.10
0.05

1

There are no U.S. registrations.

(2) A tolerance of 0.05 ppm is established for residues of the insecticide bifenthrin, (2-methyl[1,1′-biphenyl]-3-yl)
methyl-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropane-carboxylate, as follows:
(i) In or on all food/feed items (other than those covered by a higher tolerance as a result of use on growing crops) in
food/feed handling establishments.
(ii) The insecticide may be present as a residue from application of bifenthrin in food handling establishments,
including food service, manufacturing and processing establishments, such as restaurants, cafeterias, supermarkets,
bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries, feed handling establishments including
feed manufacturing and processing establishments, in accordance with the following prescribed conditions:
(A) Application shall be limited to general surface and spot and/or crack and crevice treatment in food/feed handling
establishments where food/feed and food/feed products are held, processed, prepared and served. General surface
application may be used only when the facility is not in operation provided exposed food/feed has been covered or
removed from the area being treated. Spot and/or crack and crevice application may be used while the facility is in
operation provided exposed food/feed is covered or removed from the area being treated prior to application. Spray
concentration shall be limited to a maximum of 0.06 percent active ingredient. Contamination of food/feed or food/feed
contact surfaces shall be avoided.

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(B) To assure safe use of the insecticide, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency and shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide
bifenthrin, including its metabolites and degradates, in connection with use of the pesticide under a Section 18 emergency
exemption granted by EPA. Compliance with the tolerance levels specified below is to be determined by measuring only
bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)
-2,2-dimethylcyclopropanecarboxylate. These tolerances will expire and are revoked on the dates specified in the following
table:
Commodity

Parts per million

Apple
Nectarine
Peach

Expiration/revocation date
0.5
0.5
0.5

12/31/15
12/31/15
12/31/15

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the
insecticide bifenthrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance
with the tolerance levels specified below is to be determined by measuring only bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl)
methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate.
Commodity

Parts per million

Grass, forage
Grass, hay

4.0
15

(d) Indirect or inadvertent residues. [Reserved]
[62 FR 31002, June 6, 1997]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.442, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.443 Myclobutanil; tolerances for residues.
(a) General. Tolerances are established for combined residues of the fungicide myclobutanil alpha-butylalpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile and its alcohol metabolite (alpha-(3-hydroxybutyl)
-alpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile (free and bound), in or on the following food commodities:
Commodity

Parts per million

Almond
Almond, hulls
Apple
Apple, dry pomace
Apple, wet pomace
Artichoke, globe
Asparagus
Banana, postharvest
Bean, snap, succulent
Caneberry subgroup 13A
Canistel
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Cherry, sweet
Cherry, tart
Cilantro, leaves
Cotton, undelinted seed
Currant
Egg
Fruit, stone, except cherry
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Gooseberry
Grain, aspirated fractions
Grape
Grape, dried pomace
Grape, raisin
Grape, raisin, waste

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0.1
2.0
0.5
5.0
5.0
0.90
0.02
4.0
1.0
2.0
3.0
0.05
1.0
0.1
0.2
5.0
5.0
9.0
0.02
3.0
0.02
2.0
0.05
1.0
0.1
0.2
2.0
35
1.0
10.0
10.0
25.0

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Grape, wet pomace
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Hop, dried cones
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Leafy greens, subgroup 4A, except spinach
Mango
Mayhaw
Milk
Okra
Papaya
Peppermint, tops
Plum, prune, dried
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver
Soybean, forage
Soybean, hay
Soybean, refined oil
Soybean, seed
Spearmint, tops
Star apple
Strawberry
Tomato
Tomato, puree
Tomato, paste
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8, except tomato

10.0
0.05
1.0
0.1
0.2
10
0.05
1.0
0.1
0.2
9.0
3.0
0.70
0.2
4.0
3.0
3.0
8.0
0.02
0.02
0.02
3.0
3.0
3.0
0.05
1.0
0.1
0.2
3.5
15
0.40
0.25
3.0
3.0
0.50
0.30
0.50
1.0
0.20
4.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide myclobutanil alpha-butylalpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile in or on the following food commodities:
Commodity

Parts per million

Animal feed, nongrass, group 18
Grain, cereal, forage, fodder and straw, group 16
Grain, cereal, group 15
Vegetable, brassica, leafy, group 5
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root and tuber, group 1

0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03

[54 FR 6131, Feb. 8, 1989]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.443, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.444 Sulfur dioxide; tolerances for residues.
(a) General. A tolerance is established as follows for sulfite residues of the fungicide sulfur dioxide (determined as
(SO2)) in or on the following raw agricultural commodity(ies):

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Commodity

Parts per million

Grape, postharvest

10.0

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for
residues of sulfur dioxide, including its metabolites and degradates in or on the specified agricultural commodities,
resulting from use of the pesticide pursuant to FFIFRA section 18 emergency exemptions. Compliance with the tolerance
levels specified below is to be determined by measuring only sulfur dioxide (SO2). The tolerances expire on the date
specified in the table.
Parts per
million

Commodity
Fig

Expiration/revocation date
10

12/31/14

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[54 FR 20126, May 10, 1989, as amended at 76 FR 56648, Sept. 14, 2011]

Back to Top
§180.445 Bensulfuron methyl; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide bensulfuron methyl (methyl-2[[[[[(4,6-dimethoxypyrimidin-2-yl) amino] carbonyl] amino] sulfonyl] methyl] benzoate) in or on the following raw agricultural commodities:
Commodity

Parts per million

Crayfish
Rice, grain
Rice, straw

0.05
0.02
0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 9435, Feb. 25, 1998]

Back to Top
§180.446 Clofentezine; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide clofentezine, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only clofentezine, 3,6-bis(2-chlorophenyl)-1,2,4,5-tetrazine, in or on the
commodity.
Commodity

Parts per million

Almond, hulls
Almond
Apple
Apple, dry pomace
Apple, wet pomace
Apricot
Cherry
Grape
Nectarine
Peach
Pear
Persimmon
Walnut

5.0
0.5
0.5
3.0
3.0
1.0
1.0
1.0
1.0
1.0
0.5
0.05
0.02

(2) Tolerances are established for residues of the insecticide clofentezine, including its metabolites and degradates, in
or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to
be determined by measuring only the sum of clofentezine, 3,6-bis(2-chlorophenyl)-1,2,4,5-tetrazine, and its metabolite,
3-(2-chloro-4-hydroxyphenyl)-6-(2-chlorophenyl)-1,2,4,5-tetrazine, calculated as the stoichiometric equivalent of
clofentezine, in or on commodity.

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Parts per million

Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver

0.05
0.4
0.05
0.05
0.05
0.4
0.05
0.05
0.05
0.4
0.05
0.05
0.05
0.4
0.05
0.05
0.01
0.05
0.4
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[56 FR 15503, Apr. 17, 1991, as amended at 56 FR 22335, May 15, 1991; 59 FR 26947, May 25, 1994; 60 FR 12709, Mar. 8, 1995;
64 FR 19050, Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005; 74 FR 46375, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011]

Back to Top
§180.447 Imazethapyr; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, applied as its acid or ammonium salt, in or on
the following raw agricultural commodities:
Commodity

Parts per million
0.10

Canola, seed1
Soybean
Vegetable, legume, group 6

0.1
0.1

1 There are no U.S. registrations for canola as of March 21, 2003.
(2) Tolerances are established for the sum of the residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid; its metabolite CL 288511, 2-[4,5-dihydro-4methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine carboxylic acid; and its metabolite CL
182704, 5-[1-(beta-D-glucopyranosyloxy)ethyl]-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3pyridinecarboxylic acid, applied as its acid or ammonium salt, in or on the following commodities:
Commodity

Parts per million

Alfalfa, seed
Alfalfa, seed screenings
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Peanut
Rice, bran
Rice, grain
Rice, straw

0.15
0.15
3.0
5.5
0.1
1.2
0.3
0.4

(3) A tolerance is established for the sum of residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, and its metabolite CL 288511, 2-[4,5-dihydro4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine carboxylic acid, applied as its acid or
ammonium salt, in or on the following commodities:
Commodity

Parts per million

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Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Crayfish
Goat, meat byproducts
Hog, meat byproducts
Horse, meat byproducts
Sheep, meat byproducts

0.10
0.1
0.1
0.1
0.15
0.10
0.10
0.10
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l) of this chapter,
are established for the sum of residues of the herbicide imazethapyr, 2- [4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1Himidazol-2-yl]-5-ethyl- 3-pyridine carboxylic acid, as its ammonium salt, and its metabolite, 2- [4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1- hydroxyethyl)-3-pyridine carboxylic acid, both free and conjugated, applied
as its acid or ammonium salt, in or on the following raw agricultural commodities:
Commodity

Parts per million

Endive
Lettuce, head
Lettuce, leaf

0.1
0.1
0.1

(d) Indirect or inadvertent residues. [Reserved]
[67 FR 55331, Aug. 29, 2002, as amended at 68 FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, 2006; 76 FR 34885, June 15, 2011]

Back to Top
§180.448 Hexythiazox; tolerance for residues.
(a) General. Tolerances are established for residues of hexythiazox, including its metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only hexythiazox and its metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety,
calculated as the stoichiometric equivalent of hexythiazox.
Commodity
Almond, hulls
Apple, wet pomace
Berry, low growing, subgroup 13-07G
Caneberry subgroup 13-07A
Cattle, fat
Cattle, meat byproducts
Citrus, dried pulp
Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, stover
Date, dried fruit
Egg
Fruit, pome, group 11-10
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit
Fruit, stone, group 12
Goat, fat
Goat, meat byproducts
Grain, aspirated fractions
Hog, fat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat byproducts
Milk
Nut, tree, group 14
Pepper/eggplant subgroup 8-10B
Peppermint, tops
Pistachio
Plum, prune, dried
Poultry, fat
Poultry, meat byproducts
Sheep, fat
Sheep, meat byproducts
Spearmint, tops

Parts per million

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10
0.40
6
1
0.05
0.5
0.60
24
3.0
0.02
7.0
1.0
0.05
0.4
1
1.0
0.05
0.5
5
0.02
0.05
2.0
0.05
0.5
0.05
0.30
1.5
2.0
0.30
1.3
0.05
0.05
0.05
0.5
2.0

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Tomato

0.50

(b) Section 18 emergency exemptions. A time-limited tolerance specified in the following table is established for
residues of hexythiazox and its metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety,
calculated as the stoichiometric equivalent of hexythiazox, in or on the specified agricultural commodity, resulting from use
of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerance expires on the date specified in the
table.
Parts per
million
0.15

Commodity
Beet, sugar, root

Expiration
date
12/31/19

(c) Tolerances with regional registrations. Tolerances with regional registrations as defined by §180.1(l), are
established for residues of hexythiazox, including its metabolites and degradates, in or on the commodities in the table
below. Compliance with the tolerance levels specified below is to be determined by measuring only hexythiazox and its
metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety, calculated as the stoichiometric
equivalent of hexythiazox.
Commodity
Alfalfa, forage (EPA Regions 9-11 only)
Alfalfa, hay (EPA Regions 9-11 only)
Bean, dried, seed (EPA Regions 7-12 only)
Bean, succulent (EPA Regions 7-12 only)
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage (EPA Regions 7-12 only)
Corn, sweet, kernel plus cob with husks removed (EPA Regions 7-12 only)
Cotton, gin byproducts, CA and AZ only
Cotton, undelinted seed, CA and AZ only
Fruit, citrus group 10 (CA, AZ, TX only)
Potato
Sorghum, grain, forage (EPA Regions 6-8 only)
Sorghum, grain, grain (EPA Regions 6-8 only)
Sorghum, grain, stover (EPA Regions 6-8 only)
Timothy, forage (EPA Regions 9-11 only)
Timothy, hay (EPA Regions 9-11 only)
Wheat, forage (EPA Region 11 only)
Wheat, grain (EPA Region 11 only)
Wheat, hay (EPA Region 11 only)
Wheat, straw (EPA Region 11 only)

Parts per million
15
30
0.4
0.3
6.0
0.02
2.5
4.0
0.1
3.0
0.20
0.35
0.02
5
3
6
40
40
6.0
0.02
30
8.0

(d) Indirect or inadvertent residues. [Reserved]
[54 FR 17948, Apr. 26, 1989]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.448, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.449 Avermectin B1 and its delta-8,9-isomer; tolerances for residues.
(a) General. Tolerances are established for residues of abamectin, including its metabolites and degradates, in or on
the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only avermectin B1 a mixture of avermectins containing greater than or equal to 80%
avermectin B1 a (5-O-demethyl avermectin A1) and less than or equal to 20% avermectin B1b (5-O-demethyl-25-de
(1-methylpropyl)-25-(1-methylethyl) avermectin A1) and its delta-8,9-isomer in or on the following commodities:
Commodity
Almond, hulls
Apple
Apple, wet pomace
Avocado
Bean, dry, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Celeriac, roots
Celeriac, tops
Chive, dried leaves

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Parts per
million
0.10
0.020
0.10
0.020
0.01
0.03
0.02
0.06
0.05
0.05
0.02

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Chive, fresh leaves
Citrus, dried pulp
Citrus, oil
Citrus
Cotton, gin byproducts
Cotton, undelinted seed
Food products in food handling establishments (other than those already covered by higher tolerances as a result of use on growing crops, and
other than those already covered by tolerances on milk, meat, and meat byproducts)
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grape
Herb subgroup 19A, except chive
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Nut, tree, group 14
Onion, bulb, subgroup 3-07A
Pear
Peppermint, tops
Pistachio
Plum, prune, dried
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Spearmint, tops
Strawberry
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, tuberous and corm, subgroup 01C

0.01
0.10
0.10
0.02
1.0
0.02
0.01
0.09
0.01
0.02
0.02
0.02
0.030
0.01
0.02
0.02
0.20
0.01
0.02
0.02
0.005
0.01
0.01
0.02
0.010
0.01
0.025
0.02
0.02
0.01
0.02
0.02
0.010
0.05
0.005
0.020
0.10
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 44095, Aug. 19, 1997]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.449, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the fungicide β-(4-chlorophenoxy)
-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol (triadimenol) and its butanediol metabolite, 4-(4-chlorophenoxy)
-2,2-dimethyl-4-(1H-1,2,4-triazol-l-yl)-1,3-butanediol, calculated as triadimenol, in or on the following commodities:
Commodity
Banana1
Barley, grain
Barley, straw
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Oat, forage

Parts per million

Expiration/Revocation Date
0.2

None

0.05
0.2
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.02
2.5

None
None
None
None
None
None
None
None
None
None
None
None

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Oat, grain
Oat, straw
Rye, forage
Rye, grain
Rye, straw
Wheat, forage
Wheat, grain
Wheat, straw

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0.05
0.2
2.5
0.05
0.1
2.5
0.05
0.2

None
None
None
None
None
None
None
None

1

There are no U.S. registrations for banana (whole) as of September 22, 1993.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54962, Sept. 24, 2008, as amended at 74 FR 47457, Sept. 16, 2009; 76 FR 34885, June 15, 2011]

Back to Top
§180.451 Tribenuron methyl; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide tribenuron methyl and its metabolites and
degradates in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be
determined by measuring only tribenuron methyl, methyl-2-[[[[N-(4-methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino]
carbonyl] amino] sulfonyl] benzoate, in or on the following commodities:
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Canola, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Cotton, gin byproducts
Cotton, undelinted seed
Flax, seed
Grain, aspirated fractions
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Rice, grain
Rice, straw
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Sunflower, seed
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.4
0.10
0.02
0.15
0.01
1.1
0.02
0.02
0.02
1.5
0.05
0.05
0.05
0.10
0.05
0.05
0.05
0.05
0.05
0.07
0.35
0.04
0.01
0.05
0.3
0.05
0.5
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l) are established
for residues of the herbicide tribenuron methyl (methyl-2-[[[[N-(4-methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino]
carbonyl]amino]sulfonyl] benzoate) in or on the following raw agricultural commodities:
Commodity
Grass, forage, fodder and hay, group 17, except bermudagrass; forage
Grass, forage, fodder and hay, group 17, except bermudagrass; hay

Parts per million
0.10
0.10

(d) Indirect or inadvertent residues. [Reserved]

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[69 FR 56718, Sept. 22, 2004, as amended at 72 FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, 2008; 74 FR 67128, Dec. 18,
2009; 76 FR 34885, June 15, 2011]

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§180.452 Primisulfuron-methyl; tolerances for residues.
(a) General. Tolerances are established for residues of primisulfuron-methyl (3-[4,6-bis-(difluoromethoxy)-pyrimidin-2yl]-1-(2-methoxycarbonylphenylsulfonyl) urea) in or on the following raw agricultural commodities.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.10
0.10
0.10
0.10
0.02
0.10
0.02
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.02
0.10
0.10
0.10
0.10
0.10
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[55 FR 21548, May 25, 1990, as amended at 62 FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, 1998; 67 FR 35049, May 17, 2002;
74 FR 46375, Sept. 9, 2009; 74 FR 46699, Sept. 11, 2009; 77 FR 59128, Sept. 26, 2012]

Back to Top
§180.454 Nicosulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide nicosulfuron, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only nicosulfuron, 2-[[[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]amino]
sulfonyl]-N,N-dimethyl-3-pyridinecarboxamide.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Goat, fat
Goat, meat
Goat, meat byproducts
Grass, forage
Grass, hay

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.01
0.01
0.05
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.01
0.01
0.05
9.0
25.0

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Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover

0.01
0.01
0.05
0.01
0.01
0.01
0.05
0.3
0.8
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[75 FR 17578, Apr. 7, 2010, as amended at 80 FR 68265, Nov. 4, 2015]

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§180.455 Procymidone; tolerances for residues.
A tolerance is established for the residues of the fungicide procymidone, N-(3,5-dichlorophenyl)
-1,2-dimethylcyclopropane-1,2 dicarboximide, in or on the following raw agricultural commodity:
Commodity

Parts per million

Grape, wine

5.0

[59 FR 42514, Aug. 18, 1994]

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§180.457 Bitertanol; tolerances for residues.
(a) General. A tolerance is established for the residues of the fungicide bitertanol, β-([1,1′-biphenyl]-4-yloxy)
-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, in or on the following raw agricultural commodity:
Commodity

Parts per million
0.5

Banana1
1

There are no U.S. registrations as of April 1, 1992.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[74 FR 47457, Sept. 16, 2009]

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§180.458 Clethodim; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide clethodim, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of clethodim, 2-[(1E)-1-[[[(2E)-3-chloro-2-propenyl]oxy]imino]
propyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one, and its metabolites containing the 5-(2-ethylthiopropyl)
cyclohexene-3-one and 5-(2-ethylthiopropyl)-5-hydroxycyclohexene-3-one moieties and their sulphoxides and sulphones,
calculated as the stoichiometric equivalent of clethodim, in or on the commodity.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Artichoke, globe
Asparagus
Bean, dry, seed
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Brassica, head and stem, subgroup 5A

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

6.0
10
1.2
1.7
2.5
1.0
0.20
1.0
3.0

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Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canola, meal
Canola, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Clover, forage
Clover, hay
Corn, field, forage
Corn, field, grain
Corn, field, stover
Cotton, meal
Cotton, undelinted seed
Cranberry
Egg
Flax, meal
Flax, seed
Goat, fat
Goat, meat
Goat, meat byproducts
Herb subgroup 19A
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Leaf petioles subgroup 4B
Leafy greens subgroup 4A
Melon subgroup 9A
Milk
Mustard, seed
Onion, bulb
Onion, green
Peach
Peanut
Peanut, hay
Peanut, meal
Peppermint, tops
Potato
Potato, granules/flakes
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Radish, tops
Safflower, meal
Safflower, seed
Sesame, seed
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean
Spearmint, tops
Squash/cucumber subgroup 9B
Strawberry
Sunflower, meal
Sunflower, seed
Turnip, greens
Vegetable, fruiting group 8
Vegetable, legume, group 6, except soybean
Vegetable, root, except sugar beet, subgroup 1B
Vegetable, tuberous and corm, subgroup 1C

3.0
0.20
0.30
1.0
0.50
0.2
0.2
0.2
10.0
20.0
0.2
0.2
0.2
2.0
1.0
0.50
0.2
1.0
0.6
0.2
0.2
0.2
12.0
0.2
0.2
0.2
0.5
0.2
0.2
0.2
0.60
2.0
2.0
0.05
0.50
0.20
2.0
0.20
3.0
3.0
5.0
5.0
0.5
2.0
0.2
0.2
0.2
0.70
10.0
5.0
0.35
0.2
0.2
0.2
10.0
5.0
0.50
3.0
10.0
5.0
3.0
1.0
3.5
1.0
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 23496, Apr. 27, 2011, as amended at 77 FR 59128, Sept. 26, 2012]

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§180.459 Triasulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide triasulfuron [3-(6-methoxy-4-methyl-1,3,5-triazin2-yl)-1-(2-(2-chloroethoxy)phenylsulfonyl)urea] in or on the following raw agricultural commodities:
Commodity

Parts per million

Barley, grain
Barley, straw
Cattle, fat
Cattle, kidney
Cattle, meat byproducts, except kidney
Cattle, meat
Goat, fat
Goat, kidney
Goat, meat byproducts, except kidney
Goat, meat
Grass, forage
Grass, hay
Hog, fat
Hog, kidney
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, kidney
Horse, meat byproducts, except kidney
Horse, meat
Milk
Sheep, fat
Sheep, kidney
Sheep, meat byproducts, except kidney
Sheep, meat
Wheat, forage
Wheat, grain
Wheat, straw

0.02
2.0
0.1
0.5
0.1
0.1
0.1
0.5
0.1
0.1
7.0
2.0
0.1
0.5
0.1
0.1
0.1
0.5
0.1
0.1
0.02
0.1
0.5
0.1
0.1
5.0
0.02
2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[60 FR 36731, July 18, 1995, as amended at 63 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, 1998]

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§180.460 Benoxacor; tolerances for residues.
(a) General. Tolerances are established for residues of the inert ingredient (safener) benoxacor (4-(dichloroacetyl)
-3,4-dihydro-3-methyl-2H-1, 4-benzoxazine) at 0.01 parts per million (ppm) when used in pesticide formulations containing
metolachlor or S-metolachlor in or on raw agricultural commodities for which tolerances have been established for
metolachlor or S-metolachlor.
(b) Section 18 energency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 7305, Feb. 13, 1998, as amended at 70 FR 21631, Apr. 27, 2005]

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§180.461 Cadusafos; tolerances for residues.
A tolerance is established for the residues of the nematicide/insecticide cadusafos, O-ethyl S,S-di-sec-butyl
phosphorodithioate, in or on the following raw agricultural commodity:
Commodity

Parts per million

Banana

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.01

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There are no U.S. registrations as of May 10, 1994, for the nematicide/insecticid cadusafos.
[59 FR 39467, Aug. 3, 1994]

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§180.462 Pyridate; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide pyridate, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only the sum of pyridate, O-(6-chloro-3-phenyl-4-pyridazinyl)-S-octylcarbonothioate, and its metabolites, 6-chloro-3-phenyl-pyridazine-4-ol and conjugates of 6-chloro-3-phenyl-pyridazine-4-ol,
calculated as the stoichiometric equivalent of pyridate, in or on the commodity.
Commodity

Parts per million

Brassica, head and stem, subgroup 5A
Cabbage
Chickpea, seed
Collards
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Peanut
Peppermint, tops
Spearmint, tops

0.03
0.03
0.1
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.20
0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[57 FR 54303, Nov. 18, 1992, as amended at 62 FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, 1998; 64 FR 46298, Aug. 25, 1999;
65 FR 25652, May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR 35665, June 29, 2007; 74 FR 46376, Sept. 9, 2009; 76 FR 23496,
Apr. 27, 2011]

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§180.463 Quinclorac; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a)(1) General. Tolerances are established for residues of the herbicide quinclorac, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only quinclorac, 3,7-dichloro-8-quinolinecarboxylic acid, in or on the
commodity.
Commodity
Barley, grain
Berry, low growing, except strawberry, subgroup 13-07H
Cattle, fat
Cattle, meat byproducts
Cattle, meat
Egg
Goat, fat
Goat, meat byproducts
Goat, meat
Grain, aspirated fractions
Grass, forage
Grass, hay
Hog, fat
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Milk
Poultry, fat
Poultry, meat byproducts
Poultry, meat

Parts per million

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2.0
1.5
0.7
1.5
0.05
0.05
0.7
1.5
0.05
1200
150
130
0.7
1.5
0.05
0.7
1.5
0.05
0.05
0.05
0.1
0.05

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Rhubarb
Rice, bran
Rice, grain
Rice, straw
Sheep, fat
Sheep, meat byproducts
Sheep, meat
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, hay
Wheat, straw

0.5
15.0
5.0
12.0
0.7
1.5
0.05
3.0
6.0
1.0
1.0
0.75
0.5
0.5
0.1

(2) Tolerances are established for residues of the herbicide quinclorac, including its metabolites and degradates, in or
on the commodity in the following table. Compliance with the tolerance levels specified in this paragraph is to be
determined by measuring only quinclorac, 3,7-dichloro-8-quinolinecarboxylic acid, and its methyl ester,
methyl-3,7-dichloro-8-quinolinecarboxylate, calculated as the stoichiometric equivalent of quinclorac, in or on the
commodity.
Commodity

Parts per million
1.5

Rapeseed, subgroup 20A1
1

There are no U.S. Registrations.

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide
quinclorac, including its metabolites and degradates, in or on the commodity in the table in this paragraph. Compliance
with the tolerance level specified in this paragraph is to be determined by measuring only quinclorac, 3,7-dichloro-8quinolinecarboxylic acid, in or on the commodity. The tolerance expires and is revoked on the date specified in the table in
this paragraph.
Commodity

Parts per million

Cranberry

Expiration/revocation date
15.0

12/31/12

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[57 FR 47996, Oct. 21, 1992, as amended at 64 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. 26, 1999; 65 FR 33701, May 24,
2000; 67 FR 35049, May 17, 2002; 72 FR 55073, Sept. 28, 2007; 74 FR 51490, Oct. 7, 2009; 74 FR 67090, Dec. 18, 2009; 76 FR
23497, Apr. 27, 2011; 77 FR 75566, Dec. 21, 2012; 78 FR 71528, Nov. 29, 2013]

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§180.464 Dimethenamid; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide dimethenamid, 1(R,S)-2-chloro-N-[(1-methyl-2methoxy)ethyl]-N-(2,4-dimethylthien-3-yl)-acetamide, applied as either the 90:10 or 50:50 S:R isomers, in or on the
following food commodities:
Commodity

Parts per million

Bean, dry, seed
Beet, garden, roots
Beet, garden, tops
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, forage
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cottonseed subgroup 20C

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
1.5
0.01

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Garlic
Grass, forage
Grass, hay
Grass, seed screenings
Grass, straw
Hop, dried cones
Horseradish
Leek
Onion, bulb
Onion, green
Onion, Welsh
Peanut
Peanut, hay
Radish, roots
Radish, tops
Rutabaga, roots
Rutabaga, tops
Shallot, bulb
Shallot, fresh leaves
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Turnip, greens
Turnip, roots
Turnip, tops
Vegetable, tuberous and corm, subgroup 1C

0.01
0.15
2.5
0.01
0.01
0.05
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.1
0.01
0.01
0.01
0.01
0.01
0.01
0.1
0.01
0.1
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of
dimethenamid, 1 (R,S)-2-chloro-N-[(1-methyl-2-methoxy) ethyl]-N-(2,4-dimethylthien-3-yl)-acetamide) in or on the following
raw agricultural commodities:
Commodity

Parts per million

Pumpkin
Squash, winter

0.01
0.01

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 51551, Aug. 24, 2000, as amended at 67 FR 46884, July 17, 2002; 69 FR 29459, May 24, 2004; 69 FR 57207, Sept. 24,
2004; 70 FR 24712, May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR 49354, Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; 72 FR
73630, Dec. 28, 2007; 80 FR 9215, Feb. 20, 2015]

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§180.465 4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.
(a) General. Tolerances are established for the residues of 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane, (CAS No.
71526-07-3) when used as an inert ingredient (safener) in or on the following raw agricultural commodities:
Commodity1
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover

Parts per million
0.005
0.005
0.005
0.005
0.005

1
There are no U.S. registered products containing 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17,
2002.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 4392, Jan. 29, 2003]

Back to Top

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§180.466 Fenpropathrin; tolerances for residues.
(a) General. Tolerances are established for residues of fenpropathrin, including its metabolites and degradates, in or
on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by
measuring only fenpropathrin (alpha-cyano-3-phenoxy-benzyl 2,2,3,3 tetramethylcyclopropanecarboxylate).
Commodity
Acerola
Almond, hulls
Atemoya
Avocado
Barley, grain
Barley, hay
Barley, straw
Berry, low growing, subgroup 13-07G
Biriba
Brassica, head and stem, subgroup 5A
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Cattle, fat
Cattle, meat byproducts
Cattle, meat
Cherimoya
Cherry, sweet
Cherry, tart
Citrus, dried pulp
Citrus, oil
Cotton, refined oil
Cotton, undelinted seed
Custard apple
Egg
Feijoa
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, crop group 12, except cherry
Goat, fat
Goat, meat byproducts
Goat, meat
Grape, raisin
Guava
Hog, fat
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Ilama
Jaboticaba
Longan
Lychee
Mango
Melon subgroup 9A
Milk, fat (reflecting 0.08 ppm in whole milk)
Nut, tree, crop group 14
Olive
Papaya
Passionfruit
Pea, succulent
Peanut, hay
Peanut
Pistachio
Poultry, fat
Poultry, meat byproducts
Poultry, meat
Pulasan
Rambutan
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat

Parts per million

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

3.0
4.5
1.5
1.0
0.04
3.0
2.0
2.0
1.5
3.0
3.0
12
1.0
1.0
0.1
0.1
1.5
5.0
5.0
4.0
75
3.0
1.0
1.5
0.05
3.0
2.0
5.0
5.0
1.4
1.0
0.1
0.1
10.0
3.0
1.0
0.1
0.1
1.0
0.1
0.1
1.5
3.0
7.0
7.0
1.0
0.5
2.0
0.10
5.0
1.0
3.0
0.02
20.0
0.01
0.10
0.05
0.05
0.05
7.0
7.0
1.0
1.0
1.0
1.0

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Sheep, meat byproducts
Sheep, meat
Soursop
Spanish lime
Squash/Cucumber subgroup 9B
Star apple
Starfruit
Sugar apple

0.1
0.1
1.5
7.0
0.5
1.0
3.0
1.5
2.0

Tea, dried1
Vegetable, fruiting, group 8-10
Wax jambu

1.0
3.0

1

There are no U.S. registrations as of November 28, 2012, for the use of fenpropathrin on tea, dried.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63034, Nov. 26, 1997, as amended at 63 FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, 1999; 65 FR 11242, Mar. 2, 2000;
65 FR 24397, Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; 70 FR 38789,
July 6, 2005; 70 FR 55747, Sept. 23, 2005; 74 FR 12606, Mar. 25, 2009; 77 FR 70908, Nov. 28, 2012; 78 FR 69569, Nov. 20, 2013]

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§180.467 Carbon disulfide; tolerances for residues.
Tolerances are established for the nematicide, insecticide, and fungicide carbon disulfide, from the application of
sodium tetrathiocarbonate, in or on the following raw agricultural commodities:
Commodity

Parts per million

Almond
Almond, hulls
Grape
Grapefruit
Lemon
Orange, sweet
Peach
Plum, prune, fresh

0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

[58 FR 33771, June 21, 1993, as amended at 62 FR 26949, May 16, 1997]

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§180.468 Flumetsulam; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide flumetsulam, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only flumetsulam, N-(2,6-difluorophenyl)-5-methyl-(1,2,4)-triazolo-(1,5a)
-pyrimidine-2-sulfonamide, in or on the commodity.
Commodity

Parts per million

Bean, dry, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Soybean, seed

0.05
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 23497, Apr. 27, 2011]

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§180.469 Dichlormid; tolerances for residues.

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(a) General. Tolerances are established for residues of dichlormid, including its metabolites and degradates, when
used as an inert ingredient (herbicide safener) in pesticide formulations, in or on the commodities in the following table.
Compliance with the tolerances is to be determined by measuring only dichlormid (2,2-dichloro-N,N-di-2propenylacetamide).
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 16149, Mar. 27, 2000, as amended at 67 FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, 2004; 70 FR 76699, Dec. 28,
2005; 74 FR 37623, July 29, 2009; 76 FR 16310, Mar. 23, 2011]

Back to Top
§180.470 Acetochlor; tolerances for residues.
(a) General. Tolerances are established for residues of acetochlor, including its metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only acetochlor, 2-chloro-2'-methyl-6-ethyl-N-ethoxymethylacetanilide, and its metabolites containing the ethyl
methyl aniline (EMA) moiety and the hydroxyethyl methyl aniline (HEMA) moiety. Both parent and the named metabolites
shall be determined as ethyl methyl aniline (EMA) and hydroxyethyl methyl aniline (HEMA), and calculated as the
stoichiometric equivalents of acetochlor, in or on the following commodities:
Commodity

Parts per million

Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernels plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Peanut
Peanut, hay
Peanut, meal
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, meal
Soybean, seed

0.50
0.80
0.30
0.70
4.5
0.05
2.5
0.05
2.5
1.5
0.05
1.0
4.0
0.6
0.20
7.0
0.25
1.6
0.05
1.7
1.2
1.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of acetochlor,
including its metabolites and degradates, in or on the raw agricultural commodities in the table to this paragraph when
present therein as a result of application of acetochlor to the growing crops in the table to paragraph (a) of this section.
Compliance with the tolerance levels specified below is to be determined by measuring only acetochlor, 2-chloro-2'methyl-6-ethyl-N-ethoxymethylacetanilide, and its metabolites containing the ethyl methyl aniline (EMA) moiety and the
hydroxyethyl methyl aniline (HEMA) moiety. Both parent and the named metabolites shall be determined as ethyl methyl
aniline (EMA) and hydroxyethyl methyl aniline (HEMA), and calculated as the stoichiometric equivalents of acetochlor, in
or on the following commodities.

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Commodity
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, forage
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, hay
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, stover
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, and wheat, straw
Grain, cereal, group 15, except corn, grain sorghum, and wheat, grain
Pea and bean, dried shelled, except soybean, subgroup 6C
Potato
Soybean, forage
Soybean, hay
Sunflower, seed
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

Parts per million
1.3
3.5
0.5
2.0
0.1
0.3
0.05
0.05
0.05
0.7
1.0
0.05
0.5
0.02
2.0
0.1

[72 FR 27468, May 16, 2007, as amended at 74 FR 29969, June 24, 2009; 74 FR 47450, Sept. 16, 2009; 78 FR 13268, Feb. 27,
2013; 79 FR 3517, Jan. 22, 2014]

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§180.471 Furilazole; tolerances for residues.
(a) General. Tolerances are established for residues of furilazole; 3-dichloroacetyl-5-(2-furanyl)-2,
2-dimethyloxazolidine (CAS Reg. No. 121776-33-8) when used as an inert ingredient (safener) in pesticide formulations in
or on the following raw agricultural commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Sorghum, forage
Sorghum, grain
Sorghum, stover

0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 8867, Feb. 23, 2000, as amended at 67 FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, 2007]

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§180.472 Imidacloprid; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide imidacloprid, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl) methyl]-N-nitro-2-imidazolidinimine) and its
metabolites containing the 6-chloropyridinyl moiety, calculated as the stoichiometric equivalent of imidacloprid, in or on the
following commodities:
Commodity

Parts per million

Acerola
Almond, hulls
Apple
Apple, wet pomace
Artichoke, globe
Aspirated grain fractions
Atemoya
Avocado
Banana
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Biriba
Blueberry

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1.0
4.0
0.5
3.0
2.5
240
0.30
1.0
0.50
0.30
0.05
0.50
0.30
3.5

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Borage, seed
Caneberry, subgroup 13-A
Canistel
Canola, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherimoya
Citrus, dried pulp
Coffee, bean, green
Cotton, gin byproducts
Cotton, meal
Cotton, undelinted seed
Crambe, seed
Cranberry
Currant
Custard apple
Egg
Elderberry
Feijoa
Fish
Fish-shellfish, mollusc
Flax, seed
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Gooseberry
Grain, cereal, forage, fodder and straw, group 16, forage, except rice
Grain, cereal, forage, fodder and straw, group 16, hay, except rice
Grain, cereal, forage, fodder and straw, group 16, stover, except rice
Grain, cereal, forage, fodder and straw, group 16, straw, except rice
Grain, cereal, group 15, except rice
Grape
Grape, juice
Grape, raisin
Guava
Herbs subgroup 19A, dried herbs
Herbs subgroup 19-A, fresh herbs
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Huckleberry
Ilama
Jaboticaba
Juneberry
Kava, leaves
Kava, roots
Leaf petioles subgroup 4B
Leafy greens subgroup 4A
Lettuce, head
Lettuce, leaf
Lingonberry
Longan
Lychee
Mango
Milk
Mustard, black, seed
Mustard, field, seed
Mustard, Indian, seed
Mustard, rapeseed, seed
Mustard, seed
Nut, tree, group 14
Okra
Onion, dry bulbs, subgroup 3-07A
Onion, green, subgroup 3-07B
Papaya

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0.05
2.5
1.0
0.05
0.30
0.30
0.30
0.30
5.0
0.80
4.0
8.0
6.0
0.05
0.05
3.5
0.30
0.02
3.5
1.0
0.05
0.05
0.05
0.70
0.6
3.0
0.30
0.30
0.30
3.5
7.0
6.0
0.30
3.0
0.05
1.0
1.5
1.5
1.0
48
8.0
0.30
0.30
0.30
6.0
0.30
0.30
0.30
3.5
0.30
1.0
3.5
4.0
0.40
6.0
3.5
3.5
3.5
3.5
3.0
3.0
1.0
0.10
0.05
0.05
0.05
0.05
0.05
0.05
1.0
0.15
2.5
1.0

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Passionfruit
Peanut
Peanut, hay
Peanut, meal
Pecan
Persimmon
Pistachio
Pomegranate
Potato, chip
Potato, processed potato waste
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Pulasan
Rambutan
Rapeseed, seed
Raspberry, wild
Safflower, seed
Salal
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soursop
Soybean, forage
Soybean, hay
Soybean, meal
Soybean, seed
Spanish lime
Star apple
Starfruit
Strawberry
Sugar apple
Sunflower, seed
Tomato, paste
Tomato, puree
Vegetable, brassica leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6, except soybean
Vegetable, root and tuber, group 1, except sugar beet
Watercress
Watercress, upland
Wax jambu

1.0
0.45
35
0.75
0.05
3.0
0.05
0.90
0.40
0.90
0.05
0.05
0.05
3.0
3.0
0.05
2.5
0.05
3.5
1.0
1.0
1.0
0.30
0.30
0.30
0.30
8.0
35
4.0
3.5
3.0
1.0
1.0
0.50
0.30
0.05
6.0
3.0
3.5
0.5
1.0
4.0
4.0
0.40
3.5
3.5
1.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide
imidacloprid, including its metabolites and degradates in connection with use of the pesticide under a Section 18
emergency exemption granted by EPA. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl)methyl]-N-nitro-2-imidazolidinimine) and its metabolites
containing the 6-chloropyridinyl moiety, calculated as the stoichiometric equivalent of imidacloprid. These tolerances will
expire and are revoked on the dates specified in the following table:
Commodity
Sugarcane, cane
Sugarcane, molasses

Parts per million

Expiration/revocation date
6.0
50

12/31/15
12/31/15

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide
imidacloprid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the
tolerance levels specified below is to be determined by measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl)
methyl]-N-nitro-2-imidazolidinimine) and its metabolites containing the 6-chloropyridinyl moiety, calculated as the
stoichiometric equivalent of imidacloprid, in or on the following commodities, when present therein as a result of the
application of the pesticide to growing crops listed in this section and other non-food crops as follows:
Commodity

Parts per million

Rice, grain
Vegetable, foliage of legume, group 7
Vegetable, legume, group 6

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0.05
2.5
0.3

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[75 FR 22251, Apr. 28, 2010, as amended at 78 FR 33743, June 5, 2013]

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§180.473 Glufosinate ammonium; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide glufosinate ammonium, including its metabolites
and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring the sum of glufosinate ammonium, butanoic acid, 2-amino-4-(hydroxymethylphosphinyl)
monoammonium salt, and its metabolites, 2-(acetylamino)-4-(hydroxymethyl phosphinyl)butanoic acid, and
3-(hydroxymethylphosphinyl)propanoic acid, expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid
equivalents:
Commodity

Parts per million

Almond, hulls
Apple
Banana
Banana, pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops (leaves)
Bushberry subgroup 13B
Canola, meal
Canola, seed
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernels plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Egg
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, stone, group 12-12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain aspirated fractions
Grape
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Juneberry
Lingonberry
Milk
Nut, tree, group 14
Olive
Pistachio
Potato
Potato, chips
Potato granules/flakes
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, grain
Rice, hull
Rice, straw
Salal
Sheep, fat
Sheep, meat
Sheep, meat byproducts

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0.50
0.05
0.30
0.20
5.0
0.9
1.5
0.15
1.1
0.40
0.40
0.15
6.0
4.0
0.20
6.0
1.5
0.30
6.0
15
4.0
0.15
0.15
0.25
0.25
0.40
0.15
6.0
25
0.05
0.40
0.15
6.0
0.40
0.15
6.0
0.10
0.10
0.15
0.10
0.15
0.10
0.80
1.6
2.0
0.15
0.15
0.60
1.0
2.0
2.0
0.10
0.40
0.15
6.0

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Soybean
Soybean, hulls

2.0
5.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional restrictions. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of glufosinate
ammonium, including its metabolites and degradates, in or on the commodities in the table below, as a result of the
application of glufosinate ammonium to crops listed in paragraph (a) of this section. Compliance with the tolerance levels
specified below is to be determined by measuring the sum of glufosinate ammonium, butanoic acid, 2-amino4-(hydroxymethylphosphinyl) monoammonium salt, and its metabolite, 3-(hydroxymethylphosphinyl) propanoic acid,
expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid equivalents.
Commodity

Parts per million

Barley, hay
Barley, straw
Buckwheat, fodder
Buckwheat, forage
Oat, forage
Oat, hay
Oat, straw
Rye, forage
Rye, straw
Teosinte
Triticale
Wheat, forage
Wheat, hay
Wheat, straw

0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40

[68 FR 55849, Sept. 29, 2003, as amended at 71 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, 2007; 76 FR 23497, Apr. 27, 2011;
77 FR 59113, Sept. 26, 2012]

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§180.474 Tebuconazole; tolerances for residues.
(a) General. (1) Tolerances are established for residues of tebuconazole, alpha-[2-(4-chlorophenyl)ethyl]
-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, including its metabolites and degradates, in or on the commodities
in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only
tebuconazole [α-[2-(4-chlorophenyl) ethyl]-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol], in or on the commodity.
Commodity

Parts per million

Almond, hulls
Apple, wet pomace
Asparagus
Banana
Barley, grain
Barley, hay
Barley, straw
Bean, dry seed
Bean, succulent
Beet, garden, roots
Beet, garden, tops
Brassica, leafy greens, subgroup 5B
Cherry, sweet, pre- and post-harvest
Cherry, tart, pre- and post-harvest
Coffee, green bean1
Coffee, roasted bean1
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, pome, group 11
Fruit, stone, group 12, except cherry
Grain, aspirated fractions

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6.0
0.1
0.05
0.05
0.3
7.0
3.5
0.1
0.1
0.70
7.0
2.5
5.0
5.0
0.15
0.3
4.0
0.05
3.5
0.05
3.5
7.0
0.5
6.0
25.0
2.0
0.05
1.0
16.0

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Grape
Grass, forage
Grass, hay
Grass, seed screenings
Grass, straw
Hop, dried cones
Lychee
Mango, postharvest
Nut, tree, group 14
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Orange1

5.0
8.0
25.0
55.0
30.0
35.0
1.6
0.15
0.05
0.10
0.15
0.10
0.10
0.2
1.3
1.0

Orange, oil1
Peach
Peanut
Pistachio
Plum, pre- and post-harvest
Soybean, forage
Soybean, hay
Soybean, seed
Sunflower, seed
Sunflower, meal
Sunflower, refined oil
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, hay
Wheat, shorts
Wheat, straw

1.0
0.1
0.05
1.0
25
50
0.08
0.05
0.2
0.2
0.4
1.3
3.0
0.20
0.15
7.0
0.20
1.5

10

1

There are no U.S. registrations.

(2) Tolerances are established for residues of the fungicide tebuconazole, including its metabolites and degradates, in
or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only the sum of tebuconazole (alpha-[2-(4-chlorophenyl)ethyl]-alpha-(1,1-dimethylethyl)
-1H-1,2,4-triazole-1-ethanol) and its diol metabolite (1-(4-chlorophenyl)-4,4-dimethyl-3-(1H -1,2,4-triazole-1-yl-methyl)
-pentane-3,5-diol), calculated as the stoichiometric equivalent of tebuconzole, in or on the commodity.
Commodity

Parts per million

Cattle, meat byproducts
Goat, meat byproducts
Horse, meat byproducts
Milk
Sheep, meat byproducts

0.2
0.2
0.2
0.1
0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances are established for residues of the fungicide tebuconazole,
including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance
levels specified below is to be determined by measuring only tebuconazole, alpha-[2-(4-chlorophenyl)ethyl]
-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, in or on the commodity.
Commodity

Parts per million

Turnip, roots
Turnip, tops

0.5
7.0

(d) Indirect or inadvertent residues. [Reserved]
[59 FR 39464, Aug. 3, 1994]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.474, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.475 Difenoconazole; tolerances for residues.
(a) General. (1) Tolerances are established for residues of difenoconazole, including its metabolites and degradates,
in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined
by measuring only difenoconazole, 1-[2-[2-chloro-4-(4-chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]
-1H-1,2,4-triazole, in or on the following raw agricultural commodities:
Commodity

Parts per million

Almond, hulls
Apple, wet pomace
Artichoke, globe
Aspirated grain fractions
Banana1
Barley, grain
Barley, hay
Barley, straw
Beet, sugar
Beet, sugar, dried pulp
Berry, low growing, subgroup 13-07G, except cranberry
Brassica, head and stem, subgroup 5A
Brassica, leafy green, subgroup 5B
Bushberry subgroup 13-07B
Carrot
Citrus, dried pulp
Citrus, oil
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Dragonfruit1
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, stone, group 12-12
Ginseng
Grape
Grape, raisin
Mango1
Nut, tree, group 14-12
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Papaya1
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea, field, hay
Pea, field, vines
Potato, wet peel
Rapeseed subgroup 20A
Rye, forage
Rye, grain
Rye, straw
Soybean, hulls
Soybean, seed
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, tuberous and corm, subgroup 1C
Wax jambu1
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

7.0
25
1.5
95
0.2
0.1
0.05
0.05
0.3
1.9
2.5
1.9
35
4.0
0.50
2.0
25
0.01
0.01
0.01
0.05
0.05
1.5
0.60
5.0
2.5
1.0
4.0
6.0
0.07
0.03
0.15
0.01
0.05
0.05
0.20
6.0
0.30
0.20
40
10
7.3
0.10
0.15
0.01
0.05
0.20
0.15
35
0.70
0.60
4.0
1.5
0.1
0.1
0.05
0.1

1

There are no U.S. registrations.

(2) Tolerances are established for residues of difenoconazole, including its metabolites and degradates, in the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
the sum of difenoconazole, 1-[2-[2-chloro-4-(4-chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]-1H-1,2,4-triazole,

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and its metabolite, CGA-205375, 1-[2-chloro-4-(4-chloro-phenoxy)phenyl]-2-[1,2,4]triazol-1-yl-ethanol, calculated as the
stoichiometric equivalent of difenoconazole, in the following commodities:
Commodity

Parts per million

Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproduct (except liver)
Egg
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproduct (except liver)
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproduct (except liver)
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproduct (except liver)
Milk
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproduct (except liver)

0.10
0.40
0.05
0.10
0.02
0.10
0.40
0.05
0.10
0.10
0.40
0.05
0.10
0.10
0.40
0.05
0.10
0.02
0.10
0.40
0.05
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 36254, July 6, 1999]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.475, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.476 Triflumizole; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the fungicide triflumizole, including its metabolites and
degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to
be determined by measuring only the parent compound triflumizole, 1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2propoxyethyl)-1 H -imidazole, and its metabolites containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as
stoichiometric equivalent of the parent compound.
Commodity
Apple, dry pomace
Apple, wet pomace
Berry, low growing, subgroup 13-07G, except cranberry
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Canistel
Cherry, sweet
Cherry, tart
Cilantro, leaves
Fruit, pome, group 11-10
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Grape, dried pomace
Grape, raisin, waste
Grape, wet pomace
Hazelnut
Hop, dried cones
Leafy greens subgroup 4A, except spinach
Mango
Papaya
Pineapple
Sapodilla

Parts per million

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2.0
2.0
2.0
8.0
40
2.5
1.5
1.5
35
0.50
2.5
15.0
10.0
15.0
0.05
50
35
2.5
2.5
4.0
2.5

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Sapote, black
Sapote, mamey
Star apple
Swiss chard
Tomato
Turnip, greens
Vegetable, cucurbit, Group 9

2.5
2.5
2.5
18
1.5
40
0.5

(2) Tolerances are established for residues of the fungicide triflumizole, including its metabolites and degradates, in or
on the commodities of animal origin listed in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the parent compound triflumizole, 1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2propoxyethyl)-1 H -imidazole, the metabolite 4-chloro-2-hydroxy-6-trifluoromethylaniline sulfate, and other metabolites
containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as the parent compound.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.5
0.05
0.5
0.05
0.5
0.05
0.5
0.5
0.05
0.5
0.5
0.05
0.5
0.05
0.05
0.05
0.1
0.5
0.05
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33702, May 24, 2000, as amended at 67 FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, 2002; 70 FR 7047, Feb. 10, 2005;
70 FR 17915, Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR 49358, Aug. 23, 2006; 74 FR 26543, June 3, 2009; 74 FR 46376,
Sept. 9, 2009; 76 FR 34885, June 15, 2011; 79 FR 12408, Mar. 5, 2014]

Back to Top
§180.477 Flumiclorac pentyl; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide flumiclorac pentyl, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only flumiclorac pentyl, pentyl(2-chloro-4-fluoro5-(1,3,4,5,6,7-hexahydro-1,3-dioxo-2H-isoindol-2-yl)phenoxy)acetate, in or on the commodity.
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Cotton, gin byproducts
Cotton, undelinted seed
Soybean, hulls
Soybean, seed

0.01
0.01
0.01
3.0
0.2
0.02
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33702, May 24, 2000, as amended at 71 FR 11533, Mar. 8, 2006; 76 FR 23497, Apr. 27, 2011]

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§180.478 Rimsulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide rimsulfuron, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only rimsulfuron, N-[[(4,6-dimethoxy-2-pyrimidinyl)amino] carbonyl]
-3-(ethylsulfonyl)-2-pyridinesulfonamide.
Commodity

Parts per million

Almond, hulls
Bushberry, subgroup 13-07B
Caneberry, subgroup 13-07A
Chicory, roots
Chicory, tops
Corn, field, forage
Corn, field, grain
Corn, field, stover
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grain, aspirated fractions
Grape
Nut, tree, group 14
Pistachio
Potato
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Tomato

0.09
0.01
0.01
0.01
0.01
0.4
0.1
2.5
0.01
0.01
0.01
4.5
0.01
0.01
0.01
0.1
0.01
0.01
0.01
0.25
1.2
0.04
0.01
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 16696, Apr. 6, 1998, as amended at 72 FR 41913, Aug. 1, 2007; 74 FR 67137, Dec. 18, 2009; 77 FR 3625, Jan. 25, 2012; 77
FR 46306, Aug. 3, 2012; 80 FR 66805, Oct. 30, 2015]

Back to Top
§180.479 Halosulfuron-methyl; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl
5-[(4,6-dimethoxy-2-pyrimidiny)amino] carbonylaminosulfonyl]-3-chloro-1-methyl-1H-pyrazole-4-carboxylate, including its
metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified
in the following table is to be determined by measuring only those halosulfuron-methyl residues containing the
3-chlorosulfonamide (3-CSA) moiety, expressed as the stoichiometric equivalent of halosulfuron-methyl, in or on the
commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

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0.05
0.05
1.0
0.05
0.05
1.0
0.1
0.05
0.05
1.0
0.05
0.05
0.05
1.0

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(2) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy-2pyrimidiny)amino]carbonylaminosulfonyl]-3-chloro-1-methyl-1H-pyrazole-4-carboxylate, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only halosulfuron-methyl.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Artichoke
Asparagus
Bean, dry, seed
Bushberry, subgroup 13-07B
Caneberry subgroup 13-07A
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, pome, group 11-10
Grass, forage, fodder, and hay, group 17, forage
Grass, forage, fodder, and hay, group 17, hay
Melon subgroup 9A
Millet, proso, forage
Millet, proso, grain
Millet, proso, hay
Millet, proso, straw
Nut, tree, group 14
Okra
Pea and bean, succulent shelled, subgroup 6
Pea and bean, succulent shelled, subgroup 6B
Pistachio
Rhubarb
Rice, grain
Rice, straw
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Squash/Cucumber subgroup 9B
Sugarcane, cane
Vegetable, fruiting, group 8
Vegetable, tuberous and corm, subgroup 1C

1.0
2.0
0.2
0.05
0.8
0.05
0.05
0.05
0.2
0.05
0.8
0.05
0.8
0.2
0.05
0.8
0.05
0.05
0.05
20
0.5
0.1
10
0.01
0.01
0.01
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.2
0.05
0.05
0.1
0.05
0.5
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the
herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy-2-pyrimidiny)amino]carbonylaminosulfonyl]-3-chloro-1-methyl-1Hpyrazole-4-carboxylate, including its metabolites and degradates, in or on the commodities in the following table.
Compliance with the tolerance levels specified in the following table is to be determined by measuring only halosulfuronmethyl.
Commodity
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F

Parts per million
0.05

(d) Indirect or inadvertent residues. [Reserved]
[64 FR 25448, May 12, 1999, as amended at 65 FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, 2001; 66 FR 66786, Dec. 27,
2001; 67 FR 45649, July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007; 74 FR
48401, Sept. 23, 2009; 75 FR 46853, Aug. 4, 2010; 76 FR 34886, June 15, 2011; 77 FR 71561, Dec. 3, 2012; 78 FR 53051, Aug.
28, 2013; 80 FR 55773, Sept. 17, 2015]

Back to Top
§180.480 Fenbuconazole; tolerances for residues.

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(a) Tolerances are established for residues of the fungicide fenbuconazole, including its metabolites and degradates,
in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of fenbuconazole, alpha-[2-(4-chlorophenyl)-ethyl]-alpha-phenyl-3-(1H-1,2,4-triazole)-1propanenitrile, and its metabolites RH-9129, cis-5-(4-chlorophenyl)-dihydro-3-phenyl-3-(1H-1,2,4-triazole-1-ylmethyl)-2-3
H-furanone, and RH-9130, trans-5-(4-chlorophenyl)-dihydro-3-phenyl-3-(1H-1,2,4-triazole-1-ylmethyl)-2-3 H-furanone,
calculated as the stoichiometric equivalent of fenbuconazole, in or on the following agricultural commodities.
Commodity

Parts per million

Almond
Almond, hulls
Apple
Apple, wet pomace
Banana
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Bushberry subgroup 13B
Cattle, meat byproducts
Citrus, dried pulp
Citrus, oil
Cranberry
Fruit, citrus, group 10
Fruit, stone, group 12
Goat, meat byproducts
Grain, aspirated fractions

0.05
1.0
0.4
1.0
0.3
1.0
0.4
0.3
9.0
0.3
0.05
5.0
40.0
0.5
1.0
1.0
0.05
6.0
1.0

Grape1
Horse, meat byproducts
Peanut
Pecan
Pepper
Sheep, meat byproducts
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.1
0.05
1.0
0.05
4.0
0.1
8.0
8.0

1

There are no United States registrations for grape as of August 2006.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[60 FR 11032, Mar. 1, 1995]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.480, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.481 Prosulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide prosulfuron and its metabolites and degradates
in or on the commodities in the table below. Compliance with the tolerance levels specified in the table below is to be
determined by measuring only prosulfuron, 1-(4-methoxy-6-methyl-triazin-2-yl)-3-[2-(3,3,3-trifluoropropyl)-phenylsulfonyl]
-urea, in or on the commodity.
Commodity
Grain, cereal, forage, fodder, and straw, group 16, except rice, fodder
Grain, cereal, forage, fodder, and straw, group 16, except rice, forage
Grain, cereal, forage, fodder, and straw, group 16, except rice, hay
Grain, cereal, forage, fodder, and straw, group 16, except rice, straw
Grain, cereal, group 15, except rice

Parts per million
0.01
0.10
0.20
0.02
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[74 FR 67118, Dec. 18, 2009]

Back to Top
§180.482 Tebufenozide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide tebufenozide, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)
-2-(4-ethylbenzoyl)hydrazide, in or on the commodity.
Commodity

Parts per million

Almond, hulls
Apple
Apple, dry pomace
Apple, wet pomace
Berry group 13
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Canola, refined oil
Canola, seed
Citrus, oil
Cotton
Cotton, gin byproducts
Cranberry
Fruit, citrus, group 10
Fruit, pome
Grape

25
1.0
3.0
3.0
3.0
5.0
10.0
4.0
2.0
15.0
1.5
30
1.0
0.80
1.5
3.0
0.5

Kiwifruit1
Leaf petioles subgroup 4B
Leafy greens subgroup 4A
Nut, tree, group 14
Peppermint, tops
Pistachio
Spearmint, tops
Turnip, greens
Turnip, roots
Vegetable, fruiting, group 8
Vegetable, tuberous and corm, except potato, subgroup 1D
Walnut

2.0
10.0
0.1
10.0
0.1
10.0
9.0
0.3
1.0
0.015
0.1

1

There are no U.S. registrations on kiwifruit as of June 15, 1999.

(2) Tolerances are established for residues of the insecticide tebufenozide, including its metabolites and degradates,
in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is
to be determined by measuring only the sum of tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)
-2-(4-ethylbenzoyl)hydrazide, and its metabolites, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-((4-carboxymethyl)
benzoyl)hydrazide, 3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, stearic acid
conjugate of 3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, and
3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide, calculated as the
stoichiometric equivalent of tebufenozide, in or on the commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.1
0.08
0.08
0.1
0.08
0.08
0.1
0.08
0.08
0.1
0.08
0.08
0.04
0.1
0.08
0.08

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide
tebufenozide, including its metabolites and degradates, in or on the commodities in the table in this paragraph when
present therein as a result of the application of tebufenozide to growing crops listed in the table to paragraph (a)(1) of this
section. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of
tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, and its metabolite,
3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide, calculated as the stoichiometric
equivalent of tebufenozide, in or on the commodity.
Commodity

Parts per million

Animal feed, nongrass, group 18
Grain, cereal, forage, fodder and straw, group 16
Grass, forage, fodder and hay, group 17
Vegetable, foliage of legume, group 7

1.0
1.0
1.0
0.20

[60 FR 29347, May 31, 1995]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.482, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.484 Flutolanil; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of flutolanil, N-(3-(1-methylethoxy) phenyl)-2-(trifluoromethyl)
benzamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the
tolerance levels specified below is to be determined by measuring only flutolanil and its metabolites converted to
2-(trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the following commodities:
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat byproducts
Cattle, meat
Cotton, gin byproducts
Cotton, undelinted seed
Egg
Goat, fat
Goat, kidney
Goat, liver
Goat, meat byproducts
Goat, meat
Hog, fat
Hog, kidney
Hog, liver
Hog, meat byproducts
Hog, meat
Horse, fat
Horse, kidney
Horse, liver
Horse, meat byproducts
Horse, meat
Milk
Peanut
Peanut, hay
Peanut, meal
Potato
Potato, wet peel
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, bran
Rice, grain
Rice, hulls
Rice, straw
Sheep, fat
Sheep, kidney
Sheep, liver

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0.10
1.00
2.00
0.05
0.05
0.20
0.20
0.05
0.10
1.00
2.00
0.05
0.05
0.10
1.00
2.00
0.05
0.05
0.10
1.00
2.00
0.05
0.05
0.05
0.5
15.0
1.0
0.20
0.30
0.05
0.05
0.05
10.0
7.0
25.0
10.0
0.10
1.00
2.00

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Sheep, meat
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, seed
Turnip, greens
Vegetable, brassica, leafy, group 5

0.05
0.05
8.0
2.5
0.20
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of flutolanil,
N-(3-(1-methylethoxy)phenyl)-2-(trifluoromethyl)benzamide, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only flutolanil and its metabolites converted to 2-(trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the
following commodities.
Commodity

Parts per million

Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.20
2.5
0.05
1.2
0.20

[60 FR 42458, Aug. 16, 1995, as amended at 61 FR 33044, June 26, 1996; 63 FR 42256, 42257, Aug. 7, 1998; 66 FR 10825, Feb.
20, 2001; 71 FR 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; 73 FR 33017, June 11, 2008; 75 FR 17570, Apr. 7, 2010; 75
FR 80350, Dec. 22, 2010]

Back to Top
§180.485 Cyproconazole; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the free and conjugated forms of the fungicide
cyproconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the
proposed tolerance levels specified below is to be determined by measuring only cyproconazole (α-(4-chlorophenyl)
-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) in or on the following commodities:
Commodity

Parts per million

Aspirated grain fractions
Cattle, fat
Cattle, meat byproducts (except liver)
Coffee bean, green (Imported)1
Corn, field, forage
Corn, field, grain
Corn, field, stover
Goat, fat
Goat, meat byproducts (except liver)
Horse, fat
Horse, meat byproducts (except liver)
Peanut
Peanut, hay
Sheep, fat
Sheep, meat byproducts (except liver)
Soybean, forage
Soybean, hay
Soybean, oil
Soybean, seed
Wheat, forage
Wheat, grain
Wheat, grain, milled byproducts
Wheat, hay
Wheat, straw

2.5
0.01
0.01
0.1
0.60
0.01
1.2
0.01
0.01
0.01
0.01
0.01
6.0
0.01
0.01
1.0
3.0
0.10
0.05
0.80
0.05
0.10
1.3
0.90

1

There are no U.S. registrations as of February 15, 2008 for use on coffee bean.

(2) A tolerance is established for the combined residues of the free and conjugated forms of the fungicide
cyproconazole, including its metabolites and degradates, in or on the commodity in the table below. Compliance with the
tolerance level specified below is to be determined by measuring only the sum of cyproconazole (α-(4-chlorophenyl)
-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) and its metabolite δ-(4-chlorophenyl)-β,δ-dihydroxy-γ-methyl-

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1H-1,2,4-triazole-1-hexenoic acid, calculated as the stoichiometric equivalent of cyproconazole, in or on the following
commodity:
Commodity

Parts per million

Milk

0.02

(3) Tolerances are established for the combined residues of the free and conjugated forms of the fungicide
cyproconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the
tolerance level specified below is to be determined by measuring only the sum of cyproconazole (α-(4-chlorophenyl)
-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) and its metabolite 2-(4-chlorophenyl)-3-cyclopropyl-1-[1,2,4]triazol-1-ylbutane-2,3-diol, calculated as the stoichiometric equivalent of cyproconazole, in or on the following commodities:
Commodity

Parts per million

Cattle, liver
Goat, liver
Hog, liver
Horse, liver
Sheep, liver

0.50
0.50
0.01
0.50
0.50

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 53835, Oct. 7, 1998, as amended at 71 FR 71058, Dec. 8, 2006; 73 FR 27760, May 14, 2008; 78 FR 37473, June 21, 2013]

Back to Top
§180.486 Chlorethoxyfos; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide chlorethoxyfos, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only chlorethoxyfos, O,O-diethyl O-(1,2,2,2-tetrachloroethyl)
phosphorothioate, in or on the commodity.
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 23498, Apr. 27, 2011]

Back to Top
§180.487 Pyrithiobac sodium; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide, pyrithiobac sodium, (sodium 2-chloro-6[(4,6-dimethoxypyrimidin-2-yl)thio]benzoate), resulting from the application of the pesticide chemical in or on the following
foods/feeds:
Commodity

Parts per million

Cotton, gin byproducts
Cotton, undelinted seed

0.15
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[62 FR 54783, Oct. 22, 1997, as amended at 64 FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, 2002]

Back to Top
§180.490 Imazapic; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide imazapic, including its metabolites and
degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be
determined by measuring the sum of imazapic (2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5methyl-3-pyridinecarboxylic acid) and its metabolites (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]
-5-hydroxymethyl-3-pyridinecarboxylic acid and (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]
-5-(β-D-glucopyranosyloxy)methyl-3-pyridinecarboxylic acid, calculated as the stoichiometric equivalent of imazapic.
Commodity

Parts per million

Grass, forage
Grass, hay
Peanut
Soybean, seed1

15
30
0.1
0.40

Sugarcane, cane2

0.03

1

There are no US registrations as of April 4, 2014.

2

There are no U.S. registrations as of June 4, 2014.

(2) Tolerances are established for residues of the herbicide imazapic, including its metabolites and degradates, in or
on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by
measuring the sum of imazapic (2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-methyl-3pyridinecarboxylic acid) and its metabolite (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5hydroxymethyl-3-pyridinecarboxylic acid, calculated as the stoichiometric equivalent of imazapic.
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat byproducts, except kidney
Cattle, meat
Goat, fat
Goat, kidney
Goat, meat byproducts, except kidney
Goat, meat
Horse, fat
Horse, kidney
Horse, meat byproducts, except kidney
Horse, meat
Milk
Sheep, fat
Sheep, kidney
Sheep, meat byproducts, except kidney
Sheep, meat

0.10
1.0
0.1
0.1
0.1
1.0
0.1
0.1
0.1
1.0
0.1
0.1
0.1
0.1
1.0
0.1
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 54224, Oct. 6, 1999, as amended at 66 FR 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001; 78 FR 49932, Aug. 16, 2013;
79 FR 18818, Apr. 4, 2014; 79 FR 32170, June 4, 2014]

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§180.491 Propylene oxide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fumigant propylene oxide, including its metabolites and
degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this
paragraph is to be determined by measuring only propylene oxide, when used as a postharvest fumigant, in or on the
commodity.
Commodity

Parts per
million

Cacao bean, cocoa powder
Cacao bean, dried bean

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200
200

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Fig
Garlic, dried
Grape, raisin
Herbs and spices, group 19, dried
Nut, pine
Nut, tree, group 14
Nutmeat, processed, except peanuts
Onion, dried
Pistachio
Plum, prune, dried

3.0
300
1.0
300
300
300
300
300
300
2.0

(2) Tolerances are established for residues of the reaction product, propylene chlorohydrin, including its metabolites
and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in
this paragraph is to be determined by measuring only the sum of propylene chlorohydrin (1-chloro-2-propanol), and its
isomer 2-chloro-1-propanol, calculated as the stoichiometric equivalent of propylene chlorohydrin (1-chloro-2-propanol),
that results from the use of propylene oxide as a postharvest fumigant, in or on the commodity.
Parts per
million

Commodity
Basil, dried leaves
Cacao bean, cocoa powder
Cacao bean, dried bean
Fig
Garlic, dried
Grape, raisin
Herbs and spices, group 19, dried, except basil
Nut, pine
Nut, tree, group 14
Nutmeat, processed, except peanuts
Onion, dried
Pistachio
Plum, prune, dried

6000
20.0
20.0
3.0
6000
4.0
1500
10.0
10.0
10.0
6000
10.0
2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33702, May 24, 2000, as amended at 68 FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, 2007; 73 FR 54963, Sept. 24, 2008;
76 FR 38037, June 29, 2011; 77 FR 28495, May 15, 2012]

Back to Top
§180.492 Triflusulfuron-methyl; tolerances for residues.
(a) General. Tolerances are established for residues of triflusulfuron-methyl, including its metabolites and degradates,
in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only triflusulfuron-methyl (methyl 2-[[[[[4-(dimethylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2yl]amino]carbonyl]amino]sulfonyl]-3-methylbenzoate) in or on the following commodities:
Commodity

Parts per million

Beet, garden, roots
Beet, garden, tops
Beet, sugar, roots
Beet, sugar, tops
Chicory, roots

0.01
0.02
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 40196, June 12, 2002, as amended at 76 FR 22625, Apr. 22, 2011]

Back to Top
§180.493 Dimethomorph; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide dimethomorph, 4-[3-(4-chlorophenyl)
-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its metabolites and degradates, in or on the

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commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined
by measuring only dimethomorph in or on the commodities.
Commodity

Parts per million

Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Ginseng
Grape
Grape, raisin
Hop, dried cones
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B

6.0
30.0
0.90
3.0
7.0
60
0.6
15.0
1.5

Papaya1
Potato
Potato, wet peel
Strawberry
Taro, corm
Taro, leaves
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy (except Brassica) group 4

0.05
0.20
0.90
0.5
6.0
20.0
0.5
1.5
30.0

1

There are no U.S. registrations as of January 20, 2015.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the
fungicide dimethomorph, 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its
metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified
in the following table is to be determined by measuring only dimethomorph in or on the commodity.
Commodity

Parts per million

Bean, lima, succulent

0.60

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide
dimethomorph, 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its metabolites
and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the
following table is to be determined by measuring only dimethomorph in or on the commodity.
Commodity

Parts per million

Wheat, forage
Wheat, hay
Wheat, straw

0.15
0.15
0.4

[62 FR 26416, May 14, 1997]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.493, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.494 Pyridaben; tolerance for residues.
(a) General. Tolerances are established for residues of the insecticide pyridaben [2-tert-butyl-5-(4-tert-butylbenzylthio)
-4-chloropyridazin-3(2H)-one] on the following plants, and of the insecticide pyridaben and its metabolites (2-tert-butyl5-(4-(1-carboxy-1-methylethyl)benzylthio)-4-chloropyridazin-3(2H)-one] and (2-tert-butyl-5-[4(-1,1-dimethyl-2hypdroxyethyl)benzylthio-4-chloropyridazinn-3(2H)-one) on animals, as indicated in the following table.
Commodity
Almond, hulls
Apple
Apple, wet pomace
Canistel
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Citrus
Citrus, dried pulp
Citrus, oil
Fruit, stone, group 12

Parts per million

Revocation/expiration date
4.0
0.5
0.75
0.10
0.05
0.05
0.05
0.5
1.5
10.0
2.5

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None
None
None
None
None
None
None
None
None
None
None

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Goat, fat
Goat, meat
Goat, meat byproducts
Grape
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Mango
Milk
Nut, tree, group 14
Papaya
Pear
Pistachio
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat
Sheep, meat
Sheep, meat byproduct
Star apple
Strawberry
Tomato

0.0
0.05
0.05
1.5
0.05
0.05
0.05
10.0
0.05
0.05
0.05
0.10
0.01
0.05
0.10
0.75
0.05
0.10
0.10
0.10
0.05
0.05
0.05
0.10
2.5
0.15

None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(m) are
established for residues of the insecticide pyridaben [2-tert-butyl-5(4-tert-butylbenzylthio)-4-chloropyridazin-3(2H)-one] in
or on the following raw agricultural commodity:
Commodity

Parts per million

Cranberry

Expiration Date
0.5

None

(d) Indirect or inadvertent residues. [Reserved]
[65 FR 43712, July 14, 2000, as amended at 66 FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, 2005; 76 FR 56015, Sept. 15,
2010]

Back to Top
§180.495 Spinosad; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the insecticide spinosad in or on the food commodities in the
table to this paragraph. Spinosad is a fermentation product of Saccharopolyspora spinosa. The product consists of two
related active ingredients: Spinosyn A (Factor A: CAS # 131929-60-7) or 2-[(6-deoxy-2,3,4-tri-O -methyl-α-L-mannopyranosyl)oxy]-13-[[5-(dimethylamino)-tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b-tetradecahydro-14-methyl-1H-as-Indaceno[3,2-d]oxacyclododecin-7,15dione; and Spinosyn D (Factor D; CAS # 131929-63-0) or 2-[(6-deoxy-2,3,4-tri-O-methyl-α-L-manno-pyranosyl)oxy]-13[[5-(dimethyl-amino)-tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16btetradecahydro-4,14-methyl-1H-as-Indaceno[3,2-d]oxacyclododecin-7,15-dione.
Commodity

Parts per million

Acerola
Alfalfa, seed
Alfalfa, seed screenings
Almond, hulls
Amaranth, grain, grain
Amaranth, grain, stover
Animal feed, nongrass, group, 18
Animal feed, nongrass, group, 18, forage
Animal feed, nongrass, group, 18, hay
Apple, dry pomace
Apple, wet pomace
Artichoke, globe
Asparagus
Atemoya
Avocado

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1.5
0.15
2.0
19
1.0
10
0.02
35.0
30.0
0.5
0.5
0.3
0.2
0.3
0.3

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Banana
Beet, sugar, molasses
Biriba
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13B
Caneberry subgroup 13A
Canistel
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Cherimoya
Citrus, oil
Citrus, dried pulp
Coriander, leaves
Corn, sweet, kernel plus cob with husks removed
Cotton, gin byproducts
Cotton, undelinted seed
Cranberry
Custard apple
Date
Egg
Feijoa
Fig
Fish
Fish-shellfish, crustacean
Fish-shellfish, mollusc
Food commodities
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Grain, aspirated fractions
Grain, cereal, group 15
Grain, cereal, group 16, forage, except rice
Grain, cereal, group 16, hay, except rice
Grain, cereal, group, 16, stover, except rice
Grain, cereal, group, 16, straw, except rice
Grape
Grape, raisin
Grass, forage, fodder and hay, group 17, forage
Grass, forage, fodder and hay, group 17, hay
Guava
Herb subgroup 19A, dried
Herb subgroup 19A, fresh
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Ilama
Jaboticaba
Juneberry
Lingonberry
Longan
Lychee
Mango
Milk
Milk, fat
Nut, tree, group 14
Okra
Onion, green
Papaya
Passionfruit
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B

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0.25
0.75
0.3
2.0
10.0
0.250
0.7
0.3
50
10
2.0
5.0
0.3
3.0
0.5
8.0
0.02
1.5
0.02
0.01
0.3
0.10
0.30
.05
0.10
4.0
4.0
4.0
0.02
0.3
0.20
0.20
50
10
2.0
5.0
200
1.5
2.5
10.0
10.0
1.0
0.50
0.70
10.0
5.0
0.3
22
3.0
5.0
0.50
2.0
22
50
10
2.0
5.0
0.3
0.3
0.25
0.250
0.3
0.3
0.3
7.0
85
0.10
0.40
2.0
0.3
0.3
0.02
0.02

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Peanut
Peanut, hay
Peppermint, tops
Pineapple
Pineapple, process residue
Pistachio
Pomegranate
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Pulasan
Rambutan
Rice, hulls
Salal
Sapodilla
Sapote, black
Sapote, mamey
Sapote, white
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver
Soursop
Soybean
Spanish lime
Spearmint, tops
Spice, subgroup 19B, except black pepper
Star apple
Starfruit
Strawberry
Sugar apple
Ti, leaves
Vegetable, bulb, group 3, except green onion
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root and tuber, group 1
Watercress
Wax jambu

0.02
11.0
3.5
0.02
0.08
0.10
0.30
1.3
0.10
0.20
0.3
0.3
4.0
0.250
0.3
0.3
0.3
0.3
50
10
2.0
5.0
0.3
0.02
0.3
3.5
1.7
0.3
0.3
1.0
0.3
10.0
0.10
0.3
8.0
0.4
8.0
10.0
0.30
0.10
8.0
0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[72 FR 68540, Dec. 5, 2007, as amended at 74 FR 46376, Sept. 9, 2009; 74 FR 48408, Sept. 23, 2009; 75 FR 60327, Sept. 30,
2010]

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§180.496 Thiazopyr; tolerances for residues.
Tolerances are established for combined residues of the herbicide thiazopyr (3-pyridinecaroxylic acid,
2-(difluoromethyl)-5-(4,5-dihydro-2-thiazolyl)-4-(2-methylpropyl)-6-(trifluoromethyl)-, methyl ester) and its metabolites
determined as 2-(difluoromethyl)-6-(trifluoromethyl)-3,4,5-pyridinetricarboxylic acid, all expressed as the parent
equivalents in or on the following raw agricultural commodities:
Commodities

Parts per million

Grapefruit
Orange, sweet

0.05
0.05

[62 FR 9978, Mar. 5, 1997]

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§180.497 Clofencet; tolerances for residues.

