| 1,000 ppm ECA Marine Fuel Sulfur Precision Demonstration [ECA0300 : OMB #2060-0731, Expires 1/31/2024]. This collection of information is approved by OMB under the Paperwork Reduction Act, 44 U.S.C. 3501 et seq. OMB Control No 2060-0731. Responses to this collection of information are voluntary 1090 CFR 1360 through 1090 1365. An agency may not conduct or sponsor, and a person is not required to respond to, a collection of information unless it displays a currently valid OMB control number. The public reporting and recordkeeping burden for this collection of information is estimated to average 180 hours per response. SSend comments on the Agency’s need for this information, the accuracy of the provided burden estimates and any suggested methods for minimizing respondent burden to the Regulatory Support Division Director, U.S. Environmental Protection Agency (2821T), 1200 Pennsylvania Ave., NW, Washington, D.C. 20460. Include the OMB control number in any correspondence. Do not send the completed form to this address. |
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| 1,000 ppm Sulfur Precision Criterion (§1090.1360(b)) - a standard deviation less than 20.1 ppm, computed from the results of a minimum of 20 repeat tests made over 20 days on samples taken from a single homogenous commerically available ECA Marine fuel with a sulfur range of 700 to 1,000 ppm. A lab facility may exclude a given sample or test result only if the exclusion is for a valid reason under good laboratory practices and it maintains records regarding the sample and test results and the reason for excluding them. You may make up to 4 separate measurements in a 24-hour period, as long as the interval between measurements is at least 4 hours. $1090.1350(a)(2) $1090.1360(a)(2) & §1090.1365(b)(3) Table 1. |
| Is 1,000 ppm Sulfur Precision Criterion Met? |
REQUIRED DATA MISSING |
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| standard deviation |
REQUIRED DATA MISSING |
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| Laboratory Test Identification Number |
Date |
Time |
Test Result (ppm) |
Data Entry QC Check on Test Result |
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DATA REQUIRED IN CELL D20 |
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| 1,000 ppm ECA Marine Fuel Sulfur Accuracy Demonstration [ECA0300 : OMB #2060-0731, EPA ICR number 2607.02: Expires 1/31/2024] |
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| Confidential Business Information Claim. A company may assert a business confidentiality claim covering the information contained in this submission. If no such claim is made the information may be made available to the public by EPA without further notice. All questions of confidentiality will be handled pursuant to 40 CFR Part 2. Is confidentiality claimed for the information in this submission? (Note: Please answer by typing "Yes" or "No" in the adjacent cell.) |
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| 900 to 1,000 ppm Accuracy Criterion (§1090.1365(c)(3)(ii)) - the arithmetic average of a continuous series of at least 10 tests performed on a commercially available gravimetric sulfur standard in the range of 900 to 1000 ppm sulfur shall not differ from the accepted reference value (ARV) of that standard by more than 15.075 ppm. Individual test results shall be compensated for any known chemical interferences. $1090.1350(a)(2) $1090.1360(a)(2)& §1090.1365(c)(3) Table 1. |
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| Accuracy Criterion for 900-1,000 ppm |
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| gravimetric sulfur standard |
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| Is 900-1,000 ppm Sulfur Accuracy Criterion Met? |
REQUIRED DATA MISSING |
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| Arithmetic Average (ppm) |
REQUIRED DATA MISSING |
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| Vendor Name of Gravimetric Standard |
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| Lot Identification Number of Gravimetric Standard |
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Concentration QC Check on ARV |
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| Accepted Reference Value (ARV) of Gravimetric Standard (ppm) |
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ARV TOO LOW IN CONCENTRATION |
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| Difference between Arithmetic Average and ARV of Gravimetric Standard |
REQUIRED DATA MISSING |
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| Laboratory Test Identification Number |
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Time |
Test Result (ppm) |
Data Entry QC Check on Test Result |
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DATA REQUIRED IN CELL J26 |
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| 1,000 ppm ECA Marine Fuel Sulfur Precision Demonstration [ECA0300 : OMB #2060-0731, EPA ICR number 2607.02: Expires 1/31/2024] |
| Test Method |
| Name of Method: |
Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry |
| Organization ID No. (as in ASTM D XXXX-XX): |
ASTM D2622-10 |
| Laboratory Identification |
| Laboratory Name: |
USEPA National and Vehicle Fuels Emissions Laboratory/OAR |
| Laboratory Street Address: |
2565 Plymouth Road, Mailcode AATSG |
| Laboratory City: |
Ann Arbor |
| Laboratory State: |
Michigan |
| Laboratory Zip code: |
48105 |
| Laboratory Contact Person: |
John Doe |
| Laboratory Contact Phone Number |
xxx-xxx-xxxx |
| Laboratory Contact Facsimile Number |