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(a) General. Tolerances are established for residues of the plant growth regulator (hybridizing agent) clofencet,
including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the
tolerance levels specified in this paragraph is to be determined by measuring only clofencet, potassium 2-(4-chlorophenyl)
-3-ethyl-2,5-dihydro-5-oxo-4-pyridazinecarboxylate, expressed as the free acid, in or on the commodity.

Commodity
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Egg
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

Expiration/
revocation
date

Parts per
million
0.04
10.0
0.15
0.5
1.0
0.04
10.0
0.15
0.5
0.04
10.0
0.15
0.5
0.04
10.0
0.15
0.5
0.02
0.04
0.15
0.20
0.04
10.0
0.15
0.5
10.0
250.0
40.0
50.0

7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the plant growth
regulator (hybridizing agent) clofencet, including its metabolites and degradates, in or on the commodities in the table in
this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only
clofencet, potassium 2-(4-chlorophenyl)-3-ethyl-2,5-dihydro-5-oxo-4-pyridazinecarboxylate, expressed as the free acid, in
or on the commodity when present therein as a result of the application of clofencet to the growing crops in paragraph (a)
of this section.

Commodity
Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; forage
Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; hay
Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; stover
Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; straw
Grain, cereal group 15, except rice, sweet corn, wheat, and wild rice
Soybean
Soybean, forage
Soybean, hay

Parts per
million
4.0
15.0
1.0
4.0
20.0
30.0
10.0
10.0

Expiration/
revocation
date
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12
7/14/12

[76 FR 56656, Sept. 14, 2011]

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§180.498 Sulfentrazone; tolerances for residues.
(a)(1) General. Tolerances are established for the combined residues of the free and conjugated forms of
sulfentrazone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the
tolerance levels specified below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolite HMS

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(N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)
methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the following commodities.
Commodity

Parts per million

Soybean, seed

0.05

(2) Tolerances are established for the combined residues of the free and conjugated forms of sulfentrazone, including
its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS
(N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as
the stoichiometric equivalent of sulfentrazone in or on the following commodities.
Commodity
Apple
Asparagus
Berry and small fruit, group 13-07
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Corn, field, forage
Corn, field, grain
Corn, field, stover
Flax
Fruit, citrus, group 10-10
Horseradish
Melon, subgroup 9A
Nut, tree, group 14
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea, succulent
Peanut
Peanut, meal
Peppermint, tops
Pistachio
Rhubarb
Spearmint, tops
Sugarcane, cane
Sugarcane, molasses
Sunflower subgroup 20B
Turnip, roots
Turnip, tops
Vegetable, fruiting, group 8-10
Vegetable, soybean, succulent
Vegetable, tuberous and corm, subgroup 1C

Parts per million
0.15
0.15
0.15
0.20
0.40
0.20
0.15
0.30
0.15
0.15
0.20
0.15
0.15
0.15
0.15
0.20
0.40
0.30
0.15
0.15
0.30
0.15
0.20
0.20
0.15
0.60
0.15
0.15
0.15

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for the combined
residues of the free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]
phenyl]methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on
the following commodities.
Commodity

Parts per
million

Bean, lima, succulent
Cowpea, succulent
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.15
0.15
0.50
0.15
0.30
1.5

(d) Indirect or inadvertent residues. Tolerances are established for inadvertent and indirect combined residues of the
free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the commodities in the table
below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of
sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]
methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxo-

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1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the
following commodities when present therein as a result of the application of sulfentrazone to growing crops.
Commodity
Grain, cereal (excluding sweet corn), Hulls
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; forage
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; hay
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; stover
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; straw
Grain, cereal, group 15, except sweet corn
Grain, cereal, group 15, except sweet corn; bran

Parts per million
0.30
0.2
0.2
0.1
0.6
0.1
0.15

[62 FR 10708, Mar. 10, 1997]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.498, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.499 Propamocarb; tolerances for residues.
(a) General. Tolerances are established for the residues of propamocarb, including its metabolites and degradates, in
or on the commodities specified in the following table resulting from the application of the hydrochloride salt of
propamocarb. Compliance with the following tolerance levels is to be determined by measuring only propamocarb (propyl
N-[3-(dimethylamino)propyl]carbamate):
Commodity

Parts per million

Lettuce, head
Lettuce, leaf
Potato
Tomato, paste
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8

50
90
0.06
5.0
1.5
2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerance with regional registrations. Tolerances with regional registrations are established for the residues of
propamocarb, including its metabolites and degradates, in or on the commodities specified in the following table resulting
from the application of the hydrochloride salt of propamocarb. Compliance with the following tolerance levels is to be
determined by measuring only propamocarb (propyl N-[3-(dimethylamino)propyl]carbamate):
Commodity

Parts per
million

Bean, lima, succulent

2.0

(d) Indirect or inadvertent residues. [Reserved]
[62 FR 15620, Apr. 2, 1997, as amended at 62 FR 26966, May 16, 1997; 63 FR 32136, June 12, 1998; 64 FR 16843, Apr. 7, 1999;
65 FR 58399, Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; 69 FR 47022,
Aug. 4, 2004; 70 FR 7047, Feb. 10, 2005; 78 FR 33736, June 5, 2013]

Back to Top
§180.500 Imazapyr; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide, imazapyr, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only the residues of imazapyr [2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo1H-imidazol-2-yl]-3-pyridinecarboxylic acid].
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Corn, field, forage
Corn, field, grain
Corn, field, stover
Fish
Goat, fat
Goat, kidney
Goat, meat

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0.05
0.20
0.05
0.05
0.05
0.05
0.05
1.0
0.05
0.20
0.05

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Goats, meat byproducts, except kidney
Grass, forage
Grass, hay
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney

0.05
100
30
0.05
0.20
0.05
0.05
0.2

Lentil1
Milk

0.01
0.05

Rapeseed subgroup 20A1
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney
Shellfish

0.05
0.20
0.05
0.05
0.10
4.5

Soybean, meal1

4.0

Soybean, seed1
Sunflower subgroup 20B1

0.05

1

There are no U.S. Registrations.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55484, Sept. 26, 2003, as amended at 78 FR 66653, Nov. 6, 2013; 79 FR 19487, Apr. 9, 2014]

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§180.501 Hydroprene; tolerances for residues.
(a) General. A tolerance of 0.2 part per million is established for residues of hydroprene [(S)-(Ethyl (2E,4E,7S)-3,7,11trimrthyl-2,4-dodecadienoate)], (CAS Reg. No. 65733-18-8) on food commodities in food-handling establishments in
accordance with the following prescribed conditions:
(1) Application shall be limited to spot, crack and crevice, perimeter and ultra low volume (ULV) fogging treatment in
food storage or food-handling establishments, including warehouses, food service, manufacturing, and processing
establishments such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing
plants, and canneries where food and food products are held, processed, and served: Provided that the food is removed
or covered prior to such use, and food-processing surfaces are covered during treatment or thoroughly cleaned before
using, or in the case of point-source device treatments, devices must not come into direct contact with food preparation
surfaces and must be in a minimum distance of 3 feet from exposed foods.
(2) To assure safe use of the insect growth regulator, the label and labeling shall conform to that registered by the
U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 61647, Nov. 19, 1997, as amended at 71 FR 74818, Dec. 13, 2006]

Back to Top
§180.502 Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for residues.
(a) General. Tolerances are established for residues of aminoethoxyvinylglycine hydrochloride (aviglycine HCl) in or
on the following food commodities:
Commodity

Parts per million

Apple
Fruit, stone, group 12, except cherry
Pear

0.08
0.170
0.08

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[62 FR 24838, May 7, 1997, as amended at 64 FR 31129, June 10, 1999; 66 FR 36481, 36484, July 12, 2001; 69 FR 7606, Feb. 18,
2004]

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§180.503 Cymoxanil, tolerance for residues.
(a) General. Tolerances are established for residues of the fungicide, cymoxanil, 2-cyano -N- [(ethylamino)carbonyl]
-2-(methoxyimino) acetamide, in or on the following food commodities:
Commodity

Parts per million

Caneberry, subgroup 13A-07
Cilantro, leaves
Hop, dried cones
Leafy greens, subgroup 4A
Leaf petioles, subgroup 4B

4.0
19
7.0
19
6.0
1.0

Lychee1
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Potato
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
1

0.05
1.1
0.05
0.05
0.2

There is no U.S. registration for lychee.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with a regional registration. Tolerances with a regional registration as defined in §180.1(l) are
established for the residues of the fungicide cymoxanil, 2-cyano -N- [(ethylamino)carbonyl]-2-(methoxyimino) acetamide)
in or on the raw agricultural commodities:
Commodity

Parts per million

Grape

0.10

(d) Indirect or inadvertent residues. [Reserved]
[62 FR 26411, May 14, 1997, as amended at 62 FR 39956, July 25, 1997; 63 FR 24949, May 6, 1998; 63 FR 66464, Dec. 2, 1998;
64 FR 6539, Feb. 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR 41936,
July 16, 2003; 70 FR 7047, Feb. 10, 2005; 72 FR 37646, July 11, 2007; 73 FR 58885, Oct. 8, 2008; 76 FR 34885, June 15, 2011]

Back to Top
§180.504 [Reserved]
Back to Top
§180.505 Emamectin; tolerances for residues.
(a) General. (1) Tolerances are established for emamectin, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of emamectin (a mixture of a minimum of 90% 4′-epi-methylamino-4′-deoxyavermectin B1a and maximum of
10% 4′-epi-methylamino-4′-deoxyavermectin B1b) and its metabolites 8,9-isomer of the B1a and B1b component of the
parent (8,9-ZMA), or 4′-deoxy-4′-epi-amino-avermectin B1a and 4'-deoxy-4′-epi-amino-avermectin B1b; 4′-deoxy-4′-epiamino avermectin B1a (AB1a); 4′-deoxy-4′-epi-(N-formyl-N-methyl)amino-avermectin (MFB1a); and 4′-deoxy-4′
-epi-(N-formyl)amino-avermectin B1a (FAB1a), calculated as the stoichiometric equivalent of emamectin.
Commodity

Parts per million

Almond, hulls
Apple, wet pomace
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, pome, group 11
Grape, wine1
Nut, tree, group 14
Pistachio
Tomato, paste
Turnip, greens
Vegetable, Brassica, leafy, group 5
Vegetable, cucurbit, group 9

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0.20
0.075
0.050
0.025
0.025
0.03
0.02
0.02
0.150
0.050
0.050
0.02

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Vegetable, fruiting, group 8
Vegetable, leafy, except Brassica, group 4

0.020
0.100

1

There are no U.S. registrations for use of emamectin on grape, wine.

(2) Tolerances are established for emamectin, including its metabolites and degradates, in or on the commodities in
the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring
only the sum of emamectin (MAB1a + MAB1b isomers) and the associated 8,9-Z isomers (8,9-ZB1a and 8,9-ZB1b).
Commodity

Parts per million

Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts (except liver)
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver

0.010
0.050
0.003
0.020
0.010
0.050
0.003
0.020
0.003
0.020
0.002
0.005
0.010
0.050
0.003
0.020
0.003
0.010
0.050
0.003
0.020

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. [Reserved]
[71 FR 18649, Apr. 12, 2006, as amended at 74 FR 2873, Jan. 16, 2009; 78 FR 18511, Mar. 27, 2013; 78 FR 49939, Aug. 16, 2013]

Back to Top
§180.506 Cyclanilide; tolerances for residues.
(a) General. Tolerances are established for residues of the plant growth regulator, cyclanilide,
[1-(2,4-dichlorophenylaminocarbonyl)-cyclopropane carboxylic acid] determined as 2,4-dichloroaniline (calculated as
cyclanilide) in or on the following food commodities and processed feed:
Commodity

Parts Per Million

Cattle, fat
Cattle, meat
Cattle, meat byproducts, except kidney
Cattle, kidney
Cotton, undelinted seed
Cotton, gin byproducts
Goat, fat
Goat, meat
Goat, meat byproducts, except kidney
Goat, kidney
Horse, fat
Horse, meat
Horse, meat byproducts, except kidney
Horse, kidney
Hog, fat
Hog, meat
Hog, meat byproducts, except kidney
Hog, kidney
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts, except kidney
Sheep, kidney

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0.10
0.02
0.2
2.0
0.60
25.0
0.10
0.02
0.20
2.0
0.10
0.02
0.20
2.0
0.10
0.02
0.20
2.0
0.04
0.10
0.20
0.20
2.0

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 28355, May 23, 1997; 62 FR 34182, June 25, 1997]

Back to Top
§180.507 Azoxystrobin; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for residues of the fungicide, azoxystrobin, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the table is to
be determined by measuring only the sum of azoxystrobin, [methyl(E)-2-(2-(6-(2-cyanophenoxy) pyrimidin-4-yloxy)phenyl)
-3-methoxyacrylate], and the Z-isomer of azoxystrobin [methyl(Z)-2-(2-(6-(2-cyanophenoxy)pyrimidin-4-yloxy)phenyl)-3
methoxyacrylate] in or on the commodity.
Commodity
Acerola
Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Artichoke, globe
Asparagus
Atemoya
Avocado
Banana
Barley, bran
Barley, forage
Barley, grain
Barley, hay
Barley, straw
Berry, low growing, subgroup 13-07G, except cranberry
Biriba
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Cherimoya
Cilantro, leaves
Citrus, dried pulp
Citrus, oil

Parts per million

Coffee, green bean1
Corn, field, forage
Corn, field, grain
Corn, field, refined oil
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cottonseed subgroup 20C
Cranberry
Custard apple
Dragon fruit
Feijoa
Fruit, citrus, group 10-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12
Ginseng1
Grain, aspirated fractions
Grass, forage
Grass, hay
Guava
Herb Subgroup 19A, dried leaves
Herb Subgroup 19A, fresh leaves

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2.0
4.0
45
120
4.0
0.04
2.0
2.0
*
6.0
25
3.0
10.0
15.0
10.0
2.0
3.0
25
5.0
5.0
2.0
2.0
30.0
20.0
40.0
0.03
12.0
0.05
0.3
25.0
0.05
25.0
12.0
0.05
25.0
45
0.7
0.50
2.0
2.0
2.0
15.0
2.0
1.5
0.5
420
15
20
2.0
260
50

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Hop, dried cones
Ilama
Jaboticaba
Jackfruit
Longan
Loquat
Lychee
Mango
Nut, tree, group 14
Oats, forage
Oats, grain
Oats, hay
Oats, straw
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Papaya
Passionfruit
Pawpaw
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut
Peanut, hay
Peanut, refined oil
Pear, Asian1
Pepper/eggplant subgroup 8-10B
Peppermint, tops
Persimmon
Pistachio
Pulasan
Rambutan
Rapeseed subgroup 20A
Rice, grain
Rice, hulls
Rice, straw
Rice, wild, grain
Rye, forage
Rye, grain
Rye, straw
Sapodilla
Sapote, black
Sapote, mamey
Sapote, white
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soursop
Soybean, hay
Soybean, hulls
Soybean, seed
Spanish lime
Spearmint, tops
Spice Subgroup 19B, except black pepper
Star apple
Starfruit
Sugar apple
Sugarcane, cane
Sunflower subgroup 20B
Tamarind
Tea, dried1
Tomato, paste
Tomato subgroup 8-10A
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, edible podded, subgroup 6A, except soybean
Vegetable, root, subgroup 1A
Vegetable, tuberous and corm, subgroup 1C
Wasabi, dry
Wasabi, fresh
Watercress

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20.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
0.02
5.0
1.5
10.0
3.0
1.0
7.5
2.0
2.0
2.0
0.5
0.5
0.2
15.0
0.6
0.07
3.0
30
2.0
0.50
2.0
2.0
1.0
5.0
20
12
5.0
7.0
0.2
1.5
2.0
2.0
2.0
2.0
25
11
40
2.0
55.0
1.0
0.5
2.0
30
38
2.0
2.0
2.0
0.2
0.5
2.0
20.0
0.6
0.2
25
0.3
30.0
30.0
50.0
3.0
0.5
8.0
260
50
3.0

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Wax jambu
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

2.0
15.0
0.2
30.0
10.0

*2.0 (of which not more than 0.1 is contained in the pulp)
1

There are no United States registrations for use of azoxystrobin on coffee, green bean; ginseng; pear, Asian and tea,
dried.
(2) Tolerances are established for residues of the fungicide, azoxystrobin, including its metabolites and degradates, in
or on the commodities in the following table. Compliance with the tolerance levels specified in the table is to be determined
by measuring only azoxystrobin, [methyl(E)-2-(2-(6-(2-cyanophenoxy) pyrimidin-4-yloxy)phenyl)-3-methoxyacrylate] in or
on the commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk.
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.03
0.01
0.07
0.03
0.01
0.07
0.010
0.01
0.010
0.03
0.01
0.07
0.006
0.03
0.01
0.07

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 32235, June 13, 1997]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.507, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.509 Mefenpyr-diethyl; tolerance for residues.
(a) General. Tolerances are established for residues of the safener, mefenpyr-diethyl, including its metabolites and
degradates, when applied at a rate no greater than 0.053 pound safener per acre per growing season in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of mefenpyr-diethyl (1-(2,4-dichlorophenyl)-4,5-dihydro-5-methyl-1H-pyrazole-3,5-dicarboxylic acid, diethyl
ester) and its 2,4-dichlorophenyl-pyrazoline metabolites, calculated as the stoichiometric equivalent of mefenpyr-diethyl, in
or on the commodity.
Commodity

Parts per
million

Barley, grain
Barley, hay
Barley, straw
Cattle, meat byproducts
Goat, meat byproducts
Grass, forage
Grass, hay
Hog, meat byproducts
Horse, meat byproducts
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Wheat, forage

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0.05
0.2
0.5
0.1
0.1
1.6
0.2
0.1
0.1
0.1
0.4
0.04
0.2
0.2

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Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.2
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of mefenpyrdiethyl, including its metabolites and degradates, when applied at a rate no greater than 0.053 pound safener per acre per
growing season in or on the commodities identified in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only the sum of mefenpyr-diethyl (1-(2,4-dichlorophenyl)-4,5-dihydro-5-methyl1H-pyrazole-3,5-dicarboxylic acid, diethyl ester) and its 2,4-dichlorophenyl-pyrazoline metabolites, calculated as the
stoichiometric equivalent of mefenpyr-diethyl, in or on the commodity.
Commodity

Parts per
million

Canola, seed
Soybean, forage
Soybean, hay
Soybean, seed

0.02
0.1
0.1
0.02

[73 FR 74977, Dec. 10, 2008, as amended at 76 FR 23903, Apr. 29, 2011]

Back to Top
§180.510 Pyriproxyfen; tolerances for residues.
(a) General. (1) Tolerances are established for residues of pyriproxyfen, including its metabolites and degradates, in
or on the commodities in the following table. Compliance with the tolerance levels specified is determined by measuring
only pyriproxyfen, 2-[1-methyl-2-(4-phenoxyphenoxy) ethoxy]pyridine, in or on the commodity.
Commodity
Acerola
Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Animal feed, nongrass, group 18, seed
Apple, wet pomace
Artichoke, globe
Asparagus
Atemoya
Avocado
Banana
Beet, sugar, dried pulp
Berry, low growing, except strawberry, subgroup 13-07H
Biriba
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Cacao bean, dried
Caneberry subgroup 13-07A
Canistel
Canola, seed
Cherimoya
Citrus, oil
Citrus, dried pulp
Coffee, instant
Coffee, green bean
Cotton, gin byproducts
Cotton, undelinted seed
Custard apple
Date
Feijoa
Fig
Fig, dried fruit
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small, vine climbing, except grape, subgroup 13-07E
Fruit, stone, group 12
Grain, cereal, group 15
Grain, cereal, forage, fodder and straw, group 16

Parts per million

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0.10
2.0
0.70
1.1
2.0
0.8
2.0
2.0
0.20
1.0
0.20
3.0
1.0
0.20
0.70
2.0
1.0
0.02
1.0
1.0
0.20
0.20
20
2.0
0.10
0.02
2.0
0.05
0.20
0.30
0.10
0.30
1.0
0.50
0.20
0.35
1.0
1.1
1.1

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Grape
Grass, forage, fodder, and hay, group 17, forage
Grass, forage, fodder, and hay, group 17, hay
Guava
Herb subgroup 19A
Ilama
Jaboticaba
Lychee
Mango
Nut, tree, group 14
Olive
Olive, oil
Papaya
Passionfruit
Pawpaw
Peanut
Pineapple
Pineapple, process residue
Pistachio
Pomegranate
Potato, chips
Potato, granules/flakes
Potato, wet peel
Pulasan
Rambutan
Rice, hulls
Safflower, seed
Sapodilla
Sapote, black
Sapote, mamey
Sapote, white
Sesame, seed
Soursop
Spanish lime
Star apple
Starfruit
Strawberry
Sugar apple
Sugarcane
Tea
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8-10
Vegetable, leafy, except Brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root and tuber, group 1
Walnut
Watercress
Wax jambu

2.5
0.70
1.1
0.10
100
0.20
0.10
0.30
1.0
0.02
1.0
2.0
1.0
0.10
1.0
0.20
0.30
1.1
0.02
0.20
0.75
0.75
0.75
0.30
0.30
5.5
0.20
1.0
1.0
1.0
0.30
0.02
0.20
0.30
1.0
0.10
0.30
0.20
1.1
0.02
0.70
0.10
2.0
0.80
3.0
2.0
0.20
0.15
0.02
2.0
0.10

(2) A tolerance of 0.10 parts per million is established for all food commodities as a result of the proposed use of
NYLAR in food handling establishments where food and food products are held, prepared, processed or served.
Application is limited to space, general surface, spot, and/or crack and crevice treatment in food handling establishments
where food and food products are held, processed, prepared and served. Space and general surface application may be
used only when the facility is not in operation provided exposed food is covered or removed from the area being treated
prior to application. Spot, and/or crack and crevice treatment may be used while the facility is in operation provided
exposed food is covered or removed from the area being treated prior to application. Food contact surfaces should be
thoroughly washed with an effective cleaning compound and rinced with potable water after use of the product. To assure
safe use of this additive, its label and labeling shall conform to that registered with the U.S. Environmental Protection
Agency, and shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 10233, Mar. 3, 1999]

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EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.510, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.511 Buprofezin; tolerances for residues.
(a) General. Tolerances are established for residues of buprofezin, including its metabolites and degradates in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the buprofezin, 2-[(1,1-dimethylethyl)imino]tetrahydro-3(1-methylethyl)-5-phenyl-4H-1,3,5-thiadiazin-4-one,
in the commodity.
Commodity

Parts per million

Acerola
Almond, hulls
Apricot
Atemoya
Avocado
Banana
Bean, snap, succulent
Bean, succulent
Berry, low growing, subgroup 13-07G
Birida
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Canistel
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts
Cherimoya
Citrus, dried pulp
Citrus, oil
Coffee, green bean
Cotton, gin byproducts
Cotton, undelinted seed
Custard apple
Feijoa
Fruit, citrus, group 10
Fruit, pome, group 11-10, except pear and pear, Asian
Fruit, stone, group 12, except apricot and peach
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts
Grape
Guava
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts
Ilama
Jaboticaba
Lettuce, head
Longan
Lychee
Mango
Milk
Nut, tree group 14
Olive
Olive, oil
Papaya
Passionfruit
Peach

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0.30
2.0
9.0
0.30
0.30
0.20
0.02
0.02
2.5
0.30
12.0
60
0.90
0.05
0.05
0.05
0.05
0.05
0.30
7.5
80
0.35
20.0
0.35
0.30
0.30
2.5
3.0
1.9
0.05
0.05
0.05
0.05
0.05
2.5
0.3
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.30
0.30
6.0
0.30
0.30
0.90
0.01
0.05
3.5
4.8
0.90
0.30
9.0

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Pear
Pear, Asian
Persimmon
Pistachio
Pomegranate
Pulasan
Radicchio
Rambutan
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts
Soursop
Spanish lime
Star apple
Starfruit
Sugar apple

6.0
6.0
1.9
0.05
1.9
0.30
6.0
0.30
0.90
0.90
0.90
0.05
0.05
0.05
0.05
0.05
0.30
0.30
0.90
0.30
0.30
20

Tea1
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy, except Brassica, group 4, except head lettuce and radicchio
Wax jambu

60
0.50
2.0
35
0.30

1

There are no U.S. registrations at this time.

(b) Section 18 emergency exemption. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 40741, July 30, 1997]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.511, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.512 [Reserved]
Back to Top
§180.513 Chlorfenapyr; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide chlorfenapyr [4-bromo-2-(4-chlorophenyl)
-1-(ethoxymethyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile] in or on the following raw agricultural commodities:
Commodity

Parts per million

Vegetable, fruiting, group 8

1.0

(2) A tolerance of 0.01 parts per million is established for residues of chlorfenapyr in or on all food commodities (other
than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling areas where food/feed
products are prepared, held, processed, or served and in accordance with the following prescribed conditions:
(i) Application shall be no greater than a 0.5% active ingredient solution for spot crack and crevice use in food/feed
handling establishments, where food and food products are held, processed, prepared and/or served.
(ii) Application may only be undertaken when the facility is not in operation, and provided exposed food has been
covered, or removed from the area being treated prior to application.
(iii) Food contact surfaces and equipment should be throughly washed with an effective cleaning compound, and
rinsed with potable water after each use of the product.
(iv) Contamination of food or food contact surfaces shall be avoided. Application excludes any direct application to
any food, food packaging, or any food contact surfaces.

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(v) To assure safe use, the label and labeling shall conform to that registered by the U.S. Environmental Protection
Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55527, Sept. 26, 2003, as amended at 70 FR 3654, Jan. 26, 2005]

Back to Top
§180.514 Cloransulam-methyl; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide, cloransulam-methyl, N-(2-carboxymethyl-6chlorophenyl)-5-ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-pyrimidine-2-sulfonamide, plus its acid, cloransulam, calculated as
parent ester in or on the following raw agricultural commodities:
Commodity

Parts per million

Soybean, forage
Soybean, hay
Soybean, seed

0.1
0.2
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 49163, Sept. 19, 1997]

Back to Top
§180.515 Carfentrazone-ethyl; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide carfentrazone-ethyl, including its metabolites
and degradates, in or on the commodities listed in the following table. Compliance with the following tolerance levels is to
be determined by measuring only the sum of carfentrazone-ethyl (ethyl-alpha-2-dichloro-5-[-4-(difluoromethyl)-4,5-dihydro3-methyl-5-oxo-1H -1,2,4-triazol-1-yl]-4-fluorobenzenepropanoate) and its metabolite carfentrazone-chloropropionic acid
(alpha, 2-dichloro-5-[-4-difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]-4-fluorobenzenepropanoic acid),
calculated as the stoichiometric equivalent of carfentrazone-ethyl, in or on the following commodities:
Commodity

Parts per million

Acerola
Almond, hulls
Animal feed, nongrass, crop group 18, forage
Animal feed, nongrass, crop group 18, hay
Animal feed, nongrass, crop group 18, seed
Atemoya
Avocado
Banana
Barley, bran
Barley, flour
Berry group 13
Birida
Borage
Cacao bean, bean
Cactus
Caneberry subgroup 13A
Canistel
Canola
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherimoya
Coconut
Coffee, bean, green
Corn, field, forage
Corn, sweet, forage

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0.10
0.20
2.0
5.0
15.0
0.10
0.10
0.20
0.80
0.80
0.10
0.10
0.10
0.10
0.10
0.1
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.20
0.20

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Corn, sweet, kernel plus cob with husk removed
Cotton, gin byproducts
Cotton, undelinted seed
Cotton, hulls
Cotton, meal
Cotton, refined oil
Crambe, seed
Custard apple
Date, dried fruit
Feijoa
Fig
Fish
Flax, seed
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated grain fractions
Grain, cereal, forage, fodder and straw group 16, except corn and sorghum; forage
Grain, cereal, forage, fodder and straw, group 16, hay
Grain, cereal, forage, fodder and straw, group 16, stover
Grain, cereal, forage, fodder and straw, group 16, except rice; straw
Grain, cereal, group 15
Grain, cereal, group 15 (except rice grain and sorghum grain)
Grain, cereal, stover
Grain, cereal, straw
Grape
Grass, forage
Grass, hay
Guava
Herbs and spices group 19
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Horseradish
Ilama
Jaboticaba
Juneberry
Kava, roots
Kiwifruit
Lingonberry
Longan
Lychee
Mango
Milk
Millet, flour
Mustard, seed
Noni
Nut, tree, group 14
Oat, flour
Okra
Olive
Palm heart
Palm heart, leaves
Papaya
Passionfruit
Pawpaw
Peanut
Peanut, hay
Persimmon
Pistachio
Pomegranate
Poultry, meat byproducts
Pulasan
Pummelo
Rambutan
Rapeseed, forage

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.10
10
0.20
0.60
0.35
1.0
0.10
0.10
0.10
0.10
0.10
0.30
0.10
0.10
0.10
0.10
0.10
0.10
0.10
1.8
1.0
0.30
0.30
0.10
0.10
0.10
0.80
3.0
0.10
5.0
8.0
0.10
2.0
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.05
0.80
0.10
0.10
0.10
0.80
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10

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Rapeseed, seed
Rice, grain
Rice, hulls
Rice, straw
Rye, bran
Rye, flour
Safflower, seed
Salal
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Shellfish
Sorghum, forage
Sorghum, grain
Sorghum, sweet
Soursop
Soybean, seed
Spanish lime
Star apple
Starfruit
Stevia
Strawberry
Strawberrypear
Sugar apple
Sugarcane
Sunflower, seed
Tea, dried
Ti, leaves
Ti, roots
Vanilla
Vegetable, brassica, leafy, group 5
Vegetable, bulb, group 3
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, except soybean, subgroup 7A
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root and tuber, group 1
Wasaba, roots
Wax jambu
Wheat, bran
Wheat, flour
Wheat, germ
Wheat, middlings
Wheat, shorts

0.10
1.3
3.5
1.0
0.80
0.80
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.30
0.20
0.25
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.15
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.80
0.80
0.80
0.80
0.80

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 52180, Sept. 30, 1998]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.515, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.516 Fludioxonil; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide fludioxonil, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only fludioxonil, 4-(2,2-difluoro-1,3-benzodioxol-4-yl)-1-H-pyrrole-3-carbonitrile).
Commodity

Parts per million

Acerola
Animal feed, nongrass, group 18
Atemoya

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5.0
0.01
20

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Avocado
Bean, dry
Bean, succulent
Beet, sugar, roots
Berry, low growing, subgroup 13-07G, except cranberry
Biriba
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Carrots
Cherimoya
Citrus, oil
Cotton, gin byproducts
Cotton, undelinted seed
Custard apple
Dragon fruit
Feijoa
Flax, seed
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12-12
Ginseng
Grain, cereal, group 15
Grain, cereal, forage, fodder, and straw, group 16
Grass, forage, fodder and hay, group 17
Guava
Herb subgroup 19A, dried leaves
Herb subgroup 19A, fresh leaves
Ilama
Jaboticaba
Kiwifruit, fuzzy
Leaf petioles subgroup 4B
Leafy greens subgroup 4A
Longan
Lychee
Mango
Melon subgroup 9A
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Papaya
Passionfruit
Peanut
Peanut, hay
Pineapple
Pistachio
Pomegranate
Pulasan
Rambutan
Rapeseed, forage
Rapeseed subgroup 20A, except flax seed
Safflower, seed
Sapodilla
Sapote, black
Sapote, mamey
Soursop
Spanish lime
Spice subgroup 19B
Star apple
Starfruit
Sugar apple
Sunflower, seed
Tomato
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8-10, except tomato
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root, except sugar beet, subgroup 1B
Vegetable, tuberous and corm, subgroup 1C

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

5.0
0.4
0.4
0.02
3.0
20
2.0
10
2.0
5.0
5.0
7.0
20
500
0.05
0.05
20
1.0
5.0
0.05
10
5.0
2.0
5.0
4.0
0.02
0.01
0.01
5.0
65
10
20
5.0
20
15
30
20
20
5.0
0.03
0.50
7.0
5.0
5.0
0.01
0.01
20
0.10
5.0
20
20
0.01
0.01
0.01
5.0
5.0
5.0
20
20
0.02
5.0
5.0
20
0.01
5.0
10
0.45
0.01
0.50
30
0.01
0.75
6.0

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Watercress
Wax jambu
Yam, true, tuber

7.0
5.0
8.0

(2) Tolerances are established for residues of the fungicide fludioxonil, including its metabolites and degradates, in or
on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only the sum of fludioxonil, 4-(2,2-difluoro-1,3-benzodioxol-4-yl)-1-H-pyrrole-3-carbonitrile), and
its metabolites converted to 2,2-difluoro-l,3-benzodioxole-4-carboxylic acid, calculated as the stoichiometric equivalent of
fludioxonil.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.05
0.01
0.05
0.05
0.01
0.05
0.05
0.01
0.05
0.01
0.05
0.01
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 56082, Oct. 29, 1997]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.516, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.517 Fipronil; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Therefore, tolerances are established for combined residues of the insecticide fipronil (5-amino1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile) and its metabolites
5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl) sulfonyl]-1H-pyrazole-3-carbonitrile and 5-amino1-[2,6-dichloro-4-(trifluoromethyl) phenyl]-4-[(trifluoromethyl)thio]-1H-pyrazole-3-carbonitrile and its photodegradate
5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)]-1H-pyrazole-3-carbonitrile in or on the
following items at the levels specified:
Commodity

Parts per million

Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Corn, field, grain
Corn, field, stover
Corn, field, forage
Egg
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk, fat (reflecting 0.05 ppm in whole milk)
Potato

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0.40
0.10
0.04
0.04
0.02
0.30
0.15
0.03
0.40
0.10
0.04
0.04
0.04
0.02
0.01
0.01
0.40
0.10
0.04
0.04
1.50
0.03

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Potato, wet peel
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, grain
Rice, straw
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver

0.10
0.05
0.02
0.02
0.04
0.10
0.40
0.10
0.04
0.04

(b) Section 18 emergency exemptions.. Time-limited tolerances are established for combined residues of the
insecticide, fipronil, 5-amino-1-(2,6-dichloro-4-(trifluoromethyl) phenyl)-4-((1,R,S)-trifluoromethyl)sulfinyl)-1-H-pyrazole-3carbonitrile and its 2 metabolites MB45950 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-[(trifluoromethyl)thio]-1Hpyrazole-3-carbonitrile) and MB46136 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-[(trifluoromethyl)sulfonyl]-1Hpyrazole-3-carbonitrile) and its photodegradate MB46513 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)
-(trifluoromethyl)]-1H-pyrazole-3-carbonitrile), in connection with use of the pesticide under Section 18 emergency
exemptions granted by EPA. The tolerances expire and are revoked on the dates specified in the table for this paragraph.
Commodity

Parts per million

Rutabaga
Turnip

Expiration/revocation date
1.0
1.0

12/31/16
12/31/16

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for combined indirect or inadvertent residues of the
insecticide fipronil and its metabolites and photodegradate in or on food commodities when present therein as a result of
the application of fipronil to growing crops listed in paragraphs (a) and (b) of this section and other nonfood crops to read
as follows:
Commodity

Parts per million

Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.02
0.005
0.03
0.03

[62 FR 62979, Nov. 26, 1997, as amended at 63 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, 2007; 74 FR 46377, Sept. 9,
2009; 75 FR 80346, Dec. 22, 2010; 78 FR 78748, Dec. 27, 2013]

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§180.518 Pyrimethanil; tolerances for residues.
Link to an amendment published at 80 FR 63691, October 21, 2015.
(a) General. (1) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and
degradates, in or on the commodities in the following table Compliance with the tolerance levels specified in the following
table is to be determined by measuring only pyrimethanil (4,6-dimethyl-N-phenyl-2-pyrimidinamine).
Commodity
Almond
Almond, hulls
Apple, wet pomace
Banana
Berry, low growing, subgroup 13-07G
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Citrus, oil
Cucumber
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit
Fruit, stone, group 12-12
Ginseng
Grape, raisin
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Pistachio
Pomegranate
Tomato subgroup 8-10A
Vegetable, tuberous and corm, subgroup 1C

Parts per million

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.20
12
40
0.10
3.0
8.0
15
150
1.5
10
15
5.0
10
1.5
8.0
2.0
3.0
0.20
5.0
0.50
0.05

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(2) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and degradates, in
or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only the sum of pyrimethanil and its metabolite 4-[4,6-dimethyl-2-pyrimidinyl)amino]phenol,
calculated as the stoichiometric equivalent of pyrimethanil.
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney

0.01
2.5
0.01
0.01
0.01
2.5
0.01
0.01
0.01
2.5
0.01
0.01
0.01
2.5
0.01
0.01

(3) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and degradates, in
or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only the sum of pyrimethanil and its metabolite 4,6-dimethyl-2-(phenylamino)-5-pyrimidinol,
calculated as the stoichiometric equivalent of pyrimethanil.
Commodity

Parts per million

Milk

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[62 FR 63669, Dec. 2, 1997, as amended at 69 FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, 2008; 74 FR 32448, July 8, 2009;
77 FR 45503, Aug. 1, 2012; 80 FR 7975, Feb. 13, 2015; 80 FR 63691, Oct. 21, 2015]

Back to Top
§180.519 Bromide ion and residual bromine; tolerances for residues.
(a) General. The food additives, bromide ion and residual bromine, may be present in water, potable in accordance
with the following conditions:
(1) The food additives are present as a result of treating water aboard ships with a polybrominated ion-exchange resin
(as a source of bromine) under the supervision of trained personnel.
(2) Residual bromine levels are controlled to not exceed 1.0 part per million (ppm) in the final treated water. Control is
effected using calibrated recirculating or proportioning bromine feeder equipment and periodic checks of residual bromine
using a bromine test kit. To assure safe use of the additives, the label and labeling of the disinfectant formulation
containing the food additives shall conform to the label and labeling registered by the U.S. Environmental Protection
Agency.
(3) No tolerance is established for bromide ion levels.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[41 FR 17893, Apr. 29, 1976. Redesignated at 41 FR 26568, June 28, 1976, and at 53 FR 24667, June 29, 1988. Redesignated and
amended at 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. 13, 2006]

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§180.521 Fumigants for grain-mill machinery; tolerances for residues.

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(a) General. Fumigants may be safely used in or on grain-mill machinery in accordance with the following prescribed
conditions:
(1) The fumigants consist of methyl bromide.
(2) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling registered by the
U.S. Environmental Protection Agency.
(3) Residues of inorganic bromides (calculated as Br) in milled fractions derived from cereal grain from all fumigation
sources, including fumigation of grain-mill machinery, shall not exceed 125 parts per million.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, as amended at 49 FR 44459, Nov. 7, 1984. Further
redesignated at 53 FR 24667, June 29, 1988, as amended at 54 FR 6130, Feb. 8, 1989. Further redesignated and amended at 63
FR 34319, June 24, 1998]

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§180.522 Fumigants for processed grains used in production of fermented malt beverage; tolerances for
residues.
(a) General. Fumigants for processed grain may be safely used, in accordance with the following conditions.
(1) Methyl bromide. Total residues of inorganic bromides (calculated as Br) from the use of this fumigant shall not
exceed 125 parts per milion.
(2) Methyl bromide is used to fumigate corn grits and cracked rice in the production of fermented malt beverage.
(3) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling registered by the
U.S. Environmental Protection Agency, and the usage employed should conform with such label or labeling.
(4) The total residue of inorganic bromides in fermented malt beverage, resulting from the use of corn grits and
cracked rice fumigated with the fumigant described in paragraph (a)(2) of this section plus additional residues of inorganic
bromides that may be present from uses in accordance with other regulations in this chapter promulgated under section
408 and/or 409 of the Act, does not exceed 25 parts per million bromide (calculated as Br).
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74818, Dec. 13, 2006]

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§180.523 Metaldehyde; tolerances for residues.
(a) General. Tolerances are established for residues of the molluscicide metaldehyde, including its metabolites and
degradates, in or on the commodities listed in the following table. Compliance with the specified tolerance levels is to be
determined by measuring only metaldehyde, 2,4,6,8-tetramethyl-1,3,5,7-tetroxocane, in or on the commodity.
Commodity

Parts per million

Artichoke, globe
Berry, low growing, subgroup 13-07G
Bushberry subgroup 13-07B
Cactus
Caneberry subgroup 13-07A
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Fruit, citrus, group 10-10
Ginseng
Grass, forage

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.07
6.25
0.15
0.07
0.15
0.30
0.05
0.10
0.30
0.05
0.10
0.26
0.05
2.0

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Grass, hay
Leaf petioles subgroup 4B
Lettuce
Pea and bean, succulent shelled, subgroup 6B
Peppermint, oil
Peppermint, tops
Spearmint, oil
Spearmint, tops
Taro, corm
Taro, leaves
Tomato subgroup 8-10A
Vegetable, brassica, leafy, group 5
Vegetable, foliage of legume, except soybean, subgroup 7A
Vegetable, legume, edible podded subgroup 6A
Watercress

2.0
0.50
1.73
0.20
12
4.0
12
4.0
0.15
1.0
0.24
2.5
1.5
0.80
3.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in §180.1(l) are
established for residues of the molluscicide metaldehyde, including its metabolites and degradates, in or on the following
commodities. Compliance with the specified tolerance level is to be determined by measuring only metaldehyde,
2,4,6,8-tetramethyl-1,3,5,7-tetroxocane, in or on the commodity.
Commodity

Parts per million

Clover, forage
Clover, hay
Soybean, seed

0.60
0.60
0.05

(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54963, Sept. 24, 2008, as amended at 78 FR 70869, Nov. 27, 2013; 80 FR 11588, Mar. 4, 2015]

Back to Top
§180.525 Resmethrin; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide resmethrin [5-(phenylmethyl)-3-furanyl] methyl
2,2-dimethyl-3-(2-methyl-1-propenyl) cyclopropanecarboxylate in or on food commodities at 3.0 ppm resulting from use of
the insecticide in food handling and storage areas as a space concentration for spot/or crack and crevice treatment and
shall be limited to a maximum of 3.00 percent of the active ingredient by weight, and as a space treatment shall be limited
to a maximum of 0.5 fluid ounce of 3.0 percent active ingredient by weight per 1000 cubic feet of space provided that the
food is removed or covered prior to such use. To assure safe use of the additive, its label and labeling shall conform to
that registered with the U.S. Environmental Protection Agency, and shall be used in accordance with such label and
labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 74819, Dec. 13, 2006]

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§180.526 Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.
(a) General. Synthetic isoparaffinic petroleum hydrocarbons complying with 21 CFR 172.882 (a) and (b) may be
safely used as a component of insecticide formulations for use on animal feed in an amount no greater than reasonably
required to accomplish its intended effect as an adjuvant in the insecticide formulation and shall not be intended to
accomplish any effect in animal feed. It is used or intended for use as a component of insecticide formulations used in
compliance with regulations issued in 40 CFR part 180 and in this part.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[40 FR 14161, Mar. 28, 1975, as amended at 50 FR 2959, Jan. 23, 1985, and amended at 53 FR 24668, 24669, June 29, 1988.
Redesignated and amended at 63 FR 34319, June 24, 1998]

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§180.527 Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]
acetamide and its metabolites containing the 4-fluoro-N-methylethyl benzenamine tolerances for residues.
(a) General. Tolerances are established for the combined residues of the herbicide flufenacet, N-(4-fluorophenyl)
-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide and its metabolites containing the
4-fluoro-N-methylethyl benzenamine moiety in or on the following commodities.
Commodity

Parts per million

Cattle, kidney
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Goat, kidney
Hog, kidney
Horse, kidney
Sheep, kidney
Soybean, seed
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.4
0.05
0.4
0.45
0.05
0.30
0.05
0.05
0.05
0.05
0.1
0.80
6.0
0.60
1.2
0.35

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances are established for combined residues of flufenacet,
N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide, and its metabolites
containing the 4-fluoro-N-methylethyl benzenamine moiety, with regional registration.
Commodity

Parts per million

Grass, forage
Grass, hay

7.0
0.4

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide
flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1,3,4-thiadiazol-2-yl]oxy]acetamide and its
metabolites containing the 4-fluoro-N-methylethyl benzenamine moiety in or on the following raw agricultural commodities
when present therein as a result of application of flufenacet to the growing crops in paragraph (a) of this section.
Commodity
Alfalfa, forage
Alfalfa, hay
Alfalfa, seed
Clover, forage
Clover, hay
Grain, cereal, group 15, except rice
Grain, cereal, forage, fodder, and straw, group 16, except rice
Grass, forage, fodder, and hay, group 17

Parts per million
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

[63 FR 26473, May 13, 1998, as amended at 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, 1999; 65 FR 64366, Oct. 27, 2000;
68 FR 2247, Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; 72 FR 26310,
May 9, 2007]

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§180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol methylcarbamate; tolerances for residues.
(a) General. (1) The insecticide 2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate may be safely used in spot and/or
crack and crevice treatments in animal feed handling establishments, including feed manufacturing and processing
establishments, such as stores, supermarkets, dairies, meat slaughtering and packing plants, and canneries until the
tolerance expiration/revocation date of April 26, 2005.
(2) The insecticide 2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate may be safely used in spot and/or crack and
crevice treatments in food handling establishments, including food service, manufacturing and processing establishments,
such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and
canneries until the tolerance expiration/revocation date of April 26, 2005.

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(3) To ensure safe use of the additive, its label and labeling shall conform to that registered with the U.S.
Environmental Protection Agency and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 34828, June 26, 1998, as amended at 69 FR 58083, Sept. 29, 2004]

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§180.532 Cyprodinil; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide cyprodinil, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only cyprodinil 4-cyclopropyl-6-methyl-N-phenyl-2-pyrimidinamine.
Commodity

Parts per
million

Acerola
Almond
Almond, hulls
Apple, wet pomace
Artichoke, globe
Avocado
Bean, dry
Bean, succulent
Berry, low growing, subgroup 13-07G, except cranberry
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Canola, seed1
Citrus, dried pulp
Citrus, oil
Dragon fruit
Feijoa
Fruit, pome, group 11-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12-12
Grape, raisin
Guava
Herb subgroup 19A, dried, except parsley
Herb subgroup 19A, fresh, except parsley
Jaboticaba
Kiwifruit
Leaf petioles subgroup 4B
Leafy greens subgroup 4A
Lemon
Lime
Longan
Lychee
Mango
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Papaya
Parsley, dried leaves
Parsley, leaves
Passionfruit
Pistachio
Pomegranate
Pulasan
Rambutan
Sapodilla
Sapote, black
Sapote, mamey
Spanish lime
Star apple
Starfruit

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1.5
0.02
8.0
4.6
4.0
1.2
0.6
0.6
5.0
1.0
10.0
3.0
10
1.2
0.03
8.0
60
2.0
1.5
1.7
3.0
2.0
5.0
1.5
15.0
3.0
1.5
1.8
30
50
0.60
0.60
2.0
2.0
1.2
0.6
4.0
1.2
170
35
1.5
0.10
10
2.0
2.0
1.2
1.2
1.2
2.0
1.2
1.5

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Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leaves of root and tuber, group 2
Vegetable, root, except sugarbeet, subgroup 1B
Watercress
Wax jambu

10.0
0.70
1.5
10
0.75
20
1.5

1

Import only.

(2) Tolerances are established for residues of the fungicide cyprodinil, including its metabolites and degradates, in the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of cyprodinil 4-cyclopropyl-6-methyl-N-phenyl-2-pyrimidinamine and free and conjugated CGA-304075
4-(4-cyclopropyl-6-methyl-pyrimidin-2-ylamino)-phenol, calculated as the stoichiometric equivalent of cyprodinil.
Commodity

Parts per
million

Cattle, meat byproducts
Goat, meat byproducts
Horse, meat byproducts
Sheep, meat byproducts

0.02
0.02
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 17706, Apr. 10, 1998]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.532, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.533 Esfenvalerate; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the insecticide esfenvalerate, (S)-cyano
(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, its non-racemic isomer, (R)-cyano
(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and its diastereomers (S)-cyano
(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4chloro-α-(1-methylethyl)benzeneacetate, in or on food commodities as follows:
Commodity

Parts per million

Almond
Almond, hulls
Apple
Artichoke, globe
Bean, dry, seed
Bean, snap, succulent
Beet, sugar, roots
Beet, sugar, tops
Blueberry
Broccoli
Cabbage, except Chinese cabbage
Caneberry subgroup 13A
Cantaloupe
Carrot, roots
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cauliflower
Collards
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed

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0.2
5.0
1.0
1.0
0.25
1.0
0.05
5.0
1.0
1.0
3.0
1.0
0.5
0.5
1.5
1.5
1.5
0.5
3.0
15.0
0.02
15.0
0.02
15.0
15.0
0.1
15.0
0.2

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Cucumber
Egg
Eggplant
Elderberry
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Gooseberry
Hazelnut
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Kiwifruit
Lentil, seed
Melon, honeydew
Milk
Milk, fat
Muskmelon
Mustard greens
Okra
Pea, dry, seed
Pea, succulent
Peanut
Pear
Pecan
Pepper
Potato
Poultry, fat
Poultry, liver
Poultry, meat
Poultry, meat byproducts, except liver
Pumpkin
Radish, roots
Radish, tops
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, hulls
Soybean, seed
Squash, summer
Squash, winter
Sugarcane, cane
Sunflower, seed
Sweet potato, roots
Tomato
Turnip, greens
Turnip, roots
Walnut
Watermelon

0.5
0.03
0.5
1.0
3.0
1.5
1.5
1.5
1.0
0.2
1.5
1.5
1.5
1.5
1.5
1.5
0.5
0.25
0.5
0.3
7.0
0.5
5.0
0.5
0.25
0.5
0.02
1.0
0.2
0.5
0.02
0.3
0.03
0.03
0.3
0.5
0.3
3.0
1.5
1.5
1.5
10.0
5.0
10.0
0.5
0.05
0.5
0.5
1.0
0.5
0.05
0.5
7.0
0.5
0.2
0.5

(2) A tolerance of 0.05 ppm on raw agricultural food commodities (other than those food commodities already covered
by a higher tolerance as a result of use on growing crops) is established for the combined residues of the insecticide
esfenvalerate, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, its non-racemic isomer,
(R)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and its diastereomers (S)-cyano
(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4chloro-α-(1-methylethyl)benzeneacetate as a result of the use of esfenvalerate in food-handling establishments.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registration are established for the combined
residues of the insecticide esfenvalerate, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)
benzeneacetate, its non-racemic isomer, (R)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)
benzeneacetate and its diastereomers (S)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate
and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, in or on food commodities as
follows:

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Parts per million

Cabbage, chinese, bok choy
Kohlrabi
Lettuce, head

1.0
2.0
5.0

(d) Indirect or inadvertent residues. [Reserved]
[63 FR 23401, Apr. 29, 1998, as amended at 63 FR 48615, Sept. 11, 1998; 74 FR 46699, Sept. 11, 2009]

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§180.535 Fluroxypyr 1-methylheptyl ester; tolerances for residues.
(a) General. Tolerances are established for combined residues of fluroxypyr 1-methylheptyl ester [1-methylheptyl
((4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy)acetate] and its metabolite fluroxypyr [((4-amino-3,5-dichloro-6-fluoro-2pyridinyl)oxy)acetic acid] in or on the following raw agricultural commodities. Compliance with the established tolerance
levels is determined by measuring only the sum of fluroxypyr 1-methylheptyl ester [1-methylheptyl ((4-amino-3, 5-dichloro6-fluoro-2-pyridinyl)oxy)acetate] and its metabolite fluroxypyr [((4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy)acetic acid]
calculated as the stoichiometric equivalent of fluroxypyr.
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, hay
Barley, straw
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Fruit, pome, group 11
Garlic, bulb
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grass, forage
Grass, hay
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts
Milk
Millet, forage
Millet, grain
Millet, hay
Millet, proso, straw
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Onion, bulb
Rice, bran
Rice, grain
Shallot, bulb
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover

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0.5
12.0
20.0
12.0
0.1
1.5
0.1
0.1
1.0
0.02
0.5
1.0
0.02
2.0
0.02
0.03
0.1
1.5
0.1
0.1
0.6
120
160
0.1
1.5
0.1
0.1
0.1
1.5
0.1
0.1
0.3
12.0
0.5
20.0
12.0
12.0
0.5
20.0
12.0
0.03
3.0
1.5
0.03
0.1
1.5
0.1
0.1
2.0
0.02
4.0

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Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

12.0
0.5
20.0
12.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 52169, Sept. 30, 1998, as amended at 64 FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, 2001; 66 FR 47971, Sept. 17,
2001; 67 FR 46884, July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; 70 FR
3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, 2005; 71 FR 76204, Dec. 20, 2006; 72 FR 73635, Dec. 28, 2007; 78 FR 3333, Jan. 16,
2013]

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§180.537 Isoxaflutole; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide, isoxaflutole, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of isoxaflutole ((5-cyclopropyl-4-isoxazolyl) [2-(methylsulfonyl)-4-(trifluoromethyl)
phenyl] methanone) and its metabolite 1-(2-methylsulfonyl-4-trifluoromethylphenyl)-2-cyano-3-cyclopropyl
propan-1,3-dione (RPA 202248), calculated as the stoichiometric equivalent of isoxaflutole, in or on the commodity:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Grain, aspirated fractions
Soybean, seed

0.04
0.02
0.02
0.30
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 50784, Sept. 23, 1998, as amended at 73 FR 75608, Dec. 12, 2008; 76 FR 76314, Dec. 7, 2011]

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§180.539 d-Limonene; tolerances for residues.
(a) General. (1) The insecticide d-limonene may be safely used in insect-repellent tablecloths and in insect-repellent
strips used in food- or feed-handling establishments.
(2) To assure safe use of the insect repellent, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33715, May 24, 2000, as amended at 70 FR 55268, Sept. 21, 2005]

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§180.540 Fenitrothion; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide fenitrothion, O,O-dimethyl O-(4-nitro-m-tolyl)
phosphorothioate, from the postharvest application of the insecticide to stored wheat in Australia, in or on the following
food commodity:
Commodity

Parts per million

Wheat, gluten1

3.0

1

There are no U.S. registrations on food commodities since 1987.

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 54963, Sept. 24, 2008]

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§180.541 Propetamphos; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. A tolerance of 0.1 part per million is established for residues of the insecticide propetamphos, including
its metabolites and degradates, in or on food or feed commodities when present therein as a result of the treatment of
food- or feed-handling establishments with propetamphos. Direct application shall be limited solely to spot and/or crack
and crevice treatment in food- or feed-handling establishments where food or feed and food or feed products are held,
processed, prepared, served, or sold. Spray and dust concentrations shall be limited to a maximum of 1 percent active
ingredient. For crack and crevice treatment, equipment capable of delivering a dust or a pin-stream of spray directly into
cracks and crevices shall be used. For spot treatment, a coarse, low-pressure spray shall be used to avoid contamination
of food, feed, or food-contact/feed-contact surfaces. Compliance with the tolerance level specified in this paragraph is to
be determined by measuring only propetamphos, 1-methylethyl-(2E)-3-((ethylamino)methoxyphosphinothioyl)oxy)-2butenoate, in or on the commodity.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 33716, May 24, 2000, as amended at 76 FR 23498, Apr. 27, 2011]

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§180.543 Diclosulam; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide diclosulam [N-(2,6-dichlorophenyl)-5-ethoxy-7fluoro[1,2,4] triazolo[1,5-c]pyrimidine-2-sulfonamide] in or on the following raw agricultural commodities as follows:
Parts per
million

Commodity
Peanut
Soybean, seed

0.020
0.020

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 12134, Mar. 8, 2000]

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§180.544 Methoxyfenozide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide methoxyfenozide, including its metabolites
and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the
following table is to be determined by measuring only methoxyfenozide (3-methoxy-2-methylbenzoic acid
2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide) in or on the commodity.
Commodity
Acerola
Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Apple, wet pomace
Artichoke, globe
Atemoya
Avocado
Beet, sugar, roots

Parts per million
0.4
25
50.0
150.0
7.0
3.0
0.60
0.6
0.50

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Berry, low growing, subgroup 13-07G, except cranberry
Biriba
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Cattle, fat
Cattle, meat
Cherimoya
Chive, fresh leaves
Citrus, oil
Corn, field, forage
Corn, field, grain
Corn, field, refined oil
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Cranberry
Custard apple
Date
Feijoa
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12-12, except plum, prune, fresh
Goat, fat
Goat, meat
Grain, aspirated grain fractions
Grape, raisin
Grass, forage, fodder and hay, group 17, forage
Grass, forage, fodder and hay, group 17, hay
Guava
Herb subgroup 19A, except chive, fresh leaves
Hog, fat
Hog, meat
Horse, fat
Horse, meat
Ilama
Jaboticaba
Leaf petioles subgroup 4B
Leafy greens subgroup 4A
Longan
Lychee
Mango
Milk
Nut, tree, group 14-12
Onion, green, subgroup 3-07B, except chive, fresh leaves
Papaya
Passionfruit
Pea and bean, dried shelled, except soybean, subgroup 6C, except pea, blackeyed, seed and pea, southern, seed
Pea and bean, succulent shelled, subgroup 6B
Pea, blackeyed, seed
Pea, southern, seed
Peanut
Peanut, hay
Peanut, oil
Peppermint, tops
Pineapple
Plum, prune, fresh
Pomegranate
Poultry, fat
Poultry, meat
Pulasan
Rambutan
Sapodilla
Sapote, black
Sapote, mamey

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2.0
0.60
7.0
30
3.0
6.0
0.6
0.50
0.02
0.60
30
100
15
0.05
0.20
125
0.05
125
30
0.05
60
35
2.0
0.5
0.60
8.0
0.4
3.0
2.0
1.0
3.0
0.50
0.02
120
1.5
18.0
30.0
0.4
400
0.1
0.02
0.50
0.02
0.60
0.4
25
30
2.0
2.0
0.6
0.10
0.10
5.0
0.6
0.4
0.50
0.2
4.0
4.0
0.02
55.0
0.04
7.0
0.70
0.30
0.6
0.02
0.02
2.0
2.0
0.6
0.6
0.6

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Sheep, fat
Sheep, meat
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Sorghum, sweet, forage
Sorghum, sweet, grain
Sorghum, sweet, stalk
Sorghum, sweet, stover
Soursop
Soybean, aspirated grain fractions
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Spanish lime
Spearmint, tops
Star apple
Starfruit
Sugar apple
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, except soybean, subgroup 7A
Vegetable, fruiting, group 8-10
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root, except sugar beet, Subgroup 1B
Vegetable, tuberous and corm, except potato, subgroup 1D
Wax jambu

0.50
0.02
15
6.0
20
15
6.0
15
20
0.60
160
30
80
2.0
1.0
2.0
7.0
0.6
0.4
0.60
30
0.3
35
2.0
30
1.5
0.90
0.02
0.4

(2) Tolerances are established for residues of the insecticide methoxyfenozide, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only the sum of methoxyfenozide [3-methoxy-2-methylbenzoic acid
2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide] and its glucuronide metabolite (β-D-Glucopyranuronic acid,
3-[[2-(1,1-dimethylethyl)-2-(3,5-dimethylbenzoyl)-hydrazino]carbonyl]-2-methylphenyl-), calculated as the stoichiometric
equivalent of methoxyfenozide.
Commodity

Parts per million

Cattle, liver
Cattle, meat byproducts, except liver
Egg
Goat, liver
Goat, meat byproducts, except liver
Hog, liver
Hog, meat byproducts, except liver
Horse, liver
Horse, meat byproducts, except liver
Poultry, liver
Poultry, meat byproducts, except liver
Sheep, liver
Sheep, meat byproducts, except liver

0.40
0.10
0.02
0.40
0.10
0.1
0.02
0.40
0.10
0.10
0.02
0.40
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent tolerances. (1) Tolerances are established for the indirect or inadvertent residues of the
insecticide methoxyfenozide, including its metabolites and degradates, in or on the raw agricultural commodities in the
following table, when present therein as a result of the application of methoxyfenozide to growing crops as listed in
paragraph (a) of this section. Compliance with the tolerance levels specified in the following table is to be determined by
measuring only methoxyfenozide [3-methoxy-2-methylbenzoic acid 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl)
hydrazide].
Commodity

Parts per
million

Onion, bulb, subgroup 3-07A
Potato

0.10
0.02

(2) Tolerances are established for the indirect or inadvertent residues of the insecticide methoxyfenozide, including its
metabolites and degradates, in or on the raw agricultural commodities in the following table, when present therein as a
result of the application of methoxyfenozide to growing crops as listed in paragraph (a) of this section. Compliance with the

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tolerance levels specified in the following table is to be determined by measuring only the sum of methoxyfenozide
[3-methoxy-2-methylbenzoic acid, 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide] and the following metabolites
(all calculated as the stoichiometric equivalent of methoxyfenozide): free phenol of methoxyfenozide [3,5-dimethylbenzoic
acid N-tert-butyl-N′-(3-hydroxy-2-methylbenzoyl) hydrazide], the glucose conjugate of the phenol [3,5-dimethyl benzoic
acid N-tert-butyl-N′-[3 (β-D-glucopyranosyloxy)-2-methylbenzoyl]-hydrazide] and the malonylglycosyl conjugate of the
phenol [3,5-dimethyl benzoic acid N-tert-butyl-N′-[3 (β-D-6-malonyl-glucopyranosyl-1-oxy)-2-methylbenzoyl]-hydrazide].
Parts per
million

Commodity
Animal feed, nongrass, group 18, straw
Grain, cereal, forage, fodder and straw group 16, except corn
Rapeseed subgroup 20A
Spice subgroup 19B
Sunflower subgroup 20B

8.0
6.0
1.0
4.5
1.0

[67 FR 59203, Sept. 20, 2002, as amended at 68 FR 32389, May 30, 2003; 68 FR 37765, June 25, 2003; 69 FR 58097, Sept. 29,
2004; 70 FR 7047, Feb. 10, 2005; 70 FR 51604, Aug. 31, 2005; 70 FR 75739, Dec. 21, 2005; 71 FR 32853, June 7, 2006; 73 FR
11826, Mar. 5, 2008; 74 FR 22468, May 13, 2009; 74 FR 45335, Sept. 2, 2009; 76 FR 34886, June 15, 2011; 77 FR 40812, July 11,
2012; 78 FR 60714, Oct. 2, 2013; 79 FR 51106, Aug. 27, 2014; 80 FR 65968, Oct. 28, 2015]

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§180.545 Prallethrin; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide prallethrin, including its metabolites and
degradates, in or on all raw agricultural commodities and processed food from use of prallethrin in food handling
establishments where food and food products are held, processed, prepared and/or served, or as a wide-area mosquito
adulticide at 1.0 part per million (ppm). Compliance with the tolerance level specified is to be determined by measuring
only prallethrin, 2-methyl-4-oxo-3-(2-propyn-1-yl)-2-cyclopenten-1-yl-2,2-dimethyl-3-(2-methyl-1-propen-1-yl)
cyclopropanecarboxylate.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[79 FR 64330, Oct. 29, 2014]

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§180.546 Mefenoxam; tolerances for residues.
(a) General. Tolerances are established for residues of mefenoxam, including its metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only metalaxyl (methyl N-(2,6-dimethylphenyl)-N-(methoxyacetyl)-DL-alaninate).
Commodity

Parts per million

Artichoke, globe
Atemoya
Bean, snap, succulent
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Custard apple
Herbs, dried
Herbs, fresh
Kiwifruit
Mango
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Papaya
Sapodilla
Sapote, black
Sapote, mamey
Spinach
Star apple
Starfruit
Sugar apple

0.05
0.20
0.20
2.0
0.70
0.40
0.20
55
8.0
0.10
0.40
3.0
10
0.40
0.40
0.40
0.40
10
0.40
0.20
0.20

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[65 FR 57556, Sept. 25, 2000, as amended at 66 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, 2002; 76 FR 4548, Jan. 26,
2011]

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§180.547 Prohexadione calcium; tolerances for residues.
(a) General. Tolerances are established for residues of the growth regulator, prohexadione calcium, including its
metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only prohexadione calcium (calcium 3-oxido-5-oxo-4-propionylcyclohex-3enecarboxylate)” in or on the following commodities.
Parts per
million

Commodity
Cattle, kidney
Cattle, meat byproducts, except kidney
Cherry, sweet
Fruit, pome, group 11
Goat, kidney
Goat, meat byproducts, except kidney
Grass, forage1

0.10
0.05
0.40
3.0
0.10
0.05
0.10

Grass, hay1

0.10
3.5

Grass, seed screenings1
Grass, straw1
Hog, kidney
Hog, meat byproducts, except kidney
Horse, kidney
Horse, meat byproducts, except kidney
Peanut
Peanut, hay
Sheep, kidney
Sheep, meat byproducts, except kidney
Strawberry
Watercress

1.2
0.10
0.05
0.10
0.05
1.0
0.60
0.10
0.05
0.30
4.0

1

Registration is limited to grass grown for seed.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 25660, May 3, 2000, as amended at 66 FR 29712, June 1, 2001; 76 FR 71464, Nov. 18, 2011; 80 FR 38980, July 8, 2015]

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§180.548 Tralkoxydim; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide, tralkoxydim, 2-Cyclohexen-1-one,
2-[1-(ethoxyimino)propyl]-3-hydroxy-5-(2,4,6-trimethylphenyl)-(9Cl) in or on the raw agricultural commodities:
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.02
0.02
0.05
0.05
0.02
0.02
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[63 FR 69199, Dec. 16, 1998, as amended at 68 FR 48302, Aug. 13, 2003; 70 FR 70739, Nov. 23, 2005]

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§180.549 Diflufenzopyr; tolerances for residues.
(a) General. Tolerances are established for combined residues of diflufenzopyr, 2-(1-[([3,5-difluorophenylamino]
carbonyl)hydrazono]ethyl)-3- pyridinecarboxylic acid, and its metabolites convertible to 8- methylpyrido[2,3-d]pyridazin-5
(6H)-one, expressed as diflufenzopyr, in or on the following raw agricultural commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Grass, forage
Grass, hay

0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
22.0
7.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 4308, Jan. 28, 1999, as amended at 67 FR 55338, Aug. 29, 2002; 76 FR 34886, June 15, 2011]

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§180.551 Fluthiacet-methyl; tolerances for residues.
(a) General. (1) A tolerance is established for residues of the herbicide, fluthiacet-methyl, acetic acid [[2-chloro-4fluoro-5-[(tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]-methyl ester, in or on the
food commodity:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Soybean, seed

0.050
0.010
0.050
0.010
0.050
0.050
0.010
0.050
0.01

(2) A tolerance is established for the combined residues of the herbicide fluthiacet-methyland its acid metabolite:
acetic acid, [[2-chloro-4-fluoro-5-[tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]
-methyl ester, and its acid metabolite, acetic acid, [[2-chloro-4-fluoro-5-[(tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]
pyridazin-1-ylidene)amino]phenyl]thio]- , in or on the following food commodities:
Commodity

Parts per million

Cotton, gin byproducts
Cotton, undelinted seed

0.20
0.020

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 18357, Apr. 14, 1999, as amended at 66 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, 2006]

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§180.552 Sulfosulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide sulfosulfuron, 1-(4,6-dimethoxypyrimidin-2-yl)-3[(2-ethanesulfonyl-imidazo[1,2-a]pyridine-3-yl) sulfonyl]urea and its metabolites converted to 2-(ethylsulfonyl)-imidazo
[1,2-a]pyridine and calculated as sulfosulfuron in or on the raw agricultural commodities.

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Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Grass, forage, fodder and hay, group 17, forage
Grass, forage, fodder and hay, group 17, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.02
0.01
0.3
0.02
0.01
0.3
14
25
0.005
0.005
0.05
0.02
0.01
0.3
0.02
0.02
0.01
0.3
4.0
0.02
0.3
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 27192, May 19, 1999, as amended at 70 FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, 2007]

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§180.553 Fenhexamid; tolerances for residues.
(a) General. Tolerances are established for the residues of the fungicide fenhexamid (N-2,3-dichloro-4hydroxyphenyl)-1-methyl cyclohexanecarboxamide) in or on the following commodities:
Commodity
Almond, hulls
Almond
Asparagus
Bushberry subgroup 13B
Caneberry subgroup 13A
Cilantro, leaves
Cucumber
Fruit, stone, group 12, except plum, prune, fresh, postharvest
Ginseng
Grape
Grape, raisin
Juneberry
Kiwifruit, postharvest
Leafy greens subgroup 4A, except spinach
Lingonberry
Pear
Pepper, nonbell
Pistachio
Plum, prune, dried
Plum, prune, fresh
Pomegranate
Salal
Strawberry
Vegetable, fruiting, group 8, except nonbell pepper

Parts per million
2.0
0.02
0.02
5.0
20.0
30.0
2.0
10.0
0.3
4.0
6.0
5.0
15.0
30.0
5.0
10
0.02
0.02
2.5
1.5
2.0
5.0
3.0
2.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[64 FR 28924, May 28, 1999, as amended at 65 FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, 2000; 67 FR 19120, Apr. 18,
2002; 68 FR 2247, Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006; 73 FR
19154, Apr. 9, 2008]

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§180.554 Kresoxim-methyl; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of the fungicide kresoxim-methyl (methyl (E)
-2-[2-(2-methylphenoxy)-methyl]phenyl-2-(methoxyimido)acetate) and its metabolites as follows: (E)
-2-[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid; (E)-2-[2-(2-hydroxymethylphenoxy)methyl]-phenyl2-(methoxyimido)acetic acid (free and glucose conjugated); and (E)-2-[2-(4-hydroxy-2-methylphenoxy)-methyl]phenyl2-(methoxyimido)acetic acid (free and glucose conjugated) in or on the following commodities:
Commodity

Parts per million

Apple, dry pomace
Apple, wet pomace
Fruit, pome
Grape
Grape, raisin
Pecan
Vegetable, cucurbit, group 9

1.0
1.0
0.5
1.0
1.5
0.15
0.40

(2) Tolerances are established in or on the following commodities for the residues of the metabolite (E)
-2-[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid resulting from the use of the fungicide kresoximmethyl:
Commodity

Parts per million

Cattle, meat byproducts
Goat, meat byproducts
Sheep, meat byproducts

0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 31136, June 10, 1999, as amended at 71 FR 50359, Aug. 25, 2006; 74 FR 46377, Sept. 9, 2009]

Back to Top
§180.555 Trifloxystrobin; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of trifloxystrobin, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of trifloxystrobin, benzeneacetic acid, (E,E)-α-(methoxyimino)-2-[[[[1-[3-(trifluoromethyl) phenyl]
ethylidene] amino]oxy]methyl]-, methyl ester, and the free form of its acid metabolite CGA-321113, (E,E)
-methoxyimino-[2-[1-(3-trifluoromethyl-phenyl)-ethylideneaminooxymethyl]-phenyl]acetic acid, calculated as the
stoichiometric equivalent of trifloxystrobin, in or on the commodity.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple, wet pomace
Artichoke, globe
Asparagus
Banana1
Barley, grain
Barley, hay
Barley, straw
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Beet, sugar, tops
Canistel
Cattle, fat
Cattle, meat

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0.01
0.01
9.0
5.0
1.0
0.07
0.10
0.05
0.3
5.0
0.4
0.2
0.1
4.0
0.7
0.1
0.1

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Cattle, meat byproducts
Citrus, dried pulp
Citrus, oil
Coffee, green bean2
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, field, refined oil
Corn, pop, grain
Corn, pop, stover
Corn, sweet, cannery waste
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Egg
Fruit, citrus, group 10
Fruit, pome
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grape
Grape, raisin
Grass, forage
Grass, hay
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Leaf petioles subgroup 4B
Mango
Milk
Nut, tree, group 14
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Papaya
Pea, dry, seed
Pea, field, hay
Pea, field, vines
Peanut, hay
Peanut
Pistachio
Potato
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Radish, tops
Rice, grain
Rice, hulls
Rice, straw
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, seed
Star apple
Strawberry
Vegetable, cucurbit, group 9
Vegetable, fruiting
Vegetable, root, except sugar beet, subgroup 1B
Wheat, bran
Wheat, forage
Wheat, grain

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0.1
1.0
38
0.02
6.0
0.05
7
0.1
0.05
7
0.6
7.0
0.04
4.0
0.04
0.6
0.5
2
0.1
0.1
0.1
5.0
2.0
5.0
12
17
0.05
0.05
0.05
11.0
0.1
0.1
0.1
3.5
0.7
0.02
0.04
0.3
0.05
0.3
5.0
0.7
0.06
15
4
4.0
0.05
0.04
0.04
0.04
0.04
0.04
10
3.5
8
7.5
0.7
0.7
0.7
0.1
0.1
0.1
10.0
25.0
0.08
0.7
1.1
0.50
0.5
0.1
0.15
0.3
0.05

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Wheat, hay
Wheat, straw
1

0.2
5.0

There are no U.S. registrations as of September 27, 1999 for use on banana.

2

There are no U.S. registrations as of January 18, 2012 for use on coffee, green bean.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[64 FR 51907, Sept. 27, 1999]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.555, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.556 Pymetrozine; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide pymetrozine 1,2,4-triazin-3(2H)
-one,4,5-dihydro-6-methyl-4-[(3-pyridinylmethylene) amino] in or on the following raw agricultural commodities. The
tolerance level for each commodity is expressed in terms of the parent insecticide only, which serves as an indicator of the
use of pymetrozine on these raw agricultural commodities.
Commodity

Parts per million

Asparagus
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Cotton, gin byproducts
Cotton, undelinted seed
Hop, dried cones
Pecan
Turnip, greens
Vegetable, fruiting, group 8
Vegetable, cucurbit, group 9
Vegetable, leafy, execpt brassica, group 4
Vegetable, tuberous and corm, subgroup 1C

0.04
0.5
0.25
2.0
0.3
6.0
0.02
0.25
0.2
0.1
0.6
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 48634, Aug. 9, 2000, as amended at 66 FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, 2001; 70 FR 7047, Feb. 10, 2005;
70 FR 43298, July 27, 2005]

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§180.557 Tetraconazole; tolerances for residues.
(a) General. Tolerances are established for residues of tetraconazole, including its metabolites and degradates, in or
on the commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only
tetraconazole (1-[2-(2,4-dichlorophenyl)-3-(1,1,2,2-tetrafluoroethoxy)propyl]-1H-1,2,4-triazole), in or on the following
commodities.
Commodity

Parts per million

Aspirated grain fractions
Beet sugar, dried pulp
Beet sugar, molasses
Beet sugar, root
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts (except liver)
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

1.0
0.15
0.15
0.05
0.15
1.50
0.01
0.15
1.1
0.01
1.7
0.01

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Corn, pop, stover
Eggs
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts (except liver)
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts (except liver)
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts (except liver)
Low growing berry subgroup 13-07G, except cranberry
Milk
Milk, fat
Peanut
Peanut, oil
Pecan
Poultry, fat
Poultry, meat
Poultry meat byproducts
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts (except liver)
Small fruit vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Soybean, refined oil
Soybean, seed

1.7
0.02
0.15
1.50
0.01
0.15
0.01
0.05
0.01
0.01
0.15
1.50
0.01
0.15
0.25
0.03
0.75
0.03
0.10
0.04
0.05
0.01
0.05
0.15
1.50
0.01
0.15
0.20
0.80
0.15

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[70 FR 20830, Apr. 22, 2005, as amended at 70 FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, 2007; 73 FR 67406, Nov. 14, 2008;
76 FR 53648, Aug. 29, 2011]

Back to Top
§180.559 Clodinafop-propargyl; tolerances for residues.
(a) General. Tolerances are established for clodinafop-propargyl, including its metabolites and degradates, in or on
the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only clodinafop-propargyl [(2R)-2-[4-[(5-chloro-3-fluoro-2-pyridinyl)oxy]phenoxy]propanoic acid,
2-propynyl ester] and its metabolite clodinafop [(2R)-2-[4-[(5-chloro-3-fluoro-2- pyridinyl)oxy]phenoxy]propanoic acid].
Commodity

Parts per million

Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.1
0.02
0.1
0.5

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 38774, June 22, 2000, as amended at 77 FR 72226, Dec. 5, 2012]

Back to Top
§180.560 Cloquintocet-mexyl; tolerances for residues.
(a) General. Tolerances are established for the combined residues of cloquintocet-mexyl, (acetic acid [(5-chloro-8quinolinyl)oxy]-,1-methylhexyl ester; CAS Reg. No. 99607-70-2) and its acid metabolite (5-chloro-8-quinolinoxyacetic
acid), when used as an inert ingredient (safener) in pesticide formulations containing the active ingredients clodinafoppropargyl (wheat only), dicamba (wheat only), flucarbazone-sodium (wheat only), pinoxaden (wheat or barley), or
pyroxsulum (wheat only) in or on the following food commodities:

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Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.1
0.1
0.1
0.2
0.1
0.5
0.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 38764, June 22, 2000, as amended at 70 FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, 2008; 75 FR 16020, Mar. 31,
2010; 76 FR 38035, June 29, 2011]

Back to Top
§180.561 Acibenzolar-S-methyl; tolerances for residues.
(a) General. (1) Tolerances are established for residues of acibenzolar-S-methyl, benzo(1,2,3)thiadiazole-7carbothioic acid-S-methyl ester, including its metabolites and degradates, in or on the commodities in the table below.
Compliance with the tolerance levels specified below is to be determined by measuring only those acibenzolar-S-methyl
residues convertible to benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA-210007), expressed as the stoichiometric
equivalent of acibenzolar-S-methyl, in or on the following raw agricultural commodities.
Commodity

Parts per million
0.1

Banana1
Berry, low growing, subgroup 13-07G
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Onion, bulb, subgroup 3-07A
Spinach
Tomato, paste
Vegetable, brassica, leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, group 4

0.15
0.02
0.03
0.1
1.0
3.0
1.0
2.0
1.0
0.25

1

There are no United States registrations for banana.

(2) Tolerances are established for residues of acibenzolar- S -methyl, benzo(1,2,3)thiadiazole-7-carbothioic acid- S
-methyl ester, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the
tolerance levels specified below is to be determined by measuring only those acibenzolar- S -methyl residues convertible
to benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA-210007), expressed as the Stoichiometric equivalent of acibenzolar- S
-methyl, in or on the following raw agricultural commodities.
Commodity

Parts per million

Apple
Grapefruit
Pear

Expiration/revocation date
0.05
0.05
0.05

12/31/15
12/31/15
12/31/15

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 50446, Aug. 18, 2000, as amended at 70 FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, 2006; 74 FR 24710, May 26, 2009;
76 FR 34886, June 15, 2011; 77 FR 21676, Apr. 11, 2012; 77 FR 30406, May 23, 2012; 80 FR 58620, Sept. 30, 2015]

Back to Top
§180.562 Flucarbazone-sodium; tolerances for residues.
(a) General. Tolerances are established for combined residues of the herbicide flucarbazone-sodium, 4,5-dihydro-3methoxy-4-methyl-5-oxo-N-[[2(trifluoromethoxy)phenyl] sulfonyl]-1H-1,2,4-triazole 1-carboxamide, sodium salt) and its
N-desmethyl metabolite; and its metabolites converted to 2-(trifluoromethoxy)benzene sulfonamide and calculated as
flucarbazone-sodium in or on the following food commodities:

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Commodity

Parts per million

Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

1.50
0.01
0.01
1.50
0.01
0.01
1.50
0.01
0.01
1.50
0.01
0.01
0.005
1.50
0.01
0.01
0.30
0.01
0.10
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[70 FR 67915, Nov. 9, 2005, as amended at 71 FR 76931, Dec. 22, 2006]

Back to Top
§180.563 Ethametsulfuron-methyl; tolerances for residues.
(a) General. A tolerance is established for residues of ethametsulfuron methyl (methyl 2- ((((4-ethoxy-6(methylamino)-1,3,5- triazin-2-yl) amino) carbonyl) amino) sulfonyl) benzoate) in or on the following raw agricultural
commodities.
Commodity

Parts per million

Canola, seed
Crambe, seed
Rapeseed, seed

0.02
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect of inadvertent residues. [Reserved]
[65 FR 57972, Sept. 27, 2000, as amended at 66 FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, 2002]

Back to Top
§180.564 Indoxacarb; tolerances for residues.
(a) General. (1) Tolerances are established for residues of indoxacarb, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only indoxacarb, (S)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]
carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate, and its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate.
Commodity
Apple, wet pomace
Alfalfa, forage
Alfalfa, hay
Bean, dry, seed
Bean, succulent
Beet, garden, roots
Beet, garden, tops
Berry, low growing, except strawberry, subgroup 13-07H
Bushberry subgroup 13-07B
Cattle, fat

Parts per million

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

3.0
10
50
0.2
0.9
0.30
6.0
1
1.5
1.5

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Cattle, meat
Cattle, meat byproducts
Corn, sweet, forage
Corn, sweet, kernel plus cob with husk removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Cowpea, forage
Cowpea, hay
Fruit, pome, except pear, group 11
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grape, raisin
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Milk, fat
Okra
Pea, southern, seed
Peanut
Peanut, hay
Pear
Pear, oriental
Peppermint, tops
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, hulls
Soybean, seed
Spearmint, tops
Turnip, greens
Vegetable, Brassica, leafy, group 5
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except Brassica, group 4
Vegetable, tuberous and corm, subgroup 1-C

0.05
0.03
10
0.02
15
15
2.0
50
100
1.0
2
0.90
1.5
0.05
0.03
45
5.0
1.5
0.05
0.03
1.5
0.05
0.03
0.15
4.0
0.50
0.10
0.01
40
0.20
0.20
11
1.5
0.05
0.03
4.0
0.80
11
12
12
0.60
0.50
14
0.01

(2) Tolerances are established for residues of indoxacarb, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of indoxacarb, (S)-methyl-7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)-phenyl]amino]
carbonyl]indeno[1,2e] [1,3,4]oxadiazine-4a(3H)-carboxylate, its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2[[(methoxycarbonyl)[4-(trifluoromethoxy) phenyl]amino]carbonyl]indeno [1,2-e] [1,3,4] oxadiazine-4a(3H)-carboxylate, and
the metabolites: IN-JT333, methyl 7-chloro-2,5-dihydro-2-[[[4-(trifluoromethoxy)phenyl]-amino]carbonyl]indeno[1,2-e][1,3,4]
oxadiazine-4a(3H)-carboxylate; IN-KT319, (E)-methyl 5-chloro-2,3,-dihydro-2-hydroxy-1-[[[(methoxycarbonyl)
[4-(trifluoromethoxy)phenyl]amino]-carbonyl]hydrazono]-1H-indene-2-carboxylate; IN-JU873, methyl 5-chloro-2,3-dihydro2-hydroxy-1-[[[[4-(triflurormethoxy)-phenyl]amino]carbonyl]hydrazono]-1H-indene-2-carboxylate; IN-KG433, methyl
5-chloro-2,3,-dihydro-2-hydroxy-1-[[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]-hydrazono]-1H-indene2-carboxylate; and IN-KB687, methyl [4-(trifluoromethoxy)phenyl]carbamate, calculated as the stoichiometric equivalent of
indoxacarb in the commodity.
Commodity

Parts per million

Egg
Poultry, fat
Poultry, meat
Poultry, meat byproducts

0.20
0.20
0.06
0.06

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 58424, Sept. 29, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 47309, July 18, 2002; 67 FR 58730, Sept. 18,
2002; 68 FR 25830, May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR 28842, May 19, 2004; 69 FR 29459, May 24, 2004; 69 FR
32282, June 9, 2004; 72 FR 37641, July 11, 2007; 74 FR 33165, July 10, 2009; 77 FR 8749, Feb. 15, 2012; 78 FR 78738, Dec. 27,
2013]

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Back to Top
§180.565 Thiamethoxam; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide thiamethoxam, including its metabolites and
degradates, in or on the following commodities. Compliance with the tolerance levels specified below is to be determined
by measuring only thiamethoxam 3-[(2-chloro-5-thiazolyl)methyl]tetrahydro-5-methyl-N-nitro-4H-1,3,5-oxadiazin-4-imine
and its metabolite CGA-322704 N-[(2-chloro-thiazol-5-yl)methyl]-N′-methyl-N″-nitro-guanidine, calculated as the
stoichiometric equivalent of thiamethoxam, in or on the following commodities:

Commodity
Alfalfa, forage
Alfalfa, hay
Almond, hulls
Artichoke, globe
Avocado
Barley, grain
Barley, hay
Barley, straw
Bean, succulent
Berry, low growing, subgroup 13-07G, except cranberry
Borage, seed
Brassica, head and stem, subgroup 5-A
Brassica, leafy greens, subgroup 5-B
Buckwheat, forage
Buckwheat, hay
Buckwheat, straw
Bushberry subgroup 13-07B, except lingonberry and blueberry, lowbush
Caneberry subgroup 13-07A
Canistel
Canola, seed
Cattle, meat
Cattle, meat byproducts
Citrus, dried pulp
Coffee, green, bean1
Corn, field, forage
Corn, field, stover
Corn, pop, forage
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Crambe, seed
Cranberry
Flax, seed
Food commodities and feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling
establishments
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit
Fruit, stone, group 12
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grain, cereal, group 15, except barley
Grape, raisin
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, meat
Horse, meat byproducts
Mango
Milk
Millet, pearl, forage
Millet, pearl, stover
Millet, proso, forage
Millet, proso, stover
Millet, proso, straw
Mustard, seed

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

Parts
per
million
0.05
0.12
1.2
0.45
0.40
0.4
0.40
0.40
0.02
0.30
0.02
4.5
3.0
0.50
0.02
0.02
0.20
0.35
0.40
0.02
0.02
0.04
0.60
0.20
0.10
0.05
0.10
0.05
0.10
0.02
0.05
1.5
0.10
0.02
0.02
0.02
0.02
0.40
0.2
0.20
0.5
0.02
0.04
2.0
0.02
0.30
0.02
0.02
0.10
0.02
0.04
0.40
0.02
0.02
0.02
0.02
0.02
0.02
0.02

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Nut, tree, group 14
Oat, forage
Oat, hay
Oat, straw
Onion, dry bulb
Papaya
Peanut
Peanut, hay
Peanut, meal
Peppermint, tops
Pistachio
Potato
Radish, tops
Rapeseed, seed
Rye, forage
Rye, straw
Safflower, seed
Sapodilla
Sapote, black
Sapote, mamey
Sheep, meat
Sheep, meat byproducts
Sorghum, forage
Sorghum, grain, stover
Soybean, hulls
Spearmint, tops
Star apple
Sunflower

0.02
0.50
0.02
0.02
0.03
0.40
0.05
0.25
0.15
1.5
0.02
0.25
0.80
0.02
0.50
0.02
0.02
0.40
0.40
0.40
0.02
0.04
0.02
0.02
0.08
1.5
0.40
0.02
20

Tea, dried1
Tomato, paste
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, legume, group 6
Vegetable, root, subgroup 1A
Vegetable, tuberous and corm, except potato, subgroup 1D
Wheat, forage
Wheat, hay
Wheat, straw

0.80
0.2
0.25
4.0
0.02
0.05
0.02
0.50
0.02
0.02

1

There are no U.S. registrations as of March 27, 2013.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[65 FR 79762, Dec. 20, 2000]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.565, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.566 Fenpyroximate; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to
be determined by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate and its Z-isomer, (Z)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as the stoichiometric equivalent of
fenpyroximate.
Commodity

Parts per million

Almond, hulls
Avocado
Bean, snap, succulent
Berry, low growing, subgroup 13-07G
Canistel
Citrus, dried pulp
Citrus, oil

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

3.0
0.15
0.40
1.0
0.15
2.5
10

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Corn, field, forage
Corn, field, grain
Corn, field, refined oil
Corn, field, stover
Corn, pop, forage
Corn, pop, grain
Corn, pop, stover
Cotton, gin byproducts
Cotton, undelinted seed
Cucumber
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12-12
Grain, aspirated fractions
Hop, dried cones
Mango
Melon subgroup 9A
Nut, tree, group 14
Papaya
Peppermint, tops
Pistachio
Sapodilla
Sapote, black
Sapote, mamey
Spearmint, tops
Star, apple

2.0
0.02
0.05
7.0
2.0
0.02
7.0
10
0.10
0.40
0.50
0.30
1.0
2.0
0.40
10
0.15
0.10
0.10
0.15
7.0
0.10
0.15
0.15
0.15
7.0
0.15
20

Tea, dried1
Vegetable, fruiting, group 8-10
Vegetable, tuberous and corm, subgroup 1C

0.20
0.10

1

There are no U.S. Registrations.

(2) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and degradates,
in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined
by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)
methylene]amino]oxy]methyl]benzoate and its metabolites (E)-4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)
-methyleneaminooxymethyl]benzoic acid and (E)-1,1-dimethylethyl-2-hydroxyethyl 4-[[[[(1,3-dimethyl-5-phenoxy1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as the stoichiometric equivalent of fenpyroximate.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Goat, fat
Goat, meat
Goat, meat byproducts, except kidney and liver
Horse, fat
Horse, meat
Horse, meat byproducts, except kidney and liver
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts, except kidney and liver

0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.015
0.03
0.03
0.03

(3) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and degradates,
in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined
by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)
methylene]amino]oxy]methyl]benzoate and its metabolite (E)-4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)
-methyleneaminooxymethyl]benzoic acid, calculated as the stoichiometric equivalent of fenpyroximate.
Commodity

Parts per million

Cattle, kidney
Cattle, liver
Goat, kidney
Goat, liver
Horse, kidney
Horse, liver
Sheep, kidney
Sheep, liver

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25

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(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide
fenpyroximate, including its metabolites and degradates in or on the commodities in the table below. Compliance with the
tolerance levels specified in the table is to be determined by measuring only the sum of fenpyroximate, (E)
-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl) methylene]amino]oxy]methyl]benzoate and its Z-isomer,
(Z)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as
the stoichiometric equivalent of fenpyroximate.
Commodity

Parts per million

Honey

Expiration/revocation date
0.10

12/31/13

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 18568, Apr. 10, 2001, as amended at 69 FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, 2006; 72 FR 26321, May 9, 2007;
74 FR 37617, July 29, 2009; 74 FR 63079, Dec. 2, 2009; 75 FR 80346, Dec. 22, 2010; 77 FR 73951, Dec. 12, 2012; 78 FR 36097,
June 17, 2013]

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§180.567 Zoxamide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of zoxamide including metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only zoxamide (3,5-dichloro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)-4-methylbenzamide).
Commodity

Parts per million

Grape
Grape, raisin
Tomato
Vegetable, cucurbit, group 9

3.0
15.0
2.0
1.0

(2) Tolerances are established for residues of zoxamide including metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of zoxamide (3,5-dichloro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)-4-methylbenzamide) and its metabolites
3,5-dichloro-1,4-benzenedicarboxylic acid (RH-1455 and RH-141455) and 3,5-dichloro-4-hydroxymethylbenzoic acid (RH1452 and RH-141452) calculated as the stoichiometric equivalent of zoxamide.
Commodity

Parts per million

Onion, bulb, subgroup 3-07A
Potato
Potato, granules/flakes
Potato, wet peel

0.7
0.060
0.30
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 18733, Apr. 11, 2001, as amended at 66 FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, 2004; 71 FR 31104, June 1,
2006; 71 FR 76200, Dec. 20, 2006; 75 FR 770, Jan. 6, 2010; 79 FR 41915, July 18, 2014]

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§180.568 Flumioxazin; tolerances for residues.
(a) General. Tolerances are established for residues of flumioxazin, 2-[7-fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)
-2H-1,4-benzoxazin-6-yl]-4,5,6,7-tetrahydro-1H-isoindole-1,3(2H)-dione, including its metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only flumioxazin.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Artichoke, globe
Asparagus
Bushberry subgroup 13-07B
Cabbage
Cabbage, Chinese, napa

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3.0
8.0
0.70
0.02
0.02
0.02
0.02
0.02

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Corn, field, forage
Corn, field, grain
Corn, field, stover
Cotton, gin byproducts
Cotton, undelinted seed
Fish, freshwater
Fruit, pome, group 11
Fruit, stone, group 12
Garlic
Grain, aspirated fractions
Grape
Hop, dried cones
Leaf petioles subgroup 4B
Nut, tree, group 14
Okra
Olive
Onion, bulb
Pea and bean, dried shelled, except soybean, subgroup 6C
Peanut
Peppermint, tops
Pistachio
Pomegranate
Prickly pear, fruit
Prickly pear, pads
Rapeseed subgroup 20A
Shallot, bulb
Soybean, seed
Spearmint, tops
Strawberry
Sugarcane, cane
Sunflower subgroup 20B
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, tuberous and corm, subgroup 1C
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.02
0.02
0.02
0.60
0.02
1.5
0.02
0.02
0.02
100
0.02
0.05
0.02
0.02
0.02
0.02
0.02
0.07
0.02
0.04
0.02
0.02
0.07
0.06
0.40
0.02
0.02
0.04
0.07
0.20
0.50
0.03
0.02
0.02
0.02
0.40
0.02
6.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 19878, Apr. 18, 2001, as amended at 68 FR 51471, Aug. 27, 2003; 69 FR 16831, Mar. 31, 2004; 69 FR 52198, Aug. 25,
2004; 71 FR 25956, May 3, 2006; 71 FR 61413, Oct. 18, 2006; 73 FR 11831, Mar. 5, 2008; 73 FR 39251, July 9, 2008; 75 FR 8265,
Feb. 24, 2010; 75 FR 69009, Nov. 10, 2010; 77 FR 58499, Sept. 21, 2012; 78 FR 20466, Apr. 5, 2013]

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§180.569 Forchlorfenuron; tolerances for residues.
(a) General. (1) Tolerances are established for residues of forchlorfenuron, including its metabolites and degradates,
in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only forchlorfenuron (N-(2-chloro-4-pyridinyl)-N-phenylurea).
Commodity

Parts per
million

Almond
Almond, hulls
Bushberry subgroup 13-07B
Cherry, sweet
Fig
Grape
Grape, raisin
Kiwifruit
Pear
Pistachio
Plum, prune, fresh

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.01
0.15
0.01
0.01
0.01
0.03
0.06
0.04
0.01
0.01
0.01

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(2) Temporary tolerances are established for residues of forchlorfenuron, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring on forchlorfenuron (N-(2-chloro-4-pyridinyl)-N′-phenylurea).
Expiration/
revocation
date

Parts per
million

Commodity
Almond
Almond, hulls
Cherry, sweet
Fig
Pear
Pistachio
Plum, prune, fresh

0.01
0.15
0.01
0.01
0.01
0.01
0.01

12/31/15
12/31/15
12/31/15
12/31/15
12/31/15
12/31/15
12/31/15

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional restrictions. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 22936, May 7, 2001, as amended at 69 FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, 2004; 73 FR 47846, Aug. 15,
2008; 78 FR 46283, July 31, 2013; 79 FR 18471, Apr. 2, 2014]

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§180.570 Isoxadifen-ethyl; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. (1) Tolerances are established for residues of isoxadifen-ethyl (ethyl 5,5-diphenyl-2-isoxazoline-3carboxylate, (CAS No. 163520-33-0), and its metabolite: 4,5-dihydro-5,5-diphenyl-3-isoxazolecarboxylic acid, when used
as an inert ingredient (safener) in or on the following raw agricultural commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, oil
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husk removed
Corn, sweet, stover

0.20
0.08
0.40
0.50
0.04
0.25
0.30
0.04
0.45

(2) Tolerances are established for the residues of isoxadifen-ethyl (3-isoxazolecarboxylic acid,
4,5-dihydro-5,5-diphenyl-, ethyl ester (CAS No. 164520-33-0)), and its metabolites 4,5-dihydro-5,5-diphenyl-3isoxazolecarboxylic acid and β-hydroxy-β-benzenepropanenitrile when used as an inert ingredient (safener) in or on the
following raw agricultural commodities:
Commodity

Parts per million

Rice, grain
Rice, hulls
Rice, straw

0.10
0.50
0.25

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 33187, June 21, 2001, as amended at 66 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, 2002; 69 FR 29890, May 26, 2004;
72 FR 63997, Nov. 14, 2007]

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§180.571 Mesotrione; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide mesotrione, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only mesotrione, 2-[4-(methylsulfonyl)-2-nitrobenzoyl]-1,3-cyclohexanedione, in or on the
following raw agricultural commodities:

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Commodity

Parts per million

Almond, hulls
Asparagus
Berry, group 13
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cranberry
Flax, seed
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, stone, group 12-12
Grass, forage
Grass, hay
Grass, seed screenings
Grass, straw
Lingonberry
Millet, forage
Millet, grain
Millet, hay
Millet, straw
Nut, tree, group 14-12
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Okra
Rhubarb
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Sorghum, sweet
Soybean, seed
Sugarcane, cane

0.02
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.5
0.01
1.5
0.02
0.01
0.01
0.01
0.01
0.01
0.01
0.10
0.10
0.01
0.01
0.01
0.02
0.02
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 33195, June 21, 2001, as amended at 67 FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; 69 FR 58310, Sept. 30, 2004;
70 FR 14551, Mar. 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Jan. 9, 2008; 73 FR 9226, Feb. 20, 2008; 74 FR 67123,
Dec. 18, 2009; 76 FR 34886, June 15, 2011; 80 FR 30630, May 29, 2015]

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§180.572 Bifenazate; tolerance for residues.
(a) General. (1) Tolerances are established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)
hydrazinecarboxylate) including its metabolites and degradates, in or on the commodities listed in the following table.
Compliance with the tolerance levels specified are to be determined by measuring only the sum of bifenazate and its
metabolite, diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester, (calculated as the stoichiometric
equivalent of bifenazate) in or on the following food commodities:
Commodity

Parts per million

Acerola
Almond, hulls
Apple, wet pomace
Atemoya
Avocado
Bean, dry seed
Berry, low-growing subgroup 13-07G
Biriba
Black sapote
Caneberry subgroup 13-07A
Canistel

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0.90
15
1.2
1.6
7.0
0.60
1.5
1.6
7.0
5.0
7.0

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Cattle, fat
Cherimoya
Cotton, gin byproducts
Cotton, undelinted seed
Custard apple
Feijoa
Fruit, pome, group 11-10
Fruit, small, vine climbing subgroup 13-07F, except fuzzy kiwifruit
Fruit, stone, group 12, except plum
Goat, fat
Grape
Grape, raisin
Guava
Herb, subgroup 19A, except chervil and chive
Hog, fat
Hop, dried cones
Horse, fat
Jaboticaba
Ilama
Longan
Lychee
Mango
Nut, tree, group 14
Okra
Papaya
Passionfruit
Pea and bean, succulent shelled, subgroup 6B
Peppermint, tops
Pistachio
Plum
Pulasan
Rambutan
Sapodilla
Sapote, mamey
Sheep, fat
Soursop
Soybean, succulent shelled
Spanish lime
Spearmint, tops
Star apple
Starfruit
Strawberry
Sugar apple
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, legume, edible-podded, subgroup 6A
Vegetable, tuberous and corm, subgroup 1C
Wax jambu

0.10
1.6
35
0.75
1.6
0.90
0.7
1.0
2.5
0.10
0.75
1.2
0.9
300
0.10
15
0.10
0.90
1.6
5.0
5.0
7.0
0.20
2.0
7.0
0.90
0.70
25
0.20
0.20
5.0
5.0
7.0
7.0
0.10
1.6
0.70
5.0
25
7.0
0.90
1.5
1.6
0.75
4.0
6.0
0.10
0.90

(2) Tolerances are established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)
hydrazinecarboxylate) including its metabolites and degradates, in or on the commodities listed in the following table.
Compliance with the tolerance levels specified are to be determined by measuring only the sum of bifenazate and its
metabolites diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester; 1,1′-biphenyl, 4-ol; and 1,1′
-biphenyl, 4-oxysulfonic acid (calculated as the stoichiometric equivalent of bifenazate) in or on the following food
commodities:
Commodity
Cattle, meat
Cattle, meat byproducts
Goat, meat
Goat, meat byproducts
Hog, meat
Hog, meat byproducts
Horse, meat
Horse, meat byproducts
Milk
Sheep, meat
Sheep, meat byproducts

Parts per million
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are
established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)hydrazinecarboxylate) including its
metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels
specified are to be determined by measuring only the sum of bifenazate and its metabolite, diazinecarboxylic acid,
2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester, (calculated as the stoichiometric equivalent of bifenazate) in or on
the following food commodities:
Parts per
million

Commodity
Timothy, forage
Timothy, hay

200
150

(d) Indirect or inadvertent residues. [Reserved]
[66 FR 34569, June 29, 2001]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.572, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.573 Tepraloxydim; tolerances for residues.
(a) General. (1) Tolerances are established for residues of tepraloxydim, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the combined residues of tepraloxydim, (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy5-(tetrahydro-2H-pyran-4-yl)-2-cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)
pentane-1,5-dioic acid) and OH-GP (3-hydroxy-3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), calculated as
tepraloxydim, in or on the commodities.
Commodity

Parts per million

Cotton, undelinted seed
Cotton, gin byproducts
Flax, seed
Grain, aspirated fraction

0.2
3.0
0.10
1200.0
0.10

Pea and bean, dried shelled, except soybean, subgroup 6C1
Soybean, seed
Soybean, hulls

6.0
8.0
0.20

Sunflower subgroup 20B1
1

There are no U.S. registrations for commodities in this subgroup.

(2) Tolerances are established for residues of tepraloxydim, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the combined residues of tepraloxydim (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro2H-pyran-4-yl)-2-cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid),
OH-GP (3-hydroxy-3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), and GL (3-(2-oxotetrahydropyran-4-yl)-1,5-dioic acid),
calculated as tepraloxydim, in or on the commodities.
Commodity

Parts per million

Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Egg
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Hog, fat
Hog, kidney
Hog, meat
Hog, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Milk
Poultry, fat
Poultry, liver
Poultry, meat

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0.15
0.50
0.20
0.20
0.20
0.15
0.50
0.20
0.20
0.15
0.50
0.20
0.20
0.15
0.50
0.20
0.20
0.10
0.30
1.00
0.20

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Poultry, meat byproducts, except liver
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney

0.20
0.15
0.50
0.20
0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established
for residues of tepraloxydim, including its metabolites and degradates, in or on the commodities in the table below.
Compliance with the tolerance levels specified below is to be determined by measuring only the combined residues of
tepraloxydim (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)-2-cyclohexen-1one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid) and OH-GP (3-hydroxy3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), calculated as tepraloxydim, in or on the commodities.
Commodity

Parts per million

Canola, seed

0.50

(d) Indirect or inadvertent residues. [Reserved]
[66 FR 40150, Aug. 2, 2001, as amended at 72 FR 54588, Sept. 26, 2007; 76 FR 34885, June 15, 2011; 76 FR 82152, Dec. 30,
2011]

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§180.574 Fluazinam; tolerances for residues.
(a) General. (1) Tolerances are established for residues of fluazinam (3-chloro-N-[3-chloro-2,6-dinitro4-(trifluoromethyl)phenyl]-5-(trifluoromethyl)-2-pyridinamine), including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only fluazinam.
Commodity
Apple
Apple, wet pomace
Bushberry subgroup 13-07B
Carrot, roots
Ginseng
Lettuce, head
Lettuce, leaf
Melon subgroup 9A
Onion, bulb, subgroup 3-07A
Pea and bean, dried shelled, except soybean, subgroup 6C, except pea
Pea and bean, succulent shelled, subgroup 6B, except pea
Peanut
Pepper/eggplant subgroup 8-10B
Potato
Soybean, seed
Soybean, hulls
Turnip, greens
Vegetable, Brassica leafy, group 5
Vegetable, legume, edible-podded, subgroup 6A, except pea

Parts per million
2.0
5.0
7.0
0.70
4.5
0.02
2.0
0.07
0.20
0.02
0.04
0.02
0.09
0.02
0.01
0.05
0.01
0.01
0.10

(2) Tolerances are established for residues of fluazinam, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only fluazinam and its metabolite AMGT (3-[[4-amino-3-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]amino]-2-nitro6-(trifluoromethyl) phenyl]thio]-2-(beta-D-glucopyranosyloxy) propionic acid).
Commodity

Parts per million

Grape, wine1
1

3.0

No US registration as of March 15, 2002.

(3) Tolerances are established for residues of fluazinam (3-chloro-N-[3-chloro-2,6-dinitro-4-(trifluoromethyl)phenyl]
-5-(trifluoromethyl)-2-pyridinamine), including its metabolites and degradates, in or on the commodities in the table below.
Compliance with the tolerance levels specified below is to be determined by measuring only fluazinam, AMPA
(2-(6-amino-3-chloro-α,α,α-trifluoro-2-nitro-p-toluidino)-3-chloro-5-(trifluoromethyl) pyridine), DAPA (3-chloro2-(2,6-diamino-3-chloro-α,α,α.-trifluoro-p-toluidino)-5-(trifluoromethyl)pyridine), and their sulfamate conjugates.
Commodity

Parts per
million

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Cattle, fat
Cattle, meat byproducts
Goat, fat
Goat, meat byproducts
Horse, fat
Horse, meat byproducts
Sheep, fat
Sheep, meat byproducts

0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 46738, Sept. 7, 2001, as amended at 67 FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, 2007; 75 FR 26667, May 12, 2010;
76 FR 3029, Jan. 19, 2011; 77 FR 66729, Nov. 7, 2012]

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§180.575 Sulfuryl fluoride; tolerances for residues.
(a)(1) General. Tolerances are established for residues of sulfuryl fluoride in or on the following commodities from the
postharvest fumigation with sulfuryl fluoride for the control of insects:
Commodity

Parts per million

All processed food commodities not otherwise listed
Barley, bran, postharvest
Barley, flour, postharvest
Barley, grain, postharvest
Barley, pearled barley, postharvest
Cacao bean, roasted bean, postharvest
Cattle, meat, dried
Cheese
Coconut, postharvest
Coffee, bean, roasted bean, postharvest
Corn, field, flour, postharvest
Corn, field, grain, postharvest
Corn, field, grits, postharvest
Corn, field, meal, postharvest
Corn, pop, grain, postharvest
Cotton, undelinted seed, postharvest
Egg, dried
Fruit, dried, postharvest
Ginger, postharvest
Grain, aspirated fractions, postharvest
Herbs and spices group 19, postharvest
Hog, meat
Milk, powdered
Millet, grain, postharvest
Nut, pine, postharvest
Nut, tree, Group 14, postharvest
Oat, flour, postharvest
Oat, grain, postharvest
Oat, groats/rolled oats, postharvest
Peanut, postharvest
Pistachio, postharvest
Rice, bran, postharvest
Rice, flour, postharvest
Rice, grain, postharvest
Rice, hulls, postharvest
Rice, polished rice, postharvest
Rice, wild, grain, postharvest
Sorghum, grain, grain, postharvest
Triticale, grain, postharvest
Vegetable, legume, group 6, postharvest
Wheat, bran, postharvest
Wheat, flour, postharvest
Wheat, germ, postharvest
Wheat, grain, postharvest
Wheat, milled byproducts, postharvest
Wheat, shorts, postharvest

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

2.0
0.05
0.05
0.1
0.05
0.2
0.01
2.0
1.0
1.0
0.01
0.05
15.0
0.01
0.05
0.5
1.0
0.05
0.5
0.05
0.5
0.02
2.0
0.1
0.2
3.0
0.05
0.1
0.1
0.5
3.0
0.01
0.05
0.04
0.1
0.01
0.05
0.1
0.1
0.5
0.05
0.05
0.02
0.1
0.05
0.05

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(2) To assure safe use of this pesticide commodities treated with sulfuryl fluoride must be aerated for at least 24 hours
prior to entering commerce.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[67 FR 5740, Feb. 7, 2002, as amended at 69 FR 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005]

Back to Top
§180.576 Cyhalofop-butyl; tolerances for residues.
(a) General. Tolerances are established for residues of cyhalofop-butyl, including its metabolites and degradates, in or
on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring cyhalofop butyl [R-( + )-n-butyl-2-(4(4-cyano-2-fluorophenoxy)-phenoxy)propionate], cyhalofop acid [R-( + )-2-(4
(4-cyano-2-fluorophenoxy)-phenoxy)propionic acid], and the di-acid metabolite [(2R)-4-(4-(1-carboxyethoxy)phenoxy)-3fluorobenzoic acid].
Commodity

Parts per million

Rice, grain
Wild rice, grain

0.40
0.40

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 43256, June 27, 2002, as amended at 74 FR 15880, Apr. 8, 2009; 76 FR 82157, Dec. 30, 2011]

Back to Top
§180.577 Bispyribac-sodium; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the herbicide bispyribac-sodium, including its metabolites and
degradates, in or on the commodity listed below. Compliance with the tolerance level specified below is to be determined
by measuring only bispyribac-sodium, (2,6-bis[(4,6-dimethoxy-2-pyrimidinyl)oxy]benzoic acid, sodium salt), in or on the
following raw agricultural commodities:
Commodity

Parts per million

Fish, freshwater
Rice, grain
Rice, straw

0.01
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[66 FR 48097, Sept. 18, 2001, as amended at 76 FR 5716, Feb. 2, 2011]

Back to Top
§180.578 Acetamiprid; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)
methyl]-N'-cyano-N-methylethanimidamide, including its metabolites and degradates, in or on the commodities in the table
below as a result of the application of acetamiprid. Compliance with the tolerance levels specified below is to be
determined by measuring only acetamiprid in or on the following commodities.
Commodity

Parts per million

Almond, hulls
Asparagus
Berry, low growing subgroups 13-07G
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B

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5.0
0.80
0.60
1.20
15

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Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canola, seed
Citrus, dried pulp
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12, except plum, prune
Grain, aspirated fractions
Mustard, seed
Nut, tree, group 14
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Pea and bean, succulent shelled, subgroup 6B
Pistachio
Plum, prune, dried
Plum, prune, fresh
Soybean, hulls
Soybean, seed

1.6
1.6
0.010
1.20
15
0.01
30
20.0
0.60
1.0
1.0
0.35
1.20
5.0
0.010
0.10
0.02
4.5
0.40
0.10
0.40
0.20
0.04
0.03
50.0

Tea, dried1
Tomato, paste
Turnip greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy, except brassica, group 4
Vegetable, legume, edible podded, subgroup 6A
Vegetable, tuberous and corm, group 1

0.40
15
0.50
0.20
3.00
0.60
0.01

1

There are no U.S. registrations as of February 10, 2010, for the use of acetamiprid on dried tea.

(2) Tolerances are established for residues of the insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′
-cyano-N-methylethanimidamide, including its metabolites and degradates, in or on the commodities in the table below as
a result of the application of acetamiprid. Compliance with the tolerance levels specified below is to be determined by
measuring acetamiprid and (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-ethanimidamide in or on the following
commodities.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, liver
Poultry, meat
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.20
0.30
0.70
0.010
0.20
0.30
0.70
0.10
0.10
0.20
0.20
0.30
0.70
0.30
0.010
0.050
0.010
0.20
0.30
0.70

(3) A tolerances of 0.01 ppm is established for residues of the insecticide acetamiprid, including its metabolites and
degradates, in or on all food/feed items (other than those covered by a higher tolerance in paragraph (a)(1) or (a)(2) of this
section as a result of the use on growing crops) as a result of the application of acetamiprid in food/feed handling
establishments. Compliance with the 0.01 ppm tolerance level is to be determined by measuring only acetamiprid (1E)
-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-methylethanimidamide in or on the commodities.
(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the
insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-methylethanimidamide, including its metabolites
and degradates, in or on the commodities in the table below as a result of the application of acetamiprid. Compliance with
the tolerance levels specified below is to be determined by measuring only acetamiprid in or on the following commodities.
Commodity

Parts per million

Clover, forage
Clover, hay

0.30
2.0

(d) Indirect or inadvertent residues. [Reserved]
[67 FR 14659, Mar. 27, 2002, as amended at 68 FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, 2005; 72 FR 67262, Nov. 28,
2007; 73 FR 2811, Jan. 16, 2008; 75 FR 6582, Feb. 10, 2010; 77 FR 18716, Mar. 28, 2012; 77 FR 43529, July 25, 2012; 78 FR
36676, June 19, 2013; 80 FR 68778, Nov. 6, 2015]

Back to Top
§180.579 Fenamidone; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide, fenamidone, including its metabolites and
degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring
only fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), in or on the
commodities:
Commodity
Bean, succulent, except cowpea
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Cilantro, leaves
Cotton, gin byproducts
Cotton, undelinted seed
Ginseng
Okra
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Pepper, nonbell
Sunflower
Tomato, paste
Tomato, puree
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8, except nonbell pepper
Vegetable, leafy, except Brassica, group 4
Vegetable, root, except sugar beet, subgroup 1B, except radish
Vegetable, tuberous and corm, subgroup 1C

Parts per million
0.80
5.0
55
60
0.02
0.02
0.80
3.5
0.20
1.5
3.5
0.02
2.2
2.0
55
0.15
1.0
60
0.15
0.02

(2) Tolerances are established for residues of the fungicide fenamidone, including its metabolites and degradates, in
or on the following commodities. Compliance with the tolerance levels is to be determined by measuring fenamidone (4HImidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), and its metabolite RPA 717879
(2,4-imidazolidinedione, 5-methyl-5-phenyl), in or on the commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.10
0.10
0.10
0.10
0.10
0.10
0.02
0.10
0.10
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. A tolerance with regional registration as defined in §180.1(l) is established
for residues of the fungicide fenamidone, including its metabolites and degradates, in or on the following commodities.
Compliance with the tolerance levels is to be determined by measuring only fenamidone (4H-Imidazol-4-one, 3,5-dihydro5-methyl-2-(methylthio)-5-phenyl-3 (phenylam-ino)-,(S)-), in or on the commodity:
Commodity

Parts per million

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Grape1

1.0

1

Applicable to grapes grown East of the Rocky Mountains.

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide fenamidone, including its
metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined
by measuring fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), and
its metabolite RPA 717879 (2,4-imidazolidinedione, 5-methyl-5-phenyl), in or on the following commodities when present
therein as a result of application of fenamidone to the crops in paragraph (a)(1).
Parts per
million

Commodity
Grain, cereal, group 15, except rice
Grain, cereal, forage, fodder and straw, group 16, except rice
Soybean, forage
Soybean, hay
Soybean, seed
Strawberry

0.1
0.5
0.15
0.25
0.02
0.02

[67 FR 60976, Sept. 27, 2002, as amended at 69 FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, 2006; 72 FR 60272, Oct. 24,
2007; 74 FR 34257, July 15, 2009; 76 FR 34885, June 15, 2011; 76 FR 70895, Nov. 16, 2011; 77 FR 32401, June 1, 2012; 79 FR
13882, Mar. 12, 2014]

Back to Top
§180.580 Iodosulfuron-Methyl-Sodium; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide Iodosulfuron-Methyl-Sodium (methyl 4-iodo2-[3-(4-methoxy-6-methyl-1,3,5 triazin-2-yl)ureidosulfonyl]benzoate, sodium salt) in or on the following commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.05
0.03
0.05
0.10
0.02
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 57532, Sept. 11, 2002, as amended at 74 FR 23644, May 20, 2009]

Back to Top
§180.581 Iprovalicarb; tolerances for residues.
(a) General. Tolerances are established for residues of iprovalicarb, [2-methyl-1[[[(1S)-(4-methylphenyl) ethyl] amino]
carbonyl] propyl]carbamic acid methylethylester, in or on the following commodities.
Commodity

Parts per million

Grape1

2.0

Tomato1

1.0

1

There is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 54359, Aug. 22, 2002, as amended at 70 FR 55281, Sept. 21, 2005]

Back to Top
§180.582 Pyraclostrobin; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the fungicide pyradostrobin, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of pyraclostrobin (carbamic acid, [2-[[[ 1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]
methyl]phenyl]methoxy-, methyl ester) and its desmethoxy metabolite (methyl-N-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]
methyl] phenylcarbamate), calculated as the stoichiometric equivalent of pyraclostrobin, in or on the commodity.
Commodity
Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple, wet pomace
Artichoke, globe
Avocado
Banana
Barley, grain
Barley, hay
Barley, straw
Bean, succulent shelled
Beet, sugar, dried pulp
Beet, sugar, roots
Beet, sugar, tops
Berry, low growing, subgroup 13-07G, except cranberry
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Citrus, dried pulp
Citrus, oil
Coffee, green bean

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, refined oil
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Dill, seed
Endive, belgium
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12-12
Grain, aspirated fractions
Grape, raisin
Grass, forage
Grass, hay
Grass, seed screenings
Grass, straw
Herb subgroup 19A
Hop, dried cones
Mango
Nut, tree, group 14-12, except pistachio
Oat, grain
Oat, hay
Oat, straw
Oilseed group 20
Papaya
Pea, succulent
Pea and bean, dried shelled, except soybean, subgroup 6C
Peanut
Peanut, refined oil
Peppermint, tops
Persimmon
Pistachio
Radish, tops
Rye, grain
Rye, straw
Sapodilla

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10
30
7.0
8.0
3.0
0.6
0.04
1.4
25
6.0
0.5
1.0
0.2
8.0
1.2
5.0
16.0
4.0
4.0
0.6
12.5
9.0
1

0.3
5.0
0.1
0.2
17.0
0.1
17.0
5.0
0.04
23.0
30
40
4.0
2.0
1.5
2.0
2.5
2.5
7.0
10
4.5
27
14
40
23.0
0.6
0.04
1.2
18
15
0.45
0.6
0.2
0.5
0.05
0.1
8.0
3.0
0.7
16
0.04
0.5
0.6

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Sapote, black
Sapote, mamey
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Spearmint, tops
Star apple
Sugarcane, cane
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, except soybean, subgroup 7A
Vegetable, fruiting, group 8-10
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2, except sugar beet
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root, except sugar beet, subgroup 1B
Vegetable, tuberous and corm, subgroup 1C
Vegetables, foliage of legume, group 7
Wheat, grain
Wheat, hay
Wheat, straw

0.6
0.6
5.0
0.60
0.80
11
14
0.06
0.04
8.0
0.6
0.20
0.9
0.5
25.0
1.4
29.0
16.0
0.5
0.4
0.04
25
0.02
6.0
8.5

(2) Tolerances are established for combined residues of the fungicide pyraclostrobin carbamic acid,
[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]methoxy-, methyl ester and its metabolites convertible to
1-(4-chlorophenyl)-1H-pyrazol-3-ol and 1-(4-chloro-2-hydroxyphenyl)-1H-pyrazol-3-ol, expressed as parent compound, in
or on the following raw agricultural commodities.
Commodity

Parts per million

Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Poultry, eggs
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver

0.1
1.5
0.1
0.2
0.1
1.5
0.1
0.2
0.1
1.5
0.1
0.2
0.1
0.1
0.1
0.2
0.1
0.10
0.10
0.10
0.10
0.1
1.5
0.1
0.2

(b) Section 18 emergency exemptions. A time-limited tolerance is established for combined residues of the fungicide
pyraclostrobin, (carbamic acid, [2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl] phenyl]methoxy-, methyl ester) and its
desmethoxy metabolite (methyl-N-[[[1-(4-chlorophenyl) pyrazol-3-yl]oxy]o-tolyl]carbamate) in connection with use of the
pesticide under section 18 emergency exemptions granted by EPA. The time-limited tolerance will expire and is revoked
on the date specified in the following table.
Commodity

Parts per
million

Endive, belgium

Expiration/revocation date
11.0

12/31/13

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[67 FR 60901, Sept. 27, 2002, as amended at 69 FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, 2006; 72 FR 54569, Sept. 26,
2007; 73 FR 15431, Mar. 24, 2008; 73 FR 21842, Apr. 23, 2008; 73 FR 44167, July 30, 2008; 74 FR 11499, Mar. 18, 2009; 74 FR
51496, Oct. 7, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 42329, July 21, 2010; 75 FR 80346, Dec. 22, 2010; 76 FR 81396, Dec. 28,
2011; 78 FR 53046, Aug. 28, 2013; 80 FR 19238, Apr. 10, 2015]

Back to Top
§180.583 Triticonazole; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide triticonazole, (1RS)-(E)-5-[(4-chlorophenyl)
methylene]-2,2-dimethyl-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol, from the treatment of seed prior to planting in or on
raw agricultural commodities as follows:
Commodity
Grain, cereal, forage, fodder and straw, group 16, except rice
Grain, cereal, group 15, except rice

Parts per million
0.10
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 60959, Sept. 27, 2002, as amended at 75 FR 4288, Jan. 27, 2010]

Back to Top
§180.584 Tolylfluanid; tolerances for residues.
(a) General. Tolerances are established for residues of tolylfluanid, 1,1-dichloro-N-[(dimethylamino)-sulfonyl]-1-fluoroN-(4-methylphenyl)methanesulfenamide in or on the following commodities.
Commodity

Parts per million

Apple1

5.0

Grape1

11

Hop, dried cones1

30

Tomato1

2.0

1

No U.S. registration as of August 31, 2002.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[67 FR 60141, Sept. 25, 2002]

Back to Top
§180.585 Pyraflufen-ethyl; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide, pyraflufen-ethyl, including its metabolites and
degradates, in the commodities in the table below. Compliance with the plant commodity tolerance levels specified in the
table is to be determined by measuring only the sum of the parent pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4-chloro-5difluoromethoxy)-1-methyl-1H-pyrazol-3-yl]-4-fluorophenoxy] acetate, and its acid metabolite, E-1, 2-chloro-5-(4-chloro-5difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, calculated as the stoichiometric equivalent of
pyraflufen-ethyl in or on the commodity. Compliance with the livestock commodity tolerance levels specified in the table is
to be determined by measuring only the sum of the parent pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4-chloro-5difluoromethoxy)-1-methyl-1H-pyrazol-3-yl]-4-fluorophenoxy] acetate and its acid metabolites: E-1, 2-chloro-5-(4-chloro-5difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, and E-9, 2-chloro-5-(4-chloro-5-difluoromethoxy1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, both calculated as the stoichiometric equivalent of pyraflufen-ethyl in or on
the commodity.
Commodity

Parts per million

Almond, hulls
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.02
0.03
0.03
0.03
0.01
0.01

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Corn, field, stover
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, pome, group 11-10
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grape
Grass, forage, group 17
Grass, hay, group 17
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Nut, tree, group 14
Olive
Peanut
Peanut, hay
Pistachio
Pomegranate
Potato
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, seed
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.01
1.5
0.04
0.01
0.01
0.03
0.03
0.03
0.01
1.0
1.4
0.03
0.03
0.03
0.03
0.01
0.01
0.01
0.07
0.01
0.01
0.02
0.03
0.03
0.03
0.05
0.10
0.01
0.02
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 23055, Apr. 30, 2003, as amended at 68 FR 27739, May 21, 2003; 69 FR 26312, May 12, 2004; 73 FR 51743, Sept. 5, 2008;
76 FR 31484, June 11, 2011; 77 FR 75861, Dec. 26, 2012; 78 FR 13263, Feb. 27, 2013]

Back to Top
§180.586 Clothianidin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide clothianidin, including its metabolites and
degradates. Compliance with the tolerance levels specified below is to be determined by measuring only clothianidin, (E)
-N-[(2-Chloro-5-thiazolyl)methyl]-N′ -methyl-N″ -nitroguanidine, in or on the following raw agricultural commodities:
Commodity
Almond, hulls
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Berry, low-growing, subgroup 13-07H, except strawberry
Canola, seed
Cotton, gin byproducts
Cotton, undelinted seed
Fig
Fruit, pome
Grain, cereal, forage, fodder and straw, group 16, except rice, forage
Grain, cereal, forage, fodder and straw, group 16, except rice, hay
Grain, cereal, forage, fodder and straw, group 16, except rice, stover
Grain, cereal, forage, fodder and straw, group 16, except rice, straw
Grain, cereal, group 15, except rice
Grape
Milk
Mustard, seed
Nut, tree, group 14
Peach
Pepper

Parts per million

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

1.5
0.03
0.05
0.02
0.01
0.01
4.5
0.20
0.05
1.0
0.35
0.07
0.1
0.05
0.01
0.60
0.01
0.01
0.01
0.80
0.80

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Pomegranate
Potato, chips
Potato, granules/flakes
Rice, grain
Soybean, seed

0.20
0.6
1.5
0.01
0.02
70

Tea, dried1
Vegetable, brassica, leafy, group 5
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8, except pepper
Vegetable, leafy, except brassica, group 4
Vegetable, root, except sugar beet, subgroup 1B
Vegetable, tuberous and corm, subgroup 1C

1.9
0.45
0.06
0.20
3.0
0.8
0.3

1

No U.S. registrations.

(2) Time-limited tolerances are established for residues of the insecticide clothianidin, including its metabolites and
degradates. Compliance with the tolerance levels specified below is to be determined by measuring only clothianidin, (E)
-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on the following raw agricultural commodity:
Commodity
Rice, seed

Parts per million

Expiration/revocation date
0.01

6/23/12

(b) Section 18 emergency exemptions. A time-limited tolerance specified in the following table is established for
residues of clothianidin, (E)-N-[(2-chloro-5-thiazolyl)methyl]-N'-methyl-N”-nitroguanidine, in or on the specified agricultural
commodity, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. This tolerance
expires on the date specified in the table.
Commodity

Parts per million
0.07

Fruit, citrus, group 10-10

Expiration date
12/31/17

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. Tolerances are established for the indirect or inadvertent residues of the
insecticide clothianidin, including its metabolites and degradates. Compliance with the tolerance levels specified below is
to be determined by measuring only clothianidin, (E)-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on
the following raw agricultural commodities when present therein as a result of the application of clothianidin to crops listed
in paragraph (a) of this section:
Commodity

Parts per million

Animal feed, nongrass, group 18
Grass, forage, fodder and hay, group 17
Soybean, forage
Soybean, hay

0.02
0.02
0.02
0.02

[74 FR 65028, Dec. 9, 2009, as amended at 76 FR 7718, Feb. 11, 2011; 76 FR 25246, May 4, 2011; 76 FR 34886, June 15, 2011;
77 FR 52252, Aug. 29, 2012; 78 FR 19136, Mar. 29, 2013; 80 FR 10007, Feb. 25, 2015]

Back to Top
§180.587 Famoxadone; tolerance for residues.
(a) General. Tolerances are established for residues of the fungicide famoxadone (3-anilino-5-methyl5-(4-phenoxyphenyl)-1,3-oxazolidine-2,4-dione) in or on the following commodities:
Commodity

Parts per million

Caneberry subgroup 13-07A
Cattle, fat
Cattle, liver
Cilantro, leaves
Goat, fat
Goat, liver
Grape, raisin1
Hop, dried cone
Horse, fat
Horse, liver
Milk, fat (reflecting negligible residues in whole milk)
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Potato
Sheep, fat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

10
0.02
0.05
25
0.02
0.05
4.0
80
0.02
0.05
0.06
0.45
40
0.02
0.02

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Sheep, liver
Spinach
Tomato
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8, except tomato
Vegetable, leafy, except Brassica, group 4, except spinach

0.05
50
1.0
0.30
4.0
25

1

There are no U.S. registrations as of May 15, 2003.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with a regional registrations. Tolerances with a regional registration as defined in §180.1(l) are
established for the residues of the fungicide famoxadone, 3-anilino-5-methyl-5-(4-phenoxyphenyl)
-1,3-oxazolidine-2,4-dione) in or on the raw agricultural commodities:
Commodity

Parts per million

Grape

2.5

(d) Indirect or inadvertant residues. [Reserved]
[68 FR 39471, July 2, 2003, as amended at 72 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, 2009; 76 FR 34885, June 15, 2011]

Back to Top
§180.588 Quinoxyfen; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide quinoxyfen, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only quinoxyfen (5,7-dichloro-4-(4-fluorophenoxy)quinoline).
Commodity
Artichoke, globe
Berry, low growing, subgroup 13-07G
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12
Hop, dried cones
Gourd, edible
Lettuce, head
Lettuce, leaf
Melon, subgroup 9A
Pumpkin
Squash, winter
Vegetable, fruiting, group 8-10

Parts per million
1.4
1.0
2.0
0.70
3.0
0.20
7.0
19
0.08
0.20
0.20
1.7

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55858, Sept. 29, 2003, as amended at 70 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, 2006; 74 FR 14743, Apr. 1, 2009;
78 FR 57280, Sept. 18, 2013]

Back to Top
§180.589 Boscalid; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide boscalid, including its metabolites and
degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be
determined by measuring only boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), in or on the
following raw agricultural commodities:
Commodity
Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple, wet pomace
Artichoke, globe
Avocado
Banana, import1
Berry, low growing, subgroup 13-07G, except cranberry
Brassica, head and stem, subgroup 5A

Parts per million
30.0
65.0
17
10
6.0
1.5
0.40

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

4.5
3.0

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Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Canistel
Canola, refined oil
Citrus, dried pulp
Citrus, oil

18.0
13.0
10.0
1.5
5.0
4.5
85.0
0.05

Coffee, green bean, import1
Cotton, gin byproducts
Cucumber
Dill, seed
Endive, Belgium
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12-12
Grain, aspirated fractions
Grape, raisin
Herb subgroup 19A
Hop, dried cones
Leaf petioles subgroup 4B
Leafy greens subgroup 4A, except head lettuce and leaf lettuce
Lettuce, head
Lettuce, leaf
Mango
Nut, tree, group 14-12
Oilseed group 20
Papaya
Pea and bean, dried shelled, except soybean, subgroup 6C, except cowpea, field pea and grain lupin
Pea and bean, succulent shelled, subgroup 6B, except cowpea
Peanut
Peanut, meal
Peanut, refined oil
Peppermint, tops
Persimmon
Sapodilla
Sapote, black
Sapote, mamey
Soybean, hulls
Soybean, seed
Soybean, vegetable
Spearmint, tops
Star apple
Turnip, greens
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9, except cucumber
Vegetable, fruiting, group 8-10
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root, subgroup 1A, except sugar beet, garden beet, radish, and turnip
Vegetable, tuberous and corm, subgroup 1C

55.0
0.5
100
6.0
2.0
3.0
5.0
3.5
3.0
8.5
150
35
45
60
6.5
11.0
1.5
0.70
3.5
1.5
2.5
0.6
0.05
0.15
0.15
30.0
8.0
1.5
1.5
1.5
0.2
0.1
2.0
30.0
1.5
40.0
5.0
1.6
3.0
1.6
1.0
0.05

1

No US registrations as of September 16, 2009.

(2) Tolerances are established for residues of the fungicide boscalid, including its metabolites and degradates, in or
on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), and metabolites 2-chloro-N-(4'chloro-5-hydroxy-biphenyl-2-yl) nicotinamide and glucuronic acid conjugate of 2-chloro-N-(4′-chloro-5-hydroxy-biphenyl-2yl) nicotinamide, calculated as the stoichiometric equivalent of boscalid in or on the following food commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.30
0.10
0.35
0.02
0.30
0.10
0.35
0.20
0.05
0.10
0.30
0.10

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Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.35
0.10
0.20
0.05
0.20
0.30
0.10
0.35

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fungicide boscalid,
including its metabolites and degradates, in connection with use of the pesticide under section 18 emergency exemptions
granted by EPA. Compliance with the tolerance level specified below is to be determined by measuring only boscalid,
3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl). This tolerance will expire and is revoked on the date
specified in the following table:
Commodity
Endive, Belgian

Parts per million

Expiration/revocation date
16

12/31/13

(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide
boscalid, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance
levels specified below is to be determined by measuring only boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′
-biphenyl]-2-yl), in or on the following commodities:
Commodity
Animal feed, nongrass, group 18, forage, except alfalfa
Animal feed, nongrass, group 18, hay, except alfalfa
Animal feed, nongrass, group 18, seed
Beet, garden, roots
Beet, sugar, roots
Cowpea, seed
Grain, cereal, forage, fodder and straw, group 16, forage
Grain, cereal, forage, fodder and straw, group 16, stover
Grain, cereal, forage, fodder and straw, group 16, straw
Grain, cereal, group 15
Grass, forage, fodder, and hay, group 17, forage
Grass, forage, fodder, and hay, group 17, hay
Grass, forage, fodder, and hay, group 17, seed screenings
Grass, forage, fodder, and hay, group 17, straw
Lupin, grain, grain
Pea, field, seed
Radish, roots
Rice, hulls
Turnip, roots
Vegetable, foliage of legume, group 7, forage
Vegetable, foliage of legume, group 7, hay
Vegetable, foliage of legume, group 7, vines
Vegetable, leafy, except brassica, group 4, except celery, lettuce and spinach
Vegetable, leaves of root and tuber, group 2

Parts per million
1.0
2.0
0.05
0.1
0.1
0.1
2.0
1.5
3.0
0.20
2.0
8.0
0.20
0.30
0.1
0.1
0.1
0.50
0.1
1.5
2.0
0.05
1.0
0.1

[68 FR 44651, July 30, 2003, as amended at 69 FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, 2005; 71 FR 6364, Feb. 8, 2006;
71 FR 25961, May 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, Mar. 28, 2008; 74 FR 47445, Sept. 16, 2009; 75 FR 770,
Jan. 6, 2010; 75 FR 29907, May 28, 2010; 75 FR 80346, Dec. 22, 2010; 78 FR 67048, Nov. 8, 2013; 80 FR 14014, Mar. 18, 2015]

Back to Top
§180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.
(a) General. Tolerances are established for residues of the growth inhibitor 2,6-DIPN, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only 2,6-Diisopropylnaphthalene.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts, except fat
Goat, fat
Goat, meat
Goat, meat byproducts, except fat
Horse, fat
Horse, meat

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.2
0.02
0.02
0.2
0.02
0.02
0.2
0.02

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Horse, meat byproducts, except fat
Milk, fat
Potato, granules/flakes
Potato, wet peel
Potato, whole
Sheep, fat
Sheep, meat
Sheep, meat byproducts, except fat

0.02
0.02
5.5
6.0
2.0
0.2
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 52011, Sept. 1, 2006, as amended at 74 FR 66579, Dec. 16, 2009; 77 FR 32406, June 1, 2012]

Back to Top
§180.591 Trifloxysulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide trifloxysulfuron, N-[[(4,6-dimethoxy-2-pyrimidinyl)
amino]carbonyl]-3-(2,2,2-trifluoroethoxy)-2-pyridinesulfonamide in or on the following raw agricultural commodities.
Commodity

Parts per million

Almond
Almond, hulls
Fruit, citrus, Group 10
Cotton, undelinted seed
Cotton, gin byproducts
Sugarcane
Tomato

0.02
0.01
0.03
0.05
1.0
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 54386, Sept. 17, 2003]

Back to Top
§180.592 Butafenacil; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo2-(2-propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate) in or on
the following raw agricultural commodities:
Commodity

Parts per million

Cotton, gin byproducts
Cotton, undelinted seed

10
0.50

(2) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo-2-(2-propenyloxy)ethyl
2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate) and its metabolite CGA-293731
(1-carboxy-1-methylethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate), in or
on the following livestock commodities:
Commodity

Parts per million

Cattle, kidney
Cattle, liver
Goat, kidney
Goat, liver
Hog, kidney
Hog, liver
Horse, kidney
Horse, liver
Sheep, kidney
Sheep, liver

0.05
0.50
0.05
0.50
0.05
0.50
0.05
0.50
0.05
0.50

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. [Reserved]
[68 FR 54827, Sept. 19, 2003]

Back to Top
§180.593 Etoxazole; tolerances for residues.
(a) General. Tolerances are established for residues of etoxazole, including its metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only etoxazole (2-(2,6-difluorophenyl)-4-[4-(1,1-dimethylethyl)-2-ethoxyphenyl]-4,5-dihydrooxazole) in or on the
commodity.
Commodity
Almond, hulls
Apple, wet pomace
Avocado
Berry, low growing, subgroup 13-07G
Caneberry subgroup 13-07A
Canistel
Cattle, fat
Cattle, liver
Corn, field, forage
Corn, field, grain
Corn, field, refined oil
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, pome, group 11
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12, except plum
Goat, fat
Goat, liver
Grape, raisin
Hop, dried cones
Horse, fat
Horse, liver
Mango
Melon subgroup 9A
Milk, fat
Nut, tree, group 14
Papaya
Pepper/eggplant subgroup 8-10B
Peppermint, oil
Peppermint, tops
Pistachio
Plum
Plum, prune, dried
Sapodilla
Sapote, black
Sapote, mamey
Sheep, fat
Sheep, liver
Spearmint, oil
Spearmint, tops
Squash/cucumber subgroup 9B
Star apple

Parts per million

Tangerine1
Tea, dried*
Tomato

2.0
0.50
0.20
0.50
1.5
0.20
0.02
0.01
0.80
0.01
0.03
4.0
0.01
4.0
1.0
0.05
0.20
0.50
1.0
0.02
0.01
1.5
7.0
0.02
0.01
0.20
0.20
0.01
0.01
0.20
0.20
20
10
0.01
0.15
0.30
0.20
0.20
0.20
0.02
0.01
20
10
0.02
0.20
0.10
15
0.20

1

There are no U.S. registrations for use of etoxazole on tangerines as of September 26, 2003.

*There are currently no U.S. registrations for tea as of April 13, 2011.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect and inadvertant residues. [Reserved]
[68 FR 55493, Sept. 26, 2003, as amended at 70 FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, 2007; 74 FR 25160, May 27,
2009; 76 FR 20542, Apr. 13, 2011; 77 FR 3621, Jan. 25, 2012]

Back to Top
§180.594 Thiacloprid; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide thiacloprid, including its metabolites and
degradates in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only thiacloprid ([3-[(6-chloro-3-pyridinyl)methyl]-2-thiazolidinylidene] cyanamide)
in or on the commodity.
Commodity

Parts per million

Apple, wet pomace
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts
Cherry subgroup 12-12A
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, pome, group 11
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts
Milk
Peach subgroup 12-12B
Pepper
Plum subgroup 12-12C
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts

0.60
0.020
0.050
0.15
0.030
0.050
0.5
11.0
0.020
0.30
0.020
0.050
0.15
0.030
0.050
0.020
0.050
0.15
0.030
0.050
0.030
0.5
1.0
0.05
0.020
0.050
0.15
0.030
0.050

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 55512, Sept. 26, 2003, as amended at 78 FR 8416, Feb. 6, 2013]

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§180.595 Flufenpyr-ethyl; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide, flufenpyr-ethyl; acetic acid, [2-chloro-4fluoro-5-[5-methyl-6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], in or on the following commodities:
Commodity

Parts per million

Corn, field, grain
Soybean, seed
Sugarcane, cane

0.01
0.01
0.01

(2) Tolerances are established for residues of the herbicide flufenpyr-ethyl; acetic acid, [2-chloro-4-fluoro-5-[5-methyl6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], and its metabolite, S-3153 acid-4-OH; [2-chloro-4hydroxy-5-[5-methyl-6- oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-acetic acid, free and conjugated, in or on the
following commodities:
Commodity

Parts per million

Corn, field, forage

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0.05

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Corn, field, stover

0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[68 FR 54842, Sept. 19, 2003]

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§180.596 Fosthiazate; tolerances for residues.
(a) General. A tolerance is established for residues of the insecticide fosthiazate, including its metabolites and
degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this
paragraph is to be determined by measuring only the sum of fosthiazate, O-ethyl S-(1-methylpropyl)(2-oxo-3-thiazolidinyl)
phosphonothioate, and its metabolite, O-ethyl S-(1-methylpropyl)(2-(methylsulfonyl)ethyl)phosphoramidothioate,
calculated as the stoichiometric equivalent of fosthiazate, in or on the commodity.
Commodity

Parts per million

Tomato

0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 18275, Apr. 7, 2004, as amended at 76 FR 23498, Apr. 27, 2011]

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§180.597 Mesosulfuron-methyl; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide mesosulfuron-methyl, (methyl
2-[[[[(4,6-dimethoxy-2-pyrimidinyl) amino]carbonyl]amino]sulfonyl] -4-[[(methylsulfonyl)amino] methyl]benzoate]) in or on
the following raw agricultural commodities:
Commodity

Parts per million

Cattle, meat byproducts
Goat, meat byproducts
Grain, aspirated fractions
Horse, meat byproducts
Sheep, meat byproducts
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, hay
Wheat, straw

0.01
0.01
0.60
0.01
0.01
0.60
0.10
0.03
0.06
0.30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 18263, Apr. 7, 2004]

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§180.598 Novaluron; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide novaluron, including its metabolites and
degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table is to
be determined by measuring only novaluron, (N-[[[3-chloro-4-[1,1,2-trifluoro-2- (trifluoromethoxy)ethoxy]phenyl]amino]
carbonyl]-2,6-difluorobenzamide), in or on the following raw agricultural commodities:
Commodity
Apple, wet pomace
Avocado

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Parts per
million
8.0
0.60

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Bean, dry, seed
Bean, succulent
Berry, low growing, subgroup 13-07G, except lowbush blueberry
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry subgroup 13-07B
Carrot
Cattle, fat
Cattle, kidney
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except kidney and liver
Cherry subgroup 12-12A
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Egg
Food commodities and feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food and
feed handling establishments
Fruit, pome, group 11-10
Goat, fat
Goat, kidney
Goat, liver
Goat, meat
Goat, meat byproducts, except kidney and liver
Grain, aspirated fractions
Hog, fat
Hog, kidney
Hog, liver
Hog, meat
Hog, meat byproducts, except kidney and liver
Horse, fat
Horse, kidney
Horse, liver
Horse, meat
Horse, meat byproducts, except kidney and liver
Milk
Milk, fat
Peach subgroup 12-12B
Peanut
Plum, prune, dried
Plum subgroup 12-12C
Poultry, fat
Poultry, kidney
Poultry, liver
Poultry, meat
Poultry, meat byproducts, except kidney and liver
Sheep, fat
Sheep, kidney
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except kidney and liver
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Sugarcane, cane
Swiss chard
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, tuberous and corm, subgroup 1C

0.30
0.70
0.45
0.50
25
7.0
0.05
11
1.0
1.0
0.60
11
8.0
16
0.05
50
30
0.60
1.5
0.01
3.0
11
1.0
1.0
0.60
11
25
1.5
0.10
0.10
0.07
1.5
11
1.0
1.0
0.60
11
1.0
20
1.9
0.01
3.0
1.9
7.0
0.80
0.80
0.40
7.0
11
1.0
1.0
0.60
11
6.0
3.0
40
0.07
0.50
12
25
0.20
1.0
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]

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[69 FR 31021, June 2, 2004, as amended at 71 FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, 2006; 73 FR 74982, Dec. 10, 2008;
74 FR 637, Jan. 7, 2009; 74 FR 20891, May 6, 2009; 74 FR 65033, Dec. 9, 2009; 75 FR 4278, Jan. 27, 2010; 75 FR 29447, May 26,
2010; 76 FR 55814, Sept. 9, 2011; 78 FR 40033, July 3, 2013; 80 FR 43335, July 22, 2015]

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§180.599 Acequinocyl; tolerances for residues.
(a) General. Tolerances are established for residues of acequinocyl, including its metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of acequinocyl [2-(acetyloxy)-3-dodecyl-1,4-naphthalenedione] and its metabolite, 2-dodecyl-3hydroxy-1,4-naphthoquinone, calculated as the stoichiometric equivalent of acequinocyl, in or on the commodity.
Commodity
Almond, hulls
Apple, wet pomace
Bean, edible podded
Bean, succulent shelled
Berry, low growing, subgroup 13-07G
Caneberry subgroup 13-07A
Cattle, fat
Cattle, meat byproducts
Cherry, sweet
Cherry, tart
Citrus, oil
Cowpea, forage
Cowpea, hay
Cucumber
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Goat, fat
Goat, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat byproducts
Melon subgroup 9A
Nut, tree, group 14
Okra
Pistachio
Sheep, fat
Sheep, meat byproducts
Soybean, vegetable, succulent
Vegetable, fruiting, group 8

Parts per million
2.0
1.0
0.25
0.30
0.50
4.0
0.02
0.02
0.50
1.0
30
6.0
18
0.15
0.20
0.40
1.6
0.02
0.02
4.0
0.02
0.02
0.15
0.02
0.70
0.02
0.02
0.02
0.25
0.70

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 43533, July 21, 2004, as amended at 73 FR 17910, Apr. 2, 2008; 75 FR 70148, Nov. 17, 2010; 77 FR 25909, May 2, 2012]

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§180.600 Propoxycarbazone; tolerances for residues.
(a) General. (1) Tolerances are established for combined residues of the herbicide propoxycarbazone methyl
2-[[[(4,5-dihydro-4-methyl-5-oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate and its metabolite
methyl 2-[[[(4,5-dihydro-3-(2-hydroxypropoxy)-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate in/on
the following raw agricultural commodities:
Commodity

Parts per million

Grass, forage
Grass, hay
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

20
25
17
0.02
0.15
0.05

(2) Tolerances are established for residues of the herbicide propoxycarbazone methyl 2-[[[(4,5-dihydro-4-methyl-5oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate in/on the following raw agricultural commodities:

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Commodity

Parts per million

Cattle, meat
Cattle, meat byproducts
Goat, meat
Goat, meat byproducts
Horse, meat
Horse, meat byproducts
Milk
Sheep, meat
Sheep, meat byproducts

0.05
0.3
0.05
0.3
0.05
0.3
0.03
0.05
0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 40781, July 7, 2004, as amended at 71 FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, 2009]

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§180.601 Cyazofamid; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide cyazofamid, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only the sum of 4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole1-sulfonamide and its metabolite, 4-chloro-5-(4-methylphenyl)-1H-imidazole-2-carbonitrile, calculated as the stoichiometric
equivalent of cyazofamid, in or on the following commodities:
Commodity

Parts per million

Basil, dried leaves
Basil, fresh leaves
Bean, succulent
Bean, succulent shelled
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Carrot, roots
Hop dried cones
Leafy greens subgroup 4A
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, tuberous and corm, subgroup 1C

90
30
0.5
0.08
1.2
12.0
0.09
10.0
10
12.0
0.10
0.9
0.02

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fungicide
cyazofamid, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the
tolerance levels specified in the following table is to be determined by measuring only the sum of cyazofamid, 4-chloro-2cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide and its metabolite CCIM, 4-chloro-5-(4-methylphenyl)
-1H-imidazole-2-carbonitrile, calculated as the stoichiometric equivalent of cyazofamid, resulting from use of the pesticide
under FIFRA section 18 emergency exemptions. The tolerances expire and are revoked on the date specified in the table.
Commodity
Basil, dried

Parts per million

Expiration/revocation date
144

12/31/14

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the
fungicide cyazofamid, including its metabolites and degradates, in or on the commodities in the following table.
Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of
4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide and its metabolite, 4-chloro5-(4-methylphenyl)-1H-imidazole-2-carbonitrile, calculated as the stoichiometric equivalent of cyazofamid, in or on the
following commodities:
Commodity

Parts per million

Grape

1.5

(d) Indirect or inadvertent residues. [Reserved]
[69 FR 58299, Sept. 30, 2004, as amended at 73 FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, 2009; 75 FR 40751, July 14, 2010;
77 FR 4252, Jan. 27, 2012; 77 FR 59119, Sept. 26, 2012]

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§180.602 Spiroxamine; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of the fungicide spiroxamine, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only spiroxamine, [(8-(1,1-dimethylethyl)-N-ethyl-N-propyl-1,4-dioxaspiro[4,5]
decane-2-methanamine) in or on the commodities.
Commodity

Parts per million

Artichoke, globe, import1

0.7
0.05

Asparagus1
Banana (import)
Grape (import)
Hop, dried cones

3.0
1.0
50
1.2

Vegetable, fruiting , crop group 81
1

No U.S. registration as of December 1, 2010.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 42570, July 16, 2004, as amended at 75 FR 74640, Dec. 1, 2010]

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§180.603 Dinotefuran; tolerances for residues.
(a) General. (1) Tolerances are established for residues of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)
methyl)guanidine, including its metabolites and degradates, in or on the commodities listed in the following table.
Compliance with the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran and its
metabolites DN, 1-methyl-3-(tetrahydro-3-furylmethyl)guanidine, and UF, 1-methyl-3-(tetrahydro-3-furylmethyl)urea,
calculated as the stoichiometric equivalent of dinotefuran, in or on the commodities listed in the table below:
Commodity
Berry, low growing, except strawberry, subgroup 13-07H
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Cotton, undelinted seed
Cotton, gin byproducts
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Grape, raisin
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Peach
Potato, chips
Potato, granules/flakes
Rice, grain

Parts per million
0.2
1.4
15.0
0.4
8.0
0.9
2.5
0.15
5.0
1.0
0.1
0.15
9.0
50

Tea, dried1
Tomato, paste
Turnip, greens
Vegetable, fruiting, group 8
Vegetable, cucurbit, group 9
Vegetable, leafy, except Brassica, group 4
Vegetable, tuberous and corm, subgroup 1C
Watercress

1.0
15.0
0.7
0.5
5.0
0.05
8.0

1

There are no U.S. registrations for tea.

(2) Tolerances are established for residues of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)
guanidine, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with
the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran, (RS)-1-methyl-2-nitro3-((tetrahydro-3-furanyl)methyl)guanidine in or on the commodities listed in the table below:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts

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0.05
0.05
0.05

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Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.01
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.01
0.05
0.05
0.05

(3) A tolerance of 0.01 parts per million is established for residues of the insecticide dinotefuran, (RS)-1-methyl-2nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on all food and/or feed
commodities (other than those covered by a higher tolerance as a result of use on growing crops or inadvertent residues)
when residues result from application of dinotefuran in food and/or feed handling establishments where food and/or feed
products are held, stored, processed, prepared, or served. Compliance with the tolerance level is to be determined by
measuring only dinotefuran.
(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of dinotefuran, (RS)-1methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on the
commodities in the table below resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions.
Compliance with the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran and its
metabolites DN, 1-methyl-3-(tetrahydro-3-furylmethyl)guanidine, and UF, 1-methyl-3-(tetrahydro-3-furylmethyl)urea,
calculated as the stoichiometric equivalent of dinotefuran, in or on the commodities listed in the table below. The
tolerances expire and are revoked on the dates specified in the table.