xxx-xxx-xxxx |
| Laboratory Contact E-mail Address |
[email protected] |
| 1,000 ppm Sulfur Precision Criterion (§1090.1365(b)) - a standard deviation less than 20.1 ppm, computed from the results of a minimum of 20 repeat tests made over 20 days on samples taken from a single homogenous commerically available ECA Marine fuel with a sulfur range of 700 to 1,000 ppm. A lab facility may exclude a given sample or test result only if the exclusion is for a valid reason under good laboratory practices and it maintains records regarding the sample and test results and the reason for excluding them. You may make up to 4 separate measurements in a 24-hour period, as long as the interval between measurements is at least 4 hours. $1090.1350(a)(2) $1090.1360(a)(2) & §1090.1365(b)(3) Table 1. |
| Is 15 ppm Sulfur Precision Criterion Met? |
PASSED |
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| standard deviation |
12.42 |
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| Laboratory Test Identification Number |
Date |
Time |
Test Result (ppm) |
Data Entry QC Check on Test Result |
| ######### |
3/26/2021 |
8:00 AM |
755.000 |
OK |
| ######### |
3/29/2021 |
8:01 AM |
780.000 |
OK |
| ######### |
3/30/2021 |
8:20 AM |
765.000 |
OK |
| ######### |
3/31/2021 |
8:23 AM |
750.000 |
OK |
| ######### |
4/1/2021 |
8:00 AM |
745.000 |
OK |
| ######### |
4/2/2021 |
8:00 AM |
760.000 |
OK |
| ######### |
4/3/2021 |
8:20 AM |
763.000 |
OK |
| ######### |
4/4/2021 |
8:20 AM |
772.000 |
OK |
| ######### |
4/5/2021 |
8:00 AM |
749.000 |
OK |
| ######### |
4/8/2021 |
8:01 AM |
730.000 |
OK |
| ######### |
4/9/2021 |
8:20 AM |
740.000 |
OK |
| ######### |
4/10/2021 |
8:00 AM |
760.000 |
OK |
| ######### |
4/11/2021 |
8:00 AM |
745.000 |
OK |
| ######### |
4/12/2021 |
8:01 AM |
750.000 |
OK |
| ######### |
4/15/2021 |
8:20 AM |
756.000 |
OK |
| ######### |
4/16/2021 |
8:01 AM |
763.000 |
OK |
| ######### |
4/17/2021 |
8:00 AM |
765.000 |
OK |
| ######### |
4/18/2021 |
8:00 AM |
763.000 |
OK |
| ######### |
4/19/2021 |
8:01 AM |
777.000 |
OK |
| ######### |
4/22/2021 |
8:20 AM |
750.000 |
OK |
| 1,000 ppm ECA Marine Fuel Sulfur Accuracy Demonstration [ECA0300 : OMB #2060-0731, EPA ICR number 2607.02: Expires 1/31/2024] |
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| Test Method |
| Name of Method: |
Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry |
| Organization ID No. (as in ASTM D XXXX-XX): |
ASTM D2622-10 |
| Laboratory Identification |
| Laboratory Name: |
USEPA National and Vehicle Fuels Emissions Laboratory/OAR |
| Laboratory Street Address: |
2565 Plymouth Road, Mailcode AATSG |
| Laboratory City: |
Ann Arbor |
| Laboratory State: |
Michigan |
| Laboratory Zip code: |
48105 |
| Laboratory Contact Person: |
John Doe |
| Laboratory Contact Phone Number |
xxx-xxx-xxxx |
| Laboratory Contact Facsimile Number |
xxx-xxx-xxxx |
| Laboratory Contact E-mail Address |
[email protected] |
| 900 to 1,000 ppm Accuracy Criterion (§1090.1365(c)(3)(ii)) - the arithmetic average of a continuous series of at least 10 tests performed on a commercially available gravimetric sulfur standard in the range of 900 to 1000 ppm sulfur shall not differ from the accepted reference value (ARV) of that standard by more than 15.075 ppm. Individual test results shall be compensated for any known chemical interferences. $1090.1350(a)(2) $1090.1360(a)(2)& §1090.1365(c)(3) Table 1. |
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| Accuracy Criterion for 900-1000 ppm |
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| gravimetric sulfur standard |
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| Is 900-1000 ppm Sulfur Accuracy Criterion Met? |
PASSED |
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| Arithmetic Average (ppm) |
951.70 |
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| Vendor Name of Gravimetric Standard |
NIST |
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| Lot Identification Number of Gravimetric Standard |
ALDS53478 |
Concentration QC Check on ARV |
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| Accepted Reference Value (ARV) of Gravimetric Standard (ppm) |
950.00 |
OK |
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| Difference between Arithmetic Average and ARV of Gravimetric Standard |
1.70000000000005 |
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| Laboratory Test Identification Number |
Date |
Time |
Test Result (ppm) |
Data Entry QC Check on Test Result |
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| ######### |
4/23/2021 |
8:00 AM |
960.000 |
OK |
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| ######### |
4/23/2021 |
8:05 AM |
940.000 |
OK |
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| ######### |
4/23/2021 |
8:10 AM |
942.000 |
OK |
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| ######### |
4/23/2021 |
8:15 AM |
962.000 |
OK |
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| ######### |
4/23/2021 |
8:20 AM |
953.000 |
OK |
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| ######### |
4/23/2021 |
8:25 AM |
957.000 |
OK |
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| ######### |
4/23/2021 |
8:30 AM |
949.000 |
OK |
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| ######### |
4/23/2021 |
8:35 AM |
950.000 |
OK |
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| ######### |
4/23/2021 |
8:40 AM |
956.000 |
OK |
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| ######### |
4/23/2021 |
8:45am |
948.000 |
OK |
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