Commodity

Expiration/
revocation
date

Parts per million

Fruit, pome, Group 11
Fruit, stone, Group 12

2.0
2.0

12/31/15
12/31/15

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[70 FR 14546, Mar. 23, 2005, as amended at 74 FR 12601, Mar. 25, 2009; 74 FR 67104, Dec. 18, 2009; 75 FR 770, Jan. 6, 2010;
77 FR 56138, Sept. 12, 2012; 77 FR 67285, Nov. 9, 2012; 77 FR 70913, Nov. 28, 2012; 78 FR 21272, Apr. 10, 2013; 78 FR 24683,
Apr. 26, 2013; 79 FR 3512, Jan. 22, 2014]

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§180.604 Mepanipyrim; tolerances for residues.
(a) General. [Reserved]
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect of inadvertent residues. [Reserved]
(e) Revoked tolerances subject to the channel of trade provisions. [Reserved]
(f) Import tolerances. Tolerances are established for the combined residues of mepanipyrim, 4-methyl-N-phenyl6-(1-propynyl)-2-pyrimidinamine, and its metabolite, 4-methyl-N-phenyl-6-(2-hydroxypropylk)-2-pyrimidinamine, both free
and conjugated in or on the following commodities:
Commodity

Parts per million

Grape
Grape, raisin
Strawberry
Tomato

1.5
3.0
1.5
0.5

[68 FR 60827, Oct. 13, 2004]

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§180.605 Penoxsulam; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for the herbicide, penoxsulam (2-(2,2-difluoroethoxy)-N-(5,8-dimethoxy[1,2,4]
triazolo[1,5-c]pyrimidin-2-yl)-6-(trifluoromethyl)benzenesulfonamide) in/on the following raw agricultural commodities:
Commodity

Parts per million

Almond, hulls
Fish
Fish, shellfish, crustacean
Fish, shellfish, mollusc
Grape
Nut, tree, group 14
Pistachio
Rice, grain
Rice, straw

0.01
0.01
0.01
0.02
0.01
0.01
0.01
0.02
0.50

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[69 FR 57197, Sept. 24, 2004, as amended at 72 FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, 2009]

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§180.607 Spiromesifen; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide/miticide spiromesifen, including its
metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below
is to be determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en4-yl 3,3-dimethylbutanoate] and 4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one, calculated as the
stoichiometric equivalent of spiromesifen, in or on the following primary crop commodities:
Commodity
Bean, dry
Bean, edible podded
Bean, succulent
Berry and small fruit, low growing berry, subgroup 13-07G
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Cowpea, forage
Cowpea, hay
Leaf petiole subgroup 4B
Leafy greens subgroup 4A
Pea, dry, seed
Peppermint, tops
Spearmint, tops
Tea, dry
Tomato, paste
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, tuberous and corm, subgroup 1C

Parts per million
0.02
0.80
0.10
2.0
2.0
12
5.0
0.02
8.0
0.02
4.0
17
0.02
12
15
0.50
30
86
6.0
12
0.20
45
45
40
0.80
0.10
0.45
0.02

(2) Tolerances are established for residues of the insecticide/miticide spiromesifen, including its metabolites and
degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl
3,3-dimethylbutanoate] and its metabolites containing the 4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-

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one and 4-hydroxy-3-[4-(hydroxymethyl)-2,6-dimethylphenyl]-1-oxaspiro[4.4]non-3-en-2-one moieties, calculated as the
stoichiometric equivalent of spiromesifen, in the following livestock commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Milk, fat
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.10
0.02
0.20
0.10
0.02
0.20
0.10
0.02
0.20
0.01
0.25
0.10
0.02
0.20

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for
residues of the insecticide/miticide spiromesifen, including its metabolites and degradates, in or on the commodities listed
below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of
spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate] and 4-hydroxy3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one, calculated as the stoichiometric equivalent of spiromesifen, in or
on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency
exemptions. The tolerances expire and are revoked on the date specified in the table.
Commodity
Soybean, forage
Soybean, hay
Soybean, seed

Parts per million

Expiration/revocation date
30
86
0.02

12/31/14
12/31/14
12/31/14

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the inadvertent or indirect residues of the
insecticide/miticide spiromesifen, including its metabolites and degradates, in or on the commodities listed below.
Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spiromesifen
[2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate], 4-hydroxy-3-(2,4,6-trimethylphenyl)
-1-oxaspiro[4.4]non-3-en-2-one, and its metabolites containing the 4-hydroxy-3-[4-(hydroxymethyl)-2,6-dimethylphenyl]-1oxaspiro[4.4]non-3-en-2-one moiety, calculated as the stoichiometric equivalent of spiromesifen, in the following rotational
crop commodities:
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Barley, grain
Barley, hay
Barley, straw
Beet, sugar, roots
Beet, sugar, tops
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Vegetable, bulb, group 3-07
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

1.5
3.0
0.03
0.25
0.15
0.03
0.20
0.20
0.03
0.25
0.25
0.09
0.20
0.03
0.15
0.25

[70 FR 43283, July 27, 2005, as amended at 72 FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, 2008; 73 FR 52606, Sept. 10, 2008;
74 FR 8492, Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009; 75 FR 5526, Feb. 3, 2010; 75 FR 53586, Sept. 1, 2010; 76 FR 81396, Dec.
28, 2011; 78 FR 3337, Jan. 16, 2013]

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§180.608 Spirodiclofen; tolerances for residues.
(a) General. (1) Tolerances are established for residues of spirodiclofen, including its metabolites and degradates, in
or on the commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only
spirodiclofen (3-(2,4-dichlorophenyl)-2-oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2-dimethylbutanoate).

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Commodity

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Parts per million

Almond, hulls
Apple, wet pomace
Avocado
Black sapote
Canistel
Citrus, juice
Citrus, oil
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grape
Grape, raisin
Hop, dried cones
Mamey sapote
Mango
Nut, tree, group 14
Papaya
Pistachio
Sapodilla
Star apple

20.0
2.4
1.0
1.0
1.0
0.60
35
0.50
0.80
1.0
2.0
6.0
30
1.0
1.0
0.10
1.0
0.10
1.0
1.0

(2) Tolerances are established for residues of spirodiclofen, including its metabolites and degradates, in or on the
commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only
spirodiclofen (3-(2,4-dichlorophenyl)-2-oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2-dimethylbutanoate) and its metabolite
3-(2,4-dichlorophenyl)-4-hydroxy-1-oxaspiro[4,5] dec-3-en-2-one, calculated as the stoichiometric equivalent of
spirodiclofen.
Commodity

Parts per million

Cattle, fat
Cattle, meat byproducts
Cattle, meat
Goat, fat
Goat, meat byproducts
Goat, meat
Horse, fat
Horse, meat byproducts
Horse, meat
Milk
Milk, fat
Sheep, fat
Sheep. meat byproducts
Sheep. meat

0.02
0.10
0.02
0.02
0.1
0.02
0.02
0.1
0.02
0.01
0.03
0.02
0.1
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[70 FR 40211, July 13, 2005, as amended at 73 FR 25539, May 7, 2008; 75 FR 24434, May 5, 2010; 77 FR 73939, Dec. 12, 2012;
79 FR 33464, June 11, 2014]

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§180.609 Fluoxastrobin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of fluoxastrobin, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin3-yl)methanone O-methyloxime and its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl]
(5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, calculated as the stoichiometric equivalent of fluoxastrobin.
Commodity

Parts per million

Berry, low growing, subgroup 13-07G
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Grain, aspirated grain fractions

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1.9
3.0
0.02
4.5
13
0.01
10
60

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Leaf petioles subgroup 4B
Melon subgroup 9A
Peanut
Peanut, hay
Peanut, refined oil
Rice, grain
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Squash/cucumber subgroup 9B
Tomato, paste
Vegetable, fruiting, group 8
Vegetable, tuberous and corm, subgroup 1C
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

4.0
1.5
0.02
20.0
0.06
4.0
5.0
1.5
5.0
9.0
1.2
0.20
0.05
0.50
1.5
1.0
0.010
7.0
0.15
17
11

(2) Tolerances are established for residues of fluoxastrobin, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)
methanone O-methyloxime, its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl]
(5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, and its phenoxy-hydroxypyrimidine, 6-(2-chlorophenoxy)-5fluoro-4-pyrimidinol, calculated as the stoichiometric equivalent of fluoxastrobin.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Milk, fat
Poultry, liver
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.10
0.05
0.20
0.10
0.05
0.20
0.03
0.06
0.10
0.05
0.20
0.03
0.75
0.06
0.10
0.05
0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of
fluoxastrobin, including its metabolites and degradates, in or on the commodities in the table below, when present therein
as a result of the application of fluoxastrobin to the growing crops listed in paragraph (a)(1) of this section. Compliance
with the tolerance levels specified below is to be determined by measuring only fluoxastrobin, (1E)
-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime and
its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone
O-methyloxime, calculated as the stoichiometric equivalent of fluoxastrobin.
Commodity
Alfalfa, forage
Alfalfa, hay
Cotton, gin byproducts
Grain, cereal, forage, fodder, and straw, group 16, except corn
Grass, forage
Grass, hay
Vegetable, foliage of legume, group 7

Parts per million
0.050
0.10
0.020
0.10
0.10
0.50
0.050

[74 FR 67113, Dec. 18, 2009, as amended at 75 FR 60333, Sept. 30, 2010; 76 FR 50898, Aug. 17, 2011; 77 FR 26471, May 4,
2012; 77 FR 64915, Oct. 24, 2012; 79 FR 20105, Apr. 11, 2014; 79 FR 59119, Oct. 1, 2014]

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§180.610 Aminopyralid; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide aminopyralid, 4-amino-3,6-dichloro-2pyridinecarboxylic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance
with the tolerance levels specified below is to be determined by measuring only free and conjugated aminopyralid.
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Grain, aspirated fractions
Grass, forage
Grass, hay
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.30
0.20
0.20
0.2
25
50
0.1
2.0
0.04
4.0
0.25

(2) Tolerances are established for residues of the herbicide aminopyralid, 4-amino-3,6-dichloro-2-pyridinecarboxylic
acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance
levels specified below is to be determined by measuring only aminopyralid.
Commodity
Cattle, fat
Cattle, kidney
Cattle, meat
Cattle, meat byproducts, except kidney
Goat, fat
Goat, kidney
Goat, meat
Goat, meat byproducts, except kidney
Horse, fat
Horse, kidney
Horse, meat
Horse, meat byproducts, except kidney
Milk
Sheep, fat
Sheep, kidney
Sheep, meat
Sheep, meat byproducts, except kidney

Parts per million
0.02
0.3
0.02
0.02
0.02
0.3
0.02
0.02
0.02
0.3
0.02
0.02
0.03
0.02
0.3
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[70 FR 46428, Aug. 10, 2005, as amended at 75 FR 17584, Apr. 7, 2010]

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§180.611 Pinoxaden; tolerances for residues.
(a) General. (1) Tolerances are established for the combined residues of pinoxaden (8-(2,6-diethyl-4-methylphenyl)
-1,2,4,5-tetrahydro-7-oxo-7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9-yl 2,2-dimethylpropanoate), and its metabolites
8-(2,6-diethyl-4-methyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5]oxadiazepine-7,9-dione (M2), and free and conjugated
forms of 8-(2,6-diethyl-4-hydroxymethyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione (M4), and
4-(7,9-dioxo-hexahydro-pyrazolo[1,2-d] [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-benzoic acid (M6), calculated as pinoxaden,
in/on the following commodities:
Commodity

Parts per million

Barley, bran
Barley, grain
Barley, hay
Barley, straw
Egg
Poultry, fat
Poultry, meat
Poultry, meat byproducts

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1.6
0.9
1.5
1.0
0.06
0.06
0.06
0.06

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Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

3.0
3.5
1.3
2.0
1.5

(2) For the combined residues of pinoxaden, 8-(2,6-diethyl-4-methylphenyl)-1,2,4,5-tetrahydro-7-oxo-7H-pyrazolo
[1,2-d][1,4,5] oxadiazepin-9-yl 2,2-dimethylpropanoate), and its metabolites M2, 8-(2,6-diethyl-4-methyl-phenyl)
-tetrahydro-pyrazolo[1,2-d][1,4,5]oxadiazepine-7,9-dione, and free and conjugated forms of M4, 8-(2,6-diethyl-4hydroxymethyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione, calculated as pinoxaden, in/on the
following commodities:
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Milk

0.04
0.04
0.04
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[70 FR 43322, July 27, 2005]

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§180.612 Topramezone; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide topramezone, including its metabolites and
degradates, in or on the following commodities. Compliance with the following tolerance levels is to be determined by
measuring only topramezone ([3-(4,5-dihydro-3-isoxazolyl)-2-methyl-4-(methylsulfonyl)phenyl](5-hydroxy-1-methyl1H-pyrazol-4-yl)methanone) in or on the following commodities:
Commodity

Parts per
million

Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Fish-freshwater finfish
Fish-saltwater finfish
Fish-shellfish, crustacean
Fish-shellfish, mollusk
Goat, meat byproducts
Hog, meat byproducts
Horse, meat byproducts
Poultry, meat byproducts
Sheep, meat byproducts

0.80
0.05
0.01
0.05
0.01
0.05
0.05
0.01
0.05
0.05
0.05
0.05
0.05
0.80
0.40
0.80
0.02
0.80

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[78 FR 48074, Aug. 7, 2013]

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§180.613 Flonicamid; tolerances for residues.
(a) General. (1) Tolerances are established for the residues of the insecticide flonicamid, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of flonicamid, N-(cyanomethyl)-4-(trifluoromethyl)-3-pyridinecarboxamide, and its
metabolites, TFNA (4-trifluoromethylnicotinic acid), TFNA-AM (4-trifluoromethylnicotinamide), and TFNG,

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N-(4-trifluoromethylnicotinoyl)glycine, calculated as the stoichiometric equivalent of flonicamid, in or on the following
commodities.
Commodity
Alfalfa, forage
Alfalfa, hay
Alfalfa, seed
Almond, hulls
Berry, low growing, subgroup 13-07G
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Cotton, gin byproducts
Cotton, hulls
Cotton, meal
Cotton, undelinted seed
Cucumber
Fruit, pome, group 11-10
Fruit, stone, group 12-12
Hop, dried cones
Nut, tree, group 14-12
Okra
Peppermint, tops
Potato, granules/flakes
Radish, tops
Rapeseed subgroup 20A
Spearmint, tops
Spinach
Tomato, paste
Tomato, puree
Turnip, greens
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy, except brassica, group 4, except spinach
Vegetable, root, except sugar beet, subgroup 1B
Vegetable, tuberous and corm, subgroup 1C

Parts per million
10.0
1.0
1.5
9.0
1.5
1.5
16
6.0
2.0
1.0
0.50
1.5
0.20
0.60
7.0
0.15
0.40
7.0
0.40
16
1.5
7.0
9.0
2.0
0.50
16
1.5
0.40
4.0
0.60
0.20

(2) Tolerances are established for the residues of the insecticide flonicamid, including its metabolites and degradates,
in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of flonicamid, N-(cyanomethyl)-4-(trifluoromethyl)-3-pyridinecarboxamide, and its metabolites,
TFNA (4-trifluoromethylnicotinic acid), and TFNA-AM (4-trifluoromethylnicotinamide), calculated as the Stoichiometric
equivalent of flonicamid, in or on the following commodities.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.03
0.08
0.08
0.04
0.03
0.08
0.08
0.03
0.03
0.03
0.03
0.08
0.08
0.05
0.03
0.03
0.03
0.03
0.08
0.08

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[70 FR 51614, Aug. 31, 2005, as amended at 71 FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, 2008; 77 FR 67776, Nov. 14, 2012;
78 FR 75266, Dec. 11, 2013]

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§180.614 Kasugamycin; tolerances for residues.
(a) General. Tolerances are established for residues of kasugamycin, including its metabolites and degradates, in or
on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by
measuring only kasugamycin (3-O-[2-amino-4-[(carboxyimino-methyl)amino]-2,3,4,6-tetradeoxyα-D-arabino-hexopyranosyl]-D-chiro-inositol) in or on the commodity.
Commodity

Parts per
million

Fruit, pome, group 11-10

0.20
0.04

Vegetable, fruiting, group 81
1

There is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[79 FR 51497, Aug. 29, 2014]

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§180.615 Amicarbazone; tolerances for residues.
(a) General. Tolerances are established for combined residues of the herbicide, amicarbazone [4-amino-4, 5-dihydroN-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and its metabolites DA amicarbazone
[N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and iPr-2-OH DA
amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide],
calculated as parent equivalents, in or on the following commodities:
Commodity

Parts per million

Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Corn, field, forage
Corn, field, grain
Corn, field, stover
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver
Poultry, liver

0.01
1.0
0.01
0.10
0.80
0.05
1.0
0.01
1.0
0.01
0.10
0.01
0.10
0.01
0.01
0.01
1.0
0.01
0.10
0.01
0.01
1.0
0.01
0.10
0.10

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of
amicarbazone [4-amino-4, 5-dihydro-N-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and
its metabolites DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1carboxamide] and iPr-2-OH DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1-methylethyl)-5-oxo1H-1,2,4-triazole-1-carboxamide], calculated as parent equivalents, in or on the following commodities when present
therein as a result of application of amicarbazone to the growing crops in paragraph (a) of this section:

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Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Cotton, gin byproducts
Cotton, undelinted seed
Soybean, forage
Soybean, hay
Soybean, seed
Wheat, bran
Wheat, flour
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, hay
Wheat, middlings,
Wheat, shorts
Wheat, straw

0.05
0.10
0.30
0.07
1.50
5.0
0.80
0.15
0.15
0.50
0.15
0.10
1.0
0.15
0.15
0.50

[70 FR 55760, Sept. 23, 2005, as amended at 74 FR 46377, Sept. 9, 2009]

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§180.616 Fenpropimorph; tolerances for residues.
Tolerances are established for the residues of the fungicide fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1-dimethylethyl)
phenyl]-2-methylpropyl]-2,6-dimethylmorpholine) in or on the following commodity:
Commodity

Parts per million

Banana*

2.0

*No U.S. registration as of February 10, 2006.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 15612, Mar. 29, 2006]

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§180.617 Metconazole; tolerances for residues.
(a) General. Tolerances are established for residues of metconazole, including its metabolites and degradates, in or
on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by
measuring only metconazole [5-[(4-chlorophenyl)methyl]-2,2-dimethyl-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol] as the
sum of its cis- and trans-isomers in or on the following commodities:
Commodity

Parts per
million

Almond, hulls
Banana1
Barley, grain
Barley, hay
Barley, straw
Beet, sugar, dried pulp
Beet, sugar, molasses
Beet, sugar, roots
Bushberry subgroup 13-07B
Cattle, meat byproducts
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, gin byproducts
Cotton, undelinted seed
Egg

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4.0
0.1
2.5
7.0
7.0
0.70
0.08
0.07
0.40
0.04
3.0
0.02
30
0.02
30
3.0
0.01
30.0
8.0
0.25
0.04

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Fruit, stone, group 12-12
Goat, meat byproducts
Grain, aspirated grain fractions
Horse, meat byproducts
Nut, tree, group 14-12
Oat, grain
Oat, hay
Oat, straw
Pea and bean, dried shelled, except soybean, subgroup 6C
Peanut
Peanut, refined oil
Rapeseed subgroup 20A
Rye, grain
Rye, straw
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Sugarcane, cane
Sunflower subgroup 20B
Vegetable, tuberous and corn, subgroup 1C
Wheat, grain
Wheat, hay
Wheat, milled byproducts
Wheat, straw

0.2
0.04
7.0
0.04
0.04
1.0
17
6.0
0.15
0.04
0.05
0.08
0.25
14
0.04
3.0
6.0
0.08
0.05
0.06
0.7
0.04
0.15
16
0.20
18

1

No U.S. registration as of August 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 56388, Sept. 27, 2006, as amended at 71 FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, 2008; 74 FR 21266, May 7, 2009;
76 FR 50904, Aug. 17, 2011; 76 FR 81396, Dec. 28, 2011; 77 FR 26456, May 4, 2012; 77 FR 66723, Nov. 7, 2012; 79 FR 12411,
Mar. 5, 2014; 80 FR 30625. May 29, 2015]

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§180.618 Benthiavalicarb-isopropyl; tolerance for residues.
(a) General. Tolerances are established for the combined residues of benthiavalicarb-isopropyl, isopropyl[(S)-1-[[[(1R)
-1-(6-fluoro-2-benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate and isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate, in or on the following raw agricultural commodities:
Commodity

Parts per million

Grape, imported
Grape, raisin
Tomato

0.25
1.0
0.45

Note: There are no U.S. registrations as of July 30, 2006.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect of inadvertent residues. [Reserved]
[71 FR 52003, Sept. 1, 2006]

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§180.619 Epoxiconazole; tolerances for residues.
(a) General. Tolerances are established for the residues of the fungicide epoxiconazole [(rel-1-[[(2R,3S)
-3-(2-chlorophenyl)-2-(4-fluorophenyl)oxiranyl]methyl]-1H-1,2,4-triazole]) in or on the following commodities:
Commodity

Parts per million

Banana*

0.5

Coffee*

0.05

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*

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No U.S. Registration as of August 4, 2006

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional Registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 53989, Sept. 13, 2006]

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§180.620 Etofenprox; tolerances for residues.
(a) General. A tolerance is established for residues of the insecticide etofenprox, including its metabolites and
degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this
paragraph is to be determined by measuring only etofenprox, 2-(4-ethoxyphenyl)-2-methylpropyl 3-phenoxybenzyl ether,
in or on the commodity.
Parts per
million
10.0
0.40
10.0
0.40
5.0
10.0
0.40
10.0
4.0
0.20
4.0
10.0
0.40
10.0
0.60
1.0
0.01
1.0
0.01
10.0
0.40
10.0

Commodity
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
All food commodities (including feed commodities) not otherwise listed in this subsection
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rice, grain
Sheep, fat
Sheep, meat
Sheep, meat byproducts

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 23498, Apr. 27, 2011, as amended at 78 FR 70877, Nov. 27, 2013]

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§180.621 Dithianon; tolerances for residues.
(a) General. Tolerances are established for residues of dithianon, including its metabolites and degradates, in or on
the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only dithianon, 5, 10-dihydro-5,10-dioxonaphtho(2,3-b)-1,4-dithiin-2,3-dicarbonitrile.
Commodity

Parts per
million

Fruit, pome, group 111
Grape 2
Hop, dried cones1

5
3
100

1

No U.S. registration as of September 5, 2006.

2

No U.S. registration as of January 29, 2010.

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[75 FR 5522, Feb. 3, 2010]

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§180.622 Ethaboxam; tolerances for residues.
(a) General. Tolerances are established for residues of ethaboxam, N-(cyano-2-thienylmethyl)-4-ethyl-2-(ethlyamino)
-5-thiazolecarboxamide in or on the following commodity:
Commodity

Parts per million

Grape1
1

6.0

There is no U.S. registration as of September 27, 2006

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 56392, Sept. 27, 2006]

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§180.623 Flufenoxuron; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide, flufenoxuron, 1-[4-(2-chloro-α,α,α-trifluoro-ptolyloxy)-2-fluorophenyl]-3-(2,6-difluorobenzoyl)urea, in or on the following food commodities.
Commodity

Parts per million

Apple1
Cattle, fat1

0.50
4.5

Cattle, meat1

0.10

Cattle, meat byproducts1

0.50

Goat, fat1

4.5

Goat, meat1

0.10

Goat, meat byproducts1

0.50

Grape1

0.70

Grape, raisin1
Horse, fat1

2.0
4.5

Horse, meat1

0.10

Horse, meat byproducts1
Milk

0.50

Milk, fat1

0.20
4.0

Orange1

0.30

Orange, oil1

60
0.50

Pear1
Sheep, fat1

4.5

Sheep, meat1

0.10

Sheep, meat byproducts1

0.50

1

There are no U.S. registrations as of September 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional restrictions. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 57436, Sept. 29, 2006]

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§180.624 Metrafenone; tolerances for residues.

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(a) General. Tolerances are established for residues of the fungicide metrafenone, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only metrafenone (3-bromo-6-methoxy-2-methylphenyl)(2,3,4-trimethoxy-6methylphenyl)methanone in or on the following commodities:
Commodity
Apricot
Cherry subgroup 12-12A
Fruit, pome, group 11-10
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Grape, raisin
Hop, dried cones
Peach subgroup 12-12B
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10

Parts per million
0.70
2.0
1.5
4.5
17
70
0.70
0.50
0.90

(b) Section 18 emergency exemption. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[71 FR 54917, Sept. 20, 2006, as amended at 75 FR 75393, Dec. 3, 2010; 79 FR 63053, Oct. 22, 2014]

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§180.625 Orthosulfamuron; tolerances for residues.
Link to an amendment published at 80 FR 72599, November 20, 2015.
(a) General. Tolerances are established for residues of orthosulfamuron 1-(4,6-dimethoxypyrimidin-2-yl)
-3-[2-(dimethylcarbamoyl)- phenylsulfamoyl] urea) per se in or on the following commodities:
Commodity

Parts per million

Rice, grain
Rice, straw

0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect and inadvertant residues. [Reserved]
[72 FR 8931, Feb. 28, 2007]

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§180.626 Prothioconazole; tolerances for residues.
(a) General. (1) Tolerances are established for residues of prothioconazole, 2-[2-(1-chlorocylcopropyl)
-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2-dihydro-3H-1,2,4-triazole-3-thion, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only prothioconazole and its metabolite prothioconazole-desthio, or α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)
methyl]-1H-1,2,4-triazole-1-ethanol, calculated as parent in or on the commodity.
Commodity
Alfalfa, forage
Alfalfa, hay
Beet, sugar, roots
Berry, low growing, except strawberry, subgroup 13-07H
Bushberry, subgroup 13-07B
Corn, sweet kernel plus cob with husks removed
Grain, aspirated grain fractions
Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; forage
Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; hay
Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; stover
Grain, cereal, forage, fodder and straw, group 16, except sorghum, straw
Grain, cereal, group 15, except sweet corn and sorghum
Pea and bean, dried shelled, except soybean, subgroup 6C
Peanut
Potato

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Parts per
million
0.02
0.02
0.25
0.20
2.0
0.04
11
8.0
7.0
10
5.0
0.35
0.9
0.02
0.02

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Rapeseed, seed
Rice, hulls
Soybean, forage
Soybean, hay
Soybean, seed
Vegetable, cucurbit, crop group 9

0.15
0.90
4.5
17
0.15
0.30

(2) Tolerances are established for residues of prothioconazole, 2-[2-(1-chlorocylcopropyl)-3-(2-chlorophenyl)-2hydroxypropyl]-1,2-dihydro-3H-1,2,4-triazole-3-thion, including its metabolites and degradates, in or on the commodities in
the table below. Compliance with the tolerance levels specified below is to be determined by measuring only
prothioconazole and its metabolites prothioconazole-desthio, or α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)methyl]
-1H-1,2,4-triazole-1-ethanol, and conjugates that can be converted to these two compounds by acid hydrolysis, calculated
as parent in or on the commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry liver
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.1
0.02
0.2
0.1
0.02
0.2
0.05
0.1
0.02
0.2
0.02
0.02
0.1
0.02
0.2

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 11783, Mar. 14, 2007, as amended at 73 FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, 2009; 74 FR 46699, Sept. 11,
2009; 75 FR 29914, May 28, 2010; 76 FR 61592, Oct. 5, 2011; 78 FR 67052, Nov. 8, 2013]

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§180.627 Fluopicolide; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide fluopicolide [2,6-dichloro-N-[[3-chloro5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide], including its metabolites and degradates, in or on the commodities in the
table in this paragraph. Compliance with the tolerance levels specified below is to be determined by measuring only
fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide] in or on the commodity.
Commodity

Parts per million

Brassica, head and stem, subgroup 5A
Grape
Grape, raisin
Potato, processed potato waste
Vegetable, brassica (cole) leafy subgroup 5B
Vegetable, bulb, crop group 3-07
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable root, subgroup 1A
Vegetable, tuberous and corm subgroup 1C

5.0
2.0
6.0
1.0
18
7.0
0.50
1.60
25
15.0
0.15
0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide fluopicolide
[2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide], including its metabolites and degradates, in or
on the commodities in the table in this paragraph. Compliance with the tolerance levels specified below is to be

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determined by measuring only fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide] in or
on the commodity.
Commodity

Parts per
million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Wheat, aspirated grain fractions
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, milled byproducts
Wheat, straw

0.08
0.01
0.20
0.07
0.20
0.02
0.50
0.07
0.50

[72 FR 14447, Mar. 28, 2007, as amended at 73 FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, 2008; 76 FR 22054, Apr. 20, 2011;
79 FR 12401, Mar. 5, 2014; 79 FR 45693, Aug. 6, 2014]

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§180.628 Chlorantraniliprole; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide chlorantraniliprole, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only chlorantraniliprole, 3-bromo-N-[4-chloro-2-methyl-6-[(methylamino)carbonyl]phenyl]
-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxamide.
Commodity

Parts per million

Acerola
Alfalfa, seed
Almond, hulls
Animal feed, nongrass, group 18, forage
Animal feed, nongrass, group 18, hay
Apple, wet pomace
Artichoke, globe
Asparagus
Atemoya
Avocado
Banana
Beet, sugar, molasses
Berry, large shrub/tree, subgroup 13-07C
Berry, low growing, subgroup 13-07G
Biriba
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry, subgroup 13-07B
Cacao bean
Cacao bean, chocolate
Cacao bean, cocoa powder
Cacao bean, roasted bean
Cactus
Canistel
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherimoya
Cherry, sweet
Cherry, tart
Citrus, dried pulp
Coffee, green bean
Coffee, instant
Corn, field, grain
Corn, field, milled byproducts
Corn, pop, grain
Corn, sweet, kernel plus cobs with husk removed
Cotton, gin byproduct
Cotton, hulls
Cottonseed subgroup 20C
Crayfish
Custard apple
Egg
Feijoa
Fig

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2.0
7.0
5.0
25
90
2.5
4.0
13
4.0
4.0
4.0
9.0
2.5
1.0
4.0
4.0
11
2.5
0.08
1.5
1.5
0.8
13
4.0
0.5
0.1
0.5
4.0
2.0
2.0
14
0.4
2.0
0.04
0.1
0.04
0.02
30
0.40
0.3
8.0
4.0
0.2
4.0
4.0

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Fruit, caneberry, subgroup 13-07A
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small vine climbing, subgroup 13-07F
Fruit, stone, group 12-12, except cherry, chickasaw plum, and damson plum
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated grain fractions
Grain, cereal, except rice and corn, group 15
Grain, cereal, forage, fodder and straw, group 16
Grape, raisin
Grass forage, fodder and hay, group 17
Guava
Herb subgroup 19A, dried leaves
Herb subgroup 19A, fresh leaves
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, meat
Horse, meat byproducts
Ilama
Jaboticaba
Longan
Lychee
Mango
Milk
Nut, tree, group 14
Olive
Olive, oil
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Papaya
Passionfruit
Peanut
Peanut, hay
Peppermint, tops
Persimmon
Pineapple
Pineapple, process residue
Pistachio
Plum, chickasaw
Plum, damson
Pomegranate
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Pulasan
Rambutan
Rapeseed subgroup 20A
Rice, grain
Rice, hulls
Sapodilla
Sapote, black
Sapote, mamey
Sapote, white
Sheep, fat
Sheep, meat
Sheep meat byproducts
Soursop
Spanish lime
Spearmint, tops
Spice, subgroup 19B
Star apple
Starfruit
Sugar apple
Sugarcane, cane
Sugarcane, molasses
Sunflower subgroup 20B
Tea, dried
Ti, leaves

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1.8
1.4
1.2
2.5
4.0
0.5
0.1
0.5
640
6.0
40
5.0
90
4.0
90
25
0.05
0.02
0.05
90
0.5
0.1
0.5
4.0
2.0
4.0
2.0
4.0
0.1
0.04
4.0
40
0.30
3.0
4.0
4.0
0.06
90
9.0
4.0
1.5
3.0
0.04
2.0
2.0
4.0
0.2
0.05
0.2
4.0
4.0
2.0
0.15
0.4
4.0
4.0
4.0
4.0
0.5
0.1
0.5
4.0
4.0
9.0
90
4.0
4.0
4.0
14
420
2.0
50.0
13.0

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Ti, root
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8-10
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, group 6
Vegetable, root and tuber, group 1
Wax jambu

0.3
0.5
90
1.4
13
40.0
2.0
0.30
4.0

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[75 FR 5532, Feb. 3, 2010, as amended at 75 FR 17566, Apr. 7, 2010; 76 FR 44821, July 27, 2011; 76 FR 59909, Sept. 28, 2011;
77 FR 60315, Oct. 3, 2012; 77 FR 75561, Dec. 21, 2012; 78 FR 57285, Sept. 18, 2013; 79 FR 7401, Feb. 7, 2014]
EDITORIAL NOTE: At 78 FR 57285, Sept. 18, 2013, §180.628 was amended by revising the commodity “Egg” in the table in
paragraph (a); however, no revised text was provided, so the amendment could not be incorporated.

Back to Top
§180.629 Flutriafol; tolerances for residues.
(a) General. Tolerances are established for the residues of flutriafol, [(±)-α-(2-fluorophenyl)-α-(4-fluorophenyl)
-1H-1,2,4-triazole-1-ethanol], including its metabolites and degradates in or on the following commodities. Compliance with
the following tolerances is to be determined by measuring flutriafol only.
Commodity

Parts per million

African tree nut
Almond
Almond, hull
Banana1
Beet sugar
Brassica, head and stem (subgroup 5A)
Brassica, leafy greens (subgroup 5B)
Brazil nut
Bur oak
Butternut
Cajou
Cashew
Castanha-do-maranhao
Cattle, fat
Cattle, liver
Cattle, meat byproducts, except liver
Cattle, muscle
Coconut
Coffee, green, bean1
Coffee, instant1
Coquito nut
Corn, field, forage
Corn, field, grain
Corn, field, refined oil
Corn, field, stover
Corn, pop
Corn, pop, stover
Cotton, gin byproducts
Cotton, undelinted seed
Dika nut
Egg
Fruit, pome, group 11-09
Fruit, stone, group 12-10
Goat, fat
Goat, liver
Goat, meat byproducts, except liver
Goat, muscle
Grain, aspirated fractions
Grape
Grape, raisin
Guiana chestnut

http://www.ecfr.gov/cgi-bin/text-idx?SID=2bfc27a0cb2e213f68a1dad2eb0973b9&mc=tru...

0.02
0.60
15
0.30
0.08
1.5
7.0
0.02
0.02
0.02
0.02
0.02
0.02
0.05
1.0
0.05
0.05
0.02
0.15
0.30
0.02
5.0
0.01
0.02
15
0.01
15
6.0
0.50
0.02
0.01
0.40
1.5
0.05
1.0
0.05
0.05
6.0
1.5
2.4
0.02

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Hazelnut
Heartnut
Hickory nut
Hog, fat
Hog, meat byproducts
Hog, muscle
Hop, dried cones
Horse, fat
Horse, liver
Horse, meat byproducts, except liver
Horse, muscle
Japanese horse-chestnut
Lettuce, head
Macadamia nut
Milk
Mongongo nut
Monkey-pot
Pachira nut
Peanut
Peanut, hay
Pecan
Poultry, fat
Poultry, meat byproducts
Radicchio
Sapucaia nut
Sheep, fat
Sheep, liver
Sheep, meat byproducts, except liver
Sheep, muscle
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, seed
Strawberry
Tomato, paste
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy, except Brassica, crop group 4, except head lettuce and radicchio
Walnut, black
Walnut, English
Wheat, bran
Wheat, forage
Wheat, germ
Wheat, grain
Wheat, hay
Wheat, straw

0.02
0.02
0.02
0.01
0.05
0.01
20
0.05
1.0
0.05
0.05
0.02
1.5
0.02
0.02
0.02
0.02
0.02
0.09
15
0.02
0.01
0.01
1.5
0.02
0.05
1.0
0.05
0.05
2.0
1.5
6.0
0.35
1.5
1.5
0.30
1.0
10
0.02
0.02
0.30
30
0.25
0.15
15
9.0

1

There are no U.S. registrations as of October 22, 2013.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide
flutriafol, including its metabolites and degradates, in or on the commodities in the table below when present therein as a
result of the application of flutriafol to the growing crops listed in the table to paragraph (a) of this section. Compliance with
the following tolerance levels specified below is to be determined by measuring only flutriafol ((±)-α-(2-fluorophenyl)
-α-(4-fluorophenyl)-1H-1,2,4-triazole-1-ethanol) in or on the following commodities:
Commodity

Parts per million

Corn, sweet, forage
Corn, sweet, kernel plus cob with husk removed
Corn, sweet, stover

0.09
0.01
0.07

[75 FR 26673, May 12, 2010, as amended at 76 FR 69647, Nov. 9, 2011; 77 FR 47301, Aug. 8, 2012; 77 FR 48901, Aug. 15, 2012;
78 FR 75262, Dec. 11, 2013; 79 FR 32673, June 6, 2014; 80 FR 5951, Feb. 4, 2015; 80 FR 71952, Nov. 18, 2015]

Back to Top
§180.630 Flusilazole; tolerances for residues.
(a) General. [Reserved]

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(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fungicide,
flusilazole, (1-[[bis(4-fluorophenyl)methylsilyl]methyl]-1H-1,2,4-triazole) in connection with use of the pesticide under
Section 18 emergency exemptions granted by EPA. The tolerances expire and are revoked on the dates specified in the
following table.
Commodity
Soybean, aspirated grain fractions
Soybean, seed
Soybean, oil

Parts per million

Expiration/revocation date
2.6
0.04
0.10

12/31/10
12/31/10
12/31/10

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[72 FR 49660, Aug. 29, 2007]

Back to Top
§180.631 Pyrasulfotole; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide pyrasulfotole, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of pyrasulfotole ((5-hydroxy-1,3-dimethyl-1H-pyrazol-4-yl)[2-(methylsulfonyl)
-4-(trifluoromethyl)phenyl]methanone) and its desmethyl metabolite (5-hydroxy-3-methyl-1H-pyrazol-4-yl)
[2-(methylsulfonyl)-4-(trifluoromethyl)phenyl]methanone), calculated as the stoichiometric equivalent of pyrasulfotole, in or
on the commodities:
Commodity

Parts per million

Aspirated grain fractions
Barley, grain
Barley, hay
Barley, straw
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Eggs
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Grass, forage
Grass, hay
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rye, forage
Rye, grain
Rye, straw
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Wheat, forage
Wheat, grain
Wheat, hay

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0.40
0.02
0.30
0.20
0.03
3.0
0.02
0.70
0.02
0.03
3.0
0.02
0.70
25
3.5
0.02
0.30
0.02
0.05
0.03
3.0
0.02
0.70
0.03
0.10
0.08
0.50
0.20
0.02
0.02
0.20
0.20
0.02
0.20
0.03
3.0
0.02
0.70
1.5
0.70
0.80
0.20
0.02
0.80

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Wheat, straw

0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 45649, Aug. 15, 2007, as amended at 76 FR 23898, Apr. 29, 2011]

Back to Top
§180.632 Fenazaquin; Tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide fenazaquin, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only fenazaquin, or 4-[2-[4-(1,1-dimethylethyl)phenyl]-ethoxy]quinazoline.
Parts per
million

Commodity
Almond
Almond, hulls
Apple
Cherry
Citrus Oil
Fruit, Citrus, Group 10 except Grape fruit
Pear

0.02
4.0
0.2
2.0
10
0.5
0.2

(b) Section is emergency exempotions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 44393, Aug. 8, 2007, as amended at 80 FR 25958, May 6, 2015]

Back to Top
§180.633 Florasulam; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide florasulam N-(2,6-difluorophenyl)-8-fluoro-5methoxy(1,2,4)triazolo(1,5-c)pyrimidine-2-sulfonamide in or on the following commodities:
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Rye, forage
Rye, grain
Rye, straw
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.01
0.05
0.05
0.05
0.01
0.05
0.05
0.05
0.01
0.05
0.05
0.01
0.05
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 55077, Sept. 28, 2007]

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§180.634 Tembotrione; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the herbicide tembotrione, including its metabolites and
degradates, in or on the commodities listed in the table to this paragraph. Compliance with the tolerance levels specified
below is to be determined by measuring only the sum of tembotrione, 2-[2-chloro-4-(methylsulfonyl)-3[(2,2,2-trifluoroethoxy)methyl]benzoyl]-1,3-cyclohexanedione and its metabolite, 2-[2-chloro-4-(methylsulfonyl)-3[(2,2,2-trifluoroethoxy) methyl]benzoyl]-4,6-dihydroxy-1,3-cyclohexanedione, calculated as the stoichiometric equivalent of
tembotrione, in or on the following commodities.
Commodity

Parts per million

Cattle, liver
Cattle, meat byproducts, except liver
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, stover
Goat, liver
Goat, meat byproducts, except liver
Horse, liver
Horse, meat byproducts, except liver
Poultry, liver
Sheep, liver
Sheep, meat byproducts, except liver

0.40
0.07
0.60
0.02
0.45
0.02
0.35
0.35
0.60
0.40
0.07
0.40
0.07
0.07
0.40
0.07

(2) Tolerances are established for residues of the herbicide tembotrione, including its metabolites and degradates, in
or on the commodities listed in the table to this paragraph. Compliance with the tolerance levels specified below is to be
determined by measuring only tembotrione, 2-[2-chloro-4-(methylsulfonyl)-3-[(2,2,2-trifluoroethoxy)methyl]benzoyl]
-1,3-cyclohexanedione in or on the following commodities.
Commodity

Parts per million

Corn, sweet, kernel plus cob with husks removed

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[72 FR 55085, Sept. 28, 2007, as amended at 74 FR 47894, Sept. 18, 2009]

Back to Top
§180.635 Spinetoram; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide spinetoram, expressed as a
combination of XDE-175-J: 1-H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione, 2-[(6-deoxy-3-O-ethyl-2,4-di-O-methyl-aL-mannopyranosyl) oxy]-13-[[(2R,5S,6R)-5- (dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl] oxy]-9ethyl-2,3,3a,4,5,5a,5b,6,9, 10,11,12,13,14,16a,16b- hexadecahydro 14-methyl-, (2R,3aR,5aR,5bS,9S,
13S,14R,16aS,16bR); XDE-175-L: 1H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione, 2-[(6-deoxy-3-O- ethyl-2,4-di-Omethyl-a-L-mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5-(dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9ethyl-2,3,3a,5a,5b,6,9, 10,11,12,13,14,16a,16b- tetradecahydro-4,14-dimethyl-, (2S,3aR,5aS,5bS,9S,
13S,14R,16aS,16bS); ND-J: (2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR)-9-ethyl-14-methyl-13-[[(2S,5S,6R)-6- methyl5-(methylamino)tetrahydro- 2H-pyran-2-yl]oxy]-7,15-dioxo-2,3,3a,4,5,5a,5b,6,7,9, 10,11,12,13,14,15,16a,16boctadecahydro-1H-as- indaceno[3,2-d]oxacyclododecin-2-yl 6-deoxy-3-O-ethyl-2,4-di-O-methyl- alpha-Lmannopyranoside; and NF-J: (2R,3S,6S)-6-([(2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR)- 2-[(6-deoxy-3-O-ethyl-2,4-di-Omethyl-alpha-L-mannopyranosyl) oxy]-9-ethyl-14-methyl-7,15-dioxo-2, 3,3a,4,5,5a,5b,6,7,9, 10,11,12,13,14,15,16a,16boctadecahydro-1H-as- indaceno[3,2-d]oxacyclododecin-13-yl] oxy)-2-methyltetrahydro- 2H-pyran-3-yl(methyl)formamide,
in or on the following raw agricultural commodities:
Commodity

Parts per million

Acerola
Almond, hulls
Amaranth grain, grain
Apple, wet pomace
Artichoke, globe
Asparagus
Atemoya
Avocado
Banana
Beet, sugar, molasses

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0.30
19
1.0
0.50
0.30
0.04
0.30
0.30
0.25
0.75

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Biriba
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Bushberry, subgroup 13B
Caneberry, subgroup 13A
Canistel
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts (except liver)
Cherimoya
Citrus, dried pulp
Citrus, oil
Corn, sweet, kernel plus cob with husks removed
Cotton, gin byproducts
Cotton, undelinted seed
Cranberry
Custard apple
Date
Egg
Feijoa
Fig
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts (except liver)
Grain, aspirated fractions
Grain, cereal, group 15, except rice, sorghum, pearl millet and proso millet
Grain, cereal, group 16, forage
Grain, cereal, group 16, hay
Grain, cereal, group 16, stover
Grain, cereal, straw, group 16, except rice
Grape
Grape, raisin
Guava
Herb, dried, subgroup 19A
Herb, fresh, subgroup 19A
Hog, fat
Hog, meat
Hog, meat byproducts
Hop, dried cones
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts (except liver)
Ilama
Jaboticaba
Juneberry
Lingonberry
Longan
Lychee
Mango
Milk
Milk, fat
Millet, pearl, grain
Millet, proso, grain
Nut, tree, group 14
Okra
Onion, green
Papaya
Passionfruit
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut
Peanut, hay
Peppermint, tops
Pineapple
Pineapple, processed residue
Pistachio
Pomegranate

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0.30
2.0
10
0.25
0.70
0.30
5.5
0.85
0.20
0.60
0.30
0.50
3.0
0.04
1.5
0.04
0.04
0.30
0.10
0.04
0.30
0.10
0.30
0.20
0.20
5.5
0.85
0.20
0.60
20
0.04
3.5
10
10
1.0
0.50
0.70
0.30
22
3.0
0.40
0.04
0.04
22
5.5
0.85
0.20
0.60
0.30
0.30
0.25
0.25
0.30
0.30
0.30
0.30
7.5
1.0
1.0
0.10
0.40
2.0
0.30
0.30
0.04
0.04
0.04
11
3.5
0.04
0.15
0.10
0.30

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Poultry, fat
Poultry, meat
Poultry, meat byproducts
Pulasan
Rambutan
Salal
Sapodilla
Sapote, black
Sapote, mamey
Sapote, white
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat products (except liver)
Sorghum, grain, grain
Soursop
Soybean, seed
Spanish lime
Spearmint, tops
Spice, subgroup 19B, except black pepper
Star apple
Star fruit
Strawberry
Sugar apple
Ti, leaves
Vegetable, bulb, group 3, except green onion
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8
Vegetable, leafy, except Brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root and tuber, group 1
Watercress
Wax jambu

0.10
0.04
0.04
0.30
0.30
0.25
0.30
0.30
0.30
0.30
5.5
0.85
0.20
0.60
1.0
0.30
0.04
0.30
3.5
1.7
0.30
0.30
1.0
0.30
10
0.10
0.30
8.0
0.40
8.0
10
0.30
0.10
8.0
0.30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect and invertent residues. [Reserved]
[72 FR 57499, Oct. 10, 2007, as amended at 73 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, 2009]

Back to Top
§180.636 1,3-dichloropropene; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the fungicide cis- and trans-1,3-dichloropropene
and its metabolites cis- and trans-3-chloroacrylic acid, and cis- and trans-3-chloroallyl alcohol in or on the following
commodities.
Commodity

Parts per million

Grape

0.018

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 8218, Feb. 13, 2008]

Back to Top
§180.637 Mandipropamid; tolerances for residues.
(a) General. Tolerances are established for residues of mandipropamid, including its metabolites and degradates, in
or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined
by measuring only mandipropamid (4-chloro-N-[2-[3-methoxy-4-(2-propynyloxy)phenyl]ethyl]-α-(2-propynyloxy)
benzeneacetamide) in or on the commodity.

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Commodity
Basil, dried leaves
Basil, fresh leaves
Bean, snap
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Ginseng
Grape, raisin
Hop, dried cones
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Potato, wet peel
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy except Brassica, group 4
Vegetable, tuberous and corm, subgroup 1C

Parts per million
200
30
0.90
3
25
1.4
0.30
3.0
50
0.05
4.0
0.03
0.6
1.0
20
0.01

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of mandipropamid,
including its metabolites and degradates, in or on the commodities listed in the table below resulting from use of the
pesticide pursuant to FFIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified below is
to be determined by measuring only mandipropamid (4-chloro-N-[2-[3-methoxy-4-(2-propynyloxy)phenyl]ethyl]
-α-(2-propynyloxy)benzeneacetamide) in or on the commodity. The tolerances expire on the date specified in the table.
Commodity
Basil, dried

Parts per million
240

Expiration/revocation date
12/31/15

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent tolerances. [Reserved]
[73 FR 2816, Jan. 16, 2008, as amended at 74 FR 33169, July 10, 2009; 76 FR 55804, Sept. 9, 2011; 77 FR 74119, Dec. 13, 2012;
78 FR 76992, Dec. 20, 2013]

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§180.638 Pyroxsulam; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide pyroxsulam, N-(5,7-dimethoxy[1,2,4]triazolo
[1,5-a]pyrimidin-2-yl)-2-methoxy-4-(trifluoromethyl)-3-pyridinesulfonamide in or on the raw agricultural commodities:
Commodity

Parts per million

Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.06
0.01
0.01
0.03

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 10402, Feb. 27, 2008]

Back to Top
§180.639 Flubendiamide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of flubendiamide, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined
by measuring only flubendiamide N2-[1, 1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4- [1,2,2,2-tetrafluoro1-(trifluoromethyl)ethyl]phenyl]-1,2-benzenedicarboxamide, in or on the following commodities:
Commodity

Parts per million

Almond, hulls
Apple, wet pomace
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover

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9.0
5.0
8.0
0.03
15
0.02
15

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Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton gin byproducts
Cotton, undelinted seed
Fruit, pome, group 11
Fruit, stone, group 12
Grape
Nut, tree, group 14
Okra
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8
Vegetable, leafy, except Brassica, group 4

9.0
0.01
25
60
0.90
1.5
1.6
1.4
0.06
0.30
0.20
0.60
11

(2) Tolerances are established for residues of flubendiamide, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by
measuring only flubendiamide N2-[1,1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4-[1,2,2,2-tetrafluoro1-(trifluoromethyl)ethyl]phenyl]-1,2-benzenedicarboxamide, in or on the following commodities:
Commodity
Alfalfa, forage
Alfalfa, hay
Artichoke, globe
Berry, low growing, subgroup 13-07G, except cranberry
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Fruit, small fruit vine climbing except fuzzy kiwifruit, subgroup 13-07F
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated grain fractions
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Milk, fat
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut, hay
Peanut, meal
Peanut, nutmeat
Peanut, refined oil
Pistachio
Poultry, fat
Poultry, liver
Poultry, meat

Parts per million

Rice, grain1
Safflower, seed
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Sugarcane, cane
Sunflower, seed
Turnip, greens
Vegetable, foliage of legume, except soybean, subgroup 7A
Vegetable, legume, edible podded, subgroup 6A

25
65
1.6
1.5
3.0
25
0.70
0.08
0.60
0.40
1.4
0.70
0.08
0.60
153
0.15
0.03
0.15
0.70
0.08
0.60
0.15
1.0
0.60
0.05
60
0.03
0.02
0.03
0.06
3.0
0.60
0.10
0.50
5.0
0.70
0.08
0.60
12
5.0
14
18
60
0.80
0.25
0.30
5.0
25
35
0.50

1

There are no U.S. registrations for rice, grain.

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for residues of flubendiamide, including its metabolites
and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is
to be determined by measuring only flubendiamide N2-[1, 1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl]-1, 2-benzenedicarboxamide, in or on the following commodities:
Commodity

Parts per million

Barley, hay
Barley, straw
Buckwheat
Clover, forage
Clover, hay
Grass, forage
Grass, hay
Millet, pearl, forage
Millet, pearl, hay
Millet, proso, forage
Millet, proso, hay
Millet, proso, straw
Oats, forage
Oats, hay
Oats, straw
Rye, forage
Rye, straw
Teosinte, forage
Teosinte, hay
Teosinte, straw
Triticale, forage
Triticale, hay
Triticale, straw
Wheat, forage
Wheat, hay
Wheat, straw

0.04
0.07
0.07
0.15
0.04
0.15
0.04
0.15
0.04
0.15
0.04
0.07
0.15
0.04
0.07
0.15
0.07
0.15
0.04
0.07
0.15
0.04
0.07
0.15
0.03
0.03

[76 FR 16307, Mar. 23, 2011, as amended at 76 FR 55273, Sept. 7, 2011; 77 FR 73945, Dec. 12, 2012]

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§180.640 Pyridalyl; tolerances for residues.
(a) General. Tolerances are established for residues of pyridalyl, pyridine,2-[3-[2,6-dichloro-4-[(3,3-dichloro-2propenyl)oxy]phenoxy]propoxy]-5-(trifluoromethyl, in or on the following raw agricultural commodities:)
Commodity

Parts per million

Brassica, head and stem, subgroup 5A
Mustard greens
Turnip greens
Vegetable, fruiting, group 8
Vegetables, leafy, except Brassica, group 4

3.5
30
30
1.0
20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 25533, May 7, 2008]

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§180.641 Spirotetramat; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide spirotetramat, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of spirotetramat (cis-3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3en-4-yl-ethyl carbonate) and its metabolites cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2one, cis-3-(2,5-dimethylphenyl)-3-hydroxy-8-methoxy-1-azaspiro[4.5]decane-2,4-dione, cis-3-(2,5-dimethylphenyl)-8methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl beta-D-glucopyranoside, and cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-

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methoxy-1-azaspiro[4.5]decan-2-one, calculated as the stoichiometric equivalent of spirotetramat, in or on the following
commodities.
Commodity

Parts per million

Acerola
Almond, hulls
Artichoke, globe
Aspirated grain fractions
Avocado
Berry, low growing, except strawberry, subgroup 13-07H
Black sapote
Brassica, head and stem, subgroup 5A
Brassica, leafy, subgroup 5B
Bushberry subgroup 13-07B
Canistel
Citrus, oil
Coffee, green bean
Coffee, instant
Corn, sweet, kernel plus cob with husks removed
Cotton gin byproducts1
Cotton, undelinted seed1
Feijoa
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, stone, group 12
Grape, raisin
Guava
Hop, dried cones
Jaboticaba
Longan
Lychee
Mamey sapote
Mango
Nut, tree, group 14
Papaya
Passionfruit
Persimmon
Pineapple
Pistachio
Pomegranate
Potato, flakes
Pulasan
Rambutan
Sapodilla
Small fruit vine climbing subgroup, except fuzzy kiwifruit, subgroup 13-07F
Soybean forage
Soybean hay
Soybean seed
Spanish lime
Star apple
Starfruit
Strawberry1
Taro, leaves
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, except soybean, subgroup 07A
Vegetable, fruiting, group 8-10
Vegetable, leafy, except brassica, group 4
Vegetable, legume, group 06, except soybean
Vegetable, tuberous and corm, subgroup 1C
Watercress
Wax jambu
White sapote

2.5
9.0
1.5
10.0
0.60
0.30
0.60
2.5
8.0
3.0
0.60
6.0
0.20
0.50
1.5
10.0
0.30
2.5
0.60
0.70
4.5
3.0
2.5
10.0
2.5
13.0
13.0
0.60
0.60
0.25
0.40
2.5
2.5
0.30
0.25
0.50
1.6
13.0
13.0
0.60
1.3
8.0
16.0
5.0
13
0.60
2.5
0.40
9.0
0.80
0.30
7.0
2.5
9.0
2.5
0.60
2.0
2.5
0.60

1

Import tolerance only. There are no U.S. registrations for cotton or strawberry.

(2) Tolerances are also established for residues of the insecticide spirotetramat, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of spirotetramat (cis-3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3en-4-yl-ethyl carbonate]) and its metabolite cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2one, calculated as the stoichiometric equivalent of spirotetramat, in or on the following commodities:

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Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Eggs
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.02
0.02
0.20
0.02
0.02
0.02
0.20
0.02
0.02
0.02
0.20
0.01
0.02
0.02
0.02
0.20

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the
insecticide spirotetramat, including its metabolites and degradates, in or on the commodities in the table below.
Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spirotetramat (cis3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl-ethyl carbonate) and its metabolites cis3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5-dimethylphenyl)-3-hydroxy-8methoxy-1-azaspiro[4.5]decane-2,4-dione, cis-3-(2,5-dimethylphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl betaD-glucopyranoside, and cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]decan-2-one, calculated as the
stoichiometric equivalent of spirotetramat, in or on the following commodities.
Commodity

Parts per million

Banana

4.0

(d) Indirect or inadvertant residues. [Reserved]
[73 FR 39256, July 9, 2008, as amended at 76 FR 28681, May 18, 2011; 77 FR 8746, Feb. 15, 2012; 77 FR 75859, Dec. 26, 2012;
78 FR 28512, May 15, 2013; 78 FR 66651, Nov. 6, 2013]

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§180.642 Gentamicin; tolerances for residues.
(a) General. [Reserved]
(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for
residues of gentamicin in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to
FIFRA section 18 emergency exemptions. The tolerances expire and are revoked on the date specified in the following
table.
Commodity

Parts per million

Apple

Expiration/revocation date
0.10

12/31/10

(c) Tolerance with regional restrictions. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[73 FR 44162, July 30, 2008]

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§180.643 Uniconazole; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide/plant growth regulator uniconazole-P, (E)-(S)
-1-(4-chlorophenyl)-4,4-dimethyl-2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, its R-enantiomer and its Z-isomer in or on the
following raw agricultural commodities:
Commodity

Parts per million

Vegetable, fruiting, group 8

0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertant residues. [Reserved]
[73 FR 51736, Sept. 5, 2008]

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§180.644 Cyprosulfamide; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide safener cyprosulfamide,
N-[[4-[(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, in or on the following raw agricultural
commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.20
0.01
0.20
0.01
0.20
0.40
0.01
0.35

(2) Tolerances are established for residues of the herbicide safener cyprosulfamide, N-[[4-[(cyclopropylamino)
carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, and its metabolite 4-(aminosulfonyl)-N-cyclopropylbenzamide, calculated
as cyprosulfamide, in or on the following raw agricultural commodities:
Commodity

Parts per million

Cattle, meat byproducts
Goat, meat byproducts
Horse, meat byproducts
Sheep, meat byproducts

0.02
0.02
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[73 FR 60974, Oct. 15, 2008]

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§180.645 Thiencarbazone-methyl; tolerances for residues.
(a) General. (1) Tolerances are established for residues of thiencarbazone-methyl [methyl 4-[[[(4,5-dihydro-3methoxy-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)-carbonyl]amino]sulfonyl]-5-methyl-3-thiophenecarboxylate], per se, in or on
the following food and feed commodities:
Commodity

Parts per million

Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.04
0.01
0.02
0.01
0.01
0.05
0.01
0.05
0.10
0.01
0.01
0.01

(2) Tolerances are established for combined residues of thiencarbazone-methyl and its metabolite BYH 18636-MMT
[5-methoxy-4-methyl-2,4-dihydro-3H-1,2,4-triazol-3-one], calculated as the parent compound, in or on the following food
commodities of animal origin:
Commodity

Parts per million

Cattle, meat
Cattle, meat byproducts
Goat, meat
Goat, meat byproducts
Horse, meat

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0.02
0.02
0.02
0.02
0.02

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Horse, meat byproducts
Milk
Sheep, meat
Sheep, meat byproducts

0.02
0.02
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent combined residues of
thiencarbazone-methyl and its metabolite BYH 18636-MMT-glucoside [2-hexopyranosyl-5-methoxy-4-methyl-2,4-dihydro3H-1,2,4-triazol-3-one], calculated as the parent compound, in or on the following food commodities:
Commodity

Parts per million

Soybean, forage
Soybean, hay

0.04
0.15

[73 FR 60968, Oct. 15, 2008]

Back to Top
§180.646 Ipconazole; tolerances for residues.
(a) General. Tolerances are established for residues of ipconazole, including its metabolites and degradates, in or on
the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only ipconazole (2-[(4-chlorophenyl)methyl]-5-(1-methylethyl)-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol) in or
on the commodity.
Commodity
Cotton, gin byproducts
Cotton, undelinted seed
Grain, cereal, forage, fodder and straw, group 16, except rice
Grain, cereal group 15, except rice
Peanut
Soybean, forage
Vegetable, legume, group 6

Parts per million
0.01
0.01
0.01
0.01
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[73 FR 69559, Nov. 19, 2008, as amended at 79 FR 15240, Mar. 19, 2014]

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§180.647 d-Phenothrin; tolerances for residues.
(a) General. A tolerance of 0.01 parts per million is established for residues of the insecticide d-phenothrin in or on all
food/feed crops following wide-area mosquito adulticide applications.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[74 FR 32443, July 8, 2009]

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§180.648 Meptyldinocap; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the fungicide meptyldinocap, 2-(1-methylheptyl)
-4,6-dinitrophenyl (2E)-2-butenoate and 2,4-DNOP, 2,4-dinitro-6-(1-methylheptyl)phenol expressed as meptyldinocap in or
on the following commodities:
Commodity
Grape

Parts Per Million
0.20

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[74 FR 48396, Sept. 23, 2009]

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§180.649 Saflufenacil; tolerances for residues.
(a) General. (1) Tolerances are established for residues of saflufenacil, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of saflufenacil, 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4fluoro-N-[[methyl(1-methylethyl)amino]sulfonyl]benzamide, and its metabolites N-[2-chloro-5-(2,6-dioxo-4-(trifluoromethyl)
-3,6-dihydro-1(2H)-pyrimidinyl)-4-fluorobenzoyl]-N′-isopropylsulfamide and N-[4-chloro-2-fluoro-5-({[(isopropylamino)
sulfonyl]amino}carbonyl)phenyl]urea, calculated as the stoichiometric equivalent of saflufenacil, in or on the commodities.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls

0.08
0.10
0.10
0.03

Banana1
Barley, bran
Barley, grain
Barley, straw

1.5
1.0
15
0.03

Coffee, green bean1
Cotton, gin byproducts
Cottonseed subgroup 20C
Fruit, citrus, group 10
Fruit, pome, group 11
Fruit, stone, group 12
Grain, aspirated grain fractions
Grain, cereal, forage, fodder and straw group 16 (except barley and wheat straw)
Grain, cereal, group 15 (except barley and wheat grain)
Grape
Grass, forage
Grass, hay
Grass, seed screenings
Grass, straw

0.45
0.20
0.03
0.03
0.03
50
0.10
0.03
0.03
15
20
0.15
0.15
0.03

Mango1
Nut, tree, group 14
Olive
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Pea, hay
Pistachio
Pomegranate
Rapeseed subgroup 20A
Soybean, hulls
Soybean, seed

0.03
0.03
0.30
0.03
17
0.03
0.03
0.45
0.50
0.10
0.05

Sugarcane, cane2

0.08

Sugarcane, molasses2
Sunflower subgroup 20B
Vegetable, foliage of legume, group 7 (except pea, hay)
Vegetable, legume, edible podded, subgroup 6A
Wheat, grain
Wheat, straw

1.0
0.10
0.03
0.60
6.0

1

No U.S. registration as of December 7, 2011.

2

No U.S. registration as of February 21, 2014.

(2) Tolerances are established for residues of saflufenacil, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only saflufenacil, 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluoro-N-[[methyl
(1-methylethyl)amino]sulfonyl]benzamide, in or on the commodities.
Commodity

Parts per million

Cattle, fat
Cattle, liver
Cattle, meat

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0.04
50
0.02

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Cattle, meat byproducts, except liver
Fish-freshwater finfish
Fish-shellfish, crustacean
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Hog, fat
Hog, liver
Hog, meat
Hog, meat byproducts, except liver
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Sheep, fat
Sheep, liver
Sheep, meat
Sheep, meat byproducts, except liver

0.30
0.01
0.01
0.04
50
0.02
0.30
0.01
2.0
0.01
0.02
0.04
50
0.02
0.30
0.01
0.04
50
0.02
0.30

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[74 FR 46689, Sept. 11, 2009, as amended at 76 FR 27261, May 11, 2011; 76 FR 76309, Dec. 7, 2011; 79 FR 9866, Feb. 21, 2014;
79 FR 52219, Sept. 3, 2014; 80 FR 22420, Apr. 22, 2015; 80 FR 73667, Nov. 25, 2015]

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§180.650 Isoxaben; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide isoxaben, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only isoxaben, N-[3-(1-ethyl-1-methylpropyl)-5-isoxazolyl]-2, 6-dimethoxybenzamide, in or on
the commodity.
Commodity

Parts per
million

Almond, hulls
Grape
Nut, tree, Group 14
Pistachio

0.40
0.01
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[75 FR 69360, Nov. 12, 2010]

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§180.651 Imazosulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide imazosulfuron, including its metabolites and
degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table below
is to be determined by measuring only imazosulfuron, 2-chloro-N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]
imidazo-[1,2-α]pyridine-3-sulfonamide, in or on the commodity.
Commodity

Parts per million

Melon subgroup 9A
Pepper, bell
Pepper, non-bell
Rice, grain
Tomato
Vegetable, tuberous and corm, subgroup 1C

0.02
0.02
0.02
0.02
0.02
0.02

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[75 FR 81884, Dec. 29, 2010, as amended at 78 FR 44444, July 24, 2013]

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§180.652 Ethiprole; tolerances for residues.
(a) General. Tolerances (without U.S. registrations) are established for residues of the insecticide ethiprole, including
its metabolites and degradate, in or on the following commodities listed in the table. Compliance with the tolerance levels
specified in the table is to be determined by measuring only ethiprole [5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4[(ethyl)-sulfinyl]-1H-pyrazole-3-carbonitrile], in or on the following commodities:
Parts per
million

Commodity
Rice, grain1

1.7

Tea, dried1

30

1

There are no U.S. registrations for rice and tea.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 18921, Apr. 6, 2011]

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§180.653 Indaziflam; tolerances for residues.
(a) General. Tolerances are established for residues of the herbicide indaziflam, N-[(1R,2S)-2,3-dihydro-2,6-dimethyl1H-inden-1-yl]-6-(1-fluoroethyl)-1,3,5-triazine-2,4-diamine, including its metabolites and degradates, in or on the
commodities in the following table. Compliance with the tolerance levels specified in the table below is to be determined by
measuring only indaziflam, in or on the commodity.
Commodity

Parts per
million

Almond, hulls
Banana1
Coffee, green bean1
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, stone, group 12
Grape
Nut, tree, group 14
Olive
Palm, oil1
Pistachio
Sugarcane, refined sugar1

0.15
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.03
0.01
0.01

1

No U.S. Registrations as of 12/02/2013.

2

Tolerance without a corresponding U.S. registration.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 18905, Apr. 6, 2011, as amended at 79 FR 4630, Jan. 29, 2014]

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§180.654 Isopyrazam; tolerances for residues.

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(a) General. Tolerances are established for residues of the fungicide isopyrazam, including its metabolites and
degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the
following table is to be determined by measuring only isopyrazam (3-(difluoromethyl)-1-methyl-N-[1,2,3,4-tetrahydro9-(1-methylethyl)-1,4-methano-naphthalen-5-yl]-1H-pyrazole-4-carboxamide), as the sum of its syn-isomer
(3-(difluoromethyl)-1-methyl-N-[(1RS, 4SR, 9RS)-1,2,3,4-tetrahydro-9-(1-methylethyl)-1,4-methanonaphthalen-5-yl]
-1H-pyrazole-4-carboxamide) and anti-isomer (3-(difluoromethyl)-1-methyl-N-[(1RS, 4SR, 9SR)-1,2,3,4-tetrahydro9-(1-methylethyl)-1,4-methano-naphthalen-5-yl]-1H-pyrazole-4-carboxamide) in or on the commodity.
Commodity

Parts per million

Apple1

0.70

Banana1

0.05

Peanut1

0.01

1

There are no U.S. registrations for use of isopyrazam on apple, banana, or peanut.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 61596, Oct. 5, 2011, as amended at 78 FR 78745, Dec. 27, 2013]

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§180.655 Flazasulfuron; tolerances for residues.
(a) General. Tolerances are established for residues of flazasulfuron, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only flazasulfuron (N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]-3-(trifluoromethyl)-2-pyridinesulfonamide).
Commodity

Parts per million

Almond, hulls
Fruit, citrus, group 10-10
Grape
Nut, tree, group 14-12
Sugarcane

0.01
0.01
0.01
0.01
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 10968, Feb. 24, 2012, as amended at 79 FR 52989, Sept. 5, 2014]

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§180.656 Amisulbrom; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide amisulbrom, including its metabolites and
degradates, in or on the commodities listed below. Compliance with the tolerance levels is to be determined by measuring
only amisulbrom, 3-[(3-bromo-6-fluoro-2-methyl-1H-indole-1-yl) sulfonyl]-N, N-dimethyl-1H-1, 2, 4-triazole-1-sulfonamide].
Commodity1

Parts per million

Grape
Grape, raisin
Tomato
Tomato, paste

0.40
1.0
0.50
1.2

1

There is no U.S. registration for use of amisulbrom on grape or tomato.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[76 FR 59914, Sept. 28, 2011]

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§180.657 Metaflumizone; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide metaflumizone, including its metabolites and
degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the
following table is to be determined by measuring only the sum of metaflumizone (E and Z isomers; 2-[2-(4-cyanophenyl)
-1-[3-(trifluoromethyl) phenyl]ethylidene]-N-[4-(trifluoromethoxy)phenyl] hydrazinecarboxamide) and its metabolite
4-{2-oxo-2-[3-(trifluoromethyl) phenyl]ethyl}-benzonitrile, calculated as the stoichiometric equivalent of metaflumizone, in or
on the following commodities:
Commodity

Parts per million

Almond, hulls

0.04
1.5

Eggplant1
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, stone, group 12-12
Grape
Nut, tree, group 14-12
Pepper1

0.04
0.04
0.04
0.04
0.04
1.5

Tomato1

0.60
1.2

Tomato, paste1
1

There are no U.S. registrations as of April 4, 2014.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 10386, Feb. 22, 2012, as amended at 79 FR 18810, Apr. 4, 2014; 80 FR 66800, Oct. 30, 2015]

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§180.658 Penthiopyrad; tolerances for residues.
(a) General. (1) Tolerances are established for residues of penthiopyrad, including its metabolites and degradates, in
or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only penthiopyrad (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carboxamide).
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Apple, wet pomace
Barley, grain
Barley, hay
Barley, milled byproducts
Barley, straw
Beet, sugar, dried pulp
Beet, sugar, roots
Berry, low growing, subgroup 13-07G
Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Buckwheat, grain
Canola
Corn, field, forage
Corn, field, grain
Corn, field, refined oil
Corn, field, stover
Corn, pop, grain
Corn, sweet, kernel plus cob with husks removed
Cotton, seed
Cotton, gin byproducts
Fruit, pome, group 11-10
Fruit, stone, group 12
Grain, aspirated fractions
Millet, spp.
Nut, tree, group 14
Oat, forage
Oat, grain
Oat, hay

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7.0
20
6.0
1.5
0.15
80
0.90
1.0
1.5
0.5
3.0
5.0
50
0.15
1.5
40
0.01
0.05
15
0.01
0.01
1.5
15
0.50
4.0
30
0.80
0.06
40
0.15
80

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Oat, straw
Pea and bean, dried shelled, except soybean, subgroup 6C
Peanut
Peanut, hay
Peanut, refined oil
Pistachio
Potato, processed potato waste
Rye, forage
Rye, grain
Rye, straw
Sorghum, forage
Sorghum, grain, grain
Sorghum, stover
Soybean, seed
Sunflower, seed
Teosinte, grain
Tomato, paste
Triticale, forage
Triticale, grain
Triticale, hay
Triticale, straw
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7, hay
Vegetable, foliage of legume, group 7, vines/forage
Vegetable, fruiting, group 8-10
Vegetable, leafy, except brassica, group 4
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, edible podded, subgroup 6A
Vegetable, legume, succulent shelled, subgroup 6B
Vegetable, root, subgroup 1B, except sugar beet
Vegetable, tuber and corm, subgroup 1C
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, milled byproducts
Wheat, straw

1.0
0.40
0.04
30
0.06
0.06
0.20
40
0.15
1.0
40
0.80
15
0.40
1.5
0.15
3.5
40
0.15
80
1.0
3.0
0.60
200
50
3.0
30
50
4.0
0.40
3.0
0.06
40
0.15
80
0.30
1.0

(2) Tolerances are established for residues of penthiopyrad, including its metabolites and degradates, in or on the
commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring
only the sum of penthiopyrad (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carboxamide)
and its metabolite (1-methyl-3-trifluoromethyl-1H-pyrazole-4-carboxamide), calculated as the stoichiometric equivalent of
penthiopyrad, in or on the commodity.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.03
0.03
0.09
0.03
0.03
0.09
0.03
0.03
0.09
0.02
0.03
0.03
0.09

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 14297, Mar. 9, 2012]

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§180.659 Pyroxasulfone; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolite, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)
-1H-pyrazol-4-carboxylic acid (M-3), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.
Commodity

Parts per million

Corn, field, grain
Corn, pop, grain
Corn, sweet, kernel plus cob with husks removed
Cotton, undelinted seed
Wheat, grain

0.02
0.015
0.015
0.04
0.03

(2) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates,
in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]
sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolites, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)
-1H-pyrazol-4-yl]methanesulfonic acid (M-1); 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-carboxylic acid
(M-3); and [5-(difluoromethoxy)-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-25), calculated as the
stoichiometric equivalent of pyroxasulfone, in or on the commodity.
Commodity

Parts per million

Corn, field, forage
Corn, field, stover
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, stover
Cotton, gin byproducts
Soybean, forage
Soybean, hay
Wheat, forage
Wheat, hay
Wheat, straw

0.09
0.15
0.15
0.10
0.15
0.20
1.0
2.0
6.0
1.0
0.60

(3) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates,
in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]
sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolites, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)
-1H-pyrazol-4-carboxylic acid (M-3); [5-(difluoromethoxy)-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-25);
and 3-[1-carboxy-2-(5,5-dimethyl-4,5-dihydroisoxazol-3-ylthio)ethylamino]-3-oxopropanoic acid (M-28), calculated as the
stoichiometric equivalent of pyroxasulfone, in or on the commodity.
Commodity

Parts per million

Soybean, seed

0.06

(4) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates,
in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only the sum of pyroxasulfone [3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole] and its metabolites [5-(difluoromethoxy)-1-methyl3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-1) and 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1Hpyrazol-4-carboxylic acid (M-3), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.
Commodity

Parts per million

Milk

0.003

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 12213, Feb. 29, 2012, as amended at 78 FR 13257, Feb. 27, 2013; 78 FR 46279, July 31, 2013; 79 FR 34633, June 18,
2014]

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§180.660 Pyriofenone; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide pyriofenone, including its metabolites and
degradates, in or on the following commodities listed in the table. Compliance with the tolerance levels specified in the

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table is to be determined by measuring only pyriofenone, (5-chloro-2-methoxy-4-methyl-3-pyridinyl)(2,3,4-trimethoxy-6methylphenyl) methanone, in or on the following commodities:
Commodity

Parts per million

Grape1

0.30

Grape, raisin1

0.50

1

There are no U.S. registrations for grape and grape, raisin.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 13506, Mar. 7, 2012]

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§180.661 Fluopyram; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide Fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)
-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates in or on the commodities in the
table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only fluopyram in
or on the commodity.
Commodity

Parts
per million

Almond, hull
Apple
Apple, wet pomace

8.0
0.30
0.60
1.0

Banana1
Bean, dry
Beet, sugar, root
Cotton, gin byproducts
Cotton, undelinted seed
Cherry
Grape, wine
Nut, tree, group 14
Peanut
Pistachio
Potato
Potato, processed potato waste
Soybean, seed
Strawberry
Watermelon

0.09
0.04
0.70
0.01
0.60
2.0
0.05
0.09
0.05
0.02
0.08
0.04
1.5
1.0

1

There are no U.S. registrations.

(2) Tolerances are established for residues of the fungicide fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]
ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates. Compliance with the tolerance levels
specified in the table below is to be determined by measuring only the sum of fluopyram and its metabolite,
2-(trifluoromethyl)benzamide, calculated as the stoichiometric equivalent of fluopyram, in or on the commodity.
Commodity

Parts per
million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Egg
Goat, fat
Goat, meat
Goat, meat byproducts
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Poultry, fat

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0.05
0.05
0.40
0.06
0.11
0.15
1.1
0.02
0.02
0.03
0.11
0.15
1.1
0.06
0.03

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Poultry, meat
Poultry, meat byproducts
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.03
0.10
0.11
0.15
1.1

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. It is recommended that tolerances be established for indirect or inadvertent
residues of fungicide fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including
its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
in the table is to be determined by measuring only fluopyram in or on the commodity.
Commodity

Parts per
million

Alfalfa, forage
Alfalfa, hay
Canola, seed
Grain, cereal, except rice, group 15
Grain, cereal, forage, fodder and straw, group 16
Soybean, forage
Soybean, hay
Soybean, seed

0.45
1.1
1.8
0.03
2.0
4.0
15
0.10

[77 FR 10975, Feb. 24, 2012, as amended at 79 FR 75065, Dec. 17, 2014]

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§180.662 Trinexapac-ethyl; tolerances for residues.
(a) General. Tolerances are established for residues of the plant growth inhibitor, trinexapac-ethyl, including its
metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring both trinexapac-ethyl, ethyl 4-(cyclopropylhydroxymethylene)
-3,5-dioxocyclohexanecarboxylate and the associated metabolite, trinexpac, 4-(cyclopropylhydroxymethylene)
-3,5-dioxocyclohexanecarboxylic acid, calculated as the stoichiometric equivalent of trinexapac-ethyl, in or on the
commodity.
Commodity

Parts per
million

Barley, bran
Barley, grain
Barley, hay
Barley, straw
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Grass, forage
Grass, hay
Grass, seed screenings
Grass, straw
Hog, fat
Hog, meat
Hog, meat by-products
Horse, fat
Horse, meat
Horse, meat byproducts
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Rice, bran
Rice, grain
Rice, straw
Rice, wild, grain
Rye, bran
Rye, grain
Rye, hay

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2.5
2.0
0.8
0.4
0.02
0.02
0.04
0.02
0.02
0.04
1.5
4.0
40.0
10.0
0.02
0.02
0.03
0.02
0.02
0.04
1.0
4.0
1.5
0.9
1.5
0.4
0.07
0.4
6.0
4.0
1.5

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Rye, straw
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Sugarcane, cane
Sugarcane, molasses
Wheat, bran
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, middlings
Wheat, straw

0.9
0.02
0.02
0.04
0.8
2.5
6.0
1.0
4.0
1.5
10.5
0.9

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 12745, Mar. 2, 2012, as amended at 77 FR 60919, Oct. 3, 2012; 80 FR 28848, May 20, 2015]

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§180.663 Ametoctradin; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide ametoctradin, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only ametoctradin (5-ethyl-6-octyl[1,2,4]triazolo[1,5-a]pyrimidin-7-amine).
Commodity

Parts per
million

Brassica, head and stem, subgroup 5A
Brassica, leafy greens, subgroup 5B
Grape
Grape, raisin
Hop, dried cones
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Spinach
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leafy, except Brassica, group 4, except spinach
Vegetable, tuberous and corm, subgroup 1C

9.0
50
4.0
8.0
10.0
1.5
20.0
50.0
3.0
1.5
40.0
0.05

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 21734, May 9, 2012]

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§180.664 Penflufen; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide penflufen, including its metabolites and
degradates, in or on the following commodities listed in the table. Compliance with the tolerance levels specified in the
table is to be determined by measuring only penflufen N-[2-(1,3-dimethylbutyl)phenyl]-5-fluoro-1,3-dimethyl-1H-pyrazole-4carboxamide, in or on the following commodities.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Cotton, gin by-products
Grain cereal, forage, fodder and straw, group 16
Grain, cereal, group 15
Oilseed, group 20
Vegetable, foliage of legume, group 7
Vegetable, legume, group 6
Vegetable, tuberous and corm subgroup 1C

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0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01

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(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 28281, May 14, 2012]

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§180.665 Sedaxane; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide sedaxane, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only sedaxane, N-[2-[1,1′-bicyclopropyl]-2-ylphenyl]-3-(difluoromethyl)-1-methyl1H-pyrazole-4-carboxamide, as the sum of its cis- and trans-isomers in or on the commodity.
Commodity
Barley, grain
Barley, hay
Barley, straw
Beet, sugar, roots
Canola, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cotton, undelinted seed
Cotton, gin byproducts
Oat, forage
Oat, grain
Oat, hay
Oat, straw
Pea and bean, dried shelled, except soybean, subgroup 6C
Potato
Potato, wet peel
Rapeseed, subgroup 20A
Rye, forage
Rye, grain
Rye, straw
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Vegetable, foliage of legume, except soybean, subgroup 7A
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

Parts per million
0.01
0.04
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.015
0.01
0.06
0.01
0.01
0.02
0.075
0.01
0.015
0.01
0.01
0.01
0.01
0.01
0.05
0.04
0.01
0.01
0.015
0.01
0.06
0.01

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect inadvertent residues. [Reserved]
[77 FR 36924, June 20, 2012, as amended at 78 FR 33748, June 5, 2013; 78 FR 60719, Oct. 2, 2013; 80 FR 43329, July 22, 2015]

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§180.666 Fluxapyroxad; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide fluxapyroxad, including its metabolites and
degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to
be determined by measuring only fluxapyroxad, 3-(difluoromethyl)-1-methyl-N-(3′,4′,5′-trifluoro[1,1′-biphenyl]-2-yl)
-1H-pyrazole-4-carboxamide in or on the commodity.

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Commodity
Almond, hulls
Apple, wet pomace
Beet, sugar
Beet, sugar, dried pulp
Beet, sugar, tops
Berry, low growing, subgroup 13-07G
Bushberry, subgroup 13-07B
Caneberry, subgroup 13-07A
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Corn, field, grain
Corn, oil
Corn, pop, grain
Corn, sweet, kernels plus cobs with husks removed
Cotton, gin byproducts
Cotton, undelinted seed
Egg
Fish-freshwater finfish
Fish-shellfish, crustacean
Fruit, pome, group 11
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Fruit, stone, group 12-12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions
Grain, cereal, forage, fodder and straw, group 16
Grain, cereal, group 15, (except corn, field, grain; except corn, pop, grain; except corn, kernels plus cobs with husks removed; except rice; except
wheat
Grape, raisin
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Nut, tree, group 14-12
Oilseeds, group 20 (except cottonseed)
Pea and bean, dried shelled except soybean, subgroup 6C
Pea and bean, succulent shelled, subgroup 6B
Peanut
Peanut, refined oil
Plum, prune, dried
Potato, wet peel
Rice, bran
Rice, bran
Rice, grain
Rice, hulls
Rice, hulls
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, hulls
Soybean, seed
Sugarcane, cane
Vegetable, brassica leafy, group 5
Vegetable, bulb, group 3-07
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetables, fruiting, group 8
Vegetable, leafy, except brassica, group 4
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root, except sugarbeet, subgroup 1B
Vegetable, tuberous and corm, subgroup 1C
Wheat, bran
Wheat, grain

Parts
per
million
4.0
2.0
0.1
0.1
7.0
4.0
7.0
5.0
0.05
0.01
0.03
0.01
0.03
0.01
0.15
20
0.30
0.002
0.01
0.01
0.8
2.0
3.0
0.05
0.01
0.03
20.0
20
3.0
5.7
0.01
0.05
0.01
0.03
0.005
0.06
0.9
0.4
0.5
0.01
0.02
3.0
0.1
4.5
8.5
5.0
8.0
15.0
0.05
0.01
0.03
0.3
0.15
3.0
4.0
1.5
0.50
30
0.7
30
2.0
0.90
0.02
0.6
0.3

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of
the fungicide fluxapyroxad, including its metabolites and degradates, in or on the commodities listed in the table below.
Compliance with the tolerance levels specified below is to be determined by measuring only fluxapyroxad,
3-(difluoromethyl)-1-methyl-N-(3′,4′,5′-trifluoro[1,1′-biphenyl]-2-yl)-1H-pyrazole-4-carboxamide in or on the commodity.
Commodity

Parts per
million

Nongrass animal feeds, group18
Peppermint, tops
Spearmint, tops

0.30
0.01
0.01

[77 FR 28275, May 14, 2012, as amended at 77 FR 46307, Aug. 3, 2012; 79 FR 10677, Feb. 26, 2014; 80 FR 45078, July 29, 2015]

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§180.667 Cyflufenamid, tolerance for residues.
(a) General. Tolerances are established for residues of the fungicide cyflufenamid, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only cyflufenamid, [N(Z)]-N-[[(cyclopropylmethoxy)amino][2,3-difluoro-6-(trifluoromethyl)phenyl]
methylene]benzeneacetamide.
Commodity
Apple, wet pomace
Berry, low growing, subgroup 13-07G, except cranberry
Fruit, pome, group 11
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Grape, raisin
Vegetable, cucurbit, group 9

Parts per million
0.10
0.20
0.06
0.15
0.30
0.07

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 38210, June 27, 2012]

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§180.668 Sulfoxaflor; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide sulfoxaflor, including its metabolites and
degradates, in or on the commodities in the table. Compliance with the tolerance levels specified is to be determined by
measuring only sulfoxaflor (N-[methyloxido[1-[6-(trifluoromethyl)-3-pyridinyl]ethyl]-γ4-sulfanylidene]cyanamide).
Commodity
Almond, hulls
Barley, grain
Barley, hay
Barley, straw
Bean, dry seed
Bean, succulent
Beet, sugar, dried pulp
Beet, sugar, molasses
Berry, low growing, subgroup 13-7G
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cauliflower
Citrus, dried pulp
Cotton, gin byproducts
Cotton, hulls
Cottonseed subgroup 20C
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwi fruit
Fruit, stone, group 12
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated fractions

Parts per million

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6.0
0.40
1.0
2.0
0.20
4.0
0.07
0.25
0.70
0.10
0.15
0.40
0.08
3.6
6.0
0.35
0.20
0.70
0.50
2.0
3.0
0.10
0.15
0.40
20.0

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Grape, raisin
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Leafy greens, subgroup 4A
Leafy petiole, subgroup 4B
Milk
Nuts, tree, group 14
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Pistachio
Poultry, eggs
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rapeseed, meal
Rapeseed subgroup 20A
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, seed
Tomato, paste
Tomato, puree
Vegetable, brassica, leafy, group 5, except cauliflower
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, leaves of root and tuber, group 2
Vegetable, legume, foliage, group 7
Vegetable, root and tuber, group 1
Watercress
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

6.0
0.01
0.01
0.01
0.10
0.15
0.40
6.0
2.0
0.15
0.015
0.01
0.70
0.015
0.01
0.01
0.01
0.01
0.50
0.40
0.10
0.15
0.40
0.20
2.60
1.20
2.0
0.40
0.70
3.0
3.0
0.05
6.0
1.0
0.08
1.5
2.0

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for
residues of sulfoxaflor (N-[methyloxido[1-[6-(trifluoromethyl)-3-pyridinyl]ethyl]- λ4-sulfanylidene]cyanamide), including its
metabolites and degradates, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to
FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in the following table is to be
determined by measuring only sulfoxaflor in or on the commodity. The tolerances expire on the date specified in the table.

Commodity

Parts
per
million

Sorghum, forage
Sorghum, grain
Sorghum, stover

Expiration/revocation date
0.40
0.30
0.90

12/31/17
12/31/17
12/31/17

(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 59565, Sept. 28, 2012, as amended at 78 FR 38227, June 26, 2013; 80 FR 4515, Jan. 28, 2015]

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§180.669 Picoxystrobin; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide picoxystrobin, including its metabolites and
degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be
determined by measuring only picoxystrobin, methyl (αE)-α-(methoxymethylene)-2-[[[6-(trifluoromethyl)-2-pyridinyl]oxy]
methyl]benzeneacetate.
Commodity

Parts per
million

Barley, bran
Barley, grain
Cattle, fat
Cattle, meat

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0.5
0.3
0.01
0.01

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Cattle, meat byproducts
Corn, field, refined oil
Eggs
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated grain fractions
Grain, cereal, forage, fodder, and straw, group 16, forage
Grain, cereal, forage, fodder, and straw, group 16, hay
Grain, cereal, forage, fodder, and straw, group 16, stover
Grain, cereal, forage, fodder, and straw, group 16, straw
Grain, cereal, group 15, except rice and barley
Hog, fat
Hog, meat
Hog, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Pea and bean, dried shelled, except soybean, subgroup 6C
Poultry, fat
Poultry, meat
Poultry, meat byproducts
Rapeseed subgroup 20A
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Vegetable, foliage of legume, except soybean, subgroup 7A
Wheat, bran
Wheat, germ

0.01
0.07
0.01
0.01
0.01
0.01
10
15
5
10
2
0.04
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.06
0.01
0.01
0.01
0.08
0.01
0.01
0.01
1
3
0.2
0.05
40
0.06
0.09

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[77 FR 72231, Dec. 5, 2012]

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§180.671 Fenpyrazamine; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide fenpyrazamine, in or on the following
commodities. Compliance with the tolerance levels specified in the following table is to be determined by measuring only
fenpyrazamine S-allyl 5-amino-2-isopropyl-4-(2-methylphenyl)-3-oxo-2,3-dihydropyrazole-1-carbothioate, in or on the
following commodities:
Commodity

Parts per
million

Almond
Almond, hulls
Berry, low growing, subgroup 13-07G
Bushberry subgroup 13-07B
Caneberry subgroup 13-07A
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Ginseng
Grape, juice
Lettuce, head
Lettuce, leaf
Pistachio

0.02
1.5
3
5
5
3
0.7
4
1.5
2
0.02

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]

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[78 FR 14465, Mar. 6, 2013]

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§180.672 Cyantraniliprole; tolerances for residues.
(a) General. Tolerances are established for the combined residues of the insecticide cyantraniliprole, 3-bromo1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[(methylamino)carbonyl]phenyl]-1H-pyrazole-5-carboxamide, including its
metabolites and degradates, in or on commodities in the following table. Compliance with the tolerance levels specified in
the following table is to be determined by measuring only cyantraniliprole in or on the commodity.
Commodity

Parts per million

Almond, hulls
Brassica head and stem (subgroup 5A)
Brassica leafy vegetables (subgroup 5B)
Bushberry (subgroup 13-07B)
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Cherry (subgroup 12-12A)
Citrus, oil
Cotton, gin byproducts
Fruit, citrus (group 10-10)
Fruit, pome (group 11-10)
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Nut, tree (group 14-12)
Oilseed (group 20)
Onion, bulb (subgroup 3-07A)
Onion, green (subgroup 3-07B)
Peach (subgroup 12-12B)
Plum (subgroup 12-12C)
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Vegetable, cucurbit (group 9)
Vegetable, fruiting (group 8-10)
Vegetable, leafy (except Brassica) (group 4)
Vegetable, tuberous and corm (subgroup 1C)

8.0
3.0
30
4.0
0.01
0.01
0.01
6.0
2.4
10
0.70
1.5
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.04
1.5
0.04
8.0
1.5
0.50
0.01
0.01
0.01
0.40
2.0
20
0.15

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent tolerances for residues of
cyantraniliprole, 3-bromo-1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[(methylamino)carbonyl]phenyl]-1H-pyrazole-5carboxamide, including its metabolites and degradates, in or on commodities in the following table. Compliance with the
tolerance levels specified in the following table is to be determined by measuring only cyantraniliprole in or on the
commodity.
Commodity
Animal feed, nongrass (group 18)
Grain, cereal, forage, fodder and straw (group 16)
Grass forage, fodder and hay (group 17)
Peanut, hay
Vegetable, foliage of legume (group 7)
Vegetable, leaves of root and tuber vegetables (group 2)
Vegetable, root (subgroup 1A)

Parts per million
0.20
0.50
0.50
0.01
0.70
0.04
0.02

[79 FR 6833, Feb. 5, 2014]

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§180.673 Triforine; tolerances for residues.

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(a) General. Tolerances are established for residues of triforine, including its metabolites and degradates. Compliance
with the tolerance levels specified in the following table is to be determined by measuring only triforine (N,N′
-[1,2-piperazinediylbis(2,2,2-trichloroehylidene)]bis[formamide]), in or on the following commodities.
Commodity

Parts per
million

Blueberry1

1.0

Tomato1

0.5

1

There are no U.S. registrations for blueberry and tomato.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[78 FR 32151, May 29, 2013. Redesignated at 78 FR 36677, June 19, 2013]

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§180.674 Proquinazid; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide, proquinazid, including its metabolites and
degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the
following table is to be determined by measuring only proquinazid, [6-Iodo-2-propoxy-3-propyl-3H-quinazolin-4-one), in or
on the following commodities:
Commodity

Parts per
million
0.50

Grape1

1.0

Grape, raisin1
1

No U.S. registrations for Proquinazid.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[79 FR 18815, Apr. 4, 2014]

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§180.675 Tolfenpyrad; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide tolfenpyrad, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only tolfenpyrad, 4-chloro-3-ethyl-1-methyl-N-[4-(p-tolyloxy)benzyl]pyrazole-5-carboxamide.
Commodity

Parts per million

Almond hulls
Citrus, dried pulp
Citrus, oil
Cotton, gin byproducts
Cotton, undelinted seed
Fruit, stone, group 12-12
Fruits, citrus, group 10-10
Grape
Grape, raisin
Nuts, tree, group 14-12
Persimmon
Plum, prune
Pomegranate
Potato
Tea
Vegetable, leafy, except Brassica, group 4

6.0
8.0
70.0
15.0
0.70
2.0
1.5
2.0
6.0
0.05
2.0
3.0
2.0
0.01
30.0
30.0

(2) Tolerances are established for residues of the insecticide tolfenpyrad, including its metabolites and degradates, in
or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by

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measuring only the sum of tolfenpyrad, 4-chloro-3-ethyl-1-methyl-N-[4-(p-tolyloxy)benzyl]pyrazole-5-carboxamide, and its
metabolite 4-[4-[(4-chloro-3-ethyl-1-methylpyrazol-5-yl)carbonylamino-methyl]phenoxy]-benzoic acid, calculated as the
stoichiometric equivalent of tolfenpyrad.
Commodity

Parts per million

Cattle, fat
Cattle, meat
Cattle, meat byproducts
Goat, fat
Goat, meat
Goat, meat byproducts
Horse, fat
Horse, meat
Horse, meat byproducts
Milk
Sheep, fat
Sheep, meat
Sheep, meat byproducts

0.01
0.01
0.35
0.01
0.01
0.35
0.01
0.01
0.35
0.03
0.01
0.01
0.35

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registration. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[79 FR 1605, Jan. 9, 2014]

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§180.676 Fenpropidin; tolerances for residues.
(a) General. Tolerances are established for the residues of fenpropidin, including its metabolites and degradates, in or
on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by
measuring only fenpropidin (1-[3-[4-(1,1-dimethylethyl)phenyl]-2-methylpropyl]piperidine).
Commodity

Parts per
million

Banana1

10

1

There are no U.S. registrations as of December 13, 2013.

(b) Section 18 tolerance. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[79 FR 8096, Feb. 11, 2014]

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§180.677 Cyflumetofen; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide cyflumetofen, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels for cyflumetofen is to be
determined by measuring only cyflumetofen, 2-methoxyethyl α-cyano-α-[4-(1,1-dimethylethyl)phenyl]-β-oxo2-(trifluoromethyl)benzenepropanoate, in or on the commodity.
Commodity

Parts per
million

Almond, hulls
Citrus, oil
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Grape
Nut, tree, group 14-12
Strawberry
Tomato

4.0
16
0.30
0.30
0.60
0.01
0.60
0.40

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]
[79 FR 29108, May 21, 2014]

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§180.678 Tricyclazole; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide tricyclazole, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only tricyclazole (5-methyl-1,2,4-triazolo[3,4-b ]benzothiazole).
Parts
per million
3.0

Commodity
Rice, grain1
1

There are no U.S. Registrations on Rice as of June 11, 2014.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[79 FR 33468, June 11, 2014]

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§180.679 Flupyradifurone; tolerances for residues.
(a) General. Tolerances are established for residues of the insecticide flupyradifurone, including its metabolites and
degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following
table is to be determined by measuring only flupyradifurone, 4-[[(6-chloro-3-pyridinyl)methyl](2,2-difluoroethyl)amino]- 2
(5H)-furanone.
Commodity

Parts per million

Alfalfa, forage
Alfalfa, hay
Almond, hulls
Bean, succulent
Berry, low growing, except cranberry subgroup 13-07G
Brassica, head and stem subgroup 5A
Brassica, leafy greens subgroup 5B
Bushberry, except cranberry subgroup 13-07B
Cactus, fruit
Cactus, pads
Cattle, fat
Cattle, meat
Cattle, meat byproducts
Coffee, green bean1
Corn, field, grain
Corn, pop, grain
Corn, sweet, kernels plus cobs with husks removed
Cotton, gin byproducts
Cottonseed, subgroup 20C
Egg
Fruit, citrus, dried pulp
Fruit, citrus, group 10-10
Fruit, pome, group 11-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Goat, fat
Goat, meat
Goat, meat byproducts
Grain, aspirated grain fractions
Grain, cereal, forage, fodder and straw, group 16
Grain, cereal, group 15, except rice and corn
Grape, raisin
Hog, fat
Hog, meat
Hog, meat byproducts
Hops, dried cones
Horse, fat

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9.0
20
15
0.20
1.5
6.0
40
4.0
0.30
0.70
0.20
0.30
1.0
1.5
0.05
0.05
0.05
40
0.80
0.01
10
3.0
0.70
3.0
0.20
0.30
1.0
40
30
3.0
5.0
0.01
0.01
0.04
10
0.20

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Horse, meat
Horse, meat byproducts
Leaf petioles, subgroup 4B
Leafy greens, subgroup 4A
Milk
Nut, tree, group 14-12
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Pea and bean, dried, shelled except soybean, subgroup 6C
Pea, succulent
Peanut
Peanut, hay
Pitaya
Sheep, fat
Sheep, meat
Sheep, meat byproducts
Soybean, seed
Taro leaves
Turnip greens
Vegetable, cucurbit, group 9
Vegetable, foliage of legume, group 7
Vegetable, fruiting, group 8-10
Vegetable, legume, edible podded, subgroup 6A
Vegetable, root, except sugar beet, subgroup 1B
Vegetable, tuberous and corm, subgroup 1C

0.30
1.0
9.0
30
0.15
0.02
0.09
3.0
3.0
2.0
0.04
20
0.30
0.20
0.30
1.0
1.5
30
40
0.40
30
1.5
3.0
0.90
0.05

1

No U.S. registration.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional restrictions. Tolerances are established for residues of the insecticide flupyradifurone,
including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance
levels specified in the following table is to be determined by measuring only flupyradifurone, 4-[[(6-chloro-3-pyridinyl)
methyl](2,2-difluoroethyl)amino]- 2(5H)-furanone.
Commodity

Parts per million

Clover, forage
Clover, hay

20
30

(d) Indirect or inadvertent residues. [Reserved]
[80 FR 3487, Jan. 23, 2015]

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§180.680 Fluensulfone; tolerances for residues.
(a) General. Tolerances are established for residues of the nematicide fluensulfone, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only 3,4,4-trifluoro-but-3-ene-1-sulfonic acid, calculated as the stoichiometric equivalent of
fluensulfone.
Commodity

Parts per
million

Tomato, paste
Vegetables, cucurbits, group 9
Vegetables, fruiting, group 8-10

1.0
0.50
0.50

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertant residues. [Reserved]
[79 FR 56968, Sept. 24, 2014, as amended at 80 FR 56395, Sept. 18, 2015]

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§180.681 Isofetamid; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide isofetamid, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be

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determined by measuring only isofetamid, N-[1,1-dimethyl-2-[2-methyl-4-(1-methylethoxy)phenyl]-2-oxoethyl]-3-methyl-2thiophenecarboxamide, in or on the following commodities:
Parts per
million

Commodity
Almond
Almond, hulls
Berry, low growing, subgroup 13-07G
Canola, refined oil
Flax, seed, oil
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Grape, raisin
Lettuce, head
Lettuce, leaf
Mustard, seed, oil
Rapeseed subgroup 20A
Sesame, oil

0.01
0.01
4.0
0.03
0.03
3.0
5.0
5.0
7.0
0.03
0.015
0.03

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[80 FR 45443, July 30, 2015]

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§180.682 Bicyclopyrone; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the herbicide bicyclopyrone (4-hydroxy-3[[2-[(2-methoxyethoxy)methyl]-6-(trifluoromethyl)-3-pyridinyl]carbonyl]bicyclo[3.2.1]oct-3-en-2-one), including its
metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only the sum of the common moieties SYN503780 (2-[(2-methoxyethoxy)methyl]
-6-(trifluoromethyl)-3-pyridinecarboxylic acid) and CSCD686480 (2-[(2-hydroxyethoxy)methyl]-6-(trifluoromethyl)-3pyridinecarboxylic acid), calculated as the stoichiometric equivalent of bicyclopyrone, in or on the commodities.
Parts per
million

Commodity
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover

0.30
0.02
0.40
0.02
0.40
0.40
0.03
0.70
0.02

Sugarcane, cane1
Cattle, meat byproducts
Goat, meat byproducts
Sheep, meat byproducts
Horse, meat byproducts
Hog, meat byproducts

1.5
1.5
1.5
1.5
0.15

1

There are no U.S. Registrations on Sugarcane as of March 13, 2015.

(2) [Reserved]
(b) [Reserved]
[80 FR 22654, Apr. 23, 2015]

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§180.684 Benalaxyl-M; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide benalaxyl-M, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only benalaxyl [methyl N-(2,6-dimethylphenyl)-N-(phenylacetyl)-DL-alaninate] in or on the
commodity.
Commodity

Parts per million

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Grape1

3.0
0.20

Tomato1
1

There is no U.S. registration for use on this commodity as of July 30, 2015.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[80 FR 45448, July 30, 2015]

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§180.685 Oxathiapiprolin; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the fungicide oxathiapiprolin, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only oxathiapiprolin, 1-[4-[4-[5-(2,6-difluorophenyl)-4,5-dihydro-3-isoxazolyl]-2-thiazolyl]-1piperidinyl]-2-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-ethanone, in or on the commodity.
Commodity

Parts per million

Brassica, head and stem, subgroup 5A
Ginseng

1.5
0.15
0.70

Grape1
Leafy greens subgroup 4A
Onion, bulb, subgroup 3-07A
Onion, green, subgroup 3-07B
Pea, edible-podded
Pea, succulent shelled
Tomato, dried
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, tuberous and corm, subgroup 1C

15
0.04
2.0
1.0
0.05
3.0
0.20
0.50
0.01

1

There is no associated U.S. registration as of September 4, 2015.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide oxathiapiprolin, including
its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified
below is to be determined by measuring only oxathiapiprolin, 1-[4-[4-[5-(2,6-difluorophenyl)-4,5-dihydro-3-isoxazolyl]-2thiazolyl]-1-piperidinyl]-2-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-ethanone, in or on the commodity.
Commodity
All other food commodities/feed commodities (other than those covered by a tolerance as a result of use on growing crops)

Parts per million
0.10

[80 FR 53473, Sept. 4, 2015]

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§180.686 Benzovindiflupyr; tolerances for residues.
(a) General. Tolerances are established for residues of the fungicide benzovindiflupyr, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only benzovindiflupyr (N-[9-(dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalen-5-yl]
-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxamide) in or on the commodity.
Commodity

Parts per million

Barley, grain
Barley, hay
Barley, straw
Cattle, fat
Cattle, liver
Cattle, meat
Cattle, meat byproducts, except liver
Coffee, green bean1
Corn, field, forage

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1.5
15.0
15.0
0.02
0.06
0.01
0.01
0.09
3.0

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Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, kernel plus cob with husks removed
Corn, sweet, stover
Cottonseed, subgroup 20C
Cotton, gin byproducts
Fruit, pome, group 11-10
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F
Goat, fat
Goat, liver
Goat, meat
Goat, meat byproducts, except liver
Grain, aspirated fractions
Grape, raisin
Horse, fat
Horse, liver
Horse, meat
Horse, meat byproducts, except liver
Milk
Milk, fat
Oat, grain
Oat, hay
Oat, straw
Pea and bean, dried shelled, except soybean, subgroup 6C
Pea, field, hay
Pea, field, vine
Peanut
Peanut, hay
Potato, processed potato waste
Rapeseed, subgroup 20A
Rye, grain
Rye, hay
Rye, straw
Sheep, fat
Sheep, liver
Sheep, meat
Sheep meat byproducts, except liver
Soybean, forage
Soybean, hay
Soybean, hulls
Soybean, seed
Sugarcane, cane1
Tomato, dried
Vegetable, cucurbit, group 9
Vegetable, fruiting, group 8-10
Vegetable, tuberous and corm, subgroup 1C
Wheat, forage
Wheat, grain
Wheat, hay
Wheat, straw

0.02
15.0
0.02
15.0
4.0
0.01
5.0
0.15
3.0
0.20
1.0
0.02
0.06
0.01
0.01
15.0
3.0
0.02
0.06
0.01
0.01
0.01
0.02
1.5
15.0
15.0
0.20
7.0
1.5
0.01
15.0
0.10
0.15
0.1
15.0
15.0
0.02
0.06
0.01
0.01
15.0
50.0
0.20
0.07
0.04
4.0
0.30
1.5
0.02
4.0
0.10
15.0
15.0

1

There is no U.S. registration for use of benzovindiflupyr.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[80 FR 59633, Oct. 2, 2015]

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§180.687 Teflubenzuron; tolerances for residues.
(a) General. (1) Tolerances are established for residues of the insecticide teflubenzuron, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only teflubenzuron (N-[[(3,5-dichloro-2,4-difluorophenyl)amino]carbonyl]-2,6-difluorobenzamide).

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Commodity

Parts per
million
1.0

1

Apple

Broccoli1

0.20

Cauliflower1

0.01

Citrus, oil1

100

Coffee, bean, green1

0.60

Corn, field, grain1

0.01

Corn, field, refined oil1

0.02

Lemon1

0.80

Mango1

1.5

Melon, subgroup 9A1

0.30

Orange1

0.60

Papaya1

0.50

Pineapple1

0.80

Soybean, seed1

0.05

Soybean, hulls1

0.15

Sugarcane, cane1

0.01

Sunflower, seed1

0.30

Tomato1

1.5

1

There are no U.S. registrations as of October 30, 2015.

(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues. [Reserved]
[80 FR 66809, Oct. 30, 2015]

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§180.688 Diethofencarb; tolerance for residue.
(a) General. (1) Tolerances are established for residues of the fungicide diethofencarb, including its metabolites and
degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be
determined by measuring only diethofencarb (1-methylethyl N-(3,4-diethoxyphenyl)carbamate).
Commodity

Parts per
million

Banana*

0.10

*There is no U.S. registration for use on this commodity as of November 4, 2015.
(b) Section 18 emergency exemptions. [Reserved]
(c) Tolerances with regional registrations. [Reserved]
(d) Indirect or inadvertent residues [Reserved]
[80 FR 68261, Nov. 4, 2015]

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Subpart D—Exemptions From Tolerances
Back to Top
§180.900 Exemptions from the requirement of a tolerance.
An exemption from a tolerance shall be granted when it appears that the total quantity of the pesticide chemical in or
on all raw agricultural commodities for which it is useful under conditions of use currently prevailing or proposed will
involve no hazard to the public health.
[69 FR 23117, Apr. 28, 2004]

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§180.905 Pesticide chemicals; exemptions from the requirement of a tolerance.
(a) When applied to growing crops, in accordance with good agricultural practice, the following pesticide chemicals
are exempt from the requirement of a tolerance:
(1) Petroleum oils.
(2) Piperonyl butoxide.
(3) Pyrethrins.
(4) Sabadilla.
(b) When applied to growing crops, in accordance with good agricultural practice, the pesticides rotenone or derris or
cube roots are exempt from the requirement of a tolerance. There are no U.S. registrations for use of rotenone, derris, or
cube roots on food commodities as of March 23, 2011.
(c) These pesticides are not exempted from the requirement of a tolerance when applied to a crop at the time of or
after harvest.
[77 FR 59128, Sept. 26, 2012]

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§180.910 Inert ingredients used pre- and post-harvest; exemptions from the requirement of a tolerance.
Residues of the following materials are exempted from the requirement of a tolerance when used in accordance with
good agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to growing crops or
to raw agricultural commodities after harvest:
Inert ingredients
Acetic acid
Acetic anhydride
Acetone
Alkanoic and alkenoic acids, mono- and diesters of α-hydro-ω-hydroxypoly (oxyethylene) with molecular weight (in
amu) range of 200 to 6,000
Alkyl (C8-C24) benzenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts

C10-C18-Alkyl dimethyl amine oxides (CAS Reg. Nos. 1643-20-5, 2571-88-2, 2605-79-0, 3332-27-2, 61788-90-7,
68955-55-5, 70592-80-2, 7128-91-8, 85408-48-6, and 85408-49-7)

Limits

Uses
Catalyst
Solvent, cosolvent
Do.
Emulsifiers
Surfactants, related
adjuvants of
surfactants
Surfactant

15% by weight in
pesticide
formulation
α-alkyl(C6- C15)-ω-hydroxypoly(oxyethylene)sulfate, and its ammonium, calcium, magnesium, potassium, sodium, Not to exceed 30% Surfactants, related
adjuvants of
and zinc salts, poly(oxyethylene) content averages 2-4 moles (CAS Reg. Nos.: 3088-31-1, 3694-74-4, 9004-82-4, of formulation
surfactants.
9004-84-6, 9021-91-4, 9086-52-6, 13150-00-0, 15826-16-1, 25446-78-0, 26183-44-8, 27140-00-7, 27731-62-0,
32612-48-9, 34431-25-9, 35015-74-8, 50602-06-7, 52286-18-7, 52286-19-8, 54116-08-4, 55901-67-2, 6170279-2, 61894-66-4, 62755-21-9, 63428-85-3, 63428-86-4, 63428-87-5, 65086-57-9, 65086-79-5, 65104-74-7,
65122-38-5, 67674-66-2, 67762-19-0, 67762-21-4, 67845-82-3, 67845-83-4, 67923-90-4, 68037-05-8, 6803706-9, 68171-41-5, 68424-50-0, 68511-39-7, 68585-34-2, 68610-66-2, 68611-29-0, 68611-55-2, 68649-53-6,
68890-88-0, 68891-29-2, 68891-30-5, 68891-38-3, 69011-37-6, 73665-22-2, 75422-21-8, 78330-16-2, 7833017-3, 78330-25-3, 78330-26-4, 78330-27-5, 78330-28-6, 78330-29-7, 78330-30-0, 96130-61-9, 106597-03-9,
110392-50-2, 119432-41-6, 125301-88-4, 125301-89-5, 125301-92-0, 125736-54-1, 157707-85-2, 160104-51-8,
160901-27-9, 160901-28-0, 160901-29-1, 160901-30-4, 161025-28-1, 161074-79-9, 162063-19-6, 219756-63-5)
Not more than
Surfactant
α-alkyl (C12-C15)-ω-hydroxypoly (oxypropylene) poly (oxyethylene) copolymers (where the poly (oxypropylene)
20% of pesticide
content is 3-60 moles and the poly (oxyethylene) content is 5-80 moles)
formulations
α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly (oxyethylene) polymers where the alkyl chain contains a
Surfactants, related
minimum of six carbons (CAS Reg. No.: 9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3;
adjuvants of
9038-43-1; 9040-05-5; 9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 26183-52-8; 26468-86-0;
surfactants.
26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 34398-01-1; 34398-05-5; 37251-67-5; 37311-00-5; 3731101-6; 37311-02-7; 37311-04-9; 39587-22-9; 50861-66-0; 52232-09-4; 52292-17-8; 52609-19-5; 57679-21-7;
59112-62-8; 60828-78-6; 61702-78-1; 61725-89-1; 61791-13-7; 61791-20-6; 61791-28-4; 61804-34-0; 6182742-7; 61827-84-7; 62648-50-4; 63303-01-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4;
64425-86-1; 65104-72-5; 65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 67763-08-0; 68002-96-0; 6800297-1; 68131-39-5; 68131-40-8; 68154-96-1; 68154-97-2; 68154-98-3; 68155-01-1; 68213-23-0; 68213-24-1;
68238-81-3; 68238-82-4; 68409-58-5; 68409-59-6; 68439-30-5; 68439-45-2; 68439-46-3; 68439-48-5; 6843949-6; 68439-50-9; 68439-51-0; 68439-53-2; 68439-54-3; 68458-88-8; 68526-94-3; 68526-95-4; 68551-12-2;
68551-13-3; 68551-14-4; 68603-20-3; 68603-25-8; 68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 6895494-9; 68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9; 69013-19-0; 69227-20-9; 69227-21-0; 69227-22-1;
69364-63-2; 70750-27-5; 70879-83-3; 70955-07-6; 71011-10-4; 71060-57-6; 71243-46-4; 72066-65-0; 7210890-8; 72484-69-6; 72854-13-8; 72905-87-4; 73018-31-2; 73049-34-0; 74432-13-6; 74499-34-6; 78330-19-5;
78330-20-8; 78330-21-9; 78330-23-1; 79771-03-2; 84133-50-6; 85422-93-1; 97043-91-9; 97953-22-5; 10278243-4; 103331-86-8; 103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0; 106232-83-1; 111905-54-5; 11681031-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5; 121617-09-2; 126646-02-4; 126950-62-7; 12703624-2; 139626-71-4; 152231-44-2; 154518-36-2; 157627-86-6; 157627-88-8; 157707-41-0; 157707-43-2; 15965349-3; 160875-66-1; 160901-20-2; 160901-09-7; 160901-19-9; 161025-21-4; 161025-22-5; 166736-08-9; 16910721-5; 172588-43-1; 176022-76-7; 196823-11-7; 287935-46-0; 288260-45-7; 303176-75-2; 954108-36-2)
Not to exceed 30%
α-alkyl (minimum C6 linear, branched, saturated and/or unsaturated)-ω-hydroxypolyoxyethylene polymer with or
without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, of formulation

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eCFR — Code of Federal Regulations

calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum
oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos.: 9004-80-2, 904601-9, 26982-05-8, 31800-89-2, 37280-82-3, 37281-86-0, 39341-09-8, 39341-65-6, 39464-66-9, 39464-69-2,
42612-52-2, 50643-20-4, 50668-50-3, 51325-10-1, 51884-64-1, 52019-36-0, 57486-09-6, 58206-38-5, 5831892-6, 58857-49-1, 59112-71-9, 60267-55-2, 61837-79-4, 62362-49-6, 62482-61-5, 63747-86-4, 63887-54-7,
63887-55-8, 66020-37-9, 66272-25-1, 66281-20-7, 67711-84-6, 67786-06-5, 67989-06-4, 68070-99-5, 6807117-0, 68071-35-2, 68071-37-4, 68130-44-9, 68130-45-0, 68130-46-1, 68130-47-2, 68186-29-8, 68186-34-5,
68186-36-7, 68186-37-8, 68238-84-6, 68311-02-4, 68311-04-6, 68332-75-2, 68389-72-0, 68400-75-9, 6841378-5, 68425-73-0, 68425-75-2, 68439-39-4, 68458-48-0, 68511-15-9, 68511-36-4, 68511-37-5, 68551-05-3,
68585-15-9, 68585-16-0, 68585-17-1, 68585-36-4, 68585-39-7, 68603-24-7, 68607-14-7, 68610-64-0, 6861065-1, 68649-29-6, 68649-30-9, 68650-84-0, 68815-11-2, 68855-46-9, 68856-03-1, 68890-90-4, 68890-91-5,
68891-12-3, 68891-13-4, 68891-26-9, 68908-64-5, 68909-65-9, 68909-67-1, 68909-69-3, 68921-24-4, 6892160-8, 68954-87-0, 68954-88-1, 68954-92-7, 68987-35-9, 69029-43-2, 69980-69-4, 70247-99-3, 70248-14-5,
70844-96-1, 70903-63-8, 71965-23-6, 71965-24-7, 72480-27-4, 72623-67-7, 72623-68-8, 72828-56-9, 7282857-0, 73018-34-5, 73038-25-2, 73050-08-5, 73050-09-6, 73361-29-2, 73378-71-9, 73378-72-0, 73559-42-9,
73559-43-0, 73559-44-1, 73559-45-2, 74499-76-6, 76930-25-1, 78041-18-6, 78330-22-0, 78330-24-2, 8246525-6, 84843-37-8, 91254-26-1, 93925-54-3, 95014-34-9, 96416-89-6, 99924-51-3, 103170-31-6, 103170-32-7,
106233-09-4, 106233-10-7, 108818-88-8, 110392-49-9, 111798-26-6, 111905-50-1, 116671-23-9, 117584-36-8,
119415-05-3, 120913-45-3, 121158-61-0, 121158-63-2, 123339-53-7, 125139-13-1, 125301-86-2, 125301-87-3,
126646-03-5, 129208-04-4, 129870-77-5, 129870-80-0, 130354-37-9, 136504-88-6, 143372-50-3, 143372-51-4,
144336-75-4, 146815-57-8, 151688-56-1, 154518-39-5, 154518-40-8, 155240-11-2, 159704-69-5, 160498-49-7,
160611-24-5, 171543-66-1, 172027-16-6, 172274-69-0, 176707-42-9, 181963-82-6, 188741-55-1, 191940-53-1,
210493-60-0, 210993-53-6, 246159-55-7, 251298-11-0, 261627-68-3, 290348-69-5, 290348-70-8, 317833-96-8,
340681-28-9 , 422563-19-7, 422563-26-6, 522613-09-8, 717140-06-2, 717140-09-5, 717827-29-7, 762245-80-7,
762245-81-8, 866538-89-8, 866538-90-1, 873662-29-4, 913068-96-9, 936100-29-7, 936100-30-0, 1072943-56-6,
1087209-87-7, 1174313-54-2, 1187742-89-7, 1187743-35-6, 1205632-03-6, 1233235-49-8, 1451002-50-8,
1456802-88-2, 1456802-89-3, 1456803-12-5)
N-alkyl (C8-C18) primary amines and their acetate salts where the alkyl group is linear and may be saturated
Concentration in
and/or unsaturated (CAS Reg. Nos. 61790-57-6, 61790-58-7, 61790-59-8, 61790-60-1, 61788-46-3, 61790-33-8, formulated end68155-38-4)
use products not
to exceed 10% by
weight in herbicide
products, 4% by
weight in
insecticide
products, and 4%
by weight in
fungicide products
Alkyl (C8-C18) sulfate and its ammonium, calcium, isopropylamine, magnesium, potassium, sodium, and zinc salts
Aluminum hydroxide
Aluminum oxide
Aluminum stearate
Amides, C5-C9, N-[3-(dimethylamino) propyl] (CAS Reg. No. 1044764-00-2)
Amides, C6-C12, N-[3-(dimethylamino) propyl] (CAS Reg. No. 1044764-06-8)
Ammonium bicarbonate

Ammonium carbamate

Ammonium chloride

Ammonium hydroxide

Ammonium salts of fatty acids (C8-C18 saturated) (CAS Reg. No. 5972-76-9, 63718-65-0, 16530-70-4, 32582-95-9,
2437-23-2, 191799-95-8, 16530-71-5, 93917-76-1, 5297-93-8, 94266-36-1, 1002-89-7)
Ammonium stearate
Ammonium sulfate
Ammonium thiosulfate

Amyl acetate
Ascorbyl palmitate
Attapulgite-type clay
Bacillus thuringiensis fermentation solids and/or solubles
Bentonite
Benzoic acid
Bicyclo[3.1.1]hept-2-ene, 2,6,6-trimethyl-, homopolymer (Alpha-pinene, homopolymer)(CAS Reg. No. 25766-18-1)

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Surfactants, related
adjuvants of
surfactants.

Surfactants, related
adjuvants of
surfactants

Surfactants.
Diluent, carrier
Diluent
Surfactant
Surfactant
Surfactant
Surfactant,
suspending agent,
dispersing agent
Synergist in aluminum
phosphide
formulations
Intensifier when used
with ammonium nitrate
as a dessicant or
defoliant. Fire
suppressant in
aluminum phosphide
and magnesium
phosphide
formulations
Solvent, cosolvent,
neutralizer, solubilizing
agent
Surfactant
Surfactant
Solid diluent, carrier
Intensifier when used
with ammonium nitrate
as desiccant or
defoliant
Solvent, cosolvent,
attractant
Preservative
Solid diluent, carrier,
thickener
Diluent, carrier
Solid diluent, carrier
Preservative for
formulation
Surfactants, related
adjuvants of
surfactants

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Bicyclo[3.1.1]heptane, 6,6-dimethyl-2-methylene-, homopolymer (Beta-pinene, homopolymer) (CAS Reg. No.
25719-60-2)
Bicyclo[3.1.1]hept-2-ene, 2,6,6-trimethyl-, polymer with 6,6-dimethyl-2-methylenebicyclo [3.1.1] heptane
(Copolymer of alpha- and beta-pinene) (CAS Reg. No. 31393-98-3)
2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52-51-7)

Butane
n-Butanol (CAS Reg. No. 71-36-3)
n-Butyl benzoate (CAS Reg. No.136-60-7)
Butylated hydroxyanisole
Butylated hydroxytoluene
Calcareous shale
Calcite
Calcium carbonate
Calcium chloride
Calcium phosphate
Calcium hydroxide
Calcium hypochlorite
Calcium lactate pentahydrate (CAS Reg. No. 5743-47-5)
Calcium oxide
Calcium salt of partially dimerized rosin, conforming to 21 CFR 172.210
Calcium silicate
Calcium stearate
Carbon Dioxide (CAS Reg. No. 124-38-9)
Carrageenan, conforming to 21 CFR 172.620

Cetyl alcohol (CAS Reg. No. 36653-82-4)

Charcoal, activated

Coconut shells
Cod liver oil
Croscarmellose sodium (CAS Reg. No. 74811-65-7)

n-Decyl alcohol (CAS Reg. No. 112-30-1)
Dialkyl (C8-C18) dimethyl ammonium chloride

Diatomite (diatomaceous earth)
Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-75-4)
Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-83-4)
Diethylaminoethanol, ethoxylated, reaction product with fatty acid dimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173188-72-1)
Diethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173188-81-2)
Diethylene glycol abietate

1,1-Difluoroethane (CAS Reg. No. 75-37-6)

1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene

Diisopropanolamine (CAS Reg. No. 110-97-4)

Diisopropyl adipate (CAS Reg. No. 6938-94-9)

0.04% or less by
weight of the total
pesticide
formulation

Surfactants, related
adjuvants of
surfactants
Surfactants, related
adjuvants of
surfactants
In-can preservative

Propellant
Solvent, cosolvent
Solvent
Antioxidant
Do.
Solid diluent carrier
Do.
Do.
Stabilizer
Solid diluent, carrier
Do.
Sanitizing and
bleaching agent
Nutrient, stabilizer
Solid diluent, carrier
Coating agent
Solid diluent, carrier
Do.
Propellant
Thickener

None
Minimum
molecular weight
(in amu): 100,000
Not more than
Evaporation retardant
5.0% of pesticide
formulation
Meets
Carrier
specifications in
the Food Chemical
Codex
Solid diluent and
carrier
Solvent, cosolvent
Disintegrant, solid
diluent, carrier, and
thickener
Solvent or co-solvent
Not more than
Flocculating agent in
0.2% in silica,
the manufacture of
hydrated silica
silica, hydrated silica
for use as a solid
diluent, carrier
Solid diluent carrier
Surfactant
Surfactant
Surfactant
Surfactant
Surfactants, related
adjuvants of
surfactants
Aerosol propellant

For aerosol
pesticide
formulations used
for insect control in
food- and feedhandling
establishments
and animals
Not more than
Antioxidant
0.02% of pesticide
formulation
Not to exceed 10% Neutralizer or
by weight of
stabilizer
pesticide
formulation
Solvent, co-solvent.

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40% in mosquito
control
formulations
None

Dimethyl adipate (CAS no. 627-93-0)
Dimethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-42-5)
Dimethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-67-4)
Dimethylaminoethanol, ethoxylated, reaction products with fatty acid dimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173188-38-9)
Dimethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173188-49-2)
Dimethyl ether (methane, oxybis-) (CAS Reg. No. 115-10-6)
Dimethyl glutarate (CAS no. 1119-40-0)
None
3,6-Dimethyl-4-octyn-3,6-diol
Not more than
2.5% of pesticide
formulation
Dimethyl succinate (CAS no. 106-65-0)
None
Di-n-butyl carbonate (CAS Reg. No. 542-52-9)
Dipropylene glycol
Disodium phosphate
Disodium zinc ethylenediaminetetraacetate dihydride
Distillates, (Fishcher-Tropsch), heavy, C18-C50, branched, cyclic and linear (CAS Reg. No. 848301-69-9)
Dolomite
Epoxidized linseed oil

Epoxidized soybean oil
Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No. 107-36-8)
Ethanesulfonic acid, 2-hydroxy-, ammonium salts (CAS Reg. No. 57267-78-4)
Ethanesulfonic acid, 2-hydroxy-, calcium salts (CAS Reg. No. 10550-47-7)
Ethanesulfonic acid, 2-hydroxy-, magnesium salts (CAS Reg. No. 17345-56-1)
Ethanesulfonic acid, 2-hydroxy-, potassium salts (CAS Reg. No. 1561-99-5)
Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS Reg. No. 1562-00-1)
Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS Reg. No. 129756-32-7)
Ethyl acetate
Ethyl alcohol
Ethyl esters of fatty acids derived from edible fats and oils
Ethyl maltol (CAS Reg. No.4940-11-8)

Ethylene glycol (CAS Reg. No. 107-21-1)

Ethylene oxide adducts of 2,4,7,9-tetramethyl-5-decynediol, the ethylene oxide content averages 3.5, 10 or 30
moles (CAS Reg. No. 9014-85-1)
(S,S)-Ethylenediamine disuccinic acid trisodium salt (CAS Reg. No. 178949-82-1)
Ethylenediaminetetraacetic acid
Ethylenediaminetetraacetic acid, tetrasodium salt
2-Ethyl-1-hexanol (CAS Reg. No. 104-76-7)
Fatty acids, conforming to 21 CFR 172.860
FD&C Blue No. 1

FD&C Red No. 40 (CAS Reg. No. 25956-17-6) conforming to 21 CFR 74.340

Ferric Citrate (CAS Reg. No. 2338-05-8)
Ferric sulfate
Furcelleran

Solvent/co-solvent
Surfactant
Surfactant
Surfactant
Surfactant

Propellant
Solvent/co-solvent
Surfactants, related
adjuvants of
surfactants
Solvent/co-solvent
Solvent
Solvent, cosolvent
Anticaking agent,
conditioning agent
Sequestrant
Solvent, diluent and/or
dust suppressant
Solid diluent, carrier
Surfactants, related
adjuvants of
surfactants
Do.
Chelator, sequestrant,
or conditioning agent
Do.
Do.
Do.
Do.
Do.
Do.
Solvent, cosolvent
Do.
Solvent, cosolvent
Not more than 0.2 Odor masking agent
% of the pesticide
formulation
Without limitation Encapsulating agent
for pesticides being
applied post-harvest
as residual, and crack
and crevice sprays in
and around food and
nonfood areas of
residential and
nonresidential
structures, including
food handling
establishments
Surfactants, related
adjuvants of
surfactants
Sequestrant or
chelating agent
3% of pesticide
Sequestrant
formulation
5% of pesticide
Sequestrant
formulation
Not more than
Solvent, adjuvant of
10% of pesticide surfactants
Binder, defoaming
agent, lubricant
Not more than
Dye
0.2% of pesticide
formulation
Not to exceed
Dye, coloring agent
0.002% by weight
of pesticide
formulation
Stabilizer
Solid diluent, carrier
Thickener

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D-glucopyranose, oligomeric, C10-16-alkyl glycosides (CAS Reg. No. 110615-47-9)
D-glucopyranose, oligomeric, 6-(dihydrogen citrates), C8-20 branched and linear alkyl glycosides, sodium salts
(CAS Reg. No. 1079993-97-7)
D-glucopyranose, oligomeric, 6-(hydrogen sulfosuccinates), C8-20 branched and linear alkyl glycosides, sodium
salts (CAS Reg. No. 1079993-92-2)
D-glucopyranose, oligomeric, lactates, C8-20 branched and linear alkyl glycosides (CAS Reg. No. 1079993-94-4)
Glycerides, edible fats and oils derived from plants and animals, reaction products with sucrose (CAS Reg. Nos.
100403-38-1, 100403-41-6, 100403-39-2, 100403-40-5)
Glycerol mono-, di-, and triacetate
Glyceryl monostearate
Granite
Graphite
Gum arabic (acacia)

Gypsum
Hexamethylenetetramine

3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1)

Surfactant
Surfactant
Surfactant

For use in citrus
washing solutions
only at not more
than 1%
Not more than
Odorant, alerting
0.4% of the
agent
pesticide
formulation
Solvent, cosolvent
Solvent
Solvent
Solvent
Solvent, neutralizer
Surfactant

n-Hexyl alcohol (CAS Reg. No. 111-27-3)
C9 rich aromatic hydrocarbons (CAS Reg. No. 64742-95-6)
C10-11 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5)
C11-12 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5)
Hydrochloric acid
Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-06-4)
Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-17-7)
Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid dimers, minimum number average
molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-00-8)
Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid trimers, minimum number average
molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-09-7)
Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-22-4
Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-28-0)
Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid dimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173189-20-2)
Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173189-25-7)
Hydroxyethylidine diphosphonic acid (HEDP) (CAS Reg. No. 2809-21-4)
For use in
antimicrobial
pesticide
formulations at not
more than 1
percent
Iron oxide
Isobutane (CAS Reg. No. 75-28-5)
None
Isopropyl myristate (CAS Reg. No. 110-27-0)
Kaolinite-type clay
Lactic acid
Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283-86-9)
Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No. 186817-80-1)
Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651-69-7)
Lauryl alcohol
Lignin (CAS Reg. No. 9005-53-2)

Lignin, alkali (CAS Reg. No. 8068-05-1)
Lignin, alkali, oxidized, sodium salt (CAS Reg. No. 68201-23-0)
Lignin alkali reaction products with disodium sulfite and formaldehyde (CAS Reg. No. 105859-97-0)
Lignin alkali reaction products with formaldehyde and sodium bisulfite (CAS Reg. No. 68512-35-6)
Lignosulfonic acid (CAS Reg. No. 8062-15-5)
Lignosulfonic acid, ammonium calcium salt (CAS Reg. No. 12710-04-2)
Lignosulfonic acid, ammonium magnesium salt (CAS Reg. No. 123175-37-1)
Lignosulfonic acid, ammonium salt (CAS Reg. No. 8061-53-8)
Lignosulfonic acid, ammonium sodium salt (CAS Reg. No. 166798-73-8)
Lignosulfonic acid, calcium magnesium salt (CAS Reg. No. 55598-86-2)
Lignosulfonic acid, calcium salt (CAS Reg. No. 8061-52-7)
Lignosulfonic acid, calcium sodium salt (CAS Reg. No. 37325-33-0)
Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg. No. 68611-14-3)
Lignosulfonic acid, magnesium salt (CAS Reg. No. 8061-54-9)

Surfactant
Emulsifier, dispersing
agent
Solvent, cosolvent
Emulsifier
Do.
Solid diluent, carrier
Surfactant,
suspending agent,
dispersing agent
Solid diluent, carrier
Preservative

Surfactant
Surfactant
Surfactant
Surfactant
Surfactant
Surfactant
Surfactant
Stabilizer, chelator

Solid diluent, carrier
Propellant
Solvent
Solid diluent, carrier
Solvent
Solvent
Solvent
Solvent
Surfactant
Surfactant, related
adjuvants of
surfactants
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.

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Lignosulfonic acid, potassium salt (CAS Reg. No. 37314-65-1)
Lignosulfonic acid, sodium salt (CAS Reg. No. 8061-51-6)
Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No. 68855-41-4)
Lignosulfonic acid, sodium salt, polymer with formaldehyde and phenol (CAS Reg. No. 37207-89-9)
Lignosulfonic acid, sodium salt, sulfomethylated (CAS Reg. No. 68512-34-5)
Lignosulfonic acid, zinc salt (CAS Reg. No. 57866-49-6)
d-Limonene (CAS Reg. No. 5989-27-5)
Magnesium carbonate

Do.
Do.
Do.
Do.
Do.
Do.
Solvent, fragrance
Anticaking agent,
conditioning agent
Magnesium chloride
Safener
Magnesium lime
Solid diluent, carrier
Magnesium oxide
Do.
Magnesium silicate
Do.
Magnesium stearate
Surfactant
Magnesium sulfate
Solid diluent, carrier,
safener
Methyl alcohol
Solvent
Methyl n-amyl ketone (CAS Reg. No. 110-43-0)
Solvent, cosolvent
Methyl 5-(dimethylamino)-2-methyl-5-oxopentanoate (1174627-68-9)
Solvent
Methyl esters of fatty acids derived from edible fats and oils
Solvent, cosolvent
Methyl esters of higher fatty acids conforming to 21 CFR 573.640
Antidusting agent,
surfactant
Methyl isobutyl ketone
Solvent
2-methyl-2,4-pentanediol (CAS Reg. No. 107-41-5)
Without limitation Growing crops and
food animals
2-methyl-1,3-propanediol (CAS Reg. No. 2163-42-0)
Solvent, surfactant
Methylated silicones
Antifoaming agent
Mono-, di-, and trimethylnapthalenesulfonic acids and napthalenesulfonic acids formaldehyde condensates,
Surfactants, related
ammonium and sodium salts (CAS Reg. Nos 9008-63-3, 9069-80-1, 9084-06-4, 36290-04-7, 91078-68-1, 141959adjuvants of
43-5, 68425-94-5)
surfactants
Mica
Solid diluent, carrier
Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or 178.3620(a) (CAS Reg. No. 8012-95-1)
Diluent, carrier, and
solvent
Monoammonium phosphate
No more than
Postharvest
3.75% by weight in fumigation in
formulation
formulation with
aluminum phosphide
Surfactants, related
Mono- and diglycerides of C8-C18 fatty acids
adjuvants of
surfactants
Montmorillonite-type clay
Solid diluent, carrier
Surfactant.
Nonyl, decyl, and undecyl glycoside mixture with a mixture of nonyl, decyl, and undecyl oligosaccharides and
related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65%
solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20%
C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8)
α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate Not to exceed 7% Surfactants, related
esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the
of pesticide
adjuvants of
phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 formulation
surfactants
or 30 moles (CAS Reg. Nos. 51811-79-1, 59139-23-0, 67922-57-0, 68412-53-3, 68553-97-9, 68954-84-7, 9982114-4, 152143-22-1, 51609-41-7, 37340-60-6, 106151-63-7, 68584-47-4, 52503-15-8, 68458-49-1)
α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) produced by the condensation of 1 mole of nonylphenol (nonyl
Surfactants, related
group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide; if a blend of
adjuvants of
products is used, the average number of moles of ethylene oxide reacted to produce any product that is a
surfactants
component of the blend shall be in the range of 4-14 or 30-90
α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) sulfate, ammonium, calcium, magnesium, potassium, sodium, and Not to exceed 7% Surfactants, related
zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS
of pesticide
adjuvants of
Reg. Nos. 9014-90-8, 9051-57-4, 9081-17-8, 68649-55-8, 68891-33-8
formulation
surfactants
1-Octanal (CAS Reg. No. 124-13-0)
Not more than
Odor masking agent
0.2% of the
pesticide
formulation
n-Octyl alcohol (CAS Reg. No. 111-87-5)
Solvent or co-solvent
Surfactants, related
Octyl and decyl glucosides mixture with a mixture of octyl and decyloligosaccharides and related reaction products
adjuvants of
(primarily n- decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain
surfactants
alcohols (C8(45%), C10 (55%)) with anhydrous glucose
Oleic acid
Diluent
Oleic acid diester of α-hydro-ω-hydroxypoly (oxyethylene); the poly(oxyethylene) having average molecular weight
Surfactants, related
(in amu) 400
adjuvants of
surfactants
α-Oleoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600
Emulsifier
Oleyl alcohol (CAS Reg. No. 143-28-2
15%
Cosolvent
Oxalic acid
No more oxalic
Calcium chelating
acid should be
hard water inhibitor
used than is
necessary to
chelate calcium
and in no case
should more than
2 lb oxalic acid per
acre be used

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Palmitic acid
Pentaerythritol ester of maleic anhydride modified wood rosin
Petrolatum, conforming to 21 CFR 172.880
Petroleum hydrocarbons, light odorless conforming to 21 CFR 172.884
Petroleum hydrocarbons, synthetic isoparaffinic, conforming to 21 CFR 172.882
Petroleum naphtha, conforming to 21 CFR 172.250(d)
Petroleum wax, conforming to 21 CFR 172.886(d)
Phosphoric acid
Polyethylene, conforming to 21 CFR 177.1520(c)
Polyethylene glycol[α-hydro-ω-hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms
to 21 CFR 178.3750
Polyglycerol esters of fatty acids conforming to 21 CFR 172.854

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Diluent
Plasticizer
Coating agent
Solvent, diluent.
Do.
Component of coating
agent
Coating agent
Buffer
Binder, carrier, and
coating agent
Surfactants, related
adjuvants of
surfactants
Surfactants, related
adjuvants of
surfactants
Surfactants, related
adjuvants of
surfactants
Surfactant

Polyglyceryl phthalate ester of coconut oil fatty acids, including fatty acid coco polymers with glyceryl and phthalic None
anhydride (CAS No. 67746-02-5) and coconut oil polymer with glyceryl and phthalic anhydride (CAS No. 6607087-9)
Poly(oxy-1,2-ethanediyl), α-(carboxymethyl)-ω-(nonylphenoxy) produced by the condensation of 1 mole of
nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide.
The molecular weight (in amu) ranges are 454-894 and 1598-4238
Poly(oxy-1,2-ethanediyl), α-[tris(1-phenylethyl)phenyl]-ω-hydroxy-, (CAS Reg. No. 99734-09-5)
For use in postSurfactants
harvest
applications; not to
exceed 15% by
weight in pesticide
formulations
Polyoxyethylene (20) sorbitan monostearate
Surfactants, related
adjuvants of
surfactants
Not to exceed 15% Surfactant
[Poly[oxy(methyl-1,2-ethanediyl)], α-[2-bis(2-hydroxyethyl)amino]propyl]-ω-hydroxy,-ether with α-hydro-ωin the formulated
hydroxypoly(oxy-1,2-ethanediyl) (1:2), mono-C12-16 alkyl ethers, (CAS Reg. No. 176022-82-5)
product; only for
use with
glyphosate
Polysorbate 65, conforming to 21 CFR 172.838
Emulsifier
Potassium aluminum silicate
Solid diluent, carrier
Potassium benzoate (Cas No. 582-25-2)
None
Preservative
Potassium hydroxide
Neutralizer
Potassium phosphate
Buffer
Potassium sulfate
Solid diluent
Propane
Propellant
1,3-Propanediol (CAS Reg. No. 504-63-2)
Solvent, co-solvent,
diluent, or freeze-point
depressant
2-Propanol, 1,1′,1″-nitrilotris- (CAS No. 122-20-3)
Without limitation Neutralizer
n-Propanol
Solvent, cosolvent
2-Propenoic acid, 2-methyl-, polymer with ethyl 2-propenoate and methyl 2-methyl-2-propenoate, ammonium salt
Encapsulating agent,
(CAS Registration No. 55989-05-4), minimum number average molecular weight (in amu), 18,900.
dispensers, resins,
fibers and beads
Propyl gallate
Antioxidant
Propyl p-hydroxybenzoate
Preservative for
formulations
Propylene glycol
Solvent, cosolvent.
Propylene glycol alginate (as defined in 21 CFR 172.858)
Defoaming agent
Propylene glycol monomethyl ether (CAS No. 107-98-2)
none
solvent
Pyrophyllite
Solid diluent, carrier
Rhizobium inoculants (e.g. Sinorhizobium, Bradyrhizobium & Rhizobium)
All leguminous food
commodities
Rosin, partially dimerized (as defined in 21 CFR 172.615)
Surfactants, related
adjuvants of
surfactants
Rosin, partially hydrogenated (as defined in 21 CFR 172.615)
Do.
Rosin, wood
Do.
Salts of fatty acids, conforming to 21 CFR 172.863
Binder, emulsifier,
anticaking agent
Sand
Solid diluent, carrier
Shellac, bleached; refined, food grade, arsenic and rosin-free
Coating agent
Silver nitrate (Cas Reg. No. 7761-88-8)
For use on
Stabilizer
potatoes as postharvest treatment
to control
sprouting at no
more than 0.06%
by weight in
pesticide
formulations

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Soapstone
Sodium acid pyrophosphate

Sodium alkyl naphthalenesulfonates (CAS Reg. Nos. 68909-83-1, 68909-84-2, 68909-82-0, 27213-90-7, 2626458-4, 27178-87-6, 111163-74-7, 908356-16-1, 25417-20-3, 25638-17-9, 145578-88-7, 1322-93-6, 1323-19-9,
7403-47-6, 68442-09-1, 127646-44-0, 908356-18-3)
Sodium aluminum silicate
Sodium dioctylsulfosuccinate

Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006-15-3)

Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No. 127-39-9)

Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922-80-5)

Sodium DL-lactate (CAS Reg. No. 72-17-3)
Sodium hexametaphosphate

Sodium hydroxide
Sodium L-lactate (CAS Reg. No. 867-56-1)
Sodium metasilicate

Sodium monoalkyl and dialkyl (C6-C16) phenoxy benzenedisulfonates and related acids (CAS Reg. Nos. 14773259-0, 147732-60-3, 169662-22-0, 70191-75-2, 36445-71-3, 39354-74-0, 70146-13-3, 119345-03-8, 149119-20-0,
149119-19-7, 119345-04-9, 28519-02-0, 25167-32-2, 30260-73-2, 65143-89-7, 70191-76-3)
Sodium α-olefinsulfonate (sodium C14-C16) (Olefin sulfonate)

SodiumN-oleoyl- N-methyl taurine (CAS Reg. No. 137-20-2)

Sodium and potassium salts of N-alkyl (C8-C18)-beta-iminodipropionic acid where the C8-C18 is linear and may be
saturated and/or unsaturated (CAS Reg. Nos. 110676-19-2, 3655-00-3, 61791-56-8, 14960-06-6, 26256-79-1,
90170-43-7, 91696-17-2, 97862-48-1)

Sodium salt of sulfated oleic acid

Sodium silicate

Sodium starch glycolate (CAS Reg. No. 9063-38-1)

Sodium sulfate
Sodium tripolyphosphate

Sorbic acid (CAS Reg. No. 110-44-1)
Sorbitan fatty acid esters (fatty acids limited to C12, C14, C16, and C18 containing minor amounts of associated fatty
acids) and their derivatives; the poly(oxyethylene) content averages 5-20 moles
Soybean flour
Soybean oil-derived fatty acids
Stearic acid
α-Stearoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600
α-Stearoyl-ω-hydroxypoly(oxyethylene); the poly(oxyethylene) content averages either 8, 9, or 40 moles; if a blend
of products is used, the average number of moles ethylene oxide reacted to produce any product that is a
component of the blend shall be either 8, 9, or 40
Sucrose octaacetate
Sulfite liquors and cooking liquors, spent, oxidized (CAS Reg. No. 68514-09-0)

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Solid diluent
Surfactant,
suspending agent,
dispersing agent,
buffer
Limited to no more Surfactants, related
than 30% by
adjuvants of
weight in pesticide surfactants
end-use products
Solid diluent, carrier
Surfactants, related
adjuvants of
surfactants
Surfactants, related
adjuvants of
surfactants
Surfactants, related
adjuvants of
surfactants
Surfactants, related
adjuvants of
surfactants
Surfactant
Surfactant, emulsifier,
wetting agent,
suspending agent,
dispersing agent,
buffer
Neutralizer
Surfactant
Surfactants,
emulsifiers, wetting
agents, dispersing
agents, buffer
Not to exceed 20% Surfactants, related
in pesticide
adjuvants of
formulations
surfactants
Surfactants, related
adjuvants of
surfactants
Surfactants, related
adjuvants of
surfactants
Concentration in Surfactants, related
formulated endadjuvants of
use products not surfactants
to exceed 30% by
weight in pesticide
formulations
Surfactants, related
adjuvants of
surfactants
Surfactant, emulsifier,
wetting agent,
stabilizer, inhibitor
Granular and
Disintegrant
tableted products
only; not to exceed
8% of the
formulated product
Solid diluent, carrier
Buffer, surfactant,
suspending agent,
dispersing agent,
anticaking agent,
conditioning agent
Preservative for
formulations
Surfactants, related
adjuvants or
surfactants.
Expires May 24,
Surfactant
2005.
Solvent, cosolvent
Diluent
Emulsifier
Surfactants, related
adjuvants of
surfactants
Adhesive

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Surfactant, related
adjuvants of
surfactants
Sulfuric acid (CAS Reg. No.7664-93-9)
Not to exceed 10% pH Control agent
of the pesticide
formulation; nonaerosol
formulations only
Sweet orange peel tincture (CAS Reg. No. 8028-48-6)
Not to exceed 10% Surfactant, fragrance,
(weight/weight) in related adjuvants of
pesticide
surfactants
formulation
Synthetic paraffin and its succinic derivatives conforming to 21 CFR 172.275
Carrier, binder, and
carrying agent
Synthetic petroleum wax, conforming to 21 CFR 172.888
Binder, carrier, and
coating agent
Talc
Solid diluent, carriers
Tall oil; fatty acids not less than 58%, rosin acids not more than 44%, unsaponifiables not more than 8%
Surfactants, related
adjuvants of
surfactants
Tartrazine
Dye
Terpenes and terpenoids, turpentine oil, alpha-pinene fraction, polymd. (CAS Reg. No. 70750-57-1)
Surfactants, related
adjuvants of
surfactants
1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811-97-2)
Aerosol propellant
Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No. 29118-24-9)
Propellant
Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No 97-99-4)
Expires February Solvent/cosolvent
9, 2008
N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylenediamine (CAS Reg. No. 102-60-3)
Concentration in Stabilizer for
formulated endformulation.
use products not
to exceed 20% by
weight in pesticide
formulations
α-[p-(1,1,3,3-tetramethylbutyl)phenyl]-ω-hydroxypoly(oxyethylene) produced by the condensation of 1 mole of
Not to exceed 7% Surfactants related
p-(1,1,3,3-tetramethylbutyl)phenol with a range of 1-14 or 30-70 moles of ethylene oxide: If a blend of products is of pesticide
adjuvants of
used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of formulation
surfactants
the blend shall be in the range of 1-14 or 30-70 (CAS Reg. Nos. 9036-19-5, 9002-93-1)
2,4,7,9-Tetramethyl-5-decyn-4, 7-diol
Not more than
Surfactants, related
2.5% of pesticide adjuvants of
formulation
surfactants
Tetrasodium pyrophosphate
Anticaking agent,
conditioning agent
Thiosulfuric acid, disodium salt, anhydrous. (CAS Reg. No 7772-98-7)
Dechlorinator,
reducing agent
Thiosulfuric acid, disodium salt, pentahydrate. (CAS Reg. No. 10102-17-7)
Do.
d-Alpha tocopherol (CAS Reg. No. 9-02-9
None
Safener
d-Alpha tocopheryl acetate (CAS Reg. No. 58-95-7)
None
Do.
dl-Alpha tocopherol (CAS Reg. No.10191-41-0)
None
Do.
dl-Alpha tocopheryl acetate (CAS Reg. No. 7695-91-2)
None
Do.
Tricalcium phosphate
Surfactant,
suspending agent,
dispersing agent,
anticaking agent,
conditioning agent
Trisodium phosphate
Surfactant, emulsifier,
wetting agent
Vermiculite
Solid diluent, carrier.
Vitamin E (CAS Reg. No. 1406-18-4)
None
Safener
Walnut shells
Leaching inhibitor,
binder for waterdispersible
aggregates, sticker
and suspension
stabilizer
Wintergreen oil
Attractant
Derived from wood Solid diluent and
Wood flour
free of chemical
carrier
preservatives
Xanthan gum-modified, produced by the reaction of xanthan gum and glyoxal (maximum 0.3% by weight)
Not more than
Surfactant
0.5% of pesticide
formulation
Xylene meeting the specifications listed in 21 CFR 172.884(b)(4)
In pesticide
Solvent, cosolvent
formulations for
grain storage only
Zeolite (hydrated alkali aluminum silicate)
Solid diluent, carrier
Zinc oxide
Coating agent
Zinc sulfate (basic and monohydrate)
Do.
Zinc sulfate (basic and monohydrate)
Solid diluent, carrier

[69 FR 23117, Apr. 28, 2004]

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Page 375 of 441

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.910, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.920 Inert ingredients used pre-harvest; exemptions from the requirement of a tolerance.
The following materials are exempted from the requirement of a tolerance when used in accordance with good
agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to growing crops only:
Inert ingredients
Acetophenone
Adenosine (CAS Reg. No. 58-61-7)
Alder bark
Alkyl (C12-C16) dimethyl ammonio acetate (CAS Reg. Nos. 683-10-3, 2601-33-4 and 69333-4
α-Alkyl (minimum C6 linear, branched, saturated and/or unsaturated)-ωhydroxypolyoxyethylene polymer with or without polyoxypropylene, mixture of di- and
monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium,
monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum
oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg.
Nos. 9046-01-9, 37280-82-3, 39464-66-9, 42612-52-2, 50643-20-4, 52019-36-0, 5831892-6, 60267-55-2, 61837-79-4, 67711-84-6, 68070-99-5, 68071-35-2, 68071-17-0, 6813047-2, 68186-37-8, 68186-36-7, 68311-02-4, 68425-73-0, 68458-48-0, 68511-37-5, 6861065-1, 68585-36-4, 68649-29-6, 68815-11-2, 68908-64-5, 68891-13-4, 73038-25-2, 7833024-2, 108818-88-8, 154518-39-5, 317833-96-8, 873662-29-4, 936100-29-7, 936100-30-0)
N-alkyl(C8-C18) dimethylamidopropylamines where the alkyl group is linear and may be
saturated and/or unsaturated (CAS Reg. Nos. 109-28-4, 3179-80-4, 7651-02-7, 2289010-4, 22890-11-5, 39669-97-1, 45267-19-4, 68140-01-2, 1147459-12-8, 146987-98-6)
N-alkyl (C8-C18) primary amines and their acetate salts where the alkyl group is linear and
may be saturated and/or unsaturated (CAS Reg. Nos. 61790-57-6, 61790-58-7, 6179059-8, 61790-60-1, 61788-46-3, 61790-33-8, 68155-38-4)

Limits
Maximum of 0.5% of formulation
20% by weight in pesticide
formulation
Not to exceed 30% of pesticide
formulation

Not to exceed 20% by weight in
herbicide formulations

Uses
Attractant
Synergist
Seed germination stimulator
Surfactant
Surfactants, related
adjuvants of surfactants

Surfactants, related
adjuvants of surfactants

Concentration in formulated end-use Surfactants, related
products not to exceed 10% by
adjuvants of surfactants
weight in herbicide products, 4% by
weight in insecticide products, and
4% by weight in fungicide products
Not to exceed 25% in herbicide
Surfactants, related
formulations and 10% in insecticide adjuvants of surfactants
and fungicide formulations

N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl) C8-C18 saturated and unsaturated
alkylamines; the poly(oxy-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 1021378-2, 25307-17-9, 26635-92-7, 26635-93-8, 288259-52-9, 58253-49-9, 61790-82-7,
61791-14-8, 61791-24-0, 61791-26-2, 61791-31-9, 61791-44-4, 68155-33-9, 68155-39-5,
68155-40-8,70955-14-5, 73246-96-5, 1266162-49-5)
Not to exceed 25% in herbicide
N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18
formulations and 10% in insecticide
saturated and unsaturated alkylamines; the poly(oxy-1,2-ethanediyl/oxy
and fungicide formulations
(methyl-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 68213-26-3, 68153-97-9,
75601-76-2)
Aluminum sulfate
Ammonium chloride (CAS Reg. No. 12125-02-9)
Ammonium formate (CAS Reg. No. 540-69-2)
Ammonium nitrate (CAS Reg. No. 6484-52-2)
Ammonium polyphosphate (CAS Reg. No. 68333-79-9)

Barium sulfate
1,4-Benzenedicarboxylic acid, dimethyl ester, polymer with 1,4-butanediol, adipic acid, and For use in honeybee hive miticide
hexamethylene diisocyanate, minimum number average molecular weight (in amu) 30,000 formulations
(CAS Reg. No. 55231-08-8)
1,2-Benzisothiazolin-3-one
Not more than 0.1% of formulation.
Not more than 0.02 lb to be applied
per acre
Boric acid
Buffalo gourd root powder (Cucurbita foetidissima root powder); or, Zucchini juice
No more than 2.5 lbs/acre/season
(Cucurbita pepo juice) or Hawkesbury melon Citrullus lanatus.
(3.4 gm/acre/season of
Cucurbitacin)
Butyl stearate
γ-Butyrolactone
C.I. Pigment Blue #15 (CAS Reg. No. 147-14-8; containing no more than 50 ppm
For seed treament use only
polychlorinated biphenyls (PCBs))
C.I. Pigment Green #7 (CAS Reg. No. 1328-53-6; containing no more than 50 ppm
For seed treatment use only
polychlorinated biphenyls (PCBs))
C.I. Pigment Red #112 (CAS Reg. No. 6535-46-2)
Seed treatment use only. Limited to
10% w/w of pesticide formulation
C.I. Pigment Violet #23 (CAS Reg. No. 6358-30-1; containing no more than 20 ppb of
For seed treatment use only
polychlorinated dibenzo-p-dioxins and/or polychlorinated dibenzofurans)
C.I. Pigment Yellow 1 (CAS Reg. No. 2512-29-0)
Not to exceed 10% (weight/weight)
in pesticide formulation
Calcium gluconate (CAS Reg. No. 299-28-5)
Camphor (CAS Reg. No. 76-22-2)
Not more than 5% weight to weight
(w/w) of pesticide formulations
Carbon Black (CAS Reg. No. 1333-86-4)
For seed treatment use only
Carbonic acid, dipotassium salt (CAS Reg. No. 584-08-7)
Carbonic acid, dipotassium salt, trihydrate (CAS Reg. No. 18662-52-7)

Surfactants, related
adjuvants of surfactants

Safener adjuvant
Carrier/nutrient
Complexing or fixing agent
Adjuvant/ intensifier for
herbicides
Sequestrant, buffer, or
surfactant
Carrier
Component of controlled
release agent
Preservative/stabilizer

Sequestrant
Gustatory stimulant

Defoamer
Solvent
Dye, coloring agent
Dye, coloring agent
Coloring agent
Dye, coloring agent
Colorant
Sequestrant
Deodorant, melting point
adjustment
Colorant
Buffering agent
Buffering agent

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Carboxymethyl guar gum sodium salt (CAS Reg. No. 39346-76-4)
Carboxymethyl-hydroxypropyl guar (CAS Reg. No. 68130-15-4)
Carous chloride
Carrageenan, conforming to 21 CFR 172.260

Chlorobenzene

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Without limitation
Without limitation
10 ppm in formulation
Not more than 0.15% of pesticide
formulation

Thicker/drift reduction agent
Thicker/drift reduction agent
Tagging agent
Thickener and stabilizer for
pesticide formulations
applied to seeds before
planting
Solvent, cosolvent

Contains not more than 1%
impurities. Not for use after edible
parts of plant begin to form. Do not
graze livestock in treated areas
within 48 hours after application
5-Chloro-2-methyl-4-isothiazolin-3-one (in combination with 2-methyl-4-isothiazolin-3-one) Not more than 0.0022% (22.5 ppm) Preservative
in the formulation; 0.00022% (or
2.25 ppm) in the final solution
applied to growing crops
Choline chloride (CAS Reg. No. 67-48-1)
As a solvent
Choline hydroxide (CAS Reg No. 123-41-1)
Without limitation
Neutralizer
Cis-isomer of 1-(3-chloroallyl)-3,5,7-triaza-1-azoniaadamantane chloride (CAS Reg. No.
Maximum of 0.14% by weight of
Preservative
51229-78-8)
formulation
Coco alkyl dimethyl amines (CAS Reg. No. 61788-93-0)
Not to exceed 0.5% in pesticide
Emulsifier
formulation
Copper naphthenate
Not more than 2.5% of formulation; Mercaptan scavenger in
application limited to before edible technical pesticide
portions of plants begin to form
Cyclohexane
Solvent, cosolvent
Cyclohexanone
Do.
Cysteine (CAS Reg. No. 52-90-4)
Maximum of 0.5% of formulation
Synergist
D&C Green No. 6
Dye
D&C Red No. 17, technical grade
Dye
D&C Red No. 33 (CAS Reg. No. 3567-66-6); meeting the specifications listed in 21 CFR
Dye
74.1333
D&C Violet No. 2, technical grade
Not more than 0.005% of pesticide Dye
formulation
Decanamide, N,N-dimethyl (CAS Reg. No. 14433-76-2)
Emulsifier, solvent, cosolvent
Diammonium phosphate (CAS Reg. No. 7783-28-0)
Buffer, surfactant
dibenzylidene sorbitol (32647-67-9)
Thinning agent
Diethanolamine
Stabilizer, inhibitor for
formulations used before
crop emerges from soil
Surfactants, related
Diethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 26545-53-9, Not to exceed 7% of pesticide
adjuvants of surfactants.
67815-95-6, 67889-94-5, 67889-95-6, 68259-34-7, 68478-47-7, 68567-68-0, 68815-34-9, formulation
68815-37-2, 68891-02-1, 68953-97-9, 84989-15-1, 85338-09-6, 90194-39-1, 90194-40-4,
90218-08-9)
Diethylene glycol
Deactivator, adjuvant for
formulations used before
crop emerges from soil
Diethylene Glycol (CAS No. 111-46-6)
Without limitation
Solvent, stabilizer and/or
antifreeze
Diethylene glycol and diethylene glycol monobutyl, monoethyl, and monomethyl ethers
Deactivator for formulations
used before crop emerges
from soil, stabilizer
Diethylene glycol mono butyl ether (CAS Reg. No. 112-34-5)
Without limitation
Pesticide inert ingredient as
a solvent, stabilizer and/or
antifreeze
Diethylene Glycol MonoEthyl Ether (CAS Reg. No. 111-90-0)
Without limitation
Solvent, stabilizer and/or
antifreeze
Surfactants, related
Dimethylaminopropylamine, isopropylamine, ethanolamine, and triethanolamine salts of
adjuvants of surfactants.
alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 3088-30-0, 12068-12-1, 26264-05-1,
26836-07-7, 27323-41-7, 55470-69-4, 58089-99-9, 61886-59-7, 61931-76-8, 67924-05-4,
68110-32-7, 68259-35-8, 68411-31-4, 68442-72-8, 68567-69-1, 68584-24-7, 68584-25-8,
68648-81-7, 68648-96-4, 68649-00-3, 68815-30-5, 68815-35-0, 68910-32-7, 68953-93-5,
68953-98-0, 70528-84-6, 72391-21-0, 84961-74-0, 85480-55-3, 85480-56-4, 85995-82-0,
90194-42-6, 90194-53-9, 90194-54-0, 90194-55-1, 90218-09-0, 90218-11-4, 90218-35-2,
96687-54-6, 99924-49-9, 121617-08-1, 157966-96-6, 193562-36-6, 319926-68-6, 87767748-0, 1093628-27-3)
3,6-Dimethyl-4-octyn-3,6-diol
In pesticide formulations, for soil
Surfactants, related
prior to planting or to plants before adjuvants of surfactants
edible parts form
Dimethyl sulfoxide
Solvent or cosolvent for
formulations used before
crop emerges from soil or
prior to formation of edible
parts of food plants
Dimethyl sulfoxide (CAS No. 67-68-5)
For pesticide formulations used
Solvent or co-solvent
before crop emerges from soil or
prior to formation of edible parts of
food plants; for pesticide
formulations used after crop
emerges but before harvest,
provided that the potential for
increased residues of the

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formulation's active ingredient(s) in
or on food commodities has been
assessed
Dipotassium hydrogen phosphate
Dipropylene glycol monomethyl ether
Douglas-fir bark, ground
Dysprosium chloride
10 ppm in formulation
1,2-ethanediamine,N,N,N″, N″-tetramethyl-, polymer with 1,1′-oxybis[2-chloroethane] (CAS For use in pesticide formulations
Reg. No. 31075-24-8)
applied to cotton or wheat only
(S,S)-Ethylenediaminedisuccinic acid (CAS Reg. No. 20846-91-7)
Ethylene glycol

Ethylene glycol (CAS Reg. No. 107-21-1)

Without limitation

Ethylene glycol monobutyl ether
2-Ethylhexanol

Europic chloride
FD&C Blue No. 1 (CAS Reg. No. 3844-45-9)
FD&C Blue No. 1, methyl-polyethylene glycol derivative (CAS Reg. No. 9079-34-9)

FD&C Blue No. 1, polyethylene glycol derivative (CAS Reg. No. 9079-33-8)

FD&C Red No. 40 (CAS Reg. No. 25956-17-6)

Ferric chloride

Fluoroapatite
Folic acid (CAS Reg. No. 59-30-3)
Gluconic acid (and sodium salt)
l-Glutamic acid (C5 H9 NO4; CAS Reg. No. 56-86-0)
[alpha]-D-glucopyranoside, 2-ethylhexyl 6-O-[alpha]-D glucopyranosyl- (CAS Reg. No.
330980-61-5)
[alpha]-D-glucopyranoside, 2-ethylhexyl (CAS Reg. No. 125590-73-0)
Glutamine (CAS Reg. No. 56-85-9)
Glycerol—propylene oxide polymer (CAS Reg. No. 25791-96-2)

10 ppm in formulation
For seed treatment use only
For seed treatment use only;
Number average molecular weight
(in amu) is greater than 1,000; Not
to exceed 5% of the formulated
pesticide product
For seed treatment use only;
Dye, coloring agent
Number average molecular weight
(in amu) is greater than 1,000; Not
to exceed 5% of the formulated
pesticide product
For seed treatment use only. Not to Dye, coloring agent
exceed 2% by weight of the
pesticide formulation
Not greater than 2% of
suspending, dispersing
agent, pesticide formulation
Solid diluent, carrier
Maximum of 0.5% of formulation
Synergist
Sequestrant
Seet treatment use only
Plant nutrient
Surfactant

Maximum of 0.5% of formulation

Hexamethylenetetramine

2-Hydroxy-4-n-octoxybenzophenone (CAS Reg. No. 1843-05-6)
Hydroxypropyl guar gum
Isobornyl acetate
Isobutyl alcohol
Isobutylene-butene copolymers
Isooctadecanol
Lanthanum chloride
Magnesium nitrate (in combination with 2-methyl-4-isothiazolin-3-one and 5-chloro-2methyl-4-isothiazolin-3-one)
Maleic acid and maleic anhydride

Sequestrant or chelating
agent
Antifreeze, deactivator for all
pesticides used before crop
emerges from soil and in
herbicides before or after
crop emerges
Pesticide inert ingredient as
a solvent, stabilizer and/or
antifreeze.
Cosolvent, defoamer, solvent
for all pesticides used before
crop emerges from soil and
in herbicides before or after
crop emerges
Tagging agent
Dye, coloring agent
Dye, coloring agent

Glyceryl triacetate
Glyceryl tris-12-hydroxystearate
Graphite
Guar hydroxypropyltrimethylammonium chloride (CAS Reg. No. 71329-50-5)

2-(2′-hydroxy-3′,5′-di-tert-amylphenyl) benzotriazole (CAS Reg. No. 25973-55-1)

Buffering agent
Stabilizer
Solid diluent, carrier
Tagging agent
Adjuvant or water conditioner

Maximum concentration of 0.6% in
insecticide formulations applied to
adzuki beans, canola, chickpeas,
cotton, faba beans, field peas,
lentils, linola, linseed, lucerne,
lupins, mung beans, navy beans,
pigeon peas, safflower, sunflower,
and vetch
Not more than 0.2 pt of pesticide
formulation

For soil application only
Not more than 2% of pesticide
formulation
10 ppm in formulation
None

Surfactant
Synergist
Component in water-soluble
film
Stabilizer
Flow control agent
Treatment aid for seeds
Thickener/drift reduction
agent
Stabilizer for carriers in solid
pesticide formulations
Ultraviolet (UV) stabilizer

Light stabilizer
Thickener
Solvent
Do.
Binder
Defoaming agent
Tagging agent.
Preservation
Stabilizer

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For pesticide formulations applied to
apples with a minimum preharvest
interval of 21 days
Manganese carbonate
D-mannose (CAS Reg. No. 3458-28-4)
Mesityl oxide

Plant nutrient
Sequestrant, binder, filler
Not for use after edible parts of plant Solvent, cosolvent
begin to form. Do not graze
livestock in treated areas within 48
hours after application
Methionine (CAS Reg. No. 59-51-8)
Maximum of 0.5% of formulation
Synergist
Methyl alcohol
Do.
Methyl ethyl ketone
Surfactant
Methyl p- hydroxybenzoate
Preservative for formulations
Methyl isobutyl ketone
Solvent, cosolvent
2-Methyl-4-isothiazolin-3-one (in combination with 5-chloro-2-methyl-4-isothiazolin-3-one) Not more than 0.0022% (22.5 ppm) Preservative
in the formulation; 0.00022% (or
2.25 ppm) in the final solution
applied to growing crops
Mono-, di-, and trimethylnapthalenesulfonic acids and napthalenesulfonic acids
Surfactants, related
formaldehyde condensates, ammonium and sodium salts (CAS Reg. Nos. 9008-63-3,
adjuvants of surfactants
9069-80-1, 9084-06-4, 36290-04-7, 91078-68-1, 141959-43-5, 68425-94-5)
Methyl oleate
Surfactant
2-Methyl-2,4-pentanediol
Solvent for formulations used
before crop emerges from
soil
Concentration in formulated end use Surfactants, related
Methyl poly(oxyethylene)C8-C18 alkylammonium chlorides where the poly(oxyethylene)
adjuvants of surfactants
content is n = 2-15 and where C8-C18 alkyl is linear and may be saturated or unsaturated products not to exceed 10% by
weight in herbicide products and 5%
(CAS Reg. Nos. 3010-24-0, 18448-65-2, 70750-47-9, 22340-01-8, 67784-77-4, 64755by weight in all other pesticide
05-1, 61791-10-4, 28724-32-5, 28880-55-9, 68187-69-9, 68607-27-2, 60687-90-3
products
N-Methylpyrrolidone (CAS Reg. No. 872-504)
Solvent, cosolvent
Mixed phytosterols (consisting of campesterol, sitosterol and stigmasterol, with minor
Surfactant
amounts of associated plant sterols) derived from edible vegetable oils
Surfactant, related adjvants
Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) phosphates where the alkyl group is even Not more than 0.5% of pesticide
formulation. Expires February 9,
of surfactants
numbered and in the C6-C12 range
2008
Surfactants, related
Mono- and dialkyl (C8-C18) methylated ammonium chloride compounds, where the alkyl
adjuvants of surfactants
group(s) (C8-C18) are derived from coconut, cottonseed, soya, tallow, or hogfat fatty acids
As a solvent
Morpholine 4-C6-12 Acyl Derivatives (CAS Reg. No. 887947-29-7)
Nicotinamide (CAS Reg. No. 98-92-0)
Maximum of 0.5% of formulation
Synergist
α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene); produced by the condensation of 1 mole
Surfactant
of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30100 moles of ethylene oxide; if a blend of products is used, the average number of moles
of ethylene oxide reacted to produce any product that is a component of the blend shall be
in the range 4-14 or 30-100
Octanamide, N,N-dimethyl (CAS Reg. No. 1118-92-9)
Emulsifier, solvent, cosolvent
α-Oleoyl-ω-(oleoyloxy) poly(oxyethylene) derived from α-hydro-ω-hydroxypoly
Component of defoamers
(oxyethylene) (molecular weight 600 amu)
Oxo-decyl acetate (CAS reg. No. 108419-33-6)
Solvent
Oxo-heptyl acetate (CAS Reg. No. 90438-79-2)
Solvent
Oxo-hexyl acetate (CAS Reg. No. 88230-35-7)
Solvent
Oxo-nonyl acetate (CAS Reg. No. 108419-34-7)
Solvent
Oxo-octyl acetate (CAS Reg. No. 108419-32-5)
Solvent
Oxo-tridecyl acetate (CAS Reg. No. 108419-35-8)
Solvent
Phenol
Solvent, cosolvent
Phenol, 2-(2H-benzotriazol-2-yl)-6-dodecyl-4-methyl-, (CAS Reg. No. 23328-53-2)
Not more than 10% by weight of
UV stabilizer.
pesticide formulations
Phenolsulfonic acid—formaldehyde—urea condensate and its sodium salt
Applied to growing plants only
Dispersant surfactant
(Phthalocyaninato (2)) copper; (C.I. pigment blue No. 15)
When used as a colorant in lowColoring agent, pigment
density plastic films
Pigment red 48
For seed treatment use only
Dye
α-Pinene
Not more than 2% of formulation by Stabilizer
weight
Poly(oxy-1,2-ethanediyl), α-isotridecyl-ω-methoxy (CAS Reg. No. 345642-79-7)
At a maximum of 10% in formulation Surfactant
Not to exceed 0.125% for seed
Surfactant.
Poly(oxy-1,2-ethanediyl), α-(3-carboxy-1-oxosulfopropyl)-ω-hydroxy-, (C10-C12)-alkyl
treatment use only
ethers, disodium salts, polyoxylene content averages 4-5 moles (CAS Reg. No. 6881556-5)
Poly(oxy-1,2-ethanediyl), α-(3-carboxy-1-oxosulfopropyl)-ω-hydroxy-, (C10-C16)-alkyl
Not to exceed 0.125% for seed
Surfactant
ethers, disodium salts, polyoxyethylene content averages 5 moles (CAS Reg. No. 68954- treatment use only
91-6)
Poly(oxyethylene) adducts of mixed phytosterols (such sterols to consist of campesterol,
Surfactant, related adjuvants
stigmasterol and sitosterol with minor amounts of associated plant sterols) derived from
edible vegetable oils; polyoxyethylene content averaging 5-26 moles
Polyoxyethylene polyoxypropylene mono(di-sec-butylphenyl) ether (CAS Reg. No. 69029- Limited to herbicide formulations
Surfactants, related
39-6)
only, and to no more than 30% by adjuvants of surfactants
weight in herbicide formulations
intended for application to turf
Poly(oxyethylene) (5) sorbitan monooleate
Surfactants, related
adjuvants of surfactants

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Polysorbate 60, conforming to 21 CFR 172.836
Potassium dihydrogen phosphate
2-Propanamine, compound with α-phosphono-ω-butoxypoly (oxy-1,2-ethanediyl) (2:1)
(CAS Reg. No. 431040-31-2)
2-Propanamine, compounds with polyethylene glycol dihydrogen phosphate C8-10- alkyl
ether (2:1) (CAS Reg. No. 431062-72-5)
Propylene glycol monomethyl ether
Pyridoxine (CAS Reg. No. 65-23-6)
Rosin, dark wood (as defined in 21 CFR 178.3870(a)(1)(v))
Rosin, gum
Rosin, tall oil
Scandium chloride
Sodium bisulfate (CAS Reg. No. 7681-38-1)
Sodium 1,4-dicyclohexyl sulfosuccinate

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Not more than 15% in the
formulated product
Not more than 15% in the
formulated product
Maximum of 0.5% of formulation

10 ppm in formulation

Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006-15-3)
Sodium dihydrogen phosphate (CAS Reg. No. 7558-80-7) conforming to 21 CFR
182.6778
Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No. 127-39-9)
Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922-80-5)
Sodium metaborate
Sodium molybdate
Sodium nitrate
Sodium nitrite
Sodium o-phenylphenate

Not more than 3% of pesticide
formulation
Not more than 0.1% of pesticide
formulation

Surfactant
Buffering agent
Surfactant
Surfactant
Solvent
Synergist
Surfactants, related
adjuvants of surfactants
Do.
Do.
Tagging agent
Acidifying/buffering agent
Surfactants, related
adjuvants of surfactants
Surfactants, related
adjuvants of surfactants
Buffering agent
Surfactants, related
adjuvants of surfactants
Surfactants, related
adjuvants of surfactants
Sequestrant
Plant nutrient
Solid diluent
Stabilizer, inhibitor.
Preservative for formulation

Sodium salt of the insoluble fraction of rosin

Surfactants, related
adjuvants of surfactants
Sodium salts of N-alkyl (C8-C18)-beta-iminodipropionic acid where the C8-C18 is linear
Concentration in formulated end-use Surfactants, related
and may be saturated and/or unsaturated (CAS Reg. Nos. 3655-00-3, 61791-56-8, 14960- products not to exceed 30% by
adjuvants of surfactants
06-6, 26256-79-1, 90170-43-7, 91696-17-2, 97862-48-1)
weight in pesticide formulations
Sodium tetraborate
Not more than 2% of pesticide
Buffering agent; corrosion
formulation
inhibitor
Not to exceed 40% by weight in
Surfactant
Sulfonic acids, C13-17-sec-alkane, sodium salts (CAS Reg. No. 85711-69-9)
non-residential use pesticide
formulation only
Not to exceed 40% by weight in
Sulfonic acids, C14-17-sec-alkane, sodium salts (CAS Reg. No. 97489-15-1)
Surfactant
non-residential pesticide formulation
only
Tallowamine, ethoxylated, mixture of dihydrogen phosphate and monohydrogen
Not to exceed 20% of pesticide
Surfactants, related
phosphate esters and the corresponding ammonium, calcium, potassium, and sodium
formulation
adjuvants of surfactants
salts of the phosphate esters, where the poly(oxyethylene) content averages 2-20 moles
(CAS Reg. No. 68308-48-5)
Tannin
Dispersing agent
Tertiary butylhydroquinone
Antioxidant
1-Tetradecanamine, N,N-dimethyl-, N-oxide (CAS Reg. No. 3332-27-2)
Component in water-soluble
film
Tetraethylene glycol (CAS Reg. No. 112-60-7)
Solvent
N,N,N′,N″-Tetrakis-(2-hydroxypropyl) ethylenediamine (CAS Reg. No. 102-60-3)
Concentration in formulated end-use Stabilizer for formulations
products not to exceed 20% by
weight in pesticide formulations
2,4,7,9-Tetramethyl-5-decyne 4,7-diol
In pesticide formulations, for
Surfactants, related
application to soil prior to planting or adjuvants of surfactants
to plants before edible parts form
Tetrapotassium pyrophosphate (CAS Reg. No. 7320-345)
Not to exceed 10% of formulation
Sequestrant, anticaking
agent, conditioning agent
Titanium dioxide (CAS Reg. No. 13463-67-7)
Pigment/coloring agent in
plastic bags used to wrap
growing banana
(preharvest), colorant on
seeds for planting
Toluenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and
Solvent, cosolvent
zinc salts
Triethanolamine
Stabilizer, inhibitor for
formulations used before
crop emerges from soil
Triethanolamine (CAS Reg. No. 102-71-6)
Stabilizer, inhibitor
Triethylene glycol
Deactivator
Triethyl phosphate
Stabilizer for formulations
used before crop emerges
from soil
Trimethylolpropane (CAS Reg. No. 77-99-6)
Not to exceed 15% by weight of the Component in water-soluble
film
film
Surfactant.

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α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene), the poly(oxyethylene)
content averages 4-150 moles)
α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene); mixture of
monohydrogen and dihydrogen phosphate esters and the corresponding ammonium,
calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content
averages 4-150 moles)
α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene) sulfate, and the
corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the
poly(oxyethylene) content averages 4-150 moles
Tryptophan (CAS Reg. No. 73-22-3)
Valeric acid, normal

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Not more than 15% of the
formulation
Not more than 15% of the
formulation

Not more than 15% of the pesticide
formulation
Maximum of 0.5% of formulation
Not more than 2% in pesticide
formulations

Xylene
Xylenesulfonic acid its ammonium calcium, magnesium, potassium, sodium, and zinc salts
Yucca extract from Yucca schidigera
Ytterbium chloride
Yttrium chloride
Zinc orthophosphate
Zinc stearate, conforming to 21 CFR 182.5994 and 582.5994

10 ppm in formulation
10 ppm in formulation

Do.

Do.

Synergist
Stenching agent or odorant
Solvent, cosolvent
Surfactants, related
adjuvants of surfactants
Wetting agent
Tagging agent
Tagging agent
Plant nutrient and safener
Flow control agent

[69 FR 23124, Apr. 28, 2004]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.920, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.930 Inert ingredients applied to animals; exemptions from the requirement of a tolerance.
The following materials are exempted from the requirement of a tolerance when used in accordance with good
agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to animals:
Inert ingredients
Acetic acid (CAS Reg. No. 64-19-7)

Limits
Not more than
0.5% of pesticide
formulation

Acetic anhydride

Solvent, cosolvent,
stabilizer
Solvent or cosolvent
Emulsifiers

Acetone (Cas Reg. No. 67-64-1)
Alkanoic and alkenoic acids, mono- and diesters of α-hydro-ω-hydroxypoly(oxyethylene) with molecular weight (in
amu) range of 200 to 6,000
Alkyl (C8-C24) benzenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts

Alkyl (C12-C16) dimethyl ammonio acetate (CAS Reg. Nos. 683-10-3, 2601-33-4 and 693-33-4

Uses
Catalyst

Surfactants,
emulsifier, related
adjuvants of
surfactants
Surfactant

20% by weight in
pesticide
formulation
Not to exceed
Surfactants, related
30% of formulation adjuvants of
surfactants.

α-alkyl(C6- C15)-ω-hydroxypoly(oxyethylene)sulfate, and its ammonium, calcium, magnesium, potassium, sodium,
and zinc salts, poly(oxyethylene) content averages 2-4 moles (CAS Reg. Nos.: 3088-31-1, 3694-74-4, 9004-82-4,
9004-84-6, 9021-91-4, 9086-52-6, 13150-00-0, 15826-16-1, 25446-78-0, 26183-44-8, 27140-00-7, 27731-61-9,
27731-61-9, 27731-62-0, 32612-48-9, 34431-25-9, 35015-74-8, 50602-06-7, 52286-18-7, 52286-19-8, 54116-08-4,
55901-67-2, 61702-79-2, 61894-66-4, 62755-21-9, 63428-85-3, 63428-86-4, 63428-87-5, 65086-57-9, 65086-79-5,
65104-74-7, 65122-38-5, 67674-66-2, 67762-19-0, 67762-21-4, 67845-82-3, 67845-83-4, 67923-90-4, 68037-05-8,
68037-06-9, 68171-41-5, 68424-50-0, 68511-39-7, 68585-34-2, 68610-66-2, 68611-29-0, 68611-55-2, 68649-53-6,
68890-88-0, 68891-29-2, 68891-30-5, 68891-38-3, 69011-37-6, 73665-22-2, 75422-21-8, 78330-16-2, 78330-17-3,
78330-25-3, 78330-26-4, 78330-27-5, 78330-28-6, 78330-29-7, 78330-30-0, 96130-61-9, 106597-03-9, 11039250-2, 119432-41-6, 125301-88-4, 125301-89-5, 125301-92-0, 125736-54-1, 157707-85-2, 160104-51-8, 16090127-9, 160901-28-0, 160901-29-1, 160901-30-4, 161025-28-1, 161074-79-9, 162063-19-6, 219756-63-5)
Not to exceed
α-alkyl (C12-C15)-ω-hydroxypoly (oxypropylene)poly (oxyethylene)copolymers (where the poly(oxypropylene)
20% of pesticide
content is 3-60 moles and the poly(oxyethylene) content is 5-80 moles), the resulting ethoxylated propoxylated
formulations
(C12-C15) alcohols having a minimum molecular weight (in amu) of 1,500, CAS Reg. No. 68551-13-3
α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly (oxyethylene) polymers where the alkyl chain contains a
minimum of six carbons (CAS Reg. No.: 9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3;
9038-43-1; 9040-05-5; 9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 26183-52-8; 26468-86-0;
26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 34398-01-1; 34398-05-5; 37251-67-5; 37311-00-5; 37311-01-6;
37311-02-7; 37311-04-9; 39587-22-9; 50861-66-0; 52232-09-4; 52292-17-8; 52609-19-5; 57679-21-7; 59112-62-8;
60828-78-6; 61702-78-1; 61725-89-1; 61791-13-7; 61791-20-6; 61791-28-4; 61804-34-0; 61827-42-7; 61827-84-7;
62648-50-4; 63303-01-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4; 64425-86-1; 65104-72-5;
65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 67763-08-0; 68002-96-0; 68002-97-1; 68131-39-5; 68131-40-8;
68154-96-1; 68154-97-2; 68154-98-3; 68155-01-1; 68213-23-0; 68213-24-1; 68238-81-3; 68238-82-4; 68409-58-5;
68409-59-6; 68439-30-5; 68439-45-2; 68439-46-3; 68439-48-5; 68439-49-6; 68439-50-9; 68439-51-0; 68439-53-2;
68439-54-3; 68458-88-8; 68526-94-3; 68526-95-4; 68551-12-2; 68551-13-3; 68551-14-4; 68603-20-3; 68603-25-8;
68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 68954-94-9; 68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9;
69013-19-0; 69227-20-9; 69227-21-0; 69227-22-1; 69364-63-2; 70750-27-5; 70879-83-3; 70955-07-6; 71011-10-4;
71060-57-6; 71243-46-4; 72066-65-0; 72108-90-8; 72484-69-6; 72854-13-8; 72905-87-4; 73018-31-2; 73049-34-0;
74432-13-6; 74499-34-6; 78330-19-5; 78330-20-8; 78330-21-9; 78330-23-1; 79771-03-2; 84133-50-6; 85422-93-1;
97043-91-9; 97953-22-5; 102782-43-4; 103331-86-8; 103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0;
106232-83-1; 111905-54-5; 116810-31-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5; 121617-09-2;
126646-02-4; 126950-62-7; 127036-24-2; 139626-71-4; 152231-44-2; 154518-36-2; 157627-86-6; 157627-88-8;

Surfactant

Surfactants, related
adjuvants of
surfactants.

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157707-41-0; 157707-43-2; 159653-49-3; 160875-66-1; 160901-20-2; 160901-09-7; 160901-19-9; 161025-21-4;
161025-22-5; 166736-08-9; 169107-21-5; 172588-43-1; 176022-76-7; 196823-11-7; 287935-46-0; 288260-45-7;
303176-75-2; 954108-36-2)
α-alkyl (minimum C6 linear, branched, saturated and/or unsaturated)-ω-hydroxypolyoxyethylene polymer with or
without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium,
calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum
oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles, (CAS Reg. Nos.: 9004-80-2, 904601-9, 26982-05-8, 31800-89-2, 37280-82-3, 37281-86-0, 39341-09-8, 39341-65-6, 39464-66-9, 39464-69-2,
42612-52-2, 50643-20-4, 50668-50-3, 51325-10-1, 51884-64-1, 52019-36-0, 52019-38-2, 52019-38-2, 57486-09-6,
58206-38-5, 58318-92-6, 58857-49-1, 59112-71-9, 60267-55-2, 61837-79-4, 62362-49-6, 62482-61-5, 63747-86-4,
63887-54-7, 63887-55-8, 66020-37-9, 66272-25-1, 66281-20-7, 67711-84-6, 67786-06-5, 67989-06-4, 68070-99-5,
68071-17-0, 68071-35-2, 68071-37-4, 68130-44-9, 68130-45-0, 68130-46-1, 68130-47-2, 68186-29-8, 68186-34-5,
68186-36-7, 68186-37-8, 68238-84-6, 68311-02-4, 68311-04-6, 68332-75-2, 68389-72-0, 68400-75-9, 68413-78-5,
68425-73-0, 68425-75-2, 68439-39-4, 68458-48-0, 68511-15-9, 68511-36-4, 68511-37-5, 68551-05-3, 68585-15-9,
68585-16-0, 68585-17-1, 68585-36-4, 68585-39-7, 68603-24-7, 68607-14-7, 68610-64-0, 68610-65-1, 68649-29-6,
68649-30-9, 68650-84-0, 68815-11-2, 68855-46-9, 68856-03-1, 68890-90-4, 68890-91-5, 68891-12-3, 68891-13-4,
68891-26-9, 68908-64-5, 68909-65-9, 68909-67-1, 68909-69-3, 68921-24-4, 68921-60-8, 68954-87-0, 68954-88-1,
68954-92-7, 68987-35-9, 69029-43-2, 69980-69-4, 70247-99-3, 70248-14-5, 70844-96-1, 70903-63-8, 71965-23-6,
71965-24-7, 72480-27-4, 72623-67-7, 72623-68-8, 72828-56-9, 72828-57-0, 73018-34-5, 73038-25-2, 73050-08-5,
73050-09-6, 73361-29-2, 73378-71-9, 73378-72-0, 73559-42-9, 73559-43-0, 73559-44-1, 73559-45-2, 74499-76-6,
76930-25-1, 78041-18-6, 78330-22-0, 78330-24-2, 82465-25-6, 84843-37-8, 91254-26-1, 93925-54-3, 95014-34-9,
96416-89-6, 99924-51-3, 103170-31-6, 103170-32-7, 106233-09-4, 106233-10-7, 108818-88-8, 110392-49-9,
111798-26-6, 111905-50-1, 116671-23-9, 117584-36-8, 119415-05-3, 120913-45-3, 121158-61-0, 121158-63-2,
123339-53-7, 125139-13-1, 125301-86-2, 125301-87-3, 126646-03-5, 129208-04-4, 129870-77-5, 129870-80-0,
130354-37-9, 136504-88-6, 143372-50-3, 143372-51-4, 144336-75-4, 146815-57-8, 151688-56-1, 154518-39-5,
154518-40-8, 155240-11-2, 159704-69-5, 160498-49-7, 160611-24-5, 171543-66-1, 172027-16-6, 172274-69-0,
176707-42-9, 181963-82-6, 188741-55-1, 191940-53-1, 210493-60-0, 210993-53-6, 246159-55-7, 251298-11-0,
261627-68-3, 290348-69-5, 290348-70-8, 317833-96-8, 340681-28-9, 422563-19-7, 422563-26-6, 522613-09-8,
717140-06-2, 717140-09-5, 717827-29-7, 762245-80-7, 762245-81-8, 866538-89-8, 866538-90-1, 873662-29-4,
913068-96-9, 936100-29-7, 936100-30-0, 1072943-56-6, 1087209-87-7, 1174313-54-2, 1187742-89-7, 118774335-6, 1205632-03-6, 1233235-49-8, 1451002-50-8, 1456802-88-2, 1456802-89-3, 1456803-12-5)
N-alkyl (C8-C18) primary amines and their acetate salts where the alkyl group is linear and may be saturated
and/or unsaturated (CAS Reg. Nos. 61790-57-6, 61790-58-7, 61790-59-8, 61790-60-1, 61788-46-3, 61790-33-8,
68155-38-4)

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Not to exceed
Surfactants, related
30% of formulation adjuvants of
surfactants.

Concentration in Surfactants, related
formulated endadjuvants of
use products not surfactants
to exceed 10% by
weight in herbicide
products, 4% by
weight in
insecticide
products, and 4%
by weight in
fungicide products
Surfactant
Alkyl (C8-C18) sulfate and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts
N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl) C8-C18 saturated and unsaturated alkylamines; the poly
Not to exceed
Surfactants, related
(oxy-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 10213-78-2, 25307-17-9, 26635-92-7, 26635-93-8,
25% in herbicide adjuvants of
288259-52-9, 58253-49-9, 61790-82-7, 61791-14-8, 61791-24-0, 61791-26-2, 61791-31-9, 61791-44-4, 68155formulations and surfactants
33-9, 68155-39-5, 68155-40-8,70955-14-5, 73246-96-5, 1266162-49-5)
10% in insecticide
and fungicide
formulations
Not to exceed
Surfactants, related
N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18 saturated and unsaturated
alkylamines; the poly(oxy-1,2-ethanediyl/oxy(methyl-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 68213- 25% in herbicide adjuvants of
formulations and surfactants
26-3, 68153-97-9, 75601-76-2)
10% in insecticide
and fungicide
formulations
Ascorbyl palmitate
Preservative
Attapulgite-type clay
Solid diluent, carrier
Barium sulfate (CAS Reg. No. 7727-43-7)
Carrier, density
control agent
Benzoic acid
Preservative for
formulations
2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52-51-7)
0.04% or less by In-can preservative
weight of the total
pesticide
formulation
Butane
Propellant
n-Butanol (CAS Reg. No. 71-36-3)
Solvent for blended
emulsifiers
n-Butyl benzoate (CAS RN 136-60-7)
Solvent
Butylated hydroxyanisole
Antioxidant
Butylated hydroxytoluene
Do.
Calcium carbonate
Solid diluent, carrier
Calcium chloride
Stabilizer
Calcium silicate, hydrated calcium silicate
Anticaking agent,
solid diluent, carrier
Solvent.
C9 rich aromatic hydrocarbons (CAS Reg. No. 64742-95-6)
C10-11 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5)
Solvent.
C11-12 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5)
Solvent.
Calcium stearate (CAS Reg. No. 1592-23-0)
Stabilizer, component
of plastic animal tag
Calcium sulfate
Solid diluent, carrier
Carbon black (CAS Reg. No. 1333-86-4)
Colorant/pigment in
animal tag

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Carbon Dioxide (CAS Reg. No. 124-38-9)
Carrageenan, conforming to 21 CFR 172.620

None
Propellant
Minimum
Thickener
molecular weight
(in amu): 100,000
Cyclohexanone
Solvent, cosolvent
D&C Green No. 6
Dye, coloring agent
D&C Red No. 17
Do.
D&C Violet No. 2
Do.
Not more than
Flocculating agent in
Dialkyl (C8-C18) dimethylammonium chloride
0.2% in silica
the manufacture of
hydrated silica
silica hydrated silica
for use as a solid
diluent, carrier
Diatomite (diatomaceous earth)
Solid diluent, carrier
Diethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 26545-53-9, 67815-95-6, 67889-94-5, Not to exceed 7% Surfactants, related
adjuvants of
67889-95-6, 68259-34-7, 68478-47-7, 68567-68-0, 68815-34-9, 68815-37-2, 68891-02-1, 68953-97-9, 84989-15-1, of pesticide
formulation
surfactants.
85338-09-6, 90194-39-1, 90194-40-4, 90218-08-9)
Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
Surfactant
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-75-4)
Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number
Surfactant
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-83-4)
Diethylaminoethanol, ethoxylated, reaction products with acid trimers, minimum number average molecular weight
Surfactant
(in amu), 1,200 (CAS Reg. No. 1173188-81-2)
Diethylaminoethanol, ethoxylated, reaction product with fatty acid dimers, minimum number average molecular
Surfactant
weight (in amu), 1,200 (CAS Reg. No. 1173188-72-1)
Diethylphthalate
Solvent, cosolvent
1,1-Difluoroethane (CAS Reg. No. 75-37-6)
For aerosol
Aerosol propellant
pesticide
formulations used
for insect control in
food- and feedhandling
establishments
and animals
Dimethyl ether (CAS Reg. No. 115-10-6)
Propellant
Dimethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
Surfactant
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-42-5)
Dimethylaminoethanol, ethoxylated, propoxylated reaction products with fatty acid trimers, minimum number
Surfactant
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-67-4)
Surfactant
Dimethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173188-38-9)
Dimethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular
Surfactant
weight (in amu), 1,200 (CAS Reg. No. 1173188-49-2)
Surfactants, related
Dimethylaminopropylamine, isopropylamine, ethanolamine, and triethanolamine salts of alkyl (C8-C24)
adjuvants of
benzenesulfonic acid (CAS Reg. Nos. 3088-30-0, 12068-12-1, 26264-05-1, 26836-07-7, 27323-41-7, 55470-69-4,
surfactants.
58089-99-9, 61886-59-7, 61931-76-8, 67924-05-4, 68110-32-7, 68259-35-8, 68411-31-4, 68442-72-8, 68567-69-1,
68584-24-7, 68584-25-8, 68648-81-7, 68648-96-4, 68649-00-3, 68815-30-5, 68815-35-0, 68910-32-7
68953-93-5, 68953-98-0, 70528-84-6, 72391-21-0, 84961-74-0, 85480-55-3, 85480-56-4, 85995-82-0, 90194-42-6,
90194-53-9, 90194-54-0, 90194-55-1, 90218-09-0, 90218-11-4, 90218-35-2, 96687-54-6, 99924-49-9, 12161708-1, 157966-96-6, 193562-36-6, 319926-68-6, 877677-48-0, 1093628-27-3).
3,6-Dimethyl-4-octyne-3,6-diol
Not more than
Surfactants, related
2.5% of pesticide adjuvants of
formulation
surfactants
Dimethylpolysiloxane (CAS Reg. No. 9016-00-6)
Defoaming agent
Di-n-butyl carbonate (CAS Reg. No. 542-52-9)
Solvent
Dipropylene glycol monomethyl ether
Surfactants, related
adjuvants of
surfactants
Epoxidized soybean oil (CAS Reg. No. 8013-07-8)
Stabilizer, plasticizer,
component animal tag
Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No. 107-36-8)
Chelator, sequestrant,
or conditioning agent.
Ethanesulfonic acid, 2-hydroxy-, ammonium salts (CAS Reg. No. 57267-78-4)
Do.
Ethanesulfonic acid, 2-hydroxy-, calcium salts (CAS Reg. No. 10550-47-7)
Do.
Ethanesulfonic acid, 2-hydroxy-, magnesium salts (CAS Reg. No. 17345-56-1)
Do.
Ethanesulfonic acid, 2-hydroxy-, potassium salts (CAS Reg. No. 1561-99-5)
Do.
Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS Reg. No. 1562-00-1)
Do.
Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS Reg. No. 129756-32-7)
Do.
Ethyl alcohol
Solvent, cosolvent
Ethyl maltol (CAS Reg. No.4940-11-8)
Not more than 0.2 Odor masking agent
% of the pesticide
formulation
Ethylene oxide adducts of 2,4,7,9-tetramethyl-5-decynediol, the ethylene oxide content averages 3.5, 10 or 30
Surfactants, related
moles (CAS Reg. No. 9014-85-1)
adjuvants of
surfactants
2-Ethyl-1-hexanol (CAS Reg. No. 104-76-7)
Not more than
Solvent, adjuvant of
10% of pesticide surfactants
FD&C Blue No. 1
Dye, coloring agent
FD&C Yellow No. 6 Aluminum Lake (CAS Reg. No. 15790-07-5)
Not more than 2%
by weight of

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pesticide
formulation
D-glucopyranose, oligomeric, C10-16-alkyl glycosides (CAS Reg. No. 110615-47-9)
Glycerol monooleate

Glyceryl monostearate
Glyceryl tris-12-hydroxystearate
Graphite
n-Hexyl alcohol (CAS Reg. No. 111-27-3)
Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-06-4)
Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-67-4)
Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid dimers, minimum number average
molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-00-8)
Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid trimers, minimum number average
molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-09-7)
Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-22-4)
Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number
average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-28-0)
Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid dimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173189-20-2)
Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular
weight (in amu), 1,200 (CAS Reg. No. 1173189-25-7)
2-(2′-Hydroxy-5′-methylphenyl)benzotriazole (CAS Reg. No. 2440-22-4)
Not more than
0.5% by weight of
pesticide
formulation
Iron oxide (CAS Reg. No. 1309-37-1)

Isobutane (CAS Reg. No. 75-28-5)
Isopropyl myristate, CAS Reg. No. 110-27-0
Kaolinite-type clay
Kerosene, U.S.P. reagent
Lactic acid
Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283-86-9)
Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No. 186817-80-1)
Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651-69-7)
Lignin (CAS Reg. No. 9005-53-2)

Lignin, alkali (CAS Reg. No. 8068-05-1)
Lignin, alkali, oxidized, sodium salt (CAS Reg. No. 68201-23-0)
Lignin alkali reaction products with disodium sulfite and formaldehyde (CAS Reg. No. 105859-97-0)
Lignin alkali reaction products with formaldehyde and sodium bisulfite (CAS Reg. No. 68512-35-6)
Lignosulfonic acid (CAS Reg. No. 8062-15-5)
Lignosulfonic acid, ammonium calcium salt (CAS Reg. No. 12710-04-2)
Lignosulfonic acid, ammonium magnesium salt (CAS Reg. No. 123175-37-1)
Lignosulfonic acid, ammonium salt (CAS Reg. No. 8061-53-8)
Lignosulfonic acid, ammonium sodium salt (CAS Reg. No. 166798-73-8)
Lignosulfonic acid, calcium magnesium salt (CAS Reg. No. 55598-86-2)
Lignosulfonic acid, calcium salt (CAS Reg. No. 8061-52-7)
Lignosulfonic acid, calcium sodium salt (CAS Reg. No. 37325-33-0)
Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg. No. 68611-14-3)
Lignosulfonic acid, magnesium salt (CAS Reg. No. 8061-54-9)
Lignosulfonic acid, potassium salt (CAS Reg. No. 37314-65-1)
Lignosulfonic acid, sodium salt (CAS Reg. No. 8061-51-6)
Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No. 68855-41-4)
Lignosulfonic acid, sodium salt, polymer with formaldehyde and phenol (CAS Reg. No. 37207-89-9)
Lignosulfonic acid, sodium salt, sulfomethylated (CAS Reg. No. 68512-34-5)
Lignosulfonic acid, zinc salt (CAS Reg. No. 57866-49-6)
d-Limonene (CAS Reg. No. 5989-27-5)
Magnesium carbonate
Magnesium silicate, hydrated magnesium silicate
Methane sulfonic acid (CAS Reg. No. 75-75-2)

Methyl alcohol
Methyl n-amyl ketone (CAS Reg. No. 110-43-0)
Methyl esters of higher fatty acids conforming to 21 CFR 573.640
Methyl-p-hydroxybenzoate (Methyl paraben)

None

Not to exceed
3.0% by weight in
pesticide
formulation

Meets
specifications of

Pigment in animal tag
and similar slowrelease devices
Surfactant
Surfactants, related
adjuvants of
surfactants
Emulsifier
Flow control agent
Solid diluent, carrier
Solvent, cosolvent
Surfactant
Surfactant
Surfactant
Surfactant
Surfactant
Surfactant
Surfactant
Surfactant
Ultraviolet light
absorber/stabilizer in
animal tag and similar
slow-release devices
Colorant in pesticide
formulations for
animal tags
Propellant
Solvent
Solid diluent, carrier
Solvent, cosolvent
Solvent
Solvent
Solvent
Solvent
Surfactant, related
adjuvants of
surfactants
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Do.
Solvent, fragrance
Solid diluent, carrier
Do.
Acidifying agent

Solvent, cosolvent
Solvent, cosolvent
Antidusting agent
Preservative

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Food Chemicals
Codex; not to
exceed 0.1% in
formulations
Methyl isobutyl ketone
2-methyl-2,4-pentanediol (CAS Reg. No.-107-41-5)
2-methyl-1,3-propanediol (CAS Reg. No. 2163-42-0)
Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or 178.3620(a), (b)
Montmorillonite-type clay
Nonyl, decyl, and undecyl glycoside mixture with a mixture of nonyl, decyl, and undecyl oligosaccharides and
related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65%
solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9,
40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8)
α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate
esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the
phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 or
30 moles (CAS Reg. Nos. 51811-79-1, 59139-23-0, 67922-57-0, 68412-53-3, 68553-97-9, 68954-84-7, 9982114-4, 152143-22-1, 51609-41-7, 37340-60-6, 106151-63-7, 68584-47-4, 52503-15-8, 68458-49-1)
α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) sulfate, ammonium, calcium, magnesium, potassium, sodium, and
zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS
Reg. Nos. 9014-90-8, 9051-57-4, 9081-17-8, 68649-55-8, 68891-33-8
α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) produced by the condensation of 1 mole of nonylphenol (nonyl
group is a propylene trimer isomer) with an average of 4-15 or 30-90 moles of ethylene oxide; if a blend of products
is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the
blend shall be in the range of 4-15 or 30-90 moles
Octadecyl 3,5-di-tert-butyl-4-hydroxyhydro cinnamate (CAS Reg. No. 2082-79-3)

Without limitation

Solvent, cosolvent
Growing crops and
food animals
Solvent, surfactant
Solvent, diluent
Solid diluent, carrier
Surfactant

Not to exceed 7% Surfactants, related
of pesticide
adjuvants of
formulation
surfactants

Not to exceed 7% Surfactants, related
of pesticide
adjuvants of
formulation
surfactants
Surfactants,
emulsifier, related
adjuvants of
surfactants.
Not more than
Thermal
0.5% by weight of stabilizer/antioxidant
pesticide
in animal tag and
formulation
similar slow-release
devices
1-Octanal (CAS Reg. No. 124-13-0)
Not more than
Odor masking agent
0.2% of the
pesticide
formulation
Thermal
Octyl and decyl glucosides mixture with a mixture of octyl and decyl oligosaccharides and related reaction products
stabilizer/antioxidant
(primarily n-decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain
in animal tag and
alcohols (C8(45%), C10) with anhydrous glucose
similar slow-release
devices
Octyl epoxytallate (CAS Reg. No. 61788-72-5)
Plasticizer,
component animal tag
Oleic acid, conforming to 21 CFR 172.862 (CAS Reg. No. 112-80-1)
Defoaming agent
α-Oleoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600
Emulsifier
α-Oleoyl-ω-(oleyloxy)poly(oxyethylene) derived from α-hydro-ω-hydroxypoly(oxyethylene), molecular weight (in
Emulsifier, defoaming
amu) 600
agent
Petroleum hydrocarbons, light, odorless, conforming to 21 CFR 172.884 or 178.3650
Solvent, diluent
Petroleum hydrocarbons, synthetic isoparaffinic, conforming to 21 CFR 172.882 or 178.3530
Do.
Phenol
Solvent, cosolvent
α-Pinene
Not more than 2% Stabilizer
of formulation by
weight
Polyethylene (CAS Reg. No. 9002-88-4) conforming to 21 CFR 172.615
Component of plastic
slow release tag
Polyethylene glycol [α-hydro-ω-hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms
Surfactants, related
to 21 CFR 178.3750
adjuvants of
surfactants
Potassium benzoate (Cas No. 582-25-2)
None
Preservative
Potassium hydroxide
Meeting Food
Neutralizer
Chemicals, Codex
specifications
Propane
Propellant
1,2,3-Propanetriol, homopolymer diisooctadecanoate (CAS Reg. No. 63705-03-3)
Emulsifier
n-Propanol
Solvent, for blended
emulsifiers
2-Propenoic acid, 2-methyl-, polymer with ethyl 2-propenoate and methyl 2-methyl-2-propenoate, ammonium salt
Encapsulating
(CAS Registration No. 55989-05-4), minimum number average molecular weight (in amu), 18,900.
agent,dispensers,
resins, fibers and
beads
Propylene glycol
Solvent, cosolvent
Propylene glycol monomethyl ether
Deactivator,
emmolient
Propyl gallate
Antioxidant
Propyl p-hydroxybenzoate (Propyl paraben)
Meets
Preservative
specifications of
Food Chemicals
Codex; not to
exceed 0.1% in
formulations
Pyrophylite
Solid diluent, carrier
Silica, hydrated silica

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Anticaking agent,
solid diluent, carrier
Silica aerogel (finely powdered microcellular silica foam having a minimum silica content of 89.5%)
Component of
antifoaming agent
Soapstone
Solid diluent
Sodium alkyl naphthalenesulfonates (CAS Reg. Nos. 68909-83-1, 68909-84-2, 68909-82-0, 27213-90-7, 26264Limited to no more Surfactants, related
58-4, 27178-87-6, 111163-74-7, 908356-16-1, 25417-20-3, 25638-17-9, 145578-88-7, 1322-93-6, 1323-19-9,
than 30% by
adjuvants of
7403-47-6, 68442-09-1, 127646-44-0, 908356-18-3)
weight in pesticide surfactants
end-use products
Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006-15-3)
Surfactants, related
adjuvants of
surfactants
Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No. 127-39-9)
Surfactants, related
adjuvants of
surfactants
Sodium dioctylsulfosuccinate
Surfactants, related
adjuvants of
surfactants
Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922-80-5)
Surfactants, related
adjuvants of
surfactants
Sodium hydroxide
Neutralizer
Surfactants, related
Sodium monoalkyl and dialkyl (C6-C16) phenoxy benzenedisulfonates and related acids (CAS Reg. Nos. 147732- Not to exceed
59-0, 147732-60-3, 169662-22-0, 70191-75-2, 36445-71-3, 39354-74-0, 70146-13-3, 119345-03-8, 149119-20-0, 20% in pesticide adjuvants of
surfactants
formulations
149119-19-7, 119345-04-9, 28519-02-0, 25167-32-2, 30260-73-2, 65143-89-7, 70191-76-3)
Sodium N-oleoyl-N-methyl taurine (CAS Reg. No. 137-20-2)
Surfactants, related
adjuvants of
surfactants
Sodium and potassium salts of N-alkyl (C8-C18)-beta-iminodipropionic acid where the C8-C18 is linear and may be Concentration in Surfactants, related
formulated endadjuvants of
saturated and/or unsaturated (CAS Reg. Nos. 110676-19-2, 3655-00-3, 61791-56-8, 14960-06-6, 26256-79-1,
use products not surfactants
90170-43-7, 91696-17-2, 97862-48-1)
to exceed 30% by
weight in pesticide
formulations
Sodium starch glycolate (CAS Reg. No. 9063-38-1)
Granular and
Disintegrant
tableted products
only; not to exceed
8% of the
formulated product
Sodium sulfate
Solid diluent, carrier
Buffering agent;
Sorbitan fatty acid esters (fatty acids limited to C12, C14, C16, and C18 containing minor amounts of associated fatty
corrosion inhibition
acids) and poly(oxyethylene) derivatives of sorbitan fatty acid esters; the poly(oxyethylene) content averages 16-20
moles
Sorbitol
Antidusting agent.
Stearic acid (CAS Reg. No. 57-11-4)
Lubricant, component
animal tag
α-Stearoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600
Emulsifier
α-Stearoyl-ω-hydroxypoly(oxyethylene); the poly(oxyethylene) content averages 8, 9, or 40 moles; if a blend of
Surfactants; related
products is used, the average number of moles of ethylene oxide reacted to produce any product that is a
adjuvants of
component of the blend shall be 8, 9, or 40
surfactants
Sulfite liquors and cooking liquors, spent, oxidized (CAS Reg. No. 68514-09-0)
Surfactant, related
adjuvants of
surfactants
Sulfur (CAS Reg. No. 7704-34-9)
Stabilizer
Talc
Do.
Tall oil; fatty acids not less than 58%, rosin acids not more than 44%, unsaponifiables not more than 8%
Surfactants, related
adjuvants of
surfactants
Tartrazine
Dye, coloring agent
N,N,N′,N″,-tetrakis-(2-hydroxypropyl) ethylenediamine (CAS Reg. No. 102-60-3)
Concentration in Stabilizer for
formulated endformulation.
use products not
to exceed 20% by
weight in pesticide
formulations
Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No. 29118-24-9)
Propellant.
2,4,7,9-Tetramethyl-5-decyne-4.7-diol
Not more than
Surfactants, related
2.5% of pesticide adjuvants of
formulation
surfactants
Titanium dioxide (CAS Reg. No. 13463-67-7)
Pigment/colorant in
pesticide formulations
for animal tag
Toluenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts
Do.
Triacetin (glyceryl triacetate)
Solvent, cosolvent
Trisodium phosphate
Precipitant, buffer,
filler
Xylene
Solvent, cosolvent
Xylenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts
Surfactants, related
adjuvants of
surfactants
Zinc oxide
Solid diluent, carrier

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Zinc stearate, conforming to 21 CFR 182.5994 and 582.5994

Water repellant,
dessicant, and
coating agent.
Water repellant,
desiccant, and
coating agent;
stabilizer, component
of plastic animal tag
Water repellant,
dessicant, and
coating agent

Zinc stearate (CAS Reg. No. 557-05-1)

Zinc sulfate (basic and monohydrate)

[69 FR 23130, Apr. 28, 2004]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.930, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.940 Tolerance exemptions for active and inert ingredients for use in antimicrobial formulations (Foodcontact surface sanitizing solutions).
Residues of the following chemical substances are exempted from the requirement of a tolerance when used in
accordance with good manufacturing practice as ingredients in an antimicrobial pesticide formulation, provided that the
substance is applied on a semi-permanent or permanent food-contact surface (other than being applied on food
packaging) with adequate draining before contact with food.
(a) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation may be
applied to: Food-contact surfaces in public eating places, dairy-processing equipment, and food-processing equipment
and utensils.
Pesticide Chemical
Acetic acid

64-19-7

Allyl cylcohexylpropionate

2705-87-5

α-alkyl-ω-hydroxypoly
(oxypropylene) and/or poly
(oxyethylene) polymers where the
alkyl chain contains a minimum of
six carbons

9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3; 9038-43-1; 9040-05-5;
9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 26183-52-8; 26468-86-0;
26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 34398-01-1; 34398-05-5; 37251-67-5;
37311-00-5; 37311-01-6; 37311-02-7; 37311-04-9; 39587-22-9; 50861-66-0; 52232-09-4;
52292-17-8; 52609-19-5; 57679-21-7; 59112-62-8; 60828-78-6; 61702-78-1; 61725-89-1;
61791-13-7; 61791-20-6; 61791-28-4; 61804-34-0; 61827-42-7; 61827-84-7; 62648-50-4;
63303-01-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4; 64425-86-1;
65104-72-5; 65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 67763-08-0; 68002-96-0;
68002-97-1; 68131-39-5; 68131-40-8; 68154-96-1; 68154-97-2; 68154-98-3; 68155-01-1;
68213-23-0; 68213-24-1; 68238-81-3; 68238-82-4; 68409-58-5; 68409-59-6; 68439-30-5;
68439-45-2; 68439-46-3; 68439-48-5; 68439-49-6; 68439-50-9; 68439-51-0; 68439-53-2;
68439-54-3; 68458-88-8; 68526-94-3; 68526-95-4; 68551-12-2; 68551-13-3; 68551-14-4;
68603-20-3; 68603-25-8; 68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 68954-94-9;
68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9; 69013-19-0; 69227-20-9; 69227-21-0;
69227-22-1; 69364-63-2; 70750-27-5; 70879-83-3; 70955-07-6; 71011-10-4; 71060-57-6;
71243-46-4; 72066-65-0; 72108-90-8; 72484-69-6; 72854-13-8; 72905-87-4; 73018-31-2;
73049-34-0; 74432-13-6; 74499-34-6; 78330-19-5; 78330-20-8; 78330-21-9; 78330-23-1;
79771-03-2; 84133-50-6; 85422-93-1; 97043-91-9; 97953-22-5; 102782-43-4; 103331-86-8;
103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0; 106232-83-1; 111905-54-5;
116810-31-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5; 121617-09-2;
126646-02-4; 126950-62-7; 127036-24-2; 139626-71-4; 152231-44-2; 154518-36-2;
157627-86-6; 157627-88-8; 157707-41-0; 157707-43-2; 159653-49-3; 160875-66-1;
160901-20-2; 160901-09-7; 160901-19-9; 161025-21-4; 161025-22-5; 166736-08-9;
169107-21-5; 172588-43-1; 176022-76-7; 196823-11-7; 287935-46-0; 288260-45-7;
303176-75-2; 954108-36-2
10043-01-3
When ready for use, the enduse concentration is not to
exceed 50 ppm
26062-79-3
When ready for use, the enduse concentration is not to
exceed 0.6%
12125-02-9
When ready for use, the enduse concentration is not to
exceed 48 ppm
113894-85-2
None

Aluminum sulfate

2-propen-1-aminium,
N,N-dimethyl-N-propenyl-,
chloride, homopolymer
Ammonium chloride

CAS Reg. No.

Limits
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm

Amylopectin, acid-hydrolyzed,
1-oxtenylbutanedioate
Amylopectin, hydrogen
1-octadecenylbutanedioate
Butryic acid

125109-81-1

None

107-92-6

When ready for use, the enduse concentration is not to
exceed 100 ppm

Butyl alcohol

71-36-3

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n-Butyl benzoate

136-60-7

Citral

5392-40-5

Citronellol

106-22-9

Citronellyl acetate

150-84-5

Copper sulfate pentahydrate

7758-99-8

β-Damascone, (Z)-

23726-92-3

Decanal

112-31-2

Decanoic acid

334-48-5

1-Decanol

112-30-1

(E)-4-Decenal

65405-70-1

D-Glucopyranose, oligomeric,
decyl octyl glycosides
2,6-Dimethyl-5-heptanal

68515-73-1
106-72-9

Di-n-butyl carbonate

542-52-9

2-Dodecanol, (2E)-

20407-84-5

Ethanol
Ethyl 2-methylbutyrate

64-17-5
452-79-1

Ethylenediaminetetraacetic acid
(EDTA), tetrasodium salt
FD&C Green No. 3
FD&C Red No. 40

64-02-8
CAS Reg. No. 2353-45-9
25956-17-6

FD&C Yellow No. 5

1934-21-0

(E)-Geraniol

106-24-1

(E)-Geraniol acetate

105-87-3

Heptanal

111-71-7

Heptanoic acid

111-14-8

Heptyl alcohol

111-70-6

Hexanal

66-25-1

Hexanoic acid

142-62-1

n-Hexanol

111-27-3

(Z)-3-Hexenol

928-96-1

Page 387 of 441

When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 15,000 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 80 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
None
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 15,000 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
None
When ready for use, the enduse concentration is not to
exceed 100 ppm
None
None
When ready for use, the enduse concentration is not to
exceed 20 ppm.
When ready for use, the enduse concentration is not to
exceed 1000 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm

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(Z)-3-Hexenol acetate

3681-71-8

Hexyl acetate

142-92-7

Hydrogen peroxide

7722-84-1

Hypochlorous acid, sodium salt

7681-52-9

Iodine

7553-56-2

Lauric acid

143-07-7

Lauric aldehyde

112-54-9

Lauryl alcohol

112-53-8

d-Limonene

5989-27-5

Lipase, triacylglycerol

9001-62-1

Magnesium oxide
Methane sulfonic acid

1309-48-4
75-75-2

Methylene blue

61-73-4

Methyl-α-ionone

127-42-4

3-Methyl-2-butenyl acetate

1191-16-8

2-Methylundecanal

110-41-8

2-Methyl-1,3-propanediol
Myristaldehyde

2163-42-0
124-25-4

Myristic acid

544-63-8

Neryl acetate

141-12-8

Nitric acid

7697-37-2

Nonanal

124-19-6

Nonanoic acid

112-05-0

Nonyl alcohol

143-08-8

α-(p-Nonylphenyl)-ω-hydroxypoly None
(oxyethylene) average poly
(oxyethylene) content 11 moles)
Octadecanoic acid, calcium salt 1592-23-0
1315321-93-7

Page 388 of 441

When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 91 ppm
When ready for use, the enduse concentration of all
hypochlorous acid chemicals
in the solution is not to
exceed 200 ppm determined
as total available chlorine
When ready for use, the total
end-use concentration of all
iodide-producing chemicals
in the solution is not to
exceed 25 ppm of titratable
iodine
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 500 ppm
None
When ready for use, the end
use concentration is not to
exceed 5,000 ppm
When ready for use, the enduse concentration is not to
exceed 0.4 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
None
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 1,000 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
None

None

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9-Octadecenoic acid (9Z)-,
sulfonated, oxidized
9-Octadecenoic acid (9Z)-,
1315321-94-8
sulfonated, oxidized, potassium
salts
9-Octadecenoic acid (9Z)-,
1315321-95-9
sulfonated, oxidized, sodium salts
Octanal

124-13-0

1-Octanesulfonic acid, sodium
salt

5324-84-5

Octanoic acid

124-07-2

Octanoic acid

124-07-2

1-Octanol

111-87-5

Oxirane, methyl-, polymer with
oxirane, minimum molecular
weight (in amu), 1900
Palmitic acid

9003-11-6

57-10-3

Peroxyacetic acid

79-21-0

Peroxyoctanoic acid

33734-57-5

Phosphonic acid,
(1-hydroxyethylidene)bis-

2809-21-4

Phosphoric acid, trisodium salt

7601-54-9

Potassium bromide

7758-02-3

Potassium iodide

7681-11-0

1,3-Propanediol
Propionic acid

504-63-2
79-09-4

Propylene glycol
Quaternary ammonium
compounds, alkyl (C12-C18)
benzyldimethyl, chlorides

57-55-6
8001-54-5

Quaternary ammonium
compounds: n-alkyl (C12-18)
dimethyl benzyl ammonium
chloride

68424-85-1

Quaternary Ammonium
Compounds: n-alkyl (C 12-14)
dimethyl ethylbenzyl ammonium
chloride, average molecular
weight (in amu), 377 to 384

85409-23-0

Quaternary ammonium
compounds n-alkyl (C12-C18)
dimethyl ethylbenzyl ammonium
chloride average molecular
weight (in amu) 384

None

Quaternary ammonium
compounds, Di-n-Alkyl (C8-10)

None

Page 389 of 441

When ready for use, the enduse concentration is not to
exceed 250 ppm.
When ready for use, the enduse concentration is not to
exceed 250 ppm.
When ready for use, the enduse concentration is not to
exceed 250 ppm.
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 46 ppm
When ready for use, the enduse concentration is not to
exceed 52 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
None

When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 58 ppm
When ready for use, the enduse concentration is not to
exceed 52 ppm
When ready for use, the enduse concentration is not to
exceed 14 ppm
When ready for use, the enduse concentration is not to
exceed 5916 ppm
When ready for use, the enduse concentration is not to
exceed 46 ppm total
available halogen
When ready for use, the total
end-use concentration of all
iodide-producing chemicals
in the solution is not to
exceed 25 ppm of titratable
iodine
None
When ready for use, the enduse concentration is not to
exceed 100 ppm
None
When ready for use, the enduse concentration of all
quaternary chemicals in the
solution is not to exceed 200
ppm of active quaternary
compound
When ready for use, the enduse concentration of all
quaternary chemicals in
solution is not to exceed 400
ppm of active quaternary
compound
When ready for use, the enduse concentration of all
quaternary chemicals in
solution is not to exceed 400
ppm of active quaternary
compound.
When ready for use, the enduse concentration of all
quaternary chemicals in the
solution is not to exceed 200
ppm of active quaternary
compound
When ready for use, the enduse concentration of these

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dimethyl ammonium chloride,
average molecular weight (in
amu) 332 to 361

Quaternary ammonium
148788-55-0/148812-654-1
compounds, didecyl dimethyl
ammonium carbonate/didecyl
dimethyl ammonium bicarbonate

Silver ions resulting from the use 14701-21-4
of electrolytically-generated silver
ions stabilized in citric acid as
silver dihydrogen citrate (does not
include metallic silver)
Sodium bisulfate
7681-38-1

When ready for use, the enduse concentration is not to
exceed 2,000 ppm.
None

Sorbitan, mono-9-octadecenoate, 9005-65-6
poly(oxy-1,2-ethanediyl) derivs.,
(Z)Stearic acid.
57-11-4

Sulfuric acid

When ready for use, the enduse concentration is not to
exceed 100 ppm
Food-contact surfaces in
public eating places, dairyprocessing equipment, and
food-processing equipment
and utensils in antimicrobial
formulations. Not to exceed
600 ppm.
When ready for use, the enduse concentration is not to
exceed 350 ppm
None

7664-93-9

Sulfuric acid monododecyl ester, 151-21-3
sodium salt (sodium lauryl sulfate)
Trans-1,3,3,3-tetrafluoroprop-1- 29118-24-9
ene
1,3,5-Triazine-2,4,6(1H,3H,5H)
2893-78-9
-trione, 1,3-dichloro-, sodium salt

2-Tridecanal

7774-82-5

3,5,5-Trimethylhexanal

5435-64-3

Undecanal

112-44-7

Undecyl alcohol

112-42-5

Valeraldehyde

110-62-3

Valeric acid

109-52-4

Xylenesulfonic acid, sodium salt

1300-72-7

specific in quaternary
ammonium compounds is not
to exceed 240 ppm of active
quaternary ammonium
compound; the end-use
concentration of all
quaternary chemicals in the
solution is not to exceed 400
ppm of active quaternary
compound
When ready for use, the enduse concentration of these
specific ammonium
compounds is not to exceed
400 ppm of active quaternary
ammonium compound
When ready for use, the enduse concentration of silver
ions is not to exceed 50 ppm
of active silver

When ready for use, the enduse concentration of all di- or
trichloroisocyanuric acid
chemicals in the solution is
not to exceed 100 ppm
determined as total available
chlorine
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 100 ppm
When ready for use, the enduse concentration is not to
exceed 500 ppm

(b) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation may be
applied to: Dairy processing equipment, and food-processing equipment and utensils.
Pesticide Chemical
>Acetic acid
Acetic acid, chloro-, sodium salt, reaction products with
4,5-dihydro-2-undecyl-1H-imidazole-1-ethanol and
sodium hydroxide
Benzenesulfonic acid, dodecylButanedioic acid, octenyl-

CAS Reg.
No.
Limits
64-19-7
When ready for use, the end-use concentration is not to exceed 1200 ppm
68608-66-2 When ready for use, the end-use concentration is not to exceed 42 ppm chloroacetic
acid
27176-87-0
28805-58-5

When ready for use, the end-use concentration is not to exceed 5.5 ppm
When ready for use, the end-use concentration is not to exceed 156 ppm

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Butoxy monoether of mixed (ethylene-propylene)
polyalkylene glycol, minimum average molecular weight
(in amu), 2400
Calcium chloride
n-Carboxylic acids (C6-C12), consisting of a mixture of not
less than 56% octanoic acid and not less than 40%
decanoic acid
Decanoic acid
Ethanesulfonic acid, 2-[cyclohexyl (1-oxohexadecyl)
amino]-, sodium salt
Ethylenediaminetetraacetic acid (EDTA), disodium salt
FD&C Yellow No. 5 (Tartrazine) (conforming to 21 CFR
74.705)
D-Gluconic acid, monosodium salt
Hydriodic acid

Page 391 of 441

None

None

10043-52-4
None

When ready for use, the end-use concentration is not to exceed 17 ppm
When ready for use, the end-use concentration is not to exceed 39 ppm

334-48-5
132-43-4

When ready for use, the end-use concentration is not to exceed 90 ppm
When ready for use, the end-use concentration is not to exceed 237 ppm

139-33-3
1934-21-0

When ready for use, the end-use concentration is not to exceed 1400 ppm
None

527-07-1
10034-85-2

When ready for use, the end-use concentration is not to exceed 760 ppm
When ready for use, the total end-use concentration of all iodide-producing
chemicals is not to exceed 25 ppm of titratable iodine
Hydrogen peroxide
7722-84-1
When ready for use, the end-use concentration is not to exceed 465 ppm
Hypochlorous acid
7790-92-3
When ready for use, the end-use concentration of all hypochlorous acid chemicals in
the solution is not to exceed 200 ppm determined as total available chlorine
Iodine
7553-56-2
When ready for use, the total end-use concentration of all iodide-producing
chemicals in the solution is not to exceed 25 ppm of titratable iodine
Lactic acid
50-21-5
When ready for use, the end-use concentration is not to exceed 138 ppm
Nonanoic acid
112-05-0
When ready for use, the end-use concentration is not to exceed 90 ppm
1-Octanamine, N,N-dimethyl7378-99-6
When ready for use, the end-use concentration is not to exceed 113 ppm
1,2-Octanedisulfonic acid
113669-58-2 When ready for use, the end-use concentration is not to exceed 102 ppm
1-Octanesulfonic acid
3944-72-7
When ready for use, the end-use concentration is not to exceed 172 ppm
1-Octanesulfonic acid, sodium salt
5324-84-5
When ready for use, the end-use concentration is not to exceed 297 ppm
1-Octanesulfonic acid, 2-sulfino113652-56-5 When ready for use, the end-use concentration is not to exceed 102 ppm
Octanoic acid
124-07-2
When ready for use, the end-use concentration is not to exceed 176 ppm
Oxychloro species (including chlorine dioxide) generated None
When ready for use, the end-use concentration is not to exceed 200 ppm of chlorine
by acidification of an aqueous solution of sodium chlorite
dioxide as determined by the method titled, Iodometric Method for the Determination
of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide)
Peroxyacetic acid
79-21-0
When ready for use, the end-use concentration is not to exceed 315 ppm
Peroxyoctanoic acid
33734-57-5 When ready for use, the end-use concentration is not to exceed 122 ppm
Phosphonic acid, (1-hydroxyethylidene)bis2809-21-4
When ready for use, the end-use concentration is not to exceed 34 ppm
Phosphoric acid
7664-38-2
None
Phosphoric acid, monosodium salt
7558-80-7
When ready for use, the end-use concentration is not to exceed 350 ppm
Potassium iodide
7681-11-0
When ready for use, the total end-use concentration of all iodide-producing
chemicals in the solution is not to exceed 25 ppm of titratable iodine
Propanoic acid
79-09-4
When ready for use, the end-use concentration is not to exceed 297 ppm
2,6-Pyridinedicarboxylic acid
499-83-2
When ready for use, the end-use concentration is not to exceed 1.2 ppm
Sulfuric acid monododecyl ester, sodium salt (sodium
151-21-3
When ready for use, the end-use concentration is not to exceed 350 ppm
lauryl sulfate)

(c) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation may be
applied to: Food-processing equipment and utensils.
CAS Reg.
No.
Limits
Acetic acid
64-19-7
When ready for use, the end-use concentration is not to
exceed 1,200 ppm
Acetic acid, chloro-, sodium salt, reaction products with 4,5-dihydro-2-undecyl-1H68608-66-2 When ready for use, the end-use concentration is not to
imidazole-1-ethanol and sodium hydroxide
exceed 42 ppm chloroacetic acid
Ammonium chloride
12125-02-9 When ready for use, the end-use concentration is not to
exceed 48 ppm
Benzenesulfonic acid, dodecyl27176-87-0 When ready for use, the end-use concentration is not to
exceed 400 ppm
Benzenesulfonic acid, dodecyl-, sodium salt
25155-30-0 When ready for use, the end-use concentration is not to
exceed 430 ppm
[1,1′-Biphenyl]-2-ol
90-43-7
When ready for use, the end-use concentration is not to
exceed 400 ppm
Boric acid, sodium salt
7775-19-1 None
Butanedioic acid, octenyl28805-58-5 When ready for use, the end-use concentration is not to
exceed 156 ppm
Butanedioic acid, sulfo-, 1,4-dioctyl ester, sodium salt
1639-66-3 None
None
Butoxy monoether of mixed (ethylene-propylene) polyalkylene glycol, cloudpoint of 90 None
- 100oC in 0.5 aqueous solution, average molecular weight (in amu), 3300
Butoxy monoether of mixed (ethylene-propylene) polyalkylene glycol, minimum
None
None
average molecular weight (in amu), 2400
Calcium chloride
10043-52-4 When ready for use, the end-use concentration is not to
exceed 17 ppm
When ready for use, the end-use concentration is not to
n-Carboxylic acids (C6-C12), consisting of a mixture of not less than 56% octanoic acid None
exceed 39 ppm
and not less than 40% decanoic acid
3-Cyclohexene-1-methanol,α,α,4-trimethyl98-55-5
None
1-Decanaminium, N-decyl-N, N-dimethyl-, chloride
7173-51-5 When ready for use, the end-use concentration is not to
exceed 200 ppm of active quaternary compound
Decanoic acid
3347-48-5
Pesticide Chemical

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Ethanesulfonic acid, 2-[cyclohexyl (1-oxohexadecyl) amino]-, sodium salt

132-43-4

Ethanol
Ethanol, 2 butoxyEthanol, 2-(2-ethoxyethoxy)Ethylenediaminetetraacetic acid (EDTA), disodium salt

64-17-5
111-76-2
111-90-0
139-33-3

Ethylenediaminetetraacetic acid (EDTA), tetrasodium salt
Fatty acids, coco, potassium salts
Fatty acids, tall-oil, sulfonated, sodium salts

64-02-8
61789-30-8
68309-27-3

FD&C Yellow No. 5 (Tartrazine) (conforming to 21 CFR 74.705)
D-Gluconic acid, monosodium salt

1934-21-0
527-07-1

Hydriodic acid

10034-85-2

Hydrogen peroxide

7722-84-1

Hypochlorous acid

7790-92-3

Hypochlorous acid, calcium salt

7778-54-3

Hypochlorous acid, lithium salt

13840-33-0

Hypochlorous acid, potassium salt

7778-66-7

Hypochlorous acid, sodium salt

7681-52-9

Iodine

7553-56-2

Lactic acid
Magnesium oxide
Methylene blue

50-21-5
1309-48-4
61-73-4

Neodecanoic acid

26896-20-8

Nonanoic acid

112-05-0

α-(p-Nonylphenyl)-ω-hydroxypoly (oxyethylene) maximum average molecular weight
(in amu), 748
α-(p-Nonylphenol)-ω-hydroxypoly (oxyethylene) average poly(oxyethylene) content 11
moles
α-(p-Nonylphenyl)-ω-hydroxypoly (oxyethylene) produced by the condensation of 1
mole p-nonylphenol with 9 to 12 moles ethylene oxide
α-(p-Nonylphenyl)-ω-hydroxypoly (oxyethylene), 9 to 13 moles ethylene oxide
Octadecanoic acid, calcium salt
9-Octadecenoic acid (9Z)-, sulfonated

None

When ready for use, the end-use concentration is not to
exceed 234 ppm
When ready for use, the end-use concentration is not to
exceed 237 ppm
None
None
None
When ready for use, the end-use concentration is not to
exceed 1400 ppm
None
None
When ready for use, the end-use concentration is not to
exceed 66 ppm
None
When ready for use, the end-use concentration is not to
exceed 760 ppm
When ready for use, the total end-use concentration of
all iodide-producing chemicals in the solution is not to
exceed 25 ppm of titratable iodine
When ready for use, the end-use concentration is not to
exceed 1100 ppm
When ready for use, the end-use concentration of all
hypochlorous acid chemicals in the solution is not to
exceed 200 ppm determined as total available chlorine
When ready for use, the end-use concentration of all
hypochlorous acid chemicals in the solution is not to
exceed 200 ppm determined as total available chlorine
When ready for use, the end-use concentration of all
hypochlorous acid chemicals in the solution is not to
exceed 200 ppm determined as total available chlorine
and 30 ppm lithium
When ready for use, the end-use concentration of all
hypochlorous acid chemicals in the solution is not to
exceed 200 ppm determined as total available chlorine
When ready for use, the end-use concentration of all
hypochlorous acid chemicals in the solution is not to
exceed 200 ppm determined as total available chlorine
When ready for use, the total end-use concentration of
all iodide-producing chemicals in the solution is not to
exceed 25 ppm of titratable iodine
None
None
When ready for use, the end-use concentration is not to
exceed 0.4 ppm
When ready for use, the end-use concentration is not to
exceed 174 ppm
When ready for use, the end-use concentration is not to
exceed 90 ppm
None

None

None

None

None

9-Octadecenoic acid (9Z)-sulfonated, sodium salts
1-Octanamine, N,N-dimethyl1,2-Octanedisulfonic acid
1-Octanesulfonic acid
1-Octanesulfonic acid, sodium salt
1-Octanesulfonic acid, 2-sulfinoOctanoic acid

None
None
1592-23-0 None
68988-76-1 When ready for use, the end-use concentration is not to
exceed 312 ppm
68443-05-0 When ready for use, the end-use concentration is not to
exceed 200 ppm
7378-99-6 When ready for use, the end-use concentration is not to
exceed 113 ppm
113669-58-2 When ready for use, the end-use concentration is not to
exceed 102 ppm
3944-72-7 When ready for use, the end-use concentration is not to
exceed 172 ppm
5324-84-5 When ready for use, the end-use concentration is not to
exceed 312 ppm
113652-56-5 When ready for use, the end-use concentration is not to
exceed 102 ppm
124-07-2
When ready for use, the end-use concentration is not to
exceed 234 ppm
9003-11-6 None
106392-12-5 None

Oxirane, methyl-, polymer with oxirane, minimum molecular weight (in amu), 1900
Oxirane, methyl-, polymer with oxirane, block, average molecular weight (in amu),
1900
Oxirane, methyl-, polymer with oxirane, block, minimum average molecular weight (in None
amu), 2000
Oxirane, methyl-, polymer with oxirane, block, 27 to 31 moles of polyoxypropylene,
None
average molecular weight (in amu) 2000

None
None

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Oxychloro species (predominantly chlorite, chlorate and chlorine dioxide in an
equilibrium mixture) generated either (i) by directly metering a concentrated chlorine
dioxide solution prepared just prior to use, into potable water, or (ii) by acidification of
an aqueous alkaline solution of oxychloro species (predominately chlorite and
chlorate) followed by dilution with potable water
Oxychloro species (including chlorine dioxide) generated by acidification of an
aqueous solution of sodium chlorite

2,4-Pentanediol, 2-methylPeroxyacetic acid
Peroxyoctanoic acid
Phenol, 4-chloro-2-(phenylmethyl)Phenol, 4-(1,1-dimethylpropyl)Phosphonic acid, (1-hydroxyethylidene)bisPhosphoric acid
Phosphoric acid, monosodium salt
Phosphoric acid, trisodium salt
Poly(oxy-1,2-ethanediyl), α-[(1,1,3,3-tetramethylbutyl) phenyl]-ω-hydroxy-, produced
with one mole of the phenol and 4 to 14 moles ethylene oxide
Potassium bromide

Page 393 of 441

None

When ready for use, the end-use concentration is not to
exceed 200 ppm of chlorine dioxide as determined by
the method titled, “Iodometric Method for the
Determination of Available Chlorine Dioxide (50-250
ppm available chlorine dioxide)”
None
When ready for use, the end-use concentration is not to
exceed 200 ppm of chlorine dioxide as determined by
the method titled, “Iodometric Method for the
Determination of Available Chlorine Dioxide (50-250
ppm available chlorine dioxide)”
107-41-5
None
79-21-0
When ready for use, the end-use concentration is not to
exceed 315 ppm
33734-57-5 When ready for use, the end-use concentration is not to
exceed 122 ppm
120-32-1
When ready for use, the end-use concentration is not to
exceed 320 ppm
80-46-6
When ready for use, the end-use concentration is not to
exceed 80 ppm
2809-21-4 When ready for use, the end-use concentration is not to
exceed 34 ppm
7664-38-2 None
7558-80-7 When ready for use, the end-use concentration is not to
exceed 350 ppm
7601-54-9 When ready for use, the end-use concentration is not to
exceed 5916 ppm
None
None
7758-02-3

Potassium iodide

7681-11-0

Propanoic acid

79-09-4

2,6-Pyridinedicarboxylic acid

499-83-2

Quaternary ammonium compounds, alkyl (C12-C18) benzyldimethyl, chlorides

8001-54-5

Quaternary ammonium compounds, n-alkyl (C12-C14) dimethyl ethylbenzyl ammonium None
chloride, average molecular weight (in amu), 377 to 384

Quaternary ammonium compounds, n-alkyl (C12-C18) dimethyl ethylbenzyl ammonium None
chloride average molecular weight (in amu) 384

Quaternary ammonium compounds, di-n-Alkyl (C8-C10) dimethyl ammonium chloride,
average molecular weight (in amu), 332 to 361

None

Sodium-α-alkyl(C12-C15)-ω-hydroxypoly (oxyethylene) sulfate with the poly
(oxyethylene) content averaging one mole
Sodium bromide

None
7647-15-6

Sodium iodide

7681-82-5

Sulfuric acid monododecyl ester, sodium salt (sodium lauryl sulfate)
1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-

151-21-3
2782-57-2

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, potassium salt

2244-21-5

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, sodium salt

2893-78-9

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5-trichloro-

87-90-1

1,3,5-Triazine, N,N′,N″-trichloro-2,4,6-triamino-

7673-09-8

When ready for use, the end-use concentration of all
bromide-producing chemicals in the solution is not to
exceed 200 ppm total available halogen
When ready for use, the total end-use concentration of
all iodide-producing chemicals in the solution is not to
exceed 25 ppm of titratable iodine
When ready for use, the end-use concentration is not to
exceed 297 ppm
When ready for use, the end-use concentration is not to
exceed 1.2 ppm
When ready for use, the end-use concentration of this
specific quaternary compound is not to exceed 200 ppm
within the end-use total concentration that is not to
exceed 400 ppm active quaternary compound
When ready for use, the end-use concentration of this
specific quaternary compound is not to exceed 200 ppm
within the end-use total concentration that is not to
exceed 400 ppm active quaternary compound
When ready for use, the end-use concentration of this
specific quaternary compound is not to exceed 200 ppm
within the end-use total concentration that is not to
exceed 400 ppm active quaternary compound
When ready for use, the end-use concentration of this
specific quaternary compound is not to exceed 240 ppm
within the end-use total concentration that is not to
exceed 400 ppm active quaternary compound
None
When ready for use, the end-use concentration of all
bromide-producing chemicals in the solution is not to
exceed 200 ppm total available halogen
When ready for use, the total end-use concentration of
all iodide-producing chemicals in the solution is not to
exceed 25 ppm of titratable iodine
None
When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is
not to exceed 100 ppm determined as total available
chlorine
When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is
not to exceed 100 ppm determined as total available
chlorine
When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is
not to exceed 100 ppm determined as total available
chlorine
When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is
not to exceed 100 ppm determined as total available
chlorine
When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is

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not to exceed 200 ppm determined as total available
chlorine

[69 FR 23136, Apr. 28, 2004, as amended at 71 FR 30811, May 31, 2006; 71 FR 45423, Aug. 9, 2006; 71 FR 46125, Aug. 11, 2006;
72 FR 51186, Sept. 6, 2007; 73 FR 37858, July 2, 2008; 73 FR 49107, Aug. 20, 2008; 73 FR 53725, Sept. 17, 2008; 74 FR 27454,
June 10, 2009; 74 FR 38944, Aug. 5, 2009; 74 FR 40509, Aug. 12, 2009; 75 FR 40735, July 14, 2010; 76 FR 55267, Sept. 7, 2011;
77 FR 45498, Aug. 1, 2012; 77 FR 50617, Aug. 22, 2012; 77 FR 53150, Aug. 31, 2012; 77 FR 68692, Nov. 16, 2012; 78 FR 35147,
June 12, 2013; 78 FR 46264, July 31, 2013; 78 FR 48621, Aug. 9, 2013; 78 FR 59269, Sept. 26, 2013; 78 FR 65565, Nov. 1, 2013;
78 FR 67042, Nov. 8, 2013; 78 FR 78731, Dec. 27, 2013; 79 FR 6096, Feb. 3, 2014; 79 FR 26152, May 7, 2014; 79 FR 32666, June
6, 2014; 79 FR 33473, June 11, 2014; 79 FR 52993, Sept. 5, 2014; 79 FR 66312, Nov. 7, 2014; 80 FR 11593, Mar. 4, 2015; 80 FR
28842, May 20, 2015; 80 FR 32033, 32038, June 5, 2015; 80 FR 34070, June 15, 2015; 80 FR 48752, Aug. 14, 2015; 80 FR 50211,
Aug. 19, 2015; 80 FR 61122, Oct. 9, 2015; 80 FR 62466, Oct. 16, 2015]

Back to Top
§180.950 Tolerance exemptions for minimal risk active and inert ingredients.
Unless specifically excluded, residues resulting from the use of the following substances as either an inert or an active
ingredient in a pesticide chemical formulation, including antimicrobial pesticide chemicals, are exempted from the
requirement of a tolerance under FFDCA section 408, if such use is in accordance with good agricultural or manufacturing
practices.
(a) Commonly consumed food commodities. Commonly consumed food commodities means foods that are commonly
consumed for their nutrient properties. The term commonly consumed food commodities shall only apply to food
commodities (whether a raw agricultural commodity or a processed commodity) in the form the commodity is sold or
distributed to the public for consumption.
(1) Included within the term commonly consumed food commodities are:
(i) Sugars such as sucrose, lactose, dextrose and fructose, and invert sugar and syrup.
(ii) Spices such as cinnamon, cloves, and red pepper.
(iii) Herbs such as basil, anise, or fenugreek.
(2) Excluded from the term commonly consumed food commodities are:
(i) Any food commodity that is adulterated under 21 U.S.C. 342.
(ii) Both the raw and processed forms of peanuts, tree nuts, milk, soybeans, eggs, fish, crustacea, and wheat.
(iii) Alcoholic beverages.
(iv) Dietary supplements.
(b) Animal feed items. Animal feed items means meat meal and all items derived from field crops that are fed to
livestock excluding both the raw and processed forms of peanuts, tree nuts, milk, soybeans, eggs, fish, crustacea, and
wheat. Meat meal is an animal feed composed of dried animal fat and protein that has been sterilized. Other than meat
meal, the term animal feed item does not extend to any item designed to be fed to animals that contains, to any extent,
components of animals. Included within the term animal feed items are:
(1) The hulls and shells of the commodities specified in paragraph (a)(2)(ii) of this section, and cocoa bean.
(2) Bird feed such as canary seed.
(3) Any feed component of a medicated feed meeting the definition of an animal feed item.
(c) Edible fats and oils. Edible fats and oils means all edible (food or feed) fats and oils, derived from either plants or
animals, whether or not commonly consumed, including products derived from hydrogenating (food or feed) oils, or
liquefying (food or feed) fats.
(1) Included within the term edible fats and oils are oils (such as soybean oil) that are derived from the commodities
specified in paragraph (a)(2)(ii) of this section when such oils are highly refined via a solvent extraction procedure.
(2) Excluded from the term edible fats and oils are plant oils used in the pesticide chemical formulation specifically to
impart their characteristic fragrance and/or flavoring.
(d) [Reserved]
(e) Specific chemical substances. Residues resulting from the use of the following substances as either an inert or an
active ingredient in a pesticide chemical formulation, including antimicrobial pesticide chemicals, are exempted from the

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requirement of a tolerance under FFDCA section 408, if such use is in accordance with good agricultural or manufacturing
practices.
Chemical
Acetic acid, sodium salt
Alpha-cyclodextrin
Amylopectin, acid-hydrolyzed, 1-octenylbutanedioate
Amylopectin, hydrogen 1-octadecenylbutanedioate
Animal glue
Ascorbic acid (vitamin C)
Beeswax
Benzoic acid, sodium salt
Beta-cyclodextrin
Carbonic acid, monopotassium salt
Carbonic acid, monosodium salt (sodium bicarbonate)
Carnauba wax
Carob gum (locust bean gum)
Castor oil
Castor oil, hydrogenated
Cellulose
Cellulose acetate
Cellulose, carboxy methyl ether, sodium salt
Cellulose, 2-hydroxyethyl ether
Cellulose, 2-hydroxypropyl ether
Cellulose, 2-hydroxypropyl methyl ether
Cellulose, methyl ether
Cellulose, mixture with cellulose carboxymethyl ether, sodium salt
Cellulose, pulp
Cellulose, regenerated
Citric acid
Citric acid, 2-(acetyloxy)-, tributyl ester
Citric acid, calcium salt
Citric acid, calcium salt (2:3)
Citric acid, dipotassium salt
Citric acid, disodium salt
Citric acid, monohydrate
Citric acid, monopotassium salt
Citric acid, monosodium salt
Citric acid, potassium salt
Citric acid, triethyl ester
Citric acid, tripotassium salt
Citric acid, tripotassium salt, monohydrate
Citric acid, sodium salt
Citric acid, trisodium salt
Citric acid, trisodium salt, dihydrate
Citric acid, trisodium salt, pentahydrate
Coffee grounds
Dextrins
1,3-Dioxolan-2-one, 4-methyl-(propylene carbonate)
Fumaric acid
Gamma-cyclodextrin
Gellan gum
D-Glucitol (sorbitol)
Glycerol (glycerin) (1,2,3-propanetriol)
Guar gum
Humic acid
Humic acid, potassium salt
Humic acid, sodium salt
Lactic acid, n-butyl ester
Lactic acid, n-butyl ester, (S)
Lactic acid, ethyl ester
Lactic acid, ethyl ester,(S)
Lanolin
Lecithins
Lecithins, soya
Licorice Extract
Maltodextrin
Paper
Potassium chloride
2-Propanol (isopropyl alcohol)
Red cabbage color, expressed from edible red cabbage heads via a pressing process using only acidified water

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CAS No.
127-09-3
10016-20-3
11389485-2
12510981-1
None
50-81-7
8012-89-3
532-32-1
7585-39-9
298-14-6
144-55-8
8015-86-9
9000-40-2
8001-79-4
8001-78-3
9004-34-6
9004-35-7
9004-32-4
9004-62-0
9004-64-2
9004-65-3
9004-67-5
51395-75-6
65996-61-4
68442-85-3
77-92-9
77-90-7
7693-13-2
813-94-5
3609-96-9
144-33-2
5949-29-1
866-83-1
18996-35-5
7778-49-6
77-93-0
866-84-2
6100-05-6
994-36-5
68-04-2
6132-04-3
6858-44-2
68916-18-7
9004-53-9
108-32-7
110-17-8
17465-86-0
71010-52-1
50-70-4
56-81-5
9000-30-0
1413-93-6
68514-28-3
68131-04-4
138-22-7
34451-19-9
97-64-3
687-47-8
8006-54-0
8002-43-5
8030-76-0
68916-91-6
9050-36-6
None
7447-40-7
67-63-0
None

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Silica, amorphous, fumed (crystalline free)
Silica, amorphous, precipitated and gel
Silica gel
Silica gel, precipitated, crystalline-free
Silica, hydrate
Silica, vitreous
Soap (The water soluble sodium or potassium salts of fatty acids produced by either the saponification of fats and oils, or the neutralization of
fatty acid)
Sorbic acid, potassium salt
Soapbark (Quillaja saponin)
Sodium alginate
Sodium chloride
Syrups, hydrolyzed starch, hydrogenated
Ultramarine blue (C.I. Pigment Blue 29)
Urea
Vanillin
Xanthan gum

11294552-5
7699-41-4
63231-67-4
11292600-8
10279-57-9
60676-86-0
None
24634-61-5
1393-03-9
9005-38-3
7647-14-5
68425-17-2
57455-37-5
57-13-6
121-33-5
11138-66-2

[67 FR 36537, May 24, 2002]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.950, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.960 Polymers; exemptions from the requirement of a tolerance.
Residues resulting from the use of the following substances, that meet the definition of a polymer and the criteria
specified for defining a low-risk polymer in 40 CFR 723.250, as an inert ingredient in a pesticide chemical formulation,
including antimicrobial pesticide chemical formulations, are exempted from the requirement of a tolerance under FFDCA
section 408, if such use is in accordance with good agricultural or manufacturing practices.
Polymer
Acetic acid ethenyl ester, polymer with ethane, ethenyltriethoxysilane 913187-38-9
and sodium ethenesulfonate (1:1); minimum number average
molecular weight (in amu), 16,200
Acetic acid ethenyl ester, polymer with ethenol and (α)-2137091-12-4
propenyl-(ω)-hydroxypoly (oxy-1,2-ethanediyl) minimum number
average molecular weight (in amu), 15,000
Acetic acid ethenyl ester, polymer with 1-ethenyl-2-pyrrolidinone
25086-89-9
Acetic acid ethenyl ester, polymer with oxirane, minimum number
25820-49-9
average molecular weight (in amu), 17,000
Acetic acid ethenyl ester, polymer with sodium 2-methyl-2-[(1-oxo-2- 924892-37-5
propen-1-yl)amino]-1-propanesulfonate (1:1), hydrolyzed, minimum
number average molecular weight (in amu), 61,000
Acrylic acid-benzyl methacrylate-1-propanesulfonic acid, 2-methyl-2- 1152297-42-1
[(1-oxo-2-propenyl)amino]-, monosodium salt, minimum number
average molecular weight (in amu), 1500
Acrylic acid, polymerized, and its ethyl and methyl esters
None
Acrylic acid-sodium acrylate-sodium-2-methylpropanesulfonate
97953-25-8
copolymer, minimum average molecular weight (in amu), 4,500
Acrylic acid-stearyl methacrylate copolymer, minimum number
27756-15-6
average molecular weight (in amu), 2,500
Acrylic acid, styrene, α-methyl styrene copolymer, ammonium salt, 89678-90-0
minimum number average molecular weight (in amu), 1,250
Acrylic acid terpolymer, partial sodium salt, minimum number
151006-66-5
average molecular weight (in amu), 2,400
Acrylic polymers composed of one or more of the following
None
monomers: Acrylic acid, methyl acrylate, ethyl acrylate, butyl
acrylate, hydroxyethyl acrylate, hydroxypropyl acrylate, hydroxybutyl
acrylate, carboxyethyl acrylate, methacrylic acid, methyl
methacrylate, ethyl methacrylate, butyl methacrylate, isobutyl
methacrylate, hydroxyethyl methacrylate, hydroxypropyl
methacrylate, hydroxybutyl methacrylate, lauryl methacrylate, and
stearyl methacrylate; with none and/or one or more of the following
monomers: Acrylamide, N-methyl acrylamide, N,N-dimethyl
acrylamide, N-octylacrylamide, maleic anhydride, maleic acid,
monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl
maleate; and their corresponding sodium, potassium, ammonium,
isopropylamine, triethylamine, monoethanolamine, and/or
triethanolamine salts; the resulting polymer having a minimum
number average molecular weight (in amu), 1,200
Acrylonitrile-butadiene copolymer conforming to 21 CFR 180.22,
9003-18-3
minimum average molecular weight (in amu), 1,000
Acrylonitrile-styrene-hydroxypropyl methacrylate copolymer,
None
minimum number average molecular weight (in amu), 447,000

CAS No.

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α-alkyl (C12-C15) - ω- hydroxypoly(oxypropylene)poly(oxyethylene)
copolymers (where the poly(oxypropylene) content is 3-60 moles
and the poly(oxyethylene) content is 5-80 moles), the resulting
ethoxylated propoxylated (C12-C15) alcohols having a minimum
molecular weight (in amu), 1,500
α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly (oxyethylene)
polymers where the alkyl chain contains a minimum of six carbons
and a minimum number average molecular weight (in amu) 1,100

Page 397 of 441

68551-13-3

9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3; 9038-43-1;
9040-05-5; 9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 2618352-8; 26468-86-0; 26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 3439801-1; 34398-05-5; 37251-67-5; 37311-00-5; 37311-01-6; 37311-02-7; 3731104-9; 39587-22-9; 50861-66-0; 52232-09-4; 52292-17-8; 52609-19-5; 5767921-7; 59112-62-8; 60828-78-6; 61702-78-1; 61725-89-1; 61791-13-7; 6179120-6; 61791-28-4; 61804-34-0; 61827-42-7; 61827-84-7; 62648-50-4; 6330301-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4; 6442586-1; 65104-72-5; 65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 6776308-0; 68002-96-0; 68002-97-1; 68131-39-5; 68131-40-8; 68154-96-1; 6815497-2; 68154-98-3; 68155-01-1; 68213-23-0; 68213-24-1; 68238-81-3; 6823882-4; 68409-58-5; 68409-59-6; 68439-30-5; 68439-45-2; 68439-46-3; 6843948-5; 68439-49-6; 68439-50-9; 68439-51-0; 68439-53-2; 68439-54-3; 6845888-8; 68526-94-3; 68526-95-4; 68551-12-2; 68551-13-3; 68551-14-4; 6860320-3; 68603-25-8; 68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 6895494-9; 68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9; 69013-19-0; 6922720-9; 69227-21-0; 69227-22-1; 69364-63-2; 70750-27-5; 70879-83-3; 7095507-6; 71011-10-4; 71060-57-6; 71243-46-4; 72066-65-0; 72108-90-8; 7248469-6; 72854-13-8; 72905-87-4; 73018-31-2; 73049-34-0; 74432-13-6; 7449934-6; 78330-19-5; 78330-20-8; 78330-21-9; 78330-23-1; 79771-03-2; 8413350-6; 85422-93-1; 97043-91-9; 97953-22-5; 102782-43-4; 103331-86-8;
103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0; 106232-83-1; 11190554-5; 116810-31-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5;
121617-09-2; 126646-02-4; 126950-62-7; 127036-24-2; 139626-71-4; 15223144-2; 154518-36-2; 157627-86-6; 157627-88-8; 157707-41-0; 157707-43-2;
159653-49-3; 160875-66-1; 160901-20-2; 160901-09-7; 160901-19-9; 16102521-4; 161025-22-5; 166736-08-9; 169107-21-5; 172588-43-1; 176022-76-7;
196823-11-7; 287935-46-0; 288260-45-7; 303176-75-2; 954108-36-2
None

Alkyl (C12-C20) methacrylate-methacrylic acid copolymer, minimum
molecular weight (in amu), 11,900
2H-Azepin-2-one, 1-ethenylhexahydro-, homopolymer
25189-83-7
1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-dimethyl ester, sodium 212842-88-1
salt, polymer with 1,3-benzene dicarboxylic acid, 1,4-benzene
dicarboxylic acid, dimethyl 1,4-benzene dicarboxylate and
1,2-ethanediol, minimum number average molecular weight (in amu),
2,580
3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine-2,4,6-(3H,5H)
87823-33-4
-trione, polymer with diethylenetriamine, minimum number average
molecular weight (in amu), 1,000,000
Polymer of one or more diglycidyl ethers of bisphenol A, resorcinol, None
glycerol, cyclohexanedimethanol, neopentyl glycol, and polyethylene
glycol with one or more of the following: Polyoxypropylene diamine,
polyoxypropylene triamine, N-aminoethyl-piperazine,
trimethyl-1,6-hexanediamine isophorone diamine,
N,N-dimethyl-1,3-diaminopropane, nadic methyl anhydride,
1,2-cyclohexane-dicarboxylic anhydride and
1,2,3,6-tetrahydrophthalic anhydride, minimum number average
molecular weight (in amu), 400,000
Butadiene-styrene copolymer
None
Butanedioic acid, 2-methylene-, homopolymer, sodium salt,
26099-89-8
minimum number average molecular weight (in amu), 3936
Butanedioic acid, 2-methylene-, polymer with 2,5-furandione, sodium 556055-76-6
and ammonium salts, hydrogen peroxide-initiated, minimum number 701908-99-8
average molecular weight (in amu), 2,500-3,000
1,4-Butanediol-methylenebis(4-phenylisocyanate)-poly
9018-04-6
(tetramethylene glycol) copolymer, minimum molecular weight (in
amu) 158,000
Butene, homopolymer
9003-29-6
2-butenedioic acid (2Z)-, monobutyl ester, polymer with
205193-99-3
methoxyethene, sodium salt, minimum number average molecular
weight (in amu), 18,200
2-Butenedioic acid (Z)-, polymer with ethenol and ethenyl acetate,
139871-83-3
sodium salt, minimum number average molecular weight (in amu),
75,000
Butyl acrylate-vinyl acetate-acrylic acid copolymer, minimum number 65405-40-5
average molecular weight (in amu), 18,000
Carbonic acid, diethyl ester, polymer with α-hydro-ω-hydroxypoly
1147260-65-8
[oxy(methyl-1,2-ethanediyl)] ether with 2-ethyl-2-(hydroxymethyl)
-1,3-propanediol (3:1), ester with α-[[[[5-(carboxyamino)
-1,3,3-trimethylcyclohexyl]methyl]amino]carbonyl]-ω-methoxypoly
(oxy-1,2-ethanediyl), minimum number average molecular weight (in
amu), 1,900
Castor oil, ethoxylated, dioleate, minimum number average
110531-96-9
molecular weight (in amu), 1260.
Castor oil, ethoxylated, oleate, minimum number average molecular 220037-02-5
weight (in amu), 1,600
Castor oil, polymer with adipic acid, linoleic acid, oleic acid and
1357486-09-9
ricinoleic acid, minimum number average molecular weight (in amu),
3,500

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Castor oil, polyoxyethylated; the poly(oxyethylene) content averages
5-54 moles
Cellulose carboxymethyl ether, potassium salt, minimum number
average molecular weight 9587 Daltons
Chlorinated polyethylene
Cross-linked nylon-type polymer formed by the reaction of a mixture
of sebacoyl chloride and polymethylene polyphenylisocycanate with
a mixture of ethylenediamine and diethylenetriamine
Cross-linked polyurea-type encapsulating polymer
Dimethylpolysiloxane minimum number average molecular weight (in
amu), 6,800
Dimethyl silicone polymer with silica, minimum number average
molecular weight (in amu), 1,100,000
α-(o,p-Dinonylphenyl)-ω-hydroxypoly(oxyethylene) produced by
condensation of 1 mole of dinonylphenol (nonyl group is a propylene
trimer isomer) with an average of 140-160 moles of ethylene oxide
Docosyl methacrylate-acrylic acid copolymer, or docosyl
methacrylate-octadecyl methacrylate-acrylic acid copolymer,
minimum number average molecular weight (in amu), 3,000
1,12-Dodecanediol dimethacrylate polymer, minimum molecular
weight (in amu), 100,000
α-(p-Dodecylphenyl)-ω-hydroxypoly(oxyethylene) produced by the
condensation of 1 mole of dodecylphenol (dodecyl group is a
propylene tetramer isomer) with an average of 30-70 moles of
ethylene oxide
1,2-Ethanediamine, N1-(2-aminoethyl)-, polymer with
2,4-diisocyanato-1-methylbenzene, minimum number average
molecular weight (in amu), one million
1, 2-Ethanediamine, polymer with methyl oxirane and oxirane,
minimum number average molecular weight (in amu), 1,100
Ethylene glycol dimethyacrylate-lauryl methacrylate copolymer,
minimum molecular weight (in amu), 100,000
Ethylene glycol dimethacrylate polymer, minimum molecular weight
(in amu), 100,000
Fatty acids, tall-oil, ethoxylated propoxylated, minimum number
average molecular weight (in amu), 2,009
Formaldehyde, polymer with α-[bis(1-phenylethyl)phenyl]-ωhydroxypoly(oxy-1,2-ethanediyl), number average molecular weight
(in amu), 1,803
Formaldehyde, polymer with 2-methyloxirane and 4-nonylphenol,
minimum number average molecular weight (in amu), 4,000
Fumaric acid-isophthalic acid-styrene-ethylene/propylene glycol
copolymer, minimum average molecular weight (in amu), 1 × 1018
2,5-Furandione, polymer with ethenylbenzene, hydrolyzed,
3-(dimethylamino)propyl imide, imide with polyethylenepolypropylene glycol 2-aminopropyl me ether, 2,2′-(1,2-diazenediyl)
bis[2-methylbutanenitrile]-initiated, minimum number average
molecular weight (in amu), 5,816
2,5-Furandione, polymer with ethenylbenzene, reaction products
with polyethylene-polypropylene glycol 2-aminopropyl Me ether;
minimum number average molecular weight (in amu), 14,000
2,5-Furandione, polymer with methoxyethene, butyl ethyl ester,
sodium salt, minimum number average molecular weight (in amu),
18,200
Hexadecyl acrylate-acrylic acid copolymer, hexadecyl acrylate-butyl
acrylate-acrylic acid copolymer, or hexadecyl acrylate-dodecyl
acrylate-acrylic acid copolymer, minimum number average molecular
weight (in amu), 3,000
Hexamethyl disilizane, reaction product with silica, minimum number
average molecular weight (in amu), 645,000
1,6-Hexanediol dimethyacrylate polymer, minimum molecular weight
(in amu), 100,000
α-Hydro-ω-hydroxy-poly(oxyethylene) C8 alkyl ether citrates, poly
(oxyethylene) content is 4-12 moles, minimum number average
molecular weight (in amu) 1,300
α-Hydro-ω-hydroxy-poly(oxyethylene) C10-C16-alkyl ether citrates,
poly(oxyethylene) content is 4-12 moles, minimum number average
molecular weight (in amu) 1,100
α-Hydro-ω-hydroxy-poly(oxyethylene) C16-C18-alkyl ether citrates,
poly(oxyethylene) content is 4-12 moles, minimum number average
molecular weight (in amu) 1,300
α-Hydro-ω-hydroxypoly(oxyethylene), minimum number average
molecular weight (in amu), 17,000
α-Hydro-ω-hydroxypoly(oxyethylene)poly (oxypropylene) poly
(oxyethylene) block copolymer; the minimum poly(oxypropylene)
content is 27 moles and the minimum molecular weight (in amu) is
1,900
α-Hydro-ω-hydroxypoly(oxypropylene); minimum molecular weight
(in amu) 2,000
12-Hydroxystearic acid-polyethylene glycol copolymer, minimum
number average molecular weight (in amu), 3,690

Page 398 of 441

None
54848-04-3
64754-90-1
None

None
63148-62-9
67762-90-7
9014-93-1

None

None
9014-92-0
26401-47-8

35297-61-1

26316-40-5
None
None
67784-86-5
157291-93-5

37523-33-4
None
1062609-13-5

162568-32-3

1471342-08-1

None

68909-20-6
None
330977-00-9

330985-58-5

330985-61-0

25322-68-3
None

None
70142-34-6

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Page 399 of 441

Isodecyl alcohol ethoxylated (2-8 moles) polymer with chloromethyl None
oxirane, minimum number average molecular weight (in amu) 2,500
Lauryl methacrylate-1,6-hexanediol dimethacrylate copolymer,
None
minimum molecular weight (in amu), 100,000
Maleic acid-butadiene copolymer
None
Maleic acid monobutyl ester-vinyl methyl ether copolymer, minimum 25119-68-0
average molecular weight (in amu), 52,000
Maleic acid monoethyl ester-vinyl methyl ether copolymer, minimum 25087-06-3
average molecular weight (in amu), 46,000
Maleic acid monoisopropyl ester-vinyl methyl ether copolymer,
31307-95-6
minimum average molecular weight (in amu), 49,000
Maleic anhydride-diisobutylene copolymer, sodium salt, minimum
37199-81-8
number average molecular weight (in amu) 5,0007-18,000
Maleic anhydride-methylstyrene copolymer sodium salt, minimum
60092-15-1
number average molecular weight (in amu), 15,000
Maleic anhydride-methyl vinyl ether, copolymer, average molecular None
weight (in amu), 250,000
Methacrylic acid-methyl methacrylate-polyethylene glycol methyl
100934-04-1
ether methacrylate copolymer, minimum number averge molecular
weight (in amu), 3,700
111740-36-4
Methacrylic acid-methyl methacrylate-polyethylene glycol
monomethyl ether methacrylate graft copolymer, minimum number
average molecular weight (in amu), 1,800
Methacrylic copolymer, minimum number average molecular weight 63150-03-8
(in amu), 15,000
Methyl methacrylate-methacrylic acid-monomethoxypolyethylene
119724-54-8
glycol methacrylate copolymer,) minimum number average
molecular weight (in amu), 2,730
Methyl methacrylate-2-sulfoethyl methacrylateNone
dimethylaminoethylmethacrylate-glycidyl methacrylate-styrene-2ethylhexyl acrylate graft copolymer, minimum average molecular
weight (in amu), 9,600
Methyl vinyl ether-maleic acid copolymer), minimum number average 25153-40-6
molecular weight (in amu), 75,000
Methyl vinyl ether-maleic acid copolymer, calcium sodium salt,
62386-95-2
minimum number average molecular weight (in amu), 900,000
Monophosphate ester of the block copolymer α-hydro-ω-hydroxypoly None
(oxyethylene) poly(oxypropylene) poly(oxyethylene); the poly
(oxypropylene) content averages 37-41 moles, average molecular
weight (in amu), 8,000
α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) mixture of
None
dihydrogen phosphate and monohydrogen phosphate esters and the
corresponding ammonium, calcium, magnesium,
monoethanolamine, potassium, sodium, and zinc salts of the
phosphate esters; the nonyl group is a propylene trimer isomer and
the poly(oxyethylene) content averages 30 moles
α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) sulfate, and its
None
ammonium, calcium, magnesium, monoethanolamine, potassium,
sodium, and zinc salts; the nonyl group is a propylene trimer isomer
and the poly(oxyethylene) content averages 30-90 moles of ethylene
oxide
α-(p-Nonylphenyl-ω-hydroxypoly(oxypropylene) block polymer with None
poly(oxyethylene); polyoxypropylene content of 10-60 moles;
polyoxyethylene content of 10-80 moles; molecular weight (in amu),
1,200-7,100.
37251-69-7
α-(ρ-Nonylphenyl)poly(oxypropylene) block polymer with poly
(oxyethylene); poly oxyethylene content 30 to 90 moles; minimum
number average molecular weight (in amu), 1,889
Octadecanoic Acid, 12-Hydroxy-, Homopolymer Ester with
1373125-59-7
2-Methylloxirane Polymer with Oxirane monobutyl Ether, minimum
number average molecular weight (in amu), 4,500
Octadecanoic acid, 12-hydroxy-, homopolymer, octadecanoate
58128-22-6)
minimum number average molecular weight (in amu), 1,370
α-cis-9-Octadecenyl-ω-hydroxypoly(oxyethylene); the octadecenyl
None
group is derived from oleyl alcohol and the poly(oxyethylene) content
averages 20 moles
Octadecyl acrylate-acrylic acid copolymer, octadecyl acrylateNone
dodecyl acrylate-acrylic acid copolymer, octadecyl methacrylatebutyl acrylate-acrylic acid copolymer, octadecyl methacrylate-hexyl
acrylate-acrylic acid copolymer, octadecyl methacrylate-dodecyl
acrylate-acrylic acid copolymer, or octadecyl methacrylate-dodecyl
methacrylate-acrylic acid copolymer, minimum number average
molecular weight (in amu) 3,000
Oleic acid diester of α-hydro-ω-hydroxypoly(oxyethylene); the poly None
(oxyethylene), average molecular weight (in amu), 2,300
2-oxepanone, homopolymer, minimum number average molecular
24980-41-4
weight (in amu) 52,000
Oxirane, decyl-, reaction products with polyethylene-polypropylene 903890-89-1
glycol ether with trimethylolpropane (3:1)
Oxirane, hexadecyl-, reaction products with polyethylene893427-80-0
polypropylene glycol ether with trimethylolpropane (3:1)
61419-46-3

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eCFR — Code of Federal Regulations

Oxirane, 2-methyl-, polymer with oxirane, dimethyl ether, minimum
number average molecular weight (in amu), 2,800
Oxirane, methyl-, polymer with oxirane, ether with 2-ethyl2-(hydroxymethyl)-1,3-propanediol (3:1), reaction products with
tetradecyloxirane
Oxirane, methyl-, polymer with oxirane, mono[2-(2-butoxyethoxy)
ethyl] ether, minimum number average molecular weight (in amu),
2,500
Oxirane, methyl-, polymer with Oxirane, Monobutyl Ether
Oxirane, 2-methyl-, polymer with oxirane, minimum number average
molecular weight (in amu), 1,100
Oxirane, 2-methyl-, polymer with oxirane, mono
[2-[2-(2-butoxymethylethoxy)methylethoxy]methylethyl] ether,
minimum number average molecular weight (in amu), 3,000
Oxirane, phenyl, polymer with oxirane, monooctyl ether, minimum
average molecular weight (in amu) 1,200
Polyamide polymer derived from sebacic acid, vegetable oil acids
with or without dimerization, terephthalic acid and/or
ethylenediamine
Polyethylene glycol-polyisobutenyl anhydride-tall oil fatty acid
copolymer, minimum number average molecular weight (in amu),
2,960
Polyethylene, oxidized, minimum number average molecular weight
(in amu), 1,200
Polymers produced by the reaction of either 1,6-hexanediisocyanate;
2,4,4-trimethyl-1,6-hexanediisocyanate; 5-isocyanato1-(isocyanatomethyl)-fxsp0;1,3,3fxsp0;-trimethyIcyclohexane
(isophoronediisocyanate); 4,4′-methylene-bis-1,1′
-cyclohexanediisocyanate; 4,4′-methylene-bis-1,1′
benzyldiisocyanate; or 1,3-bis-(2-isocyanatopropan-2-yl)benzene
with polyethylene glycol and end-capped with one or a mixture of
more than one of octanol, decanol, dodecanol, tetradecanol,
hexadecanol, octadecanol, and octadec-9-enol or polyethyleneglycol
ethers of octanol, decanol, dodecanol, tetradecanol, hexadecanol,
octadecanol, and octadec-9-enol, minimum number average
molecular weight (in amu), 20,000
Polymethylene polyphenylisocyanate, polymer with ethylene
diamine, diethylene triamine and sebacoyl chloride, cross-linked;
minimum number average molecular weight (in amu), 100,000
Polyoxyalkylated glycerol fatty acid esters; the mono-, di-, or
triglyceride mixtures of C8 through C22, primarily C8 through C18
saturated and unsaturated, fatty acids containing up to 15% water by
weight reacted with a minimum of three moles of either ethylene
oxide or propylene oxide; the resulting polyoxyalkylated glycerol
ester polymer minimum number average molecular weight (in amu),
1,500
Polyoxyalkylated sorbitan fatty acid esters with C6 through C22
aliphatic alkanoic and/or alkenoic fatty acids, branched or linear, the
resulting polyoxyalkylene sorbitan esters minimum number average
molecular weight (in amu), 1,300
Polyoxyalkylated trimethylopropanes with 20 to 80 moles of ethylene
and/or propylene oxide, fatty acid esters with C8 through C22
aliphatic alkanoic and/or alkenoic fatty acids, branched or linear;
minimum number average molecular weight (in amu), 3,000

Poly(oxy-1,2-ethanediyl), α-hydro-ω-hydroxy-, polymer with 1, 1′
-methylene-bis-[4-isocyanatocyclohexane], minimum number
average molecular weight (in amu), 1800
Polyoxyethylated primary amine (C14-C18); the fatty amine is derived
from an animal source and contains 3% water; the poly(oxyethylene)
content averages 20 moles
Polyoxyethylated sorbitol fatty acid esters; the polyoxyethylated
sorbitol solution containing 15% water is reacted with fatty acids
limited to C12, C14, C16, and C18, containing minor amounts of
associated fatty acids; the poly(oxyethylene) content averages 30
moles.
Polyoxyethylated sorbitol fatty acid esters; the sorbitol solution
containing up to 15% water is reacted with 20-50 moles of ethylene
oxide and aliphatic alkanoic and/or alkenoic fatty acids C8 through
C22 with minor amounts of associated fatty acids; the resulting
polyoxyethylene sorbitol ester having a minimum molecular weight
(in amu), 1,300
Poly(oxyethylene/oxypropylene) monoalkyl (C6-C10) ether sodium
fumarate adduct, minimum number average molecular weight (in
amu), 1,900
Poly[oxy(methyl-1,2-ethanediyl)], α-[(9Z)-1-oxo-9-octadecen-1-yl]-ω[[(9Z)-1-oxo-9-octadecen-1yl]oxy]-, minimum number average
molecular weight (in amu) 2,300
Polyoxymethylene copolymer, minimum number average molecular
weight (in amu), 15,000

Page 400 of 441

903890-90-4

85637-75-8

9038-95-3
9003-11-6
926031-36-9

83653-00-3
None

68650-28-2

None
1161844-26-3, 1161844-30-9, 1161844-43-4, 1161844-51-4, 1161844-53-6,
693252-31-2, 162993-60-4, 630102-86-2

None

61791-23-9, 68201-46-7, 68440-49-3, 68458-88-8, 68606-12-2, 68648-38-4,
70377-91-2, 70914-02-2, 72245-12-6, 72698-41-3, 180254-52-8, 248273-72-5,
308063-50-5, 952722-33-7

81776-11-6, 87090-31-1, 88895-72-1, 103171-31-9, 161026-53-5, 147264480-6, 1472644-81-7, 1472644-84-0, 1472644-85-1, 1472644-87-3, 147264488-4, 1472654-83-3, 1472655-32-5, 1472661-05-4, 1472661-17-8, 147266359-4, 1472663-64-1, 1472663-66-3, 1472663-92-5, 1472668-03-3
25765-36-0; 29860-47-7; 37339-03-0; 52624-57-4; 58090-24-7; 63964-38-5;
72939-62-9; 74521-14-5; 75300-70-8; 75300-90-2; 84271-03-4; 84271-04-5;
86850-92-2; 107120-02-5; 133331-01-8; 137587-60-1; 149797-40-0; 14979741-1; 150695-97-9; 152130-24-0; 163349-94-8; 163349-95-9; 163349-96-0;
163349-97-1; 163349-98-2; 165467-70-9; 183619-46-7; 183619-50-3; 18526001-9; 202606-04-0; 210420-84-1; 233660-70-3; 263011-96-7; 283602-94-8;
701980-40-7; 872038-58-9; 875709-44-7; 875709-45-8; 875709-46-9; 87570947-0; 879898-63-2; 910038-01-6; 1190748-04-9; 1225384-02-0; 1428944-41-5;
1446498-15-2.
39444-87-6

None

None

None

102900-02-7

26571-49-3

None

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eCFR — Code of Federal Regulations

Poly(oxypropylene) block polymer with poly(oxyethylene), molecular
weight (in amu), 1,800-16,000
Poly(phenylhexylurea), cross-linked, minimum average molecular
weight (in amu), 36,000
Polypropylene
Polystyrene, minimum number average molecular weight (in amu),
50,000
Polytetrafluoroethylene
Polyvinyl acetate, copolymer with maleic anhydride, partially
hydrolyzed, sodium salt, minimum number average molecular weight
(in amu), 53,000
Polyvinylpyrrolidone butylated polymer, minimum number average
molecular weight (in amu), 9,500
Polyvinyl acetate, minimum molecular weight (in amu), 2,000
Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number
average molecular weight (in amu), 50,000
Polyvinyl alcohol
Polyvinyl chloride
Polyvinyl chloride, minimum number average molecular weight (in
amu), 29,000
Poly(vinylpyrrolidone), minimum number average molecular weight
(in amu), 4,000
Poly(vinylpyrrolidone-1-eicosene), minimum average molecular
weight (in amu), 3,000
Poly(vinylpyrrolidone-1-hexadecene), minimum average molecular
weight (in amu), 4,700
1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propenyl)amino]-,
monosodium salt, polymer with ethenol and ethenyl acetate,
minimum number average molecular weight (in amu) 50,000
2-Propene-1-sulfonic acid sodium salt, polymer with ethenol and
ethenyl acetate, number average molecular weight (in amu) 6,00012,000
2-Propenoic acid, butyl ester, polymer with 1,6-diisocyanatohexane,
N-(hydroxymethyl)-2-methyl-2-propenamide and 2-propenenitrile,
minimum number average molecular weight (in amu), 100,000
2-propenoic acid, butyl ester, polymer with ethenylbenzene, methyl
2-methyl-2-propenoate and 2-propenoic acid (in amu), 1900.
2-Propenoic acid, butyl ester, polymer with ethyl 2-propenoate and
N-(hydroxymethyl)-2-propenamide, minimum number average
molecular weight (in amu), 30,000
2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene
14,000 daltons
2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene
and 2-methylpropyl 2-methyl-2-propenoate, minimum number
average molecular weight (in amu), 18,000
2-Propenoic acid, 2-hydroxyethyl ester, polymer with
α-[4-(ethenyloxy)butyl]-ω-hydroxypoly (oxy-1,2-ethanediyl), minimum
number average molecular weight (in amu), 17,000
[2-propenoic acid, 2-methyl-, C12-16-alkyl esters, telomers with
1-dodecanethiol, polyethylene-polypropylene glycol ether with
propylene glycol monomethacrylate (1:1), and styrene
2,2'-(1,2-diazenediyl)bis[2-methylbutanenitrile]-initiated, minimum
number average molecular weight (in amu), 4,000
2-Propenoic acid, methyl ester, polymer with ethenyl acetate,
hydrolyzed, sodium salts
2-Propenoic acid, 2-methyl-, 2-ethylhexyl ester, telomer with
1-dodecanethiol, ethenylbenzene and 2-methyloxirane polymer with
oxirane monoether with 1,2-propanediol mono(2-methyl-2propenoate), hydrogen 2-sulfobutanedioate, sodium salt, 2, 2′
-(1,2-diazenediyl)bis[2-methylpropanenitrile]-initiated, minimum
number average molecular weight (in amu), 1,200
>2-Propenoic acid, 2-methyl-, 2-methylpropyl ester, homopolymer,
minimum number average molecular weight (in amu), 55,000
2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with
2-propenoic acid, peroxydisulfuric acid ([(HO)S(O)2]2O2) sodium
salt (1:2)-initiated, compounds with diethanolamine, minimum
number average molecular weight (in amu), 2,000
2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with
2-propenoic acid and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl)
amino]-1-propanesulfonate (1:1), peroxydisulfuric acid ([HO)S(O)2]
202) sodium salt (1:2)-initiated minimum number average molecular
weight >1,000 Daltons; maximum number average molecular weight
10,000 Daltons
2-Propenoic acid, 2-methyl-, polymer with butyl 2-propenoate and
ethenylbenzene, minimum number average molecular weight (in
amu), 17,000
2-Propenoic acid, 2-Methyl-, Polymer with Butyl 2-Propenoate,
Methyl 2-Methyl-2-Propenoate, Methyl 2-Propenoate and
2-Propenoic Acid, graft, Compound with 2-Amino-2-Methyl-1Propanol

Page 401 of 441

None
None
9003-07-0
9003-53-6
9002-84-0
None

26160-96-3
None
25213-24-5
9002-89-5
None
9002-86-2
9003-39-8
28211-18-9
63231-81-2
107568-12-7

None

1469998-09-1

27306-39-4
33438-19-6

25153-46-2
68240-06-2

1007234-89-0

950207-35-9

886993-11-9
1283712-50-4

9011-15-8
1574486-33-1

CASRN 1246766-57-3

25036-16-2

153163-36-1

146753-99-3

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eCFR — Code of Federal Regulations

2-Propenoic Acid, 2-Methyl-, Polymer with Ethenylbenzene,
2-Ethylhexyl 2-Propenoate, 2-Hydroxyethyl 2-Propenoate,
N-(Hydroxymethyl) -2-Methyl-2-Propenamide and Methyl 2-Methyl-2Propenoate, Ammonium Salt
2-Propenoic acid, 2-methyl-, polymers with Bu acrylate, Et acrylate,
Me methacrylate and polyethylene glycol methacrylate C16-18-alkyl
ethers, minimum number average molecular weight (in amu), 13,000
2-Propenoic acid, 2-methyl-, telomer with 2-ethylhexyl 2-propenoate,
2-propanol and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl) amino]-1propanesulfonate (1:1), sodium salt, minimum number average
molecular weight (in amu): 2,900
2-Propenoic acid, monoester with 1,2-propanediol, polymer with
α-[4-(ethenyloxy) butyl]-ω-hydroxypoly (oxy-1,2-ethanediyl) and
2,5-furandione, minimum number average molecular weight (in
amu), 25,000
2-propenoic acid polymer, with 1,3-butadiene and ethenylbenzene,
minimum number average molecular weight (in amu), 9400
2-Propenoic acid, polymer with ethenyl acetate, ethenylbenzene,
2-ethylhexyl 2-propenoate and ethyl 2-propenoate, minimum number
average molecular weight (50,149 Daltons)
2-Propenoic acid, polymer with ethenylbenzene and
(1-methylethenyl)benzene, minimum number average molecular
weight (in amu), 2,000
2-Propenoic acid, polymer with ethenylbenzene and
(1-methylethenyl) benzene, sodium salt, minimum number average
molecular weight (in amu), 2,800
2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1,2-ethanediyl) and 2,5-furandione, sodium salt,
minimum number average molecular weight (in amu), 25,000
2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1,2-ethanediyl) and 1,2-propanediol mono-2propenoate, potassium sodium salt, minimum number average
molecular weight (in amu), 16,000
2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1, 2-ethanediyl), sodium salt, minimum number
average molecular weight (in amu), 24,000
2-Propenoic acid, polymer with 2-propenamide, sodium salt,
minimum number average molecular weight (in amu), 18,000
2-Propenoic acid, sodium salt, polymer with 2-propenamide,
minimum number average molecular weight (in amu), 18,000
2-Propenoic, 2-methyl-, polymers with ethyl acrylate and
polyethylene glycol methylacrylate C18-22 alkyl ethers
2-Pyrrolidone, 1-ethenyl-, polymer with ethenol, minimum number
average molecular weight (in amu), 23,000
Silane, dichloromethyl- reaction product with silica minimum number
average molecular weight (in amu), 3,340,000
Silane, trimethoxy[3-(oxiranylmethoxy)propyl]-, hydrolysis products
with silica, minimum number average molecular weight (in amu),
640,000
Silicic acid, sodium salt, reaction products with chlorotrimethylsilane
and iso-propyl alcohol, reaction with poly(oxypropylene)-poly
(oxyethylene) glycol, minimum number average molecular weight (in
amu), 75,000
Sodium polyflavinoidsulfonate, consisting chiefly of the copolymer of
catechin and leucocyanidin
Soybean oil, ethoxylated; the poly(oxyethylene) content averages 10
moles or greater
Starch, oxidized, polymers with Bu acrylate, tert-Bu acrylate and
styrene, minimum number average molecular weight (in amu),
10,000
Stearyl methacrylate-1,6-hexanediol dimethacrylate copolymer,
minimum molecular weight (in amu), 100,000
Styrene, copolymers with acrylic acid and/or methacrylic acid, with
none and/or one or more of the following monomers:
Acrylamidopropyl methyl sulfonic acid, methallyl sulfonic acid,
3-sulfopropyl acrylate, 3-sulfopropyl methacrylate, hydroxypropyl
methacrylate, hydroxypropyl acrylate, hydroxyethyl methacrylate,
hydroxyethyl acrylate, and/or lauryl methacrylate; and its sodium,
potassium, ammonium, monoethanolamine, and triethanolamine
salts; the resulting polymer having a minimum number average
molecular weight (in amu), 1200
Styrene-ethylene-propylene block copolymer, minimum number
average molecular weight (in amu), 125,000
Styrene, 2-ethylhexyl acrylate, butyl acrylate copolymer, minimum
number average molecular weight (in amu), 4,200
Styrene-2-ethylhexyl acrylate-glycidyl methacrylate-2-acrylamido-2methylpropanesulfonic acid graft copolymer, minimum number
average molecular weight (in amu), 12,500
Styrene-maleic anhydride copolymer
Styrene-maleic anhydride copolymer, ester derivative

Page 402 of 441

890051-63-5

1260001-65-7

955015-23-3

25085-39-6
85075-52-1

5283104-6
129811-24-1

251479-97-7

518026-64-7

250591-84-5

25085-02-3
25987-30-8
888969-14-0
26008-54-8
68611-44-9
68584-82-7

None

None
61791-23-9
204142-80-3

None
None

108388-87-0
30795-23-4
None

None
None
1398573-80-2

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eCFR — Code of Federal Regulations

Page 403 of 441

Tall oil, polymer with polyethylene glycol and succinic anhydride
monopolyisobutylene derivs., minimum number average molecular
weight (in amu), 1,200
Tamarind seed gum, 2-hydroxypropyl ether polymer, minimum
68551-04-2
number average molecular weight (in amu), 10,000
Tetradecyl acrylate-acrylic acid copolymer, minimum number
None
average molecular weight (in amu), 3,000
Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum
104133-09-7
number average molecular weight (in amu), 2,500
Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum
104133-09-7
number average molecular weight (in amu), 6,500
α-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-ω-hydroxypoly(oxyethylene) 9036-19-5
produced by the condensation of 1 mole of
9002-93-1
p-(1,1,3,3-tetramethylbutyl)phenol with a range of 30-70 moles of
ethylene oxide
α-[p-(1,1,3,3-Tetramethylbutyl)phenyl] poly(oxypropylene) block
None
polymer with poly(oxyethylene); the poly(oxypropylene) content
averages 25 moles, the poly(oxyethylene) content averages 40
moles, the molecular weight (in amu) averages 3,400
α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene)
None
poly(oxypropylene) copolymer, the poly(oxypropylene) content
averages 2-8 moles, the poly(oxyethylene) content averages 1630moles, average molecular weight (in amu), 1,500
Urea-formaldehyde copolymer, minimum average molecular weight 9011-05-6
(in amu), 30,000
Vinyl acetate-allyl acetate-monomethyl maleate copolymer, minimum None
average molecular weight (in amu), 20,000
Vinyl acetate-ethylene copolymer, minimum number average
24937-78-8
molecular weight (in amu), 69,000
Vinyl acetate polymer with none and/or one or more of the following None
monomers: Ethylene, propylene, N-methyl acrylamide, acrylamide,
monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl
maleate, maleic anhydride, maleic acid, octyl acrylate, butyl acrylate,
ethyl acrylate, methyl acrylate, acrylic acid, octyl methacrylate, butyl
methacrylate, ethyl methacrylate, methyl methacrylate, methacrylic
acid, carboxyethyl acrylate, and diallyl phthalate; and their
corresponding sodium, potassium, ammonium, isopropylamine,
triethylamine, monoethanolamine and/or triethanolamine salts; the
resulting polymer having a minimum number average molecular
weight (in amu), 1,200
Vinyl acetate-vinyl alcohol-alkyl lactone copolymer, minimum number None
average molecular weight (in amu), 40,000; minimum viscosity of 18
centipoise
Vinyl alcohol-disodium itaconate copolymer, minimum average
None
molecular weight (in amu), 50,290
Vinyl alcohol-vinyl acetate copolymer, benzaldehyde-o-sodium
None
sulfonate condensate, minimum number average molecular weight
(in amu), 20,000
Vinyl alcohol-vinyl acetate-monomethyl maleate, sodium salt-maleic None
acid, disodium salt-γ-butyrolactone acetic acid, sodium salt
copolymer, minimum number average molecular weight (in amu),
20,000
Vinyl chloride-vinyl acetate copolymers
None
Vinyl pyrrolidone-acrylic acid copolymer, minimum number average 28062-44-4
molecular weight (in amu), 6,000
Vinyl pyrrolidone-dimethylaminoethylmethacrylate copolymer,
30581-59-0
minimum number average molecular weight (in amu), 20,000
Vinyl pyrrolidone-styrene copolymer
25086-29-7

[67 FR 36528, May 24, 2002]
EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.960, see the List of CFR Sections Affected, which appears in
the Finding Aids section of the printed volume and at www.fdsys.gov.

Back to Top
§180.1011 Viable spores of the microorganism Bacillus thuringiensis Berliner; exemption from the requirement
of a tolerance.
(a) For the purposes of this section the microbial insecticide for which exemption from the requirement of a tolerance
is being established shall have the following specifications:
(1) The microorganism shall be an authentic strain of Bacillus thuringiensis Berliner conforming to the morphological
and biochemical characteristics of Bacillus thuringiensis as described in Bergey's Manual of Determinative Bacteriology,
Eighth Edition.
(2) Spore preparations of Bacillus thuringiensis Berliner shall be produced by pure culture fermentation procedures
with adequate control measures during production to detect any changes from the characteristics of the parent strain or
contamination by other microorganisms.

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Page 404 of 441

(3) Each lot of spore preparation, prior to the addition of other materials, shall be tested by subcutaneous injection of
at least 1 million spores into each of five laboratory test mice weighing 17 grams to 23 grams. Such test shall show no
evidence of infection or injury in the test animals when observed for 7 days following injection.
(4) Spore preparations shall be free of the Bacillus thuringiensis β-exotoxin when tested with the fly larvae toxicity test
(“Microbial Control of Insects and Mites,” R.P.M. Bond et al., p. 280 ff., 1971). This specification can be satisfied either by
determining that each master seed lot brought into production is a Bacillus thuringiensis strain which does not produce
β-exotoxin under standard manufacturing conditions or by periodically determining that β-exotoxin synthesized during
spore production is eliminated by the subsequent spore-harvesting procedure.
(b) Exemption from the requirement of a tolerance is established for residues of the microbial insecticide Bacillus
thuringiensis Berliner, as specified in paragraph (a) of this section, in or on honey and honeycomb and all other raw
agricultural commodities when it is applied either to growing crops, or when it is applied after harvest in accordance with
good agricultural practices.
[36 FR 22540, Nov. 25, 1971, as amended at 38 FR 19045, July 17, 1973; 42 FR 28540, June 3, 1977; 45 FR 43721, June 30,
1980; 45 FR 56347, Aug. 25, 1980; 74 FR 26533, June 3, 2009]

Back to Top
§180.1016 Ethylene; exemption from the requirement of a tolerance.
Ethylene is exempted from the requirement of a tolerance for residues when:
(a) For all food commodities, it is used as a plant regulator on plants, seeds, or cuttings and on all food commodities
after harvest and when applied in accordance with good agricultural practices.
(b) Injected into the soil to cause premature germination of witchweed in bean (lima and string), cabbage, cantaloupe,
collard, corn, cotton, cucumber, eggplant, okra, onion, pasture grass, pea (field and sweet), peanut, pepper, potato, sweet
potato, sorghum, soybean, squash, tomato, turnip, and watermelon fields as part of the U.S. Department of Agriculture
witchweed control program.
[39 FR 33315, Sept. 17, 1974, as amended at 40 FR 19477, May 5, 1975; 64 FR 31505, June 11, 1999]

Back to Top
§180.1017 Diatomaceous earth; exemption from the requirement of a tolerance.
(a) Diatomaceous earth is exempted from the requirement of a tolerance for residues when used in accordance with
good agricultural practice in pesticide formulations applied to growing crops, to food commodities after harvest, and to
animals.
(b) Diatomaceous earth may be safely used in accordance with the following conditions. Application shall be limited
solely to spot and/or crack and crevice treatments in food or feed processing and food or feed storage areas in accordane
with the precribed conditions:
(1) It is used or intended for use for control of insects in food or feed processing and food or feed storage areas:
Provided, That the food or feed is removed or covered prior to such use.
(2) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S.
Environmental Protection Agency, and it shall be used in accordance with such label and labeling.
[65 FR 33716, May 24, 2000]

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§180.1019 Sulfuric acid; exemption from the requirement of a tolerance.
(a) Residues of sulfuric acid are exempted from the requirement of a tolerance when used in accordance with good
agricultural practice when used as a herbicide in the production of garlic and onions, and as a potato vine dessicant in the
production of potatoes.
(b) Residues of sulfuric acid are exempted from the requirement of a tolerance in cattle, meat; goat, meat; hog, meat;
horse, meat; sheep, meat; poultry, fat; poultry, meat; poultry, meat, byproducts; egg; milk; fish, shellfish, and irrigated
crops when it results from the use of sulfuric acid as an inert ingredient in a pesticide product used in irrigation
conveyance systems and lakes, ponds, reservoirs, or bodies of water in which fish or shellfish are cultivated. The sulfuric
acid is not to exceed 10% of the pesticide formulation (non-aerosol formulations only).
[69 FR 40787, July 7, 2004, as amended at 74 FR 26533, June 3, 2009]

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§180.1020 Sodium chlorate; exemption from the requirement of a tolerance.
Sodium chlorate is exempted from the requirement of a tolerance for residues when used as a defoliant or desiccant
in accordance with good agricultural practice on the following crops:
Bean, dry, seed
Corn, field, forage
Corn, field, grain
Corn, field, stover
Corn, pop, grain
Corn, pop, stover
Corn, sweet, forage
Corn, sweet, stover
Cotton, undelinted seed
Flax, seed
Grain, aspirated fractions
Guar, seed
Pea, southern
Pepper, nonbell
Potato
Rice, grain
Rice, straw
Safflower, seed
Sorghum, forage, forage
Sorghum, grain, forage
Sorghum, grain, grain
Sorghum, grain, stover
Soybean, forage
Soybean, hay
Soybean, seed
Sunflower, seed
Wheat, grain
[74 FR 47457, Sept. 16, 2009]

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§180.1021 Copper; exemption from the requirement of a tolerance.
(a) Copper is exempted from the requirement of a tolerance in cattle, meat; goat, meat; hog, meat; horse, meat;
sheep, meat; milk, poultry, fat; poultry, meat; poultry, meat byproducts; egg, fish, shellfish, and irrigated crops when it
results from the use of:
(1) Copper sulfate as an algicide or herbicide in irrigation conveyance systems and lakes, ponds, reservoirs, or bodies
of water in which fish or shellfish are cultivated.
(2) Basic copper carbonate (malachite) as an algicide or herbicide in impounded and stagnant bodies of water
(3) Copper triethanolamine and copper monoethanolamine as an algicide or herbicide in fish hatcheries, lakes, ponds,
and reservoirs

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(4) Cuprous oxide bearing antifouling coatings for control of algae or other coatings for control of algae or other
organisms on submerged concrete or other (irrigation) structures.
(5) Copper oxide embedded in polymer emitter heads used in irrigation systems for root incursion prevention.
(b) The following copper compounds are exempt from the requirement of a tolerance when applied (primarily) as a
fungicide to growing crops using good agricultural practices:
Copper compounds

CAS Reg. No.

Basic copper carbonate (malachite)
Copper ammonia complex
Copper ethylenediamine complex
Copper hydroxide
Copper octanoate
Copper oxychloride
Copper oxychloride sulfate
Copper salts of fatty and rosin acids
Copper sulfate basic
Copper sulfate pentahydrate
Cuprous oxide

1184-64-1
16828-95-8
13426-91-0
20427-59-2
20543-04-8
1332-65-6
8012-69-9
9007-39-0
1344-73-6
7758-99-8
1317-19-1

(c) Copper sulfate pentahydrate (CAS Reg. No. 7758-99-8) is exempt from the requirement of a tolerance when
applied as a fungicide to growing crops or to raw agricultural commodities after harvest, and as a bactericide/fungicide in
or on meat, fat and meat by-products of cattle, sheep, hogs, goats, horses and poultry, milk and eggs when applied as a
bactericide/fungicide to animal premises and bedding.
(d) Copper (II) hydroxide (CAS Reg. No. 20427-59-2) is exempt from the requirement of a tolerance when applied to
growing crops or to raw agricultural commodities as an inert ingredient (for pH control) in pesticide products.
[65 FR 68912, Nov. 15, 2000, as amended at 69 FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, 2006; 74 FR 26534, June 3, 2009;
74 FR 47457, Sept. 16, 2009; 80 FR 37551, July 1, 2015]

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§180.1022 Iodine-detergent complex; exemption from the requirement of a tolerance.
The aqueous solution of hydriodic acid and elemental iodine, including one or both of the surfactants (a)
polyoxypropylene-polyoxyethylene glycol nomionic block polymers (minimum average molecular weight 1,900) and (b)
α-(p- nonylphenyl)-omega- hydroxypoly (oxyethylene) having a maximum average molecular weight of 748 and in which
the nonyl group is a propylene trimer isomer, is exempted from the requirement of a tolerance for residues in egg, and
poultry, fat; poultry, meat; poultry, meat byproducts when used as a sanitizer in poultry drinking water.
[74 FR 26534, June 3, 2009]

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§180.1023 Propanoic acid; exemptions from the requirement of a tolerance.
(a) Postharvest application of propanoic acid or a mixture of methylene bispropionate and oxy(bismethylene)
bisproprionate when used as a fungicide is exempted from the requirement of a tolerance for residues in or on the
following raw agricultural commodities: Alfalfa, forage; alfalfa, hay; alfalfa, seed; barley, grain; Bermudagrass, forage;
Bermudagrass, hay; bluegrass, forage; bluegrass, hay; bromegrass, forage; bromegrass, hay; clover, forage; clover, hay;
corn, field, grain; corn, pop, grain; cowpea, hay; fescue, forage; fescue, hay; lespedeza, forage; lespedeza, hay; lupin; oat,
grain; orchardgrass, forage; orchardgrass, hay; peanut, hay; pea, field, hay; ryegrass, Italian, hay; sorghum, grain, grain;
soybean, hay; sudangrass, forage; sudangrass, hay; timothy, forage; timothy, hay; vetch, forage; vetch, hay; and wheat,
grain.
(b) Propanoic acid is exempt from the requirement of a tolerance for residues in or on cattle, meat; cattle, meat
byproducts; goat, meat; goat, meat byproducts; hog, meat; hog meat byproducts; horse, meat; horse, meat byproducts;
sheep, meat; sheep meat byproducts; and, poultry, fat; poultry meat; poultry meat byproducts; milk, and egg when applied
as a bactericide/fungicide to livestock drinking water, poultry litter, and storage areas for silage and grain.
(c) Preharvest and postharvest application of propanoic acid (CAS Reg. No. 79-09-4), propanioc acid, calcium salt
(CAS Reg. No. 4075-81-4), and propanioc sodium salt (CAS Reg. No. 137-40-6) are exempted from the requirement of a
tolerance on all crops when used as either an active or inert ingredient in accordance with good agricultural practice in
pesticide formulations applied to growing crops, to raw agricultural commodities before and after harvest and to animals.
[69 FR 47025, Aug. 4, 2004, as amended at 74 FR 26534, June 3, 2009]

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§180.1025 Xylene; exemption from the requirement of a tolerance.
Xylene is exempted from the requirement of a tolerance when used as an aquatic herbicide applied to irrigation
conveyance systems in accordance with the following conditions:
(a) It is to be used only in programs of the Bureau of Reclamation, U.S. Department of Interior, and cooperating water
user organizations.
(b) It is to be applied as an emulsion at an initial concentration not to exceed 750 parts per million.
(c) It is not to be applied when there is any likelihood that the irrigation water will be used as a source of raw water for
a potable water system or where return flows of such treated irrigation water into receiving rivers and streams would
contain residues of xylene in excess of 10 parts per million.
(d) Xylene to be used as an aquatic herbicide shall meet the requirement limiting the presence of a polynuclear
aromatic hydrocarbons as listed in 21 CFR 172.250.
[38 FR 16352, June 22, 1973, as amended at 50 FR 2980, Jan. 3, 1985]

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§180.1027 Nuclear polyhedrosis virus of Heliothis zea; exemption from the requirement of a tolerance.
(a) For the purposes of this section, the viral insecticide must be produced with an unaltered and unadulterated
inoculum of the single-embedded Heliothis zea nuclear polyhedrosis virus (HzSNPV). The identity of the seed virus must
be assured by periodic checks.
(b) Each lot of active ingredient of the viral insecticide shall have the following specifications:
(1) The level of extraneous bacterial contamination of the final unformulated viral insecticide should not exceed 107
colonies per gram as determined by an aerobic plate on trypticase soy agar.
(2) Human pathogens, e.g., Salmonella, Shigella, or Vibrio, must be absent.
(3) Safety to mice as determined by an intraperitoneal injection study must be demonstrated.
(4) Identity of the viral product, as determined by the most sensitive and standardized analytical technique, e.g.,
restriction endonuclease and/or SDS-PAGE analysis, must be demonstrated.
(c) Exemptions from the requirement of a tolerance are established for the residues of the microbial insecticide
Heliothis zea NPV, as specified in paragraphs (a) and (b) of this section, in or on all agricultural commodities.
[60 FR 42460, Aug. 16, 1995, as amended at 74 FR 26534, June 3, 2009]

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§180.1033 Methoprene; exemption from the requirement of a tolerance.
Methoprene is exempt from the requirement of a tolerance in or on all food commodities when used to control insect
larvae.
[68 FR 34829, June 11, 2003]

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§180.1037 Polybutenes; exemption from the requirement of a tolerance.
(a) Polybutenes are exempt from the requirement of a tolerance for residues in or on the raw agricultural commodity
cotton, undelinted seed when used as a sticker agent for formulations of the attractant gossyplure (1:1 mixture of (Z,Z)and (Z,E)-7,11-hexadecadien-1-ol acetate) to disrupt the mating of the pink bollworm.
(b) Polybutenes are exempt from the requirement of a tolerance for residues in or on the raw agricultural commodity
artichoke when used as a sticker agent in multi-layered laminted controlled-release dispensers of (Z)-11-hexaadecenal to
disrupt the mating of the artichoke plume moth.
[74 FR 26534, June 3, 2009]

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§180.1040 Ethylene glycol; exemption from the requirement of a tolerance.

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Ethylene glycol as a component of pesticide formulations is exempt from the requirement of a tolerance when used in
foliar applications to peanut plants.
[43 FR 41393, Sept. 18, 1978]

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§180.1041 Nosema locustae; exemption from the requirement of a tolerance.
The insecticide Nosema locustae is exempted from the requirement of a tolerance for residues in or on all raw
agricultural commodities.
[47 FR 21537, May 19, 1982]

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§180.1043 Gossyplure; exemption from the requirement of a tolerance.
The pheromone gossyplure, a 1:1 mixture of (Z,Z)- and (Z,E)-7,11-hexadecadien-1-ol acetate) is exempt from the
requirement of a tolerance in or on the raw agricultural commodity cotton, undelinted seed when applied to cotton from
capillary fibers.
[74 FR 26534, June 3, 2009]

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§180.1049 Carbon dioxide; exemption from the requirement of a tolerance.
The insecticide carbon dioxide is exempted from the requirement of a tolerance when used after harvest in modified
atmospheres for stored insect control on food commodities.
[65 FR 33716, May 24, 2000]

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§180.1050 Nitrogen; exemption from the requirements of a tolerance.
The insecticide nitrogen is exempted from the requirements of a tolerance when used after harvest in modified
atmospheres for stored product insect control on all food commodities.
[65 FR 33716, May 24, 2000]

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§180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine; exemption from the requirement of a tolerance.
2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine is exempted from the requirement of a tolerance when used as an
inert ingredient in formulations of the herbicides S-ethyl dipropylthiocarbamate, S-propyl dipropylthiocarbamate, and
S-ethyl diisobutylthiocarbamate applied to corn fields before the corn plants emerge from the soil with a maximum of 0.5
pound of the inert ingredient per acre.
[45 FR 51201, Aug. 1, 1980]

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§180.1054 Calcium hypochlorite; exemptions from the requirement of a tolerance.
(a) Calcium hypochlorite is exempted from the requirement of a tolerance when used preharvest or postharvest in
solution on all raw agricultural commodities.
(b) Calcium hypochlorite is exempted from the requirement of a tolerance in or on grape when used as a fumigant
postharvest by means of a chlorine generator pad.
[59 FR 59165, Nov. 16, 1994, as amended at 74 FR 26534, June 3, 2009]

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§180.1056 Boiled linseed oil; exemption from requirement of tolerance.
Boiled linseed oil (containing no more than 0.33 percent manganese naphthenate and no more than 0.33 percent
cobalt naphthenate) is exempt from the requirement of a tolerance when used as a coating agent for S-ethyl hexahydro-

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1H-azepine-1-carbothioate. No more than 15 percent of the pesticide formulation may consist of “boiled linseed oil.” This
exemption is limited to use on rice before edible parts form.
[46 FR 33270, June 29, 1981]

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§180.1057 Phytophthora palmivora; exemption from requirement of tolerance.
Phytophthora palmivora is exempted from the requirement of a tolerance in or on the raw agricultural commodity fruit,
citrus.
[74 FR 26534, June 3, 2009]

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§180.1058 Sodium diacetate; exemption from the requirement of a tolerance.
Sodium diacetate, when used postharvest as a fungicide, is exempt from the requirement of a tolerance for residues
in or on alfalfa, hay; Bermudagrass, hay; bluegrass, hay; bromegrass, hay; clover,hay; corm, field, grain; corn, pop, grain;
oat, grain; orchardgrass, hay; sorghum, grain, grain; sudangrass, hay; ryegrass, Italian, hay; timothy, hay.
[74 FR 26534, June 3, 2009]

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§180.1064 Tomato pinworm insect pheromone; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for combined residues of both components of the
tomato pinworm insect pheromone (E)-4-tridecen-1-yl acetate and (Z)-4-tridecen-1-yl acetate in or on all raw agricultural
commodities (preharvest) in accordance with the following prescribed conditions:
(a) Application shall be limited solely to point source dispensers or point source chopped fibers containing the tomato
pinworm insect pheromone.
(b) Cumulative yearly application cannot exceed 200 grams of tomato pinworm pheromone per acre.
[58 FR 34376, June 25, 1993]

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§180.1065 2-Amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one; exemption from the
requirement of a tolerance.
The inert ingredient, 2-amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one is exempted from the
requirement of a tolerance when used as an emetic at not more than 0.3 percent in formulations of paraquat dichloride.
Further restrictions on this exemption are that this ingredient may not be advertised as an emetic and the paraquat product
may not be promoted in any way because of the inclusion of this inert ingredient.
[70 FR 46431, Aug. 10, 2005]

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§180.1067 Methyl eugenol and malathion combination; exemption from the requirement of a tolerance.
The insect attractant methyl eugenol and the insecticide malathion are exempt from the requirement of tolerances on
all raw agricultural commodities when used in combination in Oriental fruit fly eradication programs under the authority of
the U.S. Department of Agriculture, in accordance with the following directions and specifications:
(a) The combination shall be at the ratio of three parts methyl eugenol to one part technical malathion (3:1).
(b) This combination is to be impregnated on a carrier (cigarette filter tips (cellulose acetate); cotton strings; fiberboard
squares) or mixed with a jel cleared under 40 CFR 180.920 or 180.950.
(c) The maximum actual dosage per application per acre shall be 28.35 grams (one ounce avoirdupois) methyl
eugenol and 9.45 grams (one-third (0.33) ounce avoirdupois) technical malathion.
[47 FR 9002, Mar. 3, 1982, as amended at 69 FR 23142, Apr. 28, 2004]

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§180.1068 C12-C18 fatty acid potassium salts; exemption from the requirement of a tolerance.
C12-C18 fatty acids (saturated and unsaturated) potassium salts are exempted from the requirement of a tolerance for
residues in or on all raw agricultural commodities when used in accordance with good agricultural practice.
[60 FR 34871, July 5, 1995]

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§180.1069 (Z)-11-Hexadecenal; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biological insecticide (pheromone)
(Z)-11-hexadecenal when used as a sex attractant on artichoke plants to control the artichoke plume moth.
[47 FR 14906, Apr. 7, 1982]

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§180.1070 Sodium chlorite; exemption from the requirement of a tolerance.
Sodium chlorite is exempted from the requirement of a tolerance for residues when used in accordance with good
agricultural practice as a seed-soak treatment in the growing of the raw agricultural commodities vegetable, brassica,
leafy, group 5 and radish, roots and radish, tops.
[74 FR 26534, June 3, 2009]

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§180.1071 Peanuts, Tree Nuts, Milk, Soybeans, Eggs, Fish, Crustacea, and Wheat; exemption from the
requirement of a tolerance.
(a) General. Residues resulting from the following uses of the food commodity forms of peanuts, tree nuts, milk,
soybeans, eggs (including putrescent eggs), fish, crustacea, and wheat are exempted from the requirement of a tolerance
in or on all food commodities under FFDCA section 408 (when used as either an inert or an active ingredient in a pesticide
formulation), if such use is in accordance with good agricultural practices:
(1) Use in pesticide products intended to treat seeds.
(2) Use in nursery and greenhouse operations, as defined in 40 CFR 170.3, which includes seeding, potting and
transplanting activities.
(3) Pre-plant and at-transplant applications.
(4) Incorporation into seedling and planting beds.
(5) Applications to cuttings and bare roots.
(6) Applications to the field that occur after the harvested crop has been removed.
(7) Soil-directed applications around and adjacent to all plants.
(8) Applications to rangelands, which is land, mostly grasslands, whose plants can provide food (i.e., forage) for
grazing or browsing animals.
(9) Use in chemigation and irrigation systems (via flood, drip, or furrow application with no overhead spray
applications).
(10) Application as part of a dry fertilizer on which an active ingredient is impregnated.
(11) Aerial and ground applications that occur when no above-ground harvestable food commodities are present
(usually pre-bloom).
(12) Application as part of an animal feed-through product.
(13) Applications as gel and solid (non-liquid/non-spray) crack and crevice treatments that place the gel or bait directly
into or on top of the cracks and crevices via a mechanism such as a syringe.
(14) Applications to the same crop from which the food commodity is derived, whether the plant fraction(s) intended
for harvest are present or not, e.g., applications of peanut meal when applied to peanut plants.

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(b) Specific chemical substances. Residues resulting from the use of the following substances as either an inert or an
active ingredient in a pesticide formulation are exempted from the requirement of a tolerance under FFDCA section 408, if
such use is in accordance with good agricultural practices and such use is included in paragraph (a):
Chemical Substance

CAS No.

Caseins
Caseins, ammonium complexes
Caseins, hydrolyzates
Caseins, potassium complexes
Caseins, sodium complexes

9000-71-9
9005-42-9
65072-00-6
68131-54-4
9005-46-3

[70 FR 1360, Jan. 7, 2005]

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§180.1072 Poly-D-glucosamine (chitosan); exemption from the requirement of a tolerance.
(a) An exemption from the requirement of a tolerance is established for residues of the biological plant growth
regulator poly-D-glucosamine when used as a seed treatment in or on barley, beans, oats, peas, rice, and wheat.
(b) An exemption from the requirement of a tolerance is established for residues of the biological plant growth
regulator poly-D-glucosamine when used as a pesticide in the production any raw agricultural commodity.
[60 FR 19524, Apr. 19, 1995]

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§180.1073 Isomate-M; exemption from the requirement of a tolerance.
The oriental fruit moth pheromone (Isomate-M) (Z-8-dodecen-l-yl acetate, E-8-dodecen-l-yl acetate, Z-8-dodecen-l-ol)
is exempt from the requirement of a tolerance in or on all the raw agricultural commodities (food and feed) including,
peach; quince; nectarine; and nut, macadamia when used in orchards with encapsulated polyethylene tubing to control
oriental fruit moth.
[74 FR 26534, June 3, 2009]

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§180.1074 F.D.&C. Blue No. 1; exemption from the requirement of a tolerance.
F.D.&C. Blue No. 1 is exempted from the requirement of a tolerance when used as an aquatic plant control agent.
[47 FR 25963, June 16, 1982]

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§180.1075 Colletotrichum gloeosporioides f. sp. aeschynomene; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the mycoherbicide Colletotrichum
gloeosporioides f. sp. aeschynomene in or on the following raw agricultural commodities:
COMMODITY
Aspirated grain fractions
Rice, grain
Soybean, forage
Soybean, hay
Soybean, seed
[47 FR 25742, June 15, 1982, as amended at 74 FR 26534, June 3, 2009]

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§180.1076 Viable spores of the microorganism Bacillus popilliae; exemption from the requirement of a tolerance.
(a) For the purposes of this section the microbial insecticide for which exemption from the requirement of a tolerance
is being established shall have the following specifications:

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(1) The microorganism shall be an authentic strain of Bacillus popilliae conforming to the morphological and
biochemical characteristics of Bacillus popilliae as described in Bergey's Manual of Determinative Bacteriology, Eighth
Edition.
(2) Spore preparations of Bacillus popilliae shall be produced by an extraction process from diseased Japanese
beetles, and may contain a small percentage of the naturally occurring milky disease bacterium Bacillus lentimorbus.
(3) Each lot of spore preparation, prior to the addition of other materials, shall be tested by subcutaneous injection of
at least 1 million spores into each of five laboratory test mice weighing 17 grams to 23 grams. Such test shall show no
evidence of infection of injury in the test animals when observed for 7 days following injection.
(b) Exemption from the requirement of a tolerance is established for residues of the microbial insecticide Bacillus
popilliae, as specified in paragraph (a) of this section in or on grass, pasture, forage and grass, rangeland, forage when it
is applied to growing crops in accordance with good agricultural practices.
[47 FR 38535, Sept. 1, 1982, as amended at 74 FR 26535, June 3, 2009]

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§180.1080 Plant volatiles and pheromone; exemptions from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the plant volatiles cyclic decadiene,
cyclic decene, cyclic pentadecatriene, and decatriene and the pheromone Z-2-isopropenyl-1-methylcyclobutaneethanol;
Z-3,3-dimethyl-Δ1,β-cyclohexaneethanol; Z-3,3-dimethyl-Δ1,α-cyclohexaneethanal; E-3,3-dimethylΔ1,α-cyclohexaneethanal combination when applied to cotton in hollow synthetic fibers.
[48 FR 28442, June 22, 1983]

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§180.1083 Dimethyl sulfoxide; exemption from the requirement of a tolerance.
Dimethyl sulfoxide (DMSO) [CAS Registry Number 67-68-5] is exempted from the requirement of a tolerance when
used as an inert solvent or cosolvent in formulations with the following pesticides when used in accordance with good
agricultural practices in or on the following raw agricultural commodities:
(a) Carbaryl (1-naphthyl methyl-carbamate)
Pea, dry, seed
Pea, succulent

(b) O-O-Diethyl O-(2-isopropyl-6-methyl-4-pyrimidinyl) phosphorothioate
Pea, dry, seed
Pea, succulent
[48 FR 54819, Dec. 7, 1983, as amended at 74 FR 26535, June 3, 2009]

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§180.1084 Monocarbamide dihydrogen sulfate; exemption from the requirement of a tolerance.
Monocarbamide dihydrogen sulfate is exempted from the requirement of a tolerance when used as a herbicide or
desiccant in or on all raw agricultural commodities.
[53 FR 12152, Apr. 13, 1988]

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§180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11-trimethyl-2,6,10-dodecatriene-3-ol; exemption
from the requirement of a tolerance.
The insect pheromone containing the active ingredients 3,7,11-trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11trimethyl-2,6,10-dodecatriene-3-ol is exempted from the requirement of a tolerance in or on all raw agricultural
commodities.
[52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. 5, 1987]

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§180.1087 Sesame stalks; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biorational nematicide sesame
stalk in or on the following raw agricultural commodities: Almond; almond, hulls; cotton, undelinted seed; cotton, gin
byproducts; soybean, seed; soybean, forage; soybean, hay; aspirated grain fractions; potato; beet, sugar, roots; beet,
sugar, tops; tomato; pepper, bell; squash; strawberry; eggplant; cucumber; carrot, roots; radish, roots; radish, top; turnip,
roots; turnip, tops; onion; pea, dry; pea, succulent; melon; grape; walnut; orange; grapefruit; mulberry; peach; apple;
apricot; blackberry; loganberry; pecan; cherry; plum, and cranberry.
[74 FR 26535, June 3, 2009]

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§180.1089 Poly-N-acetyl-D-glucosamine; exemption from the requirement of tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical nematicide
poly-N-acetyl-D-glucosamine on a variety of agricultural crops.
[53 FR 10249, Mar. 30, 1988]

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§180.1090 Lactic acid; exemption from the requirement of a tolerance.
Lactic acid (2-hydroxypropanoic acid) is exempted from the requirement of a tolerance when used as a plant growth
regulator in or on all raw agricultural commodities.
[53 FR 15286, May 4, 1988]

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§180.1091 Aluminum isopropoxide and aluminum secondary butoxide; exemption from the requirement of a
tolerance.
Aluminum isopropoxide (CAS Reg. No. 555-31-7) and aluminum secondary butoxide (CAS Reg. No. 2269-22-9) are
exempted from the requirement of a tolerance when used in accordance with good agricultural practices as stabilizers in
formulations of the insecticide amitraz [N′-(2,4-dimethylphenyl)-N-[[(2,4-dimethylphenyl)imino]-N-methylmethanimidamide]
applied to growing crops or animals.
[53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. 21, 1988]

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§180.1092 Menthol; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the pesticidal chemical menthol in or
on honey and honeycomb when used in accordance with good agricultural practice in over-wintering bee hives.
[74 FR 26535, June 3, 2009]

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§180.1095 Chlorine gas; exemptions from the requirement of a tolerance.
Chlorine gas is exempted from the requirement of a tolerance when used preharvest or postharvest in solution on all
raw agricultural commodities.
[56 FR 21309, May 8, 1991]

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§180.1097 GBM-ROPE; exemption from the requirement of a tolerance.
The grape berry moth pheromone (GBM-ROPE) containing the active ingredients (Z)-9-dedecenyl acetate and (Z)-11tetradecenyl acetate is exempt from the requirement of a tolerance in or on the raw agricultural commodity grape when
used in orchards with encapsulated polyethylene tubing to control grape berry moth.
[74 FR 26535, June 3, 2009]

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§180.1098 Gibberellins [Gibberellic Acids (GA3 and GA4 + GA7), and Sodium or Potassium Gibberellate];
exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of gibberellins [gibberellic acids (GA3
and GA4 + GA7), and sodium or potassium gibberellate] in or on all food commodities when used as plant regulators on
plants, seeds, or cuttings and on all food commodities after harvest in accordance with good agricultural practices.
[64 FR 31505, June 11, 1999]

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§180.1100 Gliocladium virens isolate GL-21; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biofungicide Gliocladium virens
GL-21 in or on all raw agricultural commodities when used either as a fungicide for inoculation of plant growth media in
greenhouses or on terrestrial food crops grown outdoors in accordance with good agricultural practices.
[60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. 5, 1995]

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§180.1101 Parasitic (parasitoid) and predatory insects; exemption from the requirement of a tolerance.
Parasitic (parasitoid) and predatory insects are exempted from the requirement of a tolerance for residues when they
are used in accordance with good agricultural and pest control practices to control insect pests of stored raw whole grains
such as corn, small grains, rice, soybeans, peanuts, and other legumes either bulk or warehoused in bags. For the
purposes of this rule, the parasites (parasitoids) and predators are considered to be species of Hymenoptera in the genera
Trichogramma, Trichogrammatidae; Bracon, Braconidae; Venturia, Mesostenus, Ichneumonidae; Anisopteromalus,
Choetospila, Lariophagus, Dibrachys, Habrocytus, Pteromalus, Pteromalidae; Cephalonomia, Holepyris, Laelius,
Bethylidae; and of Hemiptera in the genera Xylocoris, Lyctocoris, and Dufouriellus, Anthocoridae. Whole insects,
fragments, parts, and other residues of these parasites and predators remain subject to 21 U.S.C. 342(a)(3).
[57 FR 14646, Apr. 22, 1992]

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§180.1102 Trichoderma harzianum KRL-AG2 (ATCC #20847) strain T-22; exemption from requirement of a
tolerance.
An exemption from the requirement of a tolerance is established for residues of the biofungicide Trichoderma
harzianum KRL-AG2 (ATCC #20847); also known as strain T-22 when applied in/or on all food commodities.
[64 FR 16860, Apr. 7, 1999]

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§180.1103 Isomate-C; exemption from the requirement of a tolerance.
The codling moth pheromone (Isomate-C) E,E-8,10-dodecenyl alcohol, dodecanol, tetradecanol is exempt from the
requirements of a tolerance in or on all raw agricultural commodities when formulated in polyethylene pheromone
dispensers for use in orchards with encapsulated polyethylene tubing to control codling moth.
[74 FR 26535, June 3, 2009]

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§180.1107 Delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed Pseudomonas
fluorescens; exemption from the requirement of a tolerance.
The delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed Pseudomonas fluorescens is
exempt from the requirements of a tolerance in or on all raw agricultural commodities.
[56 FR 28328, June 20, 1991]

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§180.1108 Delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed Pseudomonas
fluorescens; exemption from the requirement of a tolerance.
The delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed Pseudomonas fluorescens is
exempt from the requirements of a tolerance in or on all raw agricultural commodities.

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[56 FR 28326, June 20, 1991]

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§180.1110 3-Carbamyl-2,4,5-trichlorobenzoic acid; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of 3-carbamyl-2,4,5-trichlorobenzoic
acid in or on all raw agricultural commodities which occur from the direct application of chlorothalonil to crops in §180.275
(a) and (b) and/or as an inadvertent residue resulting from the soil metabolism of chlorothalonil when applied to crops in
§180.275 (a) and (b), and subsequent uptake by rotated crops when used according to approved agricultural practices.
[57 FR 24552, June 10, 1992]

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§180.1111 Bacillus subtilis GB03; exemption from the requirement of a tolerance.
The biofungicide Bacillus subtilis GB03 is exempted from the requirement of a tolerance in or on all raw agricultural
commodities when used in accordance with good agricultural practices.
[73 FR 50556, Aug. 27, 2008]

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§180.1113 Lagenidium giganteum; exemption from the requirement of a tolerance.
Lagenidium giganteum (a fungal organism) is exempt from the requirement of a tolerance in or on the raw agricultural
commodities aspirated grain fractions; grass, forage; grass, hay; rice, grain; rice, straw; soybean, seed; soybean, forage;
soybean, hay; rice, wild, grain.
[74 FR 26535, June 3, 2009]

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§180.1114 Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and Pseudomonas syringae
742RS; exemptions from the requirement of a tolerance.
The biological pesticides Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and Pseudomonas
syringae 742RS are exempted from the requirement of a tolerance in or on all raw agricultural commodities when applied
as a frost protection agent or biological control agent to growing agricultural crops in accordance with good agricultural
practices.
[57 FR 42700, Sept. 16, 1992]

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§180.1118 Spodoptera exigua nuclear polyhedrosis virus; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the microbial pest control agent Spodoptera
exigua nuclear polyhedrosis virus when used as a pesticide control agent on all raw agricultural commodities.
[58 FR 25784, Apr. 28, 1993]

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§180.1119 Azadirachtin; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the biochemical azadirachtin, which is isolated
from the berries of the Neem tree (Azadirachta indica), when used as a pesticide at 20 grams or less per acre on all raw
agricultural commodities.
[58 FR 8696, Feb. 17, 1993]

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§180.1120 Streptomyces sp. strain K61; exemption from the requirement of a tolerance.
The biological pesticide Streptomyces sp. strain K61 is exempted from the requirement of a tolerance in or on all raw
agricultural commodities when used as a fungicide for the treatment of seeds, cuttings, transplants, and plants of
agricultural crops in accordance with good agricultural practices.
[58 FR 21403, Apr. 21, 1993]

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§180.1121 Boric acid and its salts, borax (sodium borate decahydrate), disodium octaborate tetrahydrate, boric
oxide (boric anhydride), sodium borate and sodium metaborate; exemptions from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the pesticidal chemical boric acid and
its salts, borax (sodium borate decahydrate), disodium octaborate tetrahydrate, boric oxide (boric anhydride), sodium
borate and sodium metaborate, in or on raw agricultural commodities when used as an active ingredient in insecticides,
herbicides, or fungicides preharvest or postharvest in accordance with good agricultural practices.
[58 FR 44283, Aug. 20, 1993]

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§180.1122 Inert ingredients of semiochemical dispensers; exemptions from the requirement of a tolerance.
(a) All inert ingredients of semiochemical dispenser products formulated with, and/or contained in, dispensers made of
polymeric matrix materials (including the monomers, plasticizers, dispersing agents, antioxidants, UV protectants,
stabilizers, and other inert ingredients) are exempted from the requirement of a tolerance when used as carriers in
pesticide formulations for application to growing crops only. These dispensers shall conform to the following specifications:
(1) Exposure must be limited to inadvertent physical contact only. The design of the dispenser must be such as to
preclude any contamination by its components of the raw agricultural commodity (RAC) or processed foods/feeds derived
from the commodity by virtue of its proximity to the RAC or as a result of its physical size.
(2) The dispensers must be applied discretely. This exemption does not apply to components of semiochemical
formulations applied in a broadcast manner either to a crop field plot or to individual plants.
(b) A semiochemical dispenser is a single enclosed or semi-enclosed unit that releases semiochemical(s) into the
surrounding atmosphere via volatilization and is applied in a manner to provide discrete application of the semiochemical
(s) into the environment.
(c) Semiochemicals are chemicals that are emitted by plants or animals and modify the behavior of receiving
organisms. These chemicals must be naturally occurring or substantially identical to naturally occurring semiochemicals.
[58 FR 64494, Dec. 8, 1993]

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§180.1124 Arthropod pheromones; exemption from the requirement of a tolerance.
Arthropod pheromones, as described in §152.25(b) of this chapter, when used in retrievably sized polymeric matrix
dispensers are exempt from the requirement of a tolerance in or on all raw agricultural commodities when applied to
growing crops only at a rate not to exceed 150 grams active ingredient/acre/year in accordance with good agricultural
practices.
[59 FR 14759, Mar. 30, 1994]

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§180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the insect pheromone codlure, (E,E)-8,10dodecadien-1-ol, on all raw agricultural commodities in accordance with the following prescribed conditions:
(a) Application shall be limited solely to codlure dispensers that conform to the following specifications:
(1) Commodity exposure must be limited to inadvertent physical contact. The design of the dispenser must be such as
to preclude any exposure of its components to the raw agricultural commodity (RAC) or processed foods/feeds derived
from the commodity due to its proximity to the RAC or as a result of its physical size. Dispensers must be of such size and
construction that they are readily recognized post-application.
(2) The dispensers must be applied discretely, i.e., placed in the field in easily perceived distinct locations in a manner
that does not prevent later retrieval. This exemption does not apply to codlure applied in a broadcast manner either to a
crop field plot or to individual plants.
(b) A codlure dispenser is a single enclosed or semi-enclosed unit that releases codlure into the surrounding
atmosphere via volatilization and is applied in a manner to provide discrete application (i.e., in easily perceived distinct
locations in a manner that does not prevent later retrieval) of the codlure into the environment.
[59 FR 9931, Mar. 2, 1994]

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§180.1127 Biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde, cinnamyl alcohol,
4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole, and
1,2,4-trimethoxybenzene; exemptions from the requirement of a tolerance.
Residues of the biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde, cinnamyl alcohol,
4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole, and 1,2,4-trimethoxybenzene are
exempt from the requirement of a tolerance in or on the following raw agricultural commodities: the following field
crops—alfalfa, clover, cotton, dandelion, peanuts (including hay), rice, sorghum (milo), soybeans, sunflower, sweet
potatoes, and wheat; the following vegetable crops—asparagus, beans (including forage hay), beets, carrots, celery, cole
crops (cabbage, broccoli, brussels sprouts, cauliflower), collards (kale, mustard greens, turnip greens, kohlrabi), corn,
fresh (field, sweet, pop, seed), corn fodder and forage, chinese cabbage, cowpeas, cucurbitis (cucumbers, squash,
pumpkin), egg plant, endive (escarole), horseradish (radish, rutabagas, turnip roots), leafy greens (spinach, swiss chard),
lettuce (head leaf), okra, parsley, parsnip, peas, peas with pods, peppers, potatoes, sugar beets, tomatoes; the following
tree fruit, berry and nut crops—almonds, apples, apricots, berries (blackberry, boysenberry, dewberry, loganberry,
raspberry), blueberry, cherry, citrus (grapefruit, kumquat, lemon, lime, orange, tangelo, and tangerine) cranberry, grapes,
melons, (watermelon, honeydew, crenshaw, cantaloupe, casaba, persian), nectarines, pears, pecans, peaches, and
strawberry as dispersed from the end-use product Corn Rootworm Bait®, a pesticidal bait, in accordance with the
prescribed conditions in paragraph (a) of this section.
(a) Cumulative yearly application cannot exceed 20 grams of each floral attractant/acre/application.
(b) [Reserved]
[59 FR 15857, Apr. 5, 1994]

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§180.1128 Bacillus subtilis MBI 600; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biofungicide Bacillus subtilis MBI
600 in or on all food commodities, including residues resulting from post-harvest uses, when applied or used in
accordance with good agricultural practices.
[74 FR 15869, Apr. 8, 2009]

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§180.1130 N-(n-octyl)-2-pyrrolidone and N-(n-dodecyl)-2-pyrrolidone; exemptions from the requirement of a
tolerance.
(a) N-(n-octyl)-2-pyrrolidone and N-(n-dodecyl)-2-pyrrolidone are exempt from the requirement of a tolerance when
used as solvents in cotton defoliant formulations containing thidiazuron and diuron as active ingredients.
(b) N-(n-octyl)-2-pyrrolidone is exempt from the requirement of a tolerance when used as a solvent in formulations
containing pyraflufen-ethyl as an active ingredient at a concentration not to exceed 20% by weight.
[79 FR 10682, Feb. 26, 2014]

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§180.1131 Ampelomyces quisqualis isolate M10; exemption from the requirement of a tolerance.
The biological fungicide Ampelomyces quisqualis isolate M10 is exempted from the requirement of a tolerance in or
on all raw agricultural commodities when used as a fungicide on agricultural crops in accordance with good agricultural
practices.
[59 FR 33437, June 29, 1994]

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§180.1135 Pasteuria penetrans; exemption from the requirement of a tolerance.
The biological nematicide Pasteuria penetrans is exempted from the requirement of a tolerance in or on all raw
agricultural commodities, except roots and tubers, when used as a nematicide in the production of fruits and vegetables in
greenhouses.
[59 FR 66741, Dec. 28, 1994]

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§180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of a tolerance.
The biochemical sodium 5-nitroguiacolate is exempted from the requirement of a tolerance when used as a plant
growth regulator in end-use products at a concentration of 0.1% by weight and applied at an application rate of 20 g of a.i.
per acre or less per application, in or on all food commodities.
[65 FR 66181, Nov. 3, 2000]

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§180.1140 Sodium o-nitrophenolate; exemption from the requirement of a tolerance.
The biochemical sodium o-nitrophenolate is exempted from the requirement of a tolerance when used as a plant
growth regulator in end-use products at a concentration of 0.2% by weight and applied at an application rate of 20 g of a.i.
per acre or less per application, in or on all food commodities.
[65 FR 66181, Nov. 3, 2000]

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§180.1141 Sodium p-nitrophenolate; exemption from the requirement of a tolerance.
The biochemical sodium p-nitrophenolate is exempted from the requirement of a tolerance when used as a plant
growth regulator in end-use product at a concentration of 0.3% by weight and applied at an application rate of 20 g of a.i.
per acre or less per application, in or on all food commodities.
[65 FR 66181, Nov. 3, 2000]

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§180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of the plant growth regulator,
1,4-dimethylnaphthalene (1,4-DMN), when applied postharvest to all sprouting root, tuber, and bulb crops in accordance
with good agricultural practices.
[77 FR 68697, Nov. 16, 2012]

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§180.1143 Methyl anthranilate; exemption from the requirement of a tolerance.
Residues of methyl anthranilate, a biochemical pesticide, are exempt from the requirement of a tolerance in or on all
food commodities, when used in accordance with good agricultural practices.
[67 FR 51088, Aug. 7, 2002]

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§180.1144 Candida oleophila isolate I-182; exemption from the requirement of a tolerance.
Candida oleophila isolate I-182, when used as a post-harvest biological fungicide, is exempted from the requirement
of a tolerance in or on all raw agricultural commodities.
[60 FR 11033, Mar. 1, 1995]

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§180.1145 Pseudomonas syringae; exemption from the requirement of a tolerance.
Pseudomonas syringae is exempted from the requirement of a tolerance on all raw agricultural commodities when
applied postharvest according to good agricultural practices.
[60 FR 12703, Mar. 8, 1995]

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§180.1146 Beauveria bassiana Strain GHA; exemption from the requirement of a tolerance.
Beauveria bassiana Strain GHA is exempted from the requirement of a tolerance in or on all raw agricultural
commodities when applied to growing crops according to good agricultural practices.
[60 FR 18547, Apr. 12, 1995]

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§180.1148 Occlusion Bodies of the Granulosis Virus of Cydia pomenella; tolerance exemption.
An exemption from the requirement of a tolerance is established for residues of the microbial pest control agent
Occlusion Bodies of the Granulosis Virus of Cydia pomonella (codling moth) in or on all raw agricultural commodities.
[60 FR 42450, Aug. 16, 1995]

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§180.1149 Inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha falcifera; exemption from the
requirement of a tolerance.
The microbial pest control agent inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha falcifera is
exempted from the requirement of a tolerance in or on all raw agricultural commodities when used to control certain
lepidopteran pest species.
[60 FR 37020, July 19, 1995]

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§180.1150 6-Benzyladenine; exemption from the requirement of a tolerance.
The biochemical plant regulator 6-benzyladenine (6-BA) is exempt from the requirement of a tolerance in or on apple
and pear when applied at a rate of ≤182 grams of active ingredient per acre per season, and in or on pistachio when
applied at a rate of ≤60 grams of active ingredient per acre per season.
[72 FR 13179, Mar. 21, 2007]

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§180.1153 Lepidopteran pheromones; exemption from the requirement of a tolerance.
Lepidopteran pheromones that are naturally occurring compounds, or identical or substantially similar synthetic
compounds, designated by an unbranched aliphatic chain (between 9 and 18 carbons) ending in an alcohol, aldehyde or
acetate functional group and containing up to 3 double bonds in the aliphatic backbone, are exempt from the requirement
of a tolerance in or on all raw agricultural commodities. This exemption only pertains to those situations when the
pheromone is: Applied to growing crops at a rate not to exceed 150 grams active ingredient/acre/year in accordance with
good agricultural practices; and applied as a post-harvest treatment to stored food commodities at a rate not to exceed 3.5
grams active ingredient/1,000 ft2/year (equivalent to 150 grams active ingredient/acre/year) in accordance with good
agricultural practices.
[71 FR 45399, Aug. 9, 2006]

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§180.1154 CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki encapsulated in
killed Pseudomonas fluorescens, and the expression plasmid and cloning vector genetic constructs.
CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki encapsulated in killed
Pseudomonas fluorescens and the expression plasmid and cloning vector genetic constructs are exempt from the
requirement of a tolerance when used in or on all raw agricultural commodities.
[60 FR 47489, Sept. 13, 1995]

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§180.1156 Cinnamaldehyde; exemption from the requirement of a tolerance.
Cinnamaldehyde (3-phenyl-2-propenal) is exempted from the requirement of a tolerance in or on all food
commodities, when used as a fungicide, insecticide, and algaecide in accordance with good agricultual practices.
[64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, 1999]

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§180.1157 Cytokinins; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of cytokinins (specifically: aqueous
extract of seaweed meal and kinetin) in or on all food commodities when used as plant regulators on plants, seeds, or
cuttings and on all food commodities after harvest in accordance with good agricultural practices.

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[64 FR 31505, June 11, 1999]

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§180.1158 Auxins; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of auxins (specifically: indole-3-acetic
acid and indole-3-butyric acid) in or on all food commodities when used as plant regulators on plants, seeds, or cuttings
and on all food commodities after harvest in accordance with good agricultural practices.
[64 FR 31505, June 11, 1999]

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§180.1159 Pelargonic acid; exemption from the requirement of tolerances.
(a) An exemption from the requirement of a tolerance is established for residues of pelargonic acid in or on all food
commodities when used as a plant regulator on plants, seeds, or cuttings and on all food commodities after harvest in
accordance with good agricultural practices.
(b) Pelargonic acid when used as an herbicide is exempt from the requirement of a tolerance on all plant food
commodities provided that:
(1) Applications are not made directly to the food commodity except when used as a harvest aid or desiccant to: any
root and tuber vegetable, bulb vegetable or cotton.
(2) When pelargonic acid is used as a harvest aid or desiccant, applications must be made no later than 24 hours
prior to harvest.
(c) An exemption from the requirement of a tolerance is established for residues of pelargonic acid in or on all raw
agricultural commodities and in processed commodities, when such residues result from the use of pelargonic acid as an
antimicrobial treatment in solutions containing a diluted end-use concentration of pelargonic acid up to 170 ppm per
application on food contact surfaces such as equipment, pipelines, tanks, vats, fillers, evaporators, pasteurizers and
aseptic equipment in restaurants, food service operations, dairies, breweries, wineries, beverage and food processing
plants.
[62 FR 28364, May 23, 1997, as amended at 64 FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, 2003]

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§180.1160 Jojoba oil; exemption from the requirement of a tolerance.
The insecticide and spray tank adjuvant jojoba oil is exempted from the requirement of a tolerance in or on all raw
agricultural commodities when applied at the rate of 1.0% or less of the final spray in accordance with good agricultural
practices, provided the jojoba oil does not contain simmondsin, simmondsin-2-ferulate, and related conjugated
organonitriles including demethyl simmondsin and didemethylsimmondsin.
[61 FR 2121, Jan. 25, 1996]

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§180.1161 Clarified hydrophobic extract of neem oil; exemption from the requirement of a tolerance.
Clarified hydrophobic extract of neem oil is exempt from the requirement of a tolerance on all food commodities when
used as a botanical fungicide/insecticide/miticide.
[67 FR 43552, June 28, 2002]

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§180.1162 Acrylate polymers and copolymers; exemption from the requirement of a tolerance.
(a) Acrylate polymers and copolymers are exempt from the requirement of a tolerance when used as inert ingredients
in pesticidal formulations applied to growing, raw agricultural commodities. This tolerance exemption covers the acrylate
polymers/copolymers that are intrinsically safe and already listed in TSCA inventory or will meet the polymer tolerance
exemption from requirements of premanufacturing notification under 40 CFR 723.250. Polymers exempted can be used as
dispensers, resins, fibers, and beads, as long as the fibers, beads and resins particle sizes are greater than 10 microns
and insoluble in water. This exemption pertains to the acrylate polymers/copolymers used as inert ingredients for
sprayable and dispenser pesticide formulations that are applied on food crops. Any acrylate polymers/copolymers used for
encapsulating material must be cleared as an inert ingredient when used in pesticide formulation applied on food crops.

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(b) For the purposes of this exemption, acrylate polymers/copolymers used as inert ingredients in an end-use
formulation must meet the definition for a polymer as given in 40 CFR 723.250(b), are not automatically excluded by 40
723.250(d), and meet the tolerance exemption criteria in 40 CFR 723.250(e)(1), 40 CFR 723.250 (e)(2) or 40 CFR
723.250(e)(3). Therefore, acrylate polymers and copolymers that are already listed in the TSCA inventory or will meet the
polymer tolerance exemption under 40 CFR 723.250 as amended on March 29, 1995 are covered by this exemption.
[61 FR 6551, Feb. 21, 1996]

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§180.1163 Killed Myrothecium verrucaria; exemption from the requirement of a tolerance.
Killed Myrothecium verrucaria is exempted from the requirement of a tolerance in or on all raw agricultural
commodities when applied as a pre-seed or pre- or post-planting soil treatment alone or mixed with water and the mixed
suspension be applied through drip or border irrigation systems and the indicator mycotoxin levels do not exceed 15 ppm.
[61 FR 11315, Mar. 20, 1996, as amended at 61 FR 58332, Nov. 14, 1996]

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§180.1165 Capsaicin; exemption from the requirement of a tolerance.
Capsaicin is exempt from the requirement of a tolerance in or on all food commodities when used in accordance with
approved label rates and good agricultural practice.
[63 FR 39521, July 23, 1998]

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§180.1167 Allyl isothiocyanate as a component of food grade oil of mustard; exemption from the requirement of
a tolerance.
The insecticide and repellent Allyl isothiocyanate is exempt from the requirement of a tolerance for residues when
used as a component of food grade oil of mustard, in or on all raw agricultural commodities, when applied according to
approved labeling.
[61 FR 24894, May 17, 1996]

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§180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance.
The biochemical pesticide sodium bicarbonate is exempted from the requirement of a tolerance in or on all raw
agricultural commodities when applied as a fungicide or post-harvest fungicide in accordance with good agricultural
practices.
[61 FR 67473, Dec. 23, 1996]

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§180.1177 Potassium bicarbonate; exemption from the requirement of a tolerance.
The biochemical pesticide potassium bicarbonate is exempted from the requirement of a tolerance in or on all raw
agricultural commodities when applied as a fungicide or post-harvest fungicide in accordance with good agricultural
practices.
[61 FR 67473, Dec. 23, 1996]

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§180.1178 Formic acid; exemption from the requirement of a tolerance.
The pesticide formic acid is exempted from the requirement of a tolerance in or on honey and honeycomb when used
to control tracheal mites and suppress varroa mites in bee colonies, and applied in accordance with label use directions.
[74 FR 26535, June 3, 2009]

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§180.1179 Plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and Rhizophoria
mangle; exemption from the requirement of a tolerance.

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The biochemical pesticide plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and
Rhizophoria mangle is exempted from the requirement of a tolerance in or on all raw agricultural commodities when
applied as a nematicide/plant regulator in accordance with good agricultural practices.
[62 FR 24842, May 7, 1997]

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§180.1180 Kaolin; exemption from the requirement of a tolerance.
(a) The biochemical pesticide kaolin is temporarily exempted from the requirement of a tolerance for residues of the
insecticide Kaolin, when used on crops (apples, apricots, bananas, beans, cane berries, citrus fruits, corn, cotton,
cranberries, cucurbits, grapes, melons, nuts, ornamentals, peaches, peanuts, pears, peppers, plums, potatoes, seed
crops, small grains, soybeans, strawberries, sugar beets, and tomatoes) to control certain insect, fungus, and bacterial
damage to plants. This temporary exemption from the requirement of a tolerance will permit the marketing of the food
commodities in this paragraph when treated in accordance with the provisions of experimental use permit 70060-EUP-1,
which is being issued under the Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA), as amended (7 U.S.C. 136).
This temporary exemption from the requirement of a tolerance expires and is revoked December 31, 1999. This temporary
exemption from the requirement of a tolerance may be revoked at any time if the experimental use permit is revoked or if
any experience with or scientific data on this pesticide indicate that the tolerance is not safe.
(b) Kaolin is exempted from the requirement of a tolerance for residues when used on or in food commodities to aid in
the control of insects, fungi, and bacteria (food/feed use).
[62 FR 19685, Apr. 23, 1997, as amended at 63 FR 9430, Feb. 25, 1998]

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§180.1181 Bacillus cereus strain BPO1; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance for residues of the Bacillus cereus strain BPO1 in or on all raw
agricultural commodities when applied/used in accordance with label directions.
[67 FR 70017, Nov. 20, 2002]

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§180.1187 L-glutamic acid; exemption from the requirement of a tolerance.
L-glutamic acid is exempt from the requirement of a tolerance on all food commodities when used in accordance with
good agricultural practices.
[66 FR 33198, June 21, 2001]

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§180.1188 Gamma aminobutyric acid; exemption from the requirement of a tolerance.
Gamma aminobutyric acid is exempt from the requirement of a tolerance on all food commodities when used in
accordance with good agricultural practices.
[66 FR 33198, June 21, 2001]

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§180.1189 Methyl salicylate; exemption from the requirement of a tolerance.
The biochemical pesticide methyl salicylate is exempt from the requirement of a tolerance for residues in or on food or
feed when used as an insect repellant in food packaging and animal feed packaging at an application rate that does not
exceed 0.2 mg of methyl salicylate per square inch of packaging materials.
[62 FR 61639, Nov. 19, 1997]

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§180.1191 Ferric phosphate; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide, ferric
phosphate (FePO4, CAS No. 11045-86-0) in or on all food commodities.
[62 FR 56105, Oct. 29, 1997]

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§180.1193 Potassium dihydrogen phosphate; exemption from the requirement of a tolerance.
Potassium dihydrogen phosphate is exempted from the requirement of a tolerance in or on all food commodities when
applied as a fungicide in accordance with good agricultural practices.
[63 FR 43085, Aug. 12, 1998]

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§180.1195 Titanium dioxide.
Titanium dioxide (CAS Reg. No. 13463-67-7) is exempted from the requirement of a tolerance for residues in or on
growing crops, when used as an inert ingredient (UV protectant) in microencapsulated formulations of the insecticide
lambda cyhalothrin at no more than 3.0% by weight of the formulation and as an inert ingredient (UV-stabilizer) at no more
than 5% in pesticide formulations containing the active ingredient napropamide.
[77 FR 44155, July 27, 2012]

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§180.1196 Peroxyacetic acid; exemption from the requirement of a tolerance.
(a) An exemption from the requirement of a tolerance is established for residues of peroxyacetic acid in or on all food
commodities, when such residues result from the use of peroxyacetic acid as an antimicrobial treatment in solutions
containing a diluted end use concentration of peroxyacetic acid up to 100 ppm per application on fruits, vegetables, tree
nuts, cereal grains, herbs, and spices.
(b) An exemption from the requirement of a tolerance is established for residues of peroxyacetic acid, in or on all food
commodities when used in sanitizing solutions containing a diluted end-use concentration of peroxyacetic acid up to 500
ppm, and applied to tableware, utensils, dishes, pipelines, tanks, vats, fillers, evaporators, pasteurizers, aseptic
equipment, milking equipment, and other food processing equipment in food handling establishments including, but not
limited to dairies, dairy barns, restaurants, food service operations, breweries, wineries, and beverage and food
processing plants.
(c) An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide
peroxyacetic acid and its metabolites and degradates, including hydrogen peroxide and acetic acid, in or on all food
commodities, when used in accordance with good agricultural practices.
[74 FR 26535, June 3, 2009, as amended at 76 FR 11969, Mar. 4, 2011]

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§180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of hydrogen peroxide in or on all food
commodities at the rate of ≤1% hydrogen peroxide per application on growing and postharvest crops.
[67 FR 41844, June 20, 2002]

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§180.1198 Gliocladium catenulatum strain J1446; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide, Gliocladium
catenulatum strain J1446 when used in or on all food commodities.
[63 FR 37288, July 10, 1998]

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§180.1199 Lysophosphatidylethanolamine (LPE); exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide
lysophosphatidylethanolamine in or on all food commodities.
[67 FR 17636, Apr. 11, 2002]

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§180.1200 Pseudomonas fluorescens strain PRA-25; temporary exemption from the requirement of a tolerance.
A temporary exemption from the requirement of a tolerance is established for residues of the microbial pesticide,
pseudomonas fluorescens strain PRA-25 when used on peas, snap beans and sweet corn and will expire July 31, 2001.
[63 FR 38498, July 17, 1998]

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§180.1201 Trichoderma harzianum strain T-39; exemption from the requirement of a tolerance.
Trichoderma harzianum strain T-39 is exempt from the requirement of a tolerance on all food commodities.
[65 FR 38757, June 22, 2000]

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§180.1202 Bacillus sphaericus; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticides, Bacillus
sphaericus when used in or on all food crops.
[63 FR 48597, Sept. 11, 1998]

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§180.1204 Harpin protein; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of individual harpin proteins that meet
specified physiochemical and toxicological criteria when used as biochemical pesticides on all food commodities to
enhance plant growth, quality and yield, to improve overall plant health, and to aid in pest management. The
physiochemical and toxicological criteria identifying harpin proteins are as follows:
(a) Consists of a protein less than 100 kD in size, that is acidic (pI<7.0), glycine rich (>10%), and contains no more
than one cystine residue.
(b) The source(s) of genetic material encoding the protein are bacterial plant pathogens not known to be mammalian
pathogens.
(c) Elicits the hypersensitive response (HR) which is characterized as rapid, localized cell death in plant tissue after
infiltration of harpin into the intercellular spaces of plant leaves.
(d) Possesses a common secondary structure consisting of α and β units that form an HR domain.
(e) Is heat stable (retains HR activity when heated to 65 °C for 20 minutes).
(f) Is readily degraded by a proteinase representative of environmental conditions (no protein fragments >3.5 kD after
15 minutes degradation with Subtilisin A).
(g) Exhibits a rat acute oral toxicity (LD50) of greater than 5,000 mg product/kg body weight.
[69 FR 24996, May 5, 2004]

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§180.1205 Beauveria bassiana ATCC #74040; exemption from the requirements of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the insecticide Beauveria bassiana
(ATCC #74040) in or on all food commodities when applied or used as ground and aerial foliar sprays for use only on
terrestrial crops.
[64 FR 22796, Apr. 28, 1999]

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§180.1206 Aspergillus flavus AF36; exemption from the requirement of a tolerance.
(a) An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Aspergillus
flavus AF36 in or on cotton, gin byproducts; cotton, hulls; cotton, meal; cotton, refined oil; cotton, undelinted seed.
(b) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus AF36 in or on
pistachio when applied as an antifungal agent and used in accordance with good agricultural practices.

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(c) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus AF36 in or on
corn, field, forage; corn, field, grain; corn, field, stover; corn, field, aspirated grain fractions; corn, sweet, kernel plus cob
with husk removed; corn, sweet, forage; corn, sweet, stover; corn, pop, grain; and corn, pop, stover, when applied/used as
an antifungal agent.
[68 FR 41541, July 14, 2003, as amended at 72 FR 28871, May 23, 2007; 72 FR 72965, Dec. 26, 2007; 74 FR 26535, 26546, June
3, 2009; 76 FR 16301, Mar. 23, 2011; 77 FR 14291, Mar. 9, 2012]

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§180.1207 N-acyl sarcosines and sodium N-acyl sarcosinates; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the following substances when used
as inert ingredients (surfactants) at levels not to exceed 10% in pesticide formulations containing glyphosate:
Name

CAS Reg. No.

N-acyl sarcosines
N-cocoyl sarcosine mixture
N-lauroyl sarcosine
N-myristoyl sarcosine
N-oleoyl sarcosine
N-stearoyl sarcosine
Sodium N-acyl sarcosinates
N-cocoyl sarcosine sodium salt mixture
N-methyl-N-(1-oxo-9-octodecenyl) glycine
N-methyl-N-(1-oxododecyl) glycine
N-methyl-N-(1-oxooctadecyl) glycine
N-methyl-N-(1-oxotetradecyl glycine

68411-97-2
97-78-9
52558-73-3
110-25-8
142-48-3
61791-59-1
3624-77-9
137-16-6
5136-55-0
30364-51-3

[64 FR 68046, Dec. 6, 1999]

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§180.1209 Bacillus subtilis strain QST 713 and strain QST 713 variant soil; exemption from the requirement of a
tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticides Bacillus
subtilis strain QST 713 and strain QST 713 variant soil when used in or on all food commodities.
[77 FR 73937, Dec. 12, 2012]

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§180.1210 Phosphorous acid; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of phosphorous acid and its ammonium,
sodium, and potassium salts in or on all food commodities when used as an agricultural fungicide and in or on potatoes
when applied as a post-harvest treatment at 35,600 ppm or less phosphorous acid.
[71 FR 49373, Aug. 23, 2006]

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§180.1212 Pseudomonas chlororaphis Strain 63-28; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Pseudomonas
chlororaphis Strain 63-28 in or on all food commodities.
[66 FR 53346, Oct. 22, 2001]

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§180.1213 Coniothyrium minitans strain CON/M/91-08; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Coniothyrium
minitans strain CON/M/91-08 when used in or on all food commodities.
[66 FR 16874, Mar. 28, 2001]

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§180.1218 Indian Meal Moth Granulosis Virus; exemption from the requirement of a tolerance.

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An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Indian Meal
Moth Granulosis Virus when used in or on all food commodities.
[68 FR 55875, Sept. 29, 2003]

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§180.1219 Foramsulfuron; exemption from the requirement of a tolerance.
The pesticide foramsulfuron is exempted from the requirement of a tolerance in corn, field, grain/corn, field, forage/
corn, field, stover/corn, pop, grain/corn, pop, forage/corn, pop, stover; corn, sweet, forage; corn, sweet, kernel plus cob
with husks removed; corn, sweet, stover when applied as a herbicide in accordance with good agricultural practices.
[74 FR 26535, June 3, 2009]

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§180.1220 1-Methylcyclopropene; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the 1-Methylcyclopropene in or on
fruits and vegetables when:
(a) Used as a post harvest plant growth regulator, i.e., for the purpose of inhibiting the effects of ethylene.
(b) Applied or used outdoors for pre-harvest treatments.
[73 FR 19150, Apr. 9, 2008]

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§180.1221 Pseudozyma flocculosa strain PF-A22 UL; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Pseudozyma flocculosa strain PF-A22
UL in or on all food commodities.
[67 FR 60966, Sept. 27, 2002]

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§180.1222 Sucrose octanoate esters; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of sucrose octanoate esters [(α-Dglucopyranosyl-β-D-fructofuranosyl-octanoate), mono-, di-, and triesters of sucrose octanoate] in or on all food
commodities when used in accordance with good agricultural practices.
[67 FR 60152, Sept. 25, 2002]

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§180.1223 Imazamox; exemption from the requirement of a tolerance.
The herbicide imazamox, (±) 2, -[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(methoxymethyl)-3pyridinecarboxylic acid, is exempt from the requirement of a tolerance on all food commodities when applied as a
herbicide in accordance with good agricultural practices.
[68 FR 7433, Feb. 14, 2003]

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§180.1224 Bacillus pumilus GB34; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Bacillus
pumilus GB34 when used as a seed treatment in or on all food commodities. An exemption is also granted for such
residues on treated but unplanted soybean seeds.
[69 FR 76625, Dec. 22, 2004]

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§180.1225 Decanoic acid; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of decanoic acid in or on all raw
agricultural commodities and in processed commodities, when such residues result from the use of decanoic acid as an

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antimicrobial treatment in solutions containing a diluted end-use concentration of decanoic acid (up to 170 ppm per
application) on food contact surfaces such as equipment, pipelines, tanks, vats, fillers, evaporators, pasteurizers and
aseptic equipment in restaurants, food service operations, dairies, breweries, wineries, beverage and food processing
plants.
[68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, 2003]

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§180.1226 Bacillus pumilus strain QST2808; temporary exemption from the requirement of a tolerance.
A temporary exemption from the requirement of a tolerance is established for residues of the microbial pesticide
Bacillus pumilus strain QST2808 when used in or on all agricultural commodities when applied/used in accordance with
label directions.
[68 FR 36480, June 18, 2003]

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§180.1228 Diallyl sulfides; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of diallyl sulfides when used in/on garlic,
leeks, onions, and shallots.
[68 FR 40808, July 9, 2003]

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§180.1230 Ferrous sulfate; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of ferrous sulfate.
[70 FR 33363, June 8, 2005]

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§180.1231 Lime; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of lime.
[70 FR 33363, June 8, 2005]

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§180.1232 Lime-sulfur; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of lime-sulfur.
[70 FR 33363, June 8, 2005]

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§180.1233 Potassium sorbate; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of potassium sorbate.
[70 FR 33363, June 8, 2005]

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§180.1234 Sodium carbonate; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of sodium carbonate.
[70 FR 33363, June 8, 2005]

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§180.1235 Sodium hypochlorite; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of sodium hypochlorite.
[70 FR 33363, June 8, 2005]

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§180.1236 Sulfur; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of sulfur.
[70 FR 33363, June 8, 2005]

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§180.1237 Sodium metasilicate; exemption from the requirement of a tolerance.
(a) An exemption from the requirement of a tolerance is established for residues of sodium metasilicate in or on all
food commodities when used in accordance with approved label rates and good agricultural practices as a plant desiccant,
so long as the sodium metasilicate does not exceed 4% by weight in aqueous solution.
(b) An exemption from the requirement of a tolerance is established for residues of sodium metasilicate in or on all
food commodities when used in accordance with approved label rates and good agricultural practices as an insecticide
and fungicide, so long as the sodium metasilicate does not exceed 2.41% by weight in aqueous solution.
[71 FR 19441, Apr. 14, 2006]

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§180.1240 Thymol; exemption from the requirement of a tolerance.
(a) Time-limited exemptions from the requirement of a tolerance are established for residues of thymol on honey and
honeycomb in connection with use of the pesticide under section 18 emergency exemptions granted by the EPA. These
time-limited exemptions from the requirement of a tolerance for residues of thymol will expire and are revoked on June 30,
2007.
(b) An exemption from the requirement of a tolerance for residues of the thymol (as present in thyme oil) in or on food
commodities when applied/used in/on public eating places, dairy processing equipment, and/or food processing
equipment and utensils.
[70 FR 37696, June 30, 2005, as amended at 71 FR 2895, Jan. 18, 2006; 74 FR 12617, Mar. 25, 2009]

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§180.1241 Eucalyptus oil; exemption from the requirement of a tolerance.
Time-limited exemptions from the requirement of a tolerance are established for residues of eucalyptus oil on honey
and honeycomb in connection with use of the pesticide under section 18 emergency exemptions granted by the EPA.
These time-limited exemptions from the requirement of a tolerance for residues of eucalyptus oil will expire and are
revoked on June 30, 2007.
[70 FR 37696, June 30, 2005]

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§180.1243 Bacillus subtilis var. amyloliquefaciens strain FZB24; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance for residues of the Bacillus subtilis var. amyloliquefaciens strain
FZB24 in or on all agricultural commodities when applied/used in accordance with label directions.
[68 FR 44640, July 30, 2003]

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§180.1244 Ammonium bicarbonate; exemption from the requirement of a tolerance.
An exemption from the requirement of tolerance is established for residues of ammonium bicarbonate used in or on
all food commodities when used in accordance with good agricultural practices.
[69 FR 13745, Mar. 24, 2004]

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§180.1245 Rhamnolipid biosurfactant; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of rhamnolipid biosurfactant when used
in accordance with good agricultural practices as a fungicide in or on all food commodities.

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[69 FR 16800, Mar. 31, 2004]

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§180.1246 Yeast Extract Hydrolysate from Saccharomyces cerevisiae: exemption from the requirement of a
tolerance.
This regulation establishes an exemption from the requirement of a tolerance for residues of the biochemical pesticide
Yeast Extract Hydrolysate from Saccharomyces cerevisiae on all food commodities when applied/used for the
management of plant diseases.
[69 FR 9958, Mar. 3, 2004]

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§180.1248 Exemption of citronellol from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide citronellol in
or on all food commodities.
[69 FR 23146, Apr. 28, 2004]

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§180.1250 C8, C10, and C12 fatty acid monoesters of glycerol and propylene glycol; exemption from the
requirement of a tolerance.
The C8, C10, and C12 straight-chain fatty acid monoesters of glycerol (glycerol monocaprylate, glycerol
monocaprate, and glycerol monolaurate) and propylene glycol (propylene glycol monocaprylate, propylene glycol
monocaprate, and propylene glycol monolaurate) are exempt from the requirement of a tolerance in or on all food
commodities when used in accordance with approved label rates and good agricultural practice.
[69 FR 34944, June 23, 2004]

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§180.1251 Geraniol; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide geraniol in
or on all food commodities.
[69 FR 23151, Apr. 28, 2004]

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§180.1253 Streptomyces lydicus WYEC 108; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Streptomyces
lydicus WYEC 108 when used in or on all agricultural commodities when applied/used in accordance with label directions.
[69 FR 31301, June 3, 2004]

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§180.1254 Aspergillus flavus NRRL 21882; exemption from the requirement of a tolerance.
(a) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus NRRL 21882 on
peanut; peanut, hay; peanut, meal; and peanut, refined oil.
(b) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus NRRL 21882 on
corn, field, forage; corn, field, grain; corn, field, stover; corn, field, aspirated grain fractions; corn, sweet, kernel plus cob
with husk removed; corn, sweet, forage; corn, sweet, stover; corn, pop, grain; and corn, pop, stover.
[75 FR 6576, Feb. 10, 2010]

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§180.1255 Bacillus pumilus strain QST 2808; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Bacillus
pumilus strain QST 2808 when used in or on all agricultural commodities when applied/used in accordance with label
directions.

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[69 FR 63954, Nov. 3, 2004]

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§180.1256 Alternaria destruens strain 059; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Alternaria
destruens Strain 059 when used in or on all raw agricultural commodities when applied/used in accordance with label
directions.
[70 FR 28459, May 18, 2005]

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§180.1257 Paecilomyces lilacinus strain 251; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Paecilomyces
lilacinus strain 251 when used in or on all agricultural commodities when applied/used in accordance with label directions.
[70 FR 19283, Apr. 13, 2005]

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§180.1258 Acetic acid; exemption from the requirement of a tolerance.
(a) An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide acetic
acid when used as a preservative on post-harvest agricultural commodities intended for animal feed, including Alfalfa,
seed; alfalfa, hay; barley, grain; bermudagrass, hay; bluegrass, hay; bromegrass, hay; clover, hay; corn, field, grain; corn,
pop, grain; cowpea, hay; fescue, hay; lespedeza, hay; lupin; oat, grain; orchardgrass, hay; peanut, hay; timothy, hay;
vetch, hay; and wheat, grain, or commodities described as grain or hay.
(b) An exemption from the requirement of a tolerance is established for residues of acetic acid in or on all food crops
resulting from unintentional spray and drift to non-target vegetation including non-food, food and feed crops when used as
a non-selective contact herbicide spray.
[75 FR 40741, July 14, 2010]

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§180.1259 Reynoutria sachalinensis extract; exemption from the requirement of a tolerance.
Residues of the biochemical pesticide Reynoutria sachalinensis extract, when derived from the whole plant extract,
are exempt from the requirement of a tolerance in or on all food commodities.
[70 FR 55277, Sept. 21, 2005]

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§180.1260 Muscodor albus QST 20799 and the volatiles produced on rehydration; exemption from the
requirement of a tolerance.
An exemption from the requirement of a tolerance is established on all food/feed commodities, for residues of
Muscodor albus QST 20799, and the volatiles produced on its rehydration, when the pesticide is used for all agricultural
applications, including seed, propagule and post harvest treatments.
[70 FR 56576, Sept. 28, 2005]

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§180.1261 Xanthomonas campestris pv. vesicatoria and Pseudomonas syringae pv. tomato specific
Bacteriophages.
An exemption from the requirement of a tolerance is established for residues of Xanthomonas campestris pv.
vesicatoria and Pseudomonas syringae pv. tomato specific bacteriophages in or on pepper and tomato.
[74 FR 26536, June 3, 2009]

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§180.1262 Sorbitol octanoate; exemption from the requirement of a tolerance.

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An exemption from the requirement of a tolerance is established for residues of sorbitol octanoate in or on all food
commodities when used in accordance with label directions.
[71 FR 4518, Jan. 27, 2006]

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§180.1263 Tetrahydrofurfuryl alcohol; exemption from the requirement of a tolerance.
Tetrahydrofurfuryl alcohol (THFA, CAS Reg. No. 97-99-4) is exempt from the requirement of a tolerance in or on all
raw agricultural commodities when used in accordance with good agricultural practices as an inert ingredient applied only:
(a) For use as a seed treatment.
(b) For applications prior to planting and at the time of planting.
(c) For use on cotton.
(d) For use in herbicides with one application to wheat and barley prior to the pre-boot stage, and two applications to
canola and soybeans pre-bloom.
(e) For use in herbicides with two applications to field corn up to 24 inches tall (V 5 stage).
[71 FR 45415, Aug. 9, 2006]

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§180.1267 Pantoea agglomerans strain C9-1; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Pantoea agglomerans strain C9-1
when used on apples and pears.
[71 FR 24596, Apr. 26, 2006]

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§180.1268 Potassium silicate; exemption from the requirement of a tolerance.
Potassium silicate is exempt from the requirement of a tolerance in or on all food commodities so long as the
potassium silicate is not applied at rates exceeding 1% by weight in aqueous solution and when used in accordance with
good agricultural practices.
[71 FR 34272, June 14, 2006]

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§180.1269 Bacillus mycoides isolate J; exemption from the requirement of a tolerance.
Bacillus mycoides isolate J is temporarily exempt from the requirement of a tolerance when used as a fungicide on
potatoes in accordance with a valid Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA) section 18 emergency
exemption. This temporary exemption from the requirement of a tolerance expires and is revoked on December 31, 2015.
[78 FR 24353, Apr. 25, 2013]

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§180.1270 Isophorone; exemption from the requirement of a tolerance.
Isophorone (CAS Reg. No. 78-59-1) is exempt from the requirement of a tolerance when used as an inert ingredient
in pesticide formulations applied to beets, ginseng, rice, spinach, sugar beets, and Swiss chard.
[71 FR 45408, Aug. 9, 2006]

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§180.1271 Eucalyptus oil; exemption from the requirement of a tolerance.
An exemption from the requirement of tolerance is established for residues of eucalyptus oil in or on honey,
honeycomb, and honeycomb with honey when used at 2g or less eucalyptus oil per hive, where the eucalyptus oil
contains 80% or more eucalyptol.
[71 FR 53979, Sept. 13, 2006]

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§180.1272 Pantoea agglomerans strain E325; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Pantoea agglomerans strain E325
when used on apples and pears.
[71 FR 54933, Sept. 20, 2006]

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§180.1273 Beauveria bassiana HF23; exemption from the requirement of a tolerance.
Residues of Beauveria bassiana HF23 are exempt from the requirement of a tolerance on all food/feed commodities,
when the pesticide is used for the treatment of chicken and livestock facilities, including the treatment of chicken and
livestock manure.
[75 FR 10190, Mar. 5, 2010]

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§180.1274 Tris (2-ethylhexyl) phosphate; exemption from the requirement of a tolerance.
Tris (2-ethylhexyl) phosphate (TEHP, CAS Reg. No. 78-42-2) is exempt from the requirement of a tolerance for
residues in grain, aspirated fractions; barley, grain, barley, hay, barley, straw; wheat, grain; wheat, forage; wheat, hay;
wheat, straw when used under the following conditions:
(a) The use is in accordance with good agricultural practices;
(b) Tris (2-ethylhexyl) phosphate is used as an inert ingredient in pesticide formulations with the active ingredients
pinoxaden, clodinafop-propargyl, and tralkoxydium;
(c) Tris (2-ethylhexyl) phosphate is applied no more than twice per season; and
(d) The applications occur no later than the pre-boot stage (prior to formation of edible grain).
[72 FR 5624, Feb. 7, 2007, as amended at 74 FR 26536, June 3, 2009]

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§180.1275 Pythium; exception from the requirement of a tolerance.
An exemption from the requirement of tolerance is established on all food/feed commodities, for residues of pythium
oligandrum DV 74 when the pesticide is used on food crops.
[72 FR 27452, May 16, 2007]

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§180.1276 Tobacco mild green mosaic tobamovirus strain U2; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Tobacco mild green mosaic
tobamovirus strain U2 in or on all commodities of crop groups 17 and 18 when applied as a post-emergent herbicide and
used in accordance with label directions and good agricultural practices.
[79 FR 75756, Dec. 19, 2014]

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§180.1277 Dibasic esters; exemption from the requirement of a tolerance.
Dibasic esters (CAS Reg. No. 95481-62-2) is exempted from the requirement of a tolerance for residues when used
as an inert ingredient (solvent and/or anti-freeze) at 10% W/W or less in microencapsulated pesticide formulations with the
active ingredient cyfluthrin.
[73 FR 10398, Feb. 27, 2008]

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§180.1278 Quillaja saponaria extract (saponins); exemption from the requirement of a tolerance.

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Residues of the biochemical pesticide Quillaja saponaria extract (saponins) are exempt from the requirement of a
tolerance in or on all food commodities.
[72 FR 41935, Aug. 1, 2007]

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§180.1279 Zucchini yellow mosaic virus—weak strain; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance for residues of the ZYMV-WK strain in or on all raw cucurbit when
applied/used in accordance with label directions.
[74 FR 26536, June 3, 2009]

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§180.1280 Poly(hexamethylenebiguanide) hydrochloride (PHMB); exemption from the requirement of a tolerance.
Poly(hexamethylenebiguanide) hydrochloride (PHMB)(CAS Reg. No. 32289-58-0) is exempt from the requirement of
a tolerance for residues of the antimicrobial in or on all food commodities when the residues are the result of the lawful
application of a food contact surface sanitizer containing PHMB at 550 parts per million (ppm).
[73 FR 1517, Jan. 9, 2008]

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§180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy-2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)-3-methyl-penta-(2Z,4E)
-dienoic Acid; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of S-Abscisic Acid in or on all food
commodities when applied or used preharvest as a plant regulator.
[75 FR 11744, Mar. 12, 2010]

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§180.1282 Bacillus firmus I-1582; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established in/on all food/feed commodities, for residues of
Bacillus firmus I-1582 when used as a soil application or seed treatment.
[73 FR 25528, May 7, 2008]

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§180.1283 (Z)-7,8-epoxy-2-methyloctadecane (Disparlure); exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of (Z)-7,8-epoxy-2-methyloctadecane on
all food and feed crops that occur when it is used to treat trees, shrubs, and pastures and such use results in unintentional
spray and drift to non-target vegetation including non-food, food, and feed crops. This active ingredient is also known as
Disparlure.
[73 FR 33714, June 13, 2008]

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§180.1284 Ammonium salts of higher fatty acids (C8-C18 saturated; C8-C12 unsaturated); exemption from the
requirement of a tolerance.
Ammonium salts of C8-C18 saturated and C8-C12 unsaturated higher fatty acids are exempted from the requirement of
a tolerance for residues in or on all food commodities when used in accordance with good agricultural practice.
[74 FR 47457, Sept. 16, 2009]

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§180.1285 Polyoxin D zinc salt; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of polyoxin D zinc salt in or on all
food commodities when applied as a fungicide and used in accordance with good agricultural practices.
[77 FR 56133, Sept. 12, 2012]

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§180.1287 Extract of Chenopodium ambrosioides near ambrosioides; exemption from the requirement of a
tolerance.
An exemption from the requirement of a tolerance is established for the residues of Extract of Chenopodium
ambrosioides near ambrosioides when used as an insecticide/acaricide on all food commodities.
[74 FR 634, Jan. 7, 2009]

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§180.1288 Tristyrylphenol ethoxylates; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of poly(oxy-1,2-ethanediyl), α-[2,4,6-tris
(1-phenylethyl)phenyl]-ω-hydroxy-, (CAS Reg. No. 70559-25-0) and poly(oxy-1,2-ethanediyl), α-[tris(1-phenylethyl)phenyl]
-ω-hydroxy-, (CAS Reg. No. 99734-09-5) on citrus crops, group 10, when used as inert ingredients under the following
conditions:
(a) They are applied post-harvest;
(b) They are used as inert ingredients in pesticide formulations with azoxystrobin and fludioxonil; and
(c) They constitute no more than 10.0% of the formulated pesticide product.
[74 FR 12625, Mar. 25, 2009]

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§180.1289 Candida oleophila Strain O; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of the microbial pesticide, Candida
oleophila Strain O, on apples and pears when applied/used as a post-harvest biofungicide.
[74 FR 22464, May 13, 2009]

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§180.1290 Pasteuria usgae; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Pasteuria usgae in or on all food
commodities when applied preharvest and used as a nematicide in accordance with good agricultural practices.
[75 FR 37737, June 30, 2010]

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§180.1291 Cold pressed neem oil; exemption from the requirement of a tolerance.
Residues of the biochemical pesticide cold pressed neem oil are exempt from the requirement of a tolerance in or on
all food commodities.
[74 FR 55463, Oct. 28, 2009]

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§180.1292 Ulocladium oudemansii (U3 Strain); exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established in/on all food commodities for residues of Ulocladium
oudemansii (U3 Strain), when applied or used pre-harvest-only, excluding applications made post-harvest or to processed
commodities, as a microbial fungicide in accordance with good agricultural practices.
[74 FR 55458, Oct. 28, 2009]

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§180.1293 Trichoderma gamsii strain ICC 080; exemption from the requirement of a tolerance.
Trichoderma gamsii strain ICC 080 is exempted from the requirement of a tolerance in or on all food and feed
commodities when applied preharvest and used in accordance with good agricultural practices.
[75 FR 8507, Feb. 25, 2010]

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§180.1294 Trichoderma asperellum strain ICC 012; exemption from the requirement of a tolerance.
Trichoderma asperellum strain ICC 012 is exempted from the requirement of a tolerance in or on all food and feed
commodities when applied pre-harvest and used in accordance with good agricultural practices.
[75 FR 9530, Mar. 3, 2010]

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§180.1295 Laminarin; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of laminarin in or on all food
commodities when laminarin is applied preharvest.
[75 FR 8256, Feb. 24, 2010]

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§180.1296 Terpene Constituents α-terpinene, d-limonene and p-cymene, of the Extract of Chenopodium
ambrosioides near ambrosioides as Synthetically Manufactured; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of the biochemical pesticide Terpene
Constituents α-terpinene, d-limonene and p-cymene, of the Extract of Chenopodium ambrosioides near ambrosioides as
Synthetically Manufactured when used as an insecticide/acaricide in or on all food commodities.
[75 FR 39455, July 9, 2010]

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§180.1297 Homobrassinolide; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of homobrassinolide in or on all food
commodities when applied/used as a plant growth regulator in accordance with good agricultural practices.
[75 FR 39459, July 9, 2010]

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§180.1298 Trichoderma hamatum isolate 382; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Trichoderma hamatum isolate 382 in
or on all food commodities when applied as a fungicide and used in accordance with good agricultural practices.
[75 FR 43076, July 23, 2010]

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§180.1299 Prohydrojasmon; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide
prohydrojasmon (PDJ), propyl-3-oxo-2-pentylcyclo-pentylacetate, when used as a plant growth regulator in or on apple
and grape pre-harvest, in accordance with label directions and good agricultural practices.
[78 FR 75257, Dec. 11, 2013]

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§180.1300 Potassium hypochlorite; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of potassium hypochlorite in or on all
commodities.
[76 FR 11343, Mar. 2, 2011]

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§180.1301 Escherichia coli O157:H7 specific bacteriophages; temporary exemption from the requirement of a
tolerance.
A temporary exemption from the requirement of a tolerance is established for residues of lytic bacteriophages that are
specific to Escherichia coli O157:H7, sequence negative for shiga toxins I and II, and grown on atoxigenic host bacteria

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when used/applied on food contact surfaces in food processing plants in accordance with the terms of Experimental Use
Permit (EUP) No. 74234-EUP-2. This temporary exemption expires on April 1, 2013.
[76 FR 20546, Apr. 13, 2011]

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§180.1302 Sodium Ferric Ethylenediaminetetraacetate (EDTA); exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of sodium ferric EDTA in or on all food
commodities when applied as a molluscicide and used in accordance with good agricultural practices.
[76 FR 17561, Mar. 30, 2011]

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§180.1303 Metarhizium anisopliae strain F52; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Metarhizium anisopliae strain F52 in
or on all food commodities when applied as an insecticide, miticide, or ixodicide and used in accordance with good
agricultural practices.
[76 FR 26198, May 6, 2011]

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§180.1304 Pseudomonas fluorescens strain CL145A; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Pseudomonas fluorescens strain
CL145A in or on all food commodities when applied as a molluscicide.
[76 FR 52875, Aug. 24, 2011]

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§180.1305 Chromobacterium subtsugae strain PRAA4-1T; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Chromobacterium subtsugae strain
PRAA4-1T in or on all food commodities when applied as an insecticide or miticide and used in accordance with good
agricultural practices.
[76 FR 55272, Sept. 7, 2011]

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§180.1306 Isaria fumosorosea (formerly Paecilomyces fumosoroseus) Apopka strain 97; exemption from the
requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Isaria fumosorosea (formerly
Paecilomyces fumosoroseus) Apopka strain 97 in or on all food commodities when applied as an insecticide or miticide
and used in accordance with good agricultural practices.
[76 FR 59905, Sept. 28, 2011]

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§180.1307 Bacteriophage of Clavibacter michiganensis subspecies michiganensis; exemption from the
requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of lytic bacteriophage of Clavibacter
michiganensis subspecies michiganensis produced in Clavibacter michiganensis subspecies michiganensis in or on
tomato when applied as a bactericide in accordance with good agricultural practices.
[76 FR 66192, Oct. 26, 2011]

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§180.1308 Bacillus amyloliquefaciens strain D747; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide, Bacillus
amyloliquefaciens strain D747 in or on all food commodities when used in accordance with good agricultural practices.

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[77 FR 749, Jan. 6, 2012. Redesignated at 77 FR 2911, Jan. 20, 2012]

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§180.1309 Bacillus subtilis strain CX-9060; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Bacillus
subtilis strain CX-9060, in or on all food commodities, when applied or used in accordance with good agricultural practices.
[77 FR 1637, Jan. 11, 2012]

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§180.1310 Trichoderma virens strain G-41; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Trichoderma virens strain G-41, in or
on all food commodities, when applied as a fungicide and used in accordance with good agricultural practices.
[77 FR 4908, Feb. 1, 2012]

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§180.1311 Pasteuria nishizawae—Pn1; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Pasteuria nishizawae—Pn1 in or on
all food commodities when applied as a nematicide and used in accordance with good agricultural practices.
[77 FR 8741, Feb. 15, 2012]

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§180.1312 Aureobasidium pullulans strains DSM 14940 and DSM 14941; exemption from the requirement of a
tolerance.
An exemption from the requirement of a tolerance is established for residues of Aureobasidium pullulans strains DSM
14940 and DSM 14941 in or on all food commodities when used in accordance with label directions and good agricultural
practices.
[80 FR 73662, Nov. 25, 2015]

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§180.1313 Bacillus pumilus strain GHA 180; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Bacillus pumilus strain GHA 180 in or
on all food commodities when used in accordance with good agricultural practices.
[77 FR 19112, Mar. 30, 2012]

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§180.1314 Killed, nonviable Streptomyces acidiscabies strain RL-110T; exemption from the requirement of a
tolerance.
An exemption from the requirement of a tolerance is established for residues of killed, nonviable Streptomyces
acidiscabies strain RL-110T in or on all food commodities when applied as a pre- or post-emergent herbicide and used in
accordance with good agricultural practices.
[77 FR 35295, June 13, 2012]

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§180.1315 Natamycin; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of natamycin in or on mushrooms when
applied as a fungistat to prevent the germination of fungal spores on mushrooms produced in enclosed mushroom
production facilities, and in or on pineapples when applied as a fungistat in accordance with label directions and good
agricultural practices.
[79 FR 75068, Dec. 17, 2014]

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§180.1316 Pasteuria spp. (Rotylenchulus reniformis nematode)—Pr3; exemption from the requirement of a
tolerance.
An exemption from the requirement of a tolerance is established for residues of Pasteuria spp. (Rotylenchulus
reniformis nematode)—Pr3 in or on all food commodities when applied as a nematicide and used in accordance with label
directions and good agricultural practices.
[77 FR 40276, July 9, 2012]

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§180.1317 Pesticide chemicals; exemption from the requirements of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Didecyl dimethyl ammonium chloride
in or on broccoli resulting from the use of Didecyl dimethyl ammonium chloride as a seed treatment at a treatment
concentration of 1200 ppm prior to planting by immersion.
[77 FR 47296, Aug. 8, 2012]

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§180.1318 3-decen-2-one; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide, 3-decen-2one, in or on potatoes when applied as a potato sprout inhibitor and used in accordance with label directions and good
agricultural practices.
[78 FR 11766, Feb. 20, 2013]

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§180.1319 Banda de Lupinus albus doce (BLAD); exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of Banda de Lupinus albus doce
(BLAD), a naturally occurring polypeptide from the catabolism of a seed storage protein (β-conglutin) of sweet lupines
(Lupinus albus), in or on all food commodities when applied as a fungicide and used in accordance with label directions
and good agricultural practices.
[78 FR 17604, Mar. 22, 2013]

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§180.1320 Methyl jasmonate; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of methyl jasmonate in or on all food
commodities when methyl jasmonate is applied pre-harvest.
[78 FR 22794, Apr. 17, 2013]

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§180.1321 Complex Polymeric Polyhydroxy Acids; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for the residues of complex polymeric polyhydroxy
acids in or on all food commodities when applied as a plant growth regulator and used in accordance with good
agricultural practices.
[78 FR 46267, July 31, 2013]

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§180.1322 Bacillus pumilus strain BU F-33; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Bacillus pumilus strain BU F-33 in or
on all food commodities when applied to elicit induced systemic resistance in plants and used in accordance with label
directions and good agricultural practices.
[78 FR 35149, June 12, 2013]

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§180.1323 Ethyl-2E,4Z-decadienoate (Pear Ester); exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide, ethyl2E,4Z-decadienoate (pear ester), in or on all food commodities, when used in accordance with label directions and good
agricultural practices.
[78 FR 53054, Aug. 28, 2013]

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§180.1324 GS-omega/kappa-Hxtx-Hv1a; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the pesticide GS-omega/kappa-HxtxHv1a in or on all food commodities when applied or used in accordance with label directions and good agricultural
practices.
[79 FR 10685, Feb. 26, 2014]

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§180.1325 Heat-killed Burkholderia spp. strain A396 cells and spent fermentation media exemption from the
requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of heat-killed Burkholderia spp. strain
A396 cells and spent fermentation media in or on all food commodities when applied as a biological insecticide to
agricultural crops and used in accordance with label directions and good agricultural practices.
[79 FR 15704, Mar. 21, 2014]

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§180.1326 Pseudomonas fluorescens strain D7; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Pseudomonas fluorescens strain D7
in or on all food commodities when used in accordance with label directions and good agricultural practices.
[79 FR 60750, Oct. 8, 2014]

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§180.1327 Tetraacetylethylenediamine (TAED) and its metabolite Diacetylethylenediamine (DAED); exemption
from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the pesticide,
tetraacetylethylenediamine (TAED), and its metabolite diacetylethylenediamine (DAED), in or on rice and strawberries,
when used as a fungicide and bactericide in accordance with label directions and good agricultural practices.
[79 FR 59121, Oct. 1, 2014]

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§180.1328 Beauveria bassiana strain ANT-03; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Beauveria bassiana strain ANT-03 in
or on all food commodities, when applied as a microbial insecticide and used in accordance with label directions and good
agricultural practices.
[79 FR 77396, Dec. 24, 2014]

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§180.1329 Bacillus subtilis strain IAB/BS03, exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Bacillus subtilis strain IAB/BS03 in or
on all food commodities when used in accordance with label directions and good agricultural practices.
[80 FR 9217, Feb. 20, 2015]

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§180.1330 1-Octanol; exemption from the requirement of a tolerance.

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Page 440 of 441

An exemption from the requirement of a tolerance is established for residues of 1-octanol in or on root and tuber
vegetables when applied as a plant growth regulator in accordance with label directions and good agricultural practices.
[80 FR 25953, May 6, 2015]

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§180.1331 Trichoderma asperelloides strain JM41R; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of Trichoderma asperelloides strain
JM41R in or on all food commodities when used in accordance with label directions and good agricultural practices.
[80 FR 28203, May 18, 2015]

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§180.1332 Lavandulyl senecioate; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the arthropod pheromone, lavandulyl
senecioate (5-methyl-2-(1-methylethenyl)-4-hexenyl 3-methyl-2-butonate), in or on all raw agricultural commodities when
applied or used in microbeads/dispensers at a rate not to exceed 150 grams active ingredient/acre/year in accordance
with good agricultural practices.
[80 FR 49171, Aug. 17, 2015]

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§180.1333 Potassium Salts of Hops Beta acids; exemption from the requirement of a tolerance.
An exemption from the requirement of a tolerance is established for residues of the biochemical potassium salts of
hops beta acids in or on honey and honeycomb, when used for the control of Varroa mites in accordance with label
directions and good agricultural practices.
[80 FR 63683, Oct. 21, 2015]

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Subpart E—Pesticide Chemicals Not Requiring a Tolerance or an Exemption From a
Tolerance
SOURCE: 66 FR 66772, Dec. 27, 2001, unless otherwise noted.

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§180.2000 Scope.
This subpart sets forth the pesticide chemicals for use in agricultural or other food-related settings for which neither a
tolerance nor an exemption is deemed to be needed by EPA.
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§180.2003 Definitions.
(a) Food uses are the uses of a pesticide chemical that are likely to yield residues in food or feed crops, meat, milk,
poultry or egg.
(b) Non-food uses are those uses that are not likely to yield residues in food or feed crops, meat, milk, poultry or egg.
[66 FR 66772, Dec. 27, 2001, as amended at 73 FR 60158, Oct. 10, 2008]

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§180.2010 Threshold of regulation determinations.
The following pesticide chemical uses on food or feed, or food or feed crops, do not need a tolerance or exemption
from the requirement of a tolerance, and may be registered under the Federal Insecticide, Fungicide, and Rodenticide Act,
7 U.S.C. 136 et seq., without obtaining such tolerance or exemption, based on EPA's determination that the uses are
below the threshold of regulation.
Pesticide
Chemical

CAS
Reg.
No.

Use/Limits

Analytical Method

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Thiabendazole

148- As a seed treatment for dry pea (including field pea, pigeon
79-8 pea, chickpea or lentil), using a maximum application rate of
0.075 pounds of active ingredient per 100 pounds of seed.
Vines or hay grown from treated seed may not be fed to
livestock.

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High Performance Liquid Chromatography/Florescence Detector
method1; Modification of Ion-Pairing Liquid Chromatographic
Determination of Benzimidazole Fungicides in Foods, Gilvydis and
Walters, JAOAC, vol. 73, no. 5, 1990.

1
Available from: Chief, Analytical Chemistry Branch, Environmental Science Center, 701 Mapes Rd., Ft. Meade, MD
20755-5350; telephone number: (410) 305-2905; e-mail address: [email protected]

[73 FR 1978, Jan. 11, 2008]

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§180.2020 Non-food determinations.
The following pesticide chemical uses do not need a tolerance or exemption from the requirement of a tolerance
based on EPA's determination that they are not likely to result in residues in or on food.
Pesticide Chemical
Methyl bromide
Potassium triiodide (KI3)
Rhodamine B

CAS Reg. No.
Limits
Uses
74-83-9
When applied as a pre-plant soil fumigant
All pre-plant soil uses
12298-68-9
When applied to growing crops in foreign countries
Bananas, grapes, and melons
81-88-9
Not to exceed 2% by weight of the formulated product and 60 ppm on the treated seed Dye for seed treatment

[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]

